CN110537724A - Nicotine salt, electronic cigarette oil and production process thereof - Google Patents
Nicotine salt, electronic cigarette oil and production process thereof Download PDFInfo
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- CN110537724A CN110537724A CN201910926105.2A CN201910926105A CN110537724A CN 110537724 A CN110537724 A CN 110537724A CN 201910926105 A CN201910926105 A CN 201910926105A CN 110537724 A CN110537724 A CN 110537724A
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/10—Chemical features of tobacco products or tobacco substitutes
- A24B15/16—Chemical features of tobacco products or tobacco substitutes of tobacco substitutes
- A24B15/167—Chemical features of tobacco products or tobacco substitutes of tobacco substitutes in liquid or vaporisable form, e.g. liquid compositions for electronic cigarettes
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
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- General Chemical & Material Sciences (AREA)
- Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
Abstract
the invention discloses a nicotine salt, which comprises, by weight, 35-55 parts of organic acid and 15-65 parts of nicotine, wherein the organic acid comprises sorbic acid, glycolic acid, ascorbic acid, glycyrrhizic acid, citric acid, tartaric acid and gluconic acid. Sorbic acid in the nicotine salt has an antibacterial effect, participates in the metabolism process in a human body, is digested and absorbed by the human body, generates carbon dioxide and water, and has the effect of moistening the lung; meanwhile, a small amount of ascorbic acid, glycyrrhizic acid and glycolic acid is added into the nicotine salt, so that the nicotine salt has the effects of resisting tumors and fungi and improving immunity and plays a role in protecting the lung; the electronic cigarette oil disclosed by the invention is added with various volatile oils, can be selected and combined according to tastes and medicinal value requirements, has the effects of moistening the throat, moistening the lung and relieving asthma, improves the immunity and relieves the nerves, and improves the enjoyment of the electronic cigarette oil in use.
Description
Technical Field
the invention belongs to the technical field of electronic cigarette oil, and particularly relates to nicotine salt and electronic cigarette oil, and also relates to a production process of the nicotine salt and the electronic cigarette oil.
Background
an electronic cigarette (i.e., an electronic atomizer) is an electronic product that simulates a cigarette and has the same appearance, smoke, taste and sensation as a cigarette. It is a product which is heated to change nicotine and the like into steam by means of atomization and the like and is sucked by a user.
the use of the electronic cigarette cannot become a smoking cessation means, only can reduce the harm to the human body after improving the formula of the electronic cigarette oil, particularly eliminates a large amount of tar components in the electronic cigarette, and has lower harm to the lung than the cigarette under the condition of equally satisfying the smoking addiction. Most of the tobacco tar used by the existing electronic cigarettes only enables users to meet the requirements of smoking addiction, and cannot provide better help for the physical health of the users, so that nicotine salt, electronic tobacco tar and production processes thereof which relatively guarantee the lung health of the users need to be provided.
disclosure of Invention
The invention aims to provide a nicotine salt, electronic cigarette oil and a production process thereof, and aims to solve the problems that the electronic cigarette oil in the prior art only meets the smoking addiction of users and does not provide better further guarantee for the physical health of the users.
in order to achieve the purpose, the invention adopts the following technical scheme:
A nicotine salt comprises, by weight, 35-55 parts of organic acid and 15-65 parts of nicotine, wherein the organic acid comprises sorbic acid, glycolic acid, ascorbic acid, glycyrrhizic acid, citric acid, tartaric acid and gluconic acid.
Preferably, the organic acid comprises the following components in percentage by mass: wherein, the sorbic acid accounts for 15 to 25 percent, the glycolic acid accounts for 2 to 4 percent, the ascorbic acid accounts for 3 to 6 percent, the glycyrrhizic acid accounts for 2 to 5 percent, the citric acid accounts for 20 to 35 percent, the tartaric acid accounts for 1 to 2 percent and the grape acid accounts for 35 to 55 percent.
preferably, the organic acid comprises the following components in percentage by mass: wherein, the content of sorbic acid is 20 percent, the content of glycolic acid is 3 percent, the content of ascorbic acid is 5 percent, the content of glycyrrhizic acid is 4 percent, the content of citric acid is 20 percent, the content of tartaric acid is 1 percent, and the content of gluconic acid is 47 percent.
Preferably, the organic acid further comprises 0-1% by mass of pseudolaric acid.
Preferably, the organic acid comprises the following components in percentage by mass: wherein, the content of sorbic acid is 22 percent, the content of glycolic acid is 2 percent, the content of ascorbic acid is 4 percent, the content of glycyrrhizic acid is 3 percent, the content of citric acid is 28 percent, the content of tartaric acid is 2 percent, the content of gluconic acid is 38 percent, and the content of pseudolaric acid is 1 percent.
the invention provides electronic cigarette oil which comprises, by mass, 2-10 parts of nicotine salt, 50-100 parts of propylene glycol, 50-100 parts of glycerol and 1-5 parts of volatile oil.
preferably, the volatile oil is one or a mixture of garlic volatile oil, wild yam volatile oil, licorice root volatile oil, thyme volatile oil and apricot volatile oil.
The invention also provides a production process of the electronic cigarette oil, which comprises the following steps:
s1, weighing and preparing nicotine salt, propylene glycol, glycerol and volatile oil according to the mass ratio;
S2, preparing nicotine salt: firstly, uniformly mixing sorbic acid, citric acid and gluconic acid in a heating and stirring tank, heating while mixing, preheating ascorbic acid, glycyrrhizic acid, tartaric acid and glycolic acid, sequentially putting the ascorbic acid, the glycyrrhizic acid, the tartaric acid, the glycolic acid and nicotine into the heating and stirring tank for full reaction, and crushing the reacted solid to obtain nicotine salt;
S3, placing the mixture of propylene glycol and glycerol into a stirring tank, then placing the nicotine salt obtained in the step S2 into the stirring tank to be stirred, continuously stirring, mixing and dissolving for 1-3 hours at the temperature of 25-50 ℃, and then filtering through filter cloth at room temperature to obtain pure filtrate;
And S4, adding the volatile oil into the filtrate, mixing for 3-5 minutes, and finally sealing and packaging to finish the production of the electronic cigarette oil.
Preferably, the heating temperature is maintained at 55-85 ℃ during the heating and stirring in the S2, and the stirring speed is maintained at 60-80 rpm.
Preferably, the aperture of the filter cloth in the S3 is set to be 80-120 meshes.
the invention has the technical effects and advantages that: compared with the prior art, the nicotine salt, the electronic cigarette oil and the production process thereof provided by the invention have the following advantages:
1. sorbic acid in the nicotine salt has an antibacterial effect, and the sorbic acid is the same as natural fatty acid, participates in the metabolism process in a human body, is digested and absorbed by the human body, generates carbon dioxide and water, and has the effect of moistening the lung; meanwhile, a small amount of ascorbic acid, glycyrrhizic acid and glycolic acid is added into the nicotine salt, so that the nicotine salt has the effects of resisting tumors and fungi, preventing fungal infection, improving immunity and playing a role in protecting the lung;
2. According to the invention, the garlic volatile oil, the wild yam volatile oil, the licorice root volatile oil, the thyme volatile oil and the apricot volatile oil are added into the electronic cigarette oil, so that the electronic cigarette oil can be selected and combined according to the taste and the medicinal value requirements, has the effects of moistening throat, moistening lung and relieving asthma, can remove free radicals, improves the immunity, has the effect of relieving nerves, and improves the enjoyment of the electronic cigarette oil in use.
3. the electronic cigarette oil has simple production process and easy implementation, and is suitable for mass production.
Detailed Description
The technical solutions in the embodiments of the present invention will be clearly and completely described below, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all embodiments. The specific embodiments described herein are merely illustrative of the invention and do not delimit the invention. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
Example 1
A nicotine salt comprises, by weight, 35 parts of organic acid and 15 parts of nicotine, wherein the organic acid comprises sorbic acid, glycolic acid, ascorbic acid, glycyrrhizic acid, citric acid, tartaric acid and gluconic acid. In specific implementation, the organic acid comprises the following components in percentage by mass: wherein, the content of sorbic acid is 20 percent, the content of glycolic acid is 3 percent, the content of ascorbic acid is 5 percent, the content of glycyrrhizic acid is 4 percent, the content of citric acid is 20 percent, the content of tartaric acid is 1 percent, and the content of gluconic acid is 47 percent.
The electronic cigarette oil comprises, by mass, 2-10 parts of the nicotine salt, 50-100 parts of propylene glycol, 50-100 parts of glycerol and 1-5 parts of volatile oil. When the electronic cigarette liquid is produced, the method comprises the following steps:
S1, weighing and preparing nicotine salt (5 parts), propylene glycol (80 parts), glycerol (80 parts) and volatile oil (3 parts) according to the mass ratio;
S2, preparing nicotine salt: firstly, uniformly mixing sorbic acid, citric acid and gluconic acid in a heating and stirring tank, heating while mixing (the heating temperature is kept at 55-85 ℃, and the stirring speed is kept at 60-80rpm), preheating ascorbic acid, glycyrrhizic acid, tartaric acid and glycolic acid, then sequentially putting the ascorbic acid, the glycyrrhizic acid, the tartaric acid, the glycolic acid and nicotine into the heating and stirring tank for full reaction, and crushing the reacted solid to obtain nicotine salt;
s3, placing the mixture of propylene glycol and glycerol into a stirring tank, then placing the nicotine salt obtained in the step S2 into the stirring tank to be stirred, continuously stirring, mixing and dissolving for 1-3 hours at the temperature of 25-50 ℃, and then filtering through filter cloth (the aperture of the filter cloth is set to be 80-120 meshes) at the room temperature environment to obtain pure filtrate;
S4, adding volatile oil (mixing garlic volatile oil and wild yam volatile oil at equal ratio) into the filtrate, mixing for 3-5 minutes, and finally sealing and packaging to complete the production of the electronic cigarette oil.
Example 2
a nicotine salt comprises, by weight, 45 parts of organic acid and 35 parts of nicotine, wherein the organic acid comprises sorbic acid, glycolic acid, ascorbic acid, glycyrrhizic acid, citric acid, tartaric acid, gluconic acid and pseudolaric acid. In specific implementation, the organic acid comprises the following components in percentage by mass: wherein, the content of sorbic acid is 22 percent, the content of glycolic acid is 2 percent, the content of ascorbic acid is 4 percent, the content of glycyrrhizic acid is 3 percent, the content of citric acid is 28 percent, the content of tartaric acid is 2 percent, the content of gluconic acid is 38 percent, and the content of pseudolaric acid is 1 percent.
The electronic cigarette oil comprises, by mass, 2-10 parts of the nicotine salt, 50-100 parts of propylene glycol, 50-100 parts of glycerol and 1-5 parts of volatile oil. When the electronic cigarette liquid is produced, the method comprises the following steps:
S1, weighing and preparing nicotine salt (2 parts), propylene glycol (50 parts), glycerol (50 parts) and volatile oil (1 part) according to the mass ratio;
S2, preparing nicotine salt: firstly, uniformly mixing sorbic acid, citric acid and grape acid in a heating and stirring tank, heating while mixing (the heating temperature is kept at 55-85 ℃, and the stirring speed is kept at 60-80rpm), preheating ascorbic acid, glycyrrhizic acid, pseudolaric acid, tartaric acid and glycolic acid, sequentially putting the ascorbic acid, glycyrrhizic acid, pseudolaric acid, tartaric acid, glycolic acid and nicotine into the heating and stirring tank for full reaction, and crushing the reacted solid to obtain nicotine salt;
S3, placing the mixture of propylene glycol and glycerol into a stirring tank, then placing the nicotine salt obtained in the step S2 into the stirring tank to be stirred, continuously stirring, mixing and dissolving for 1-3 hours at the temperature of 25-50 ℃, and then filtering through filter cloth (the aperture of the filter cloth is set to be 80-120 meshes) at the room temperature environment to obtain pure filtrate;
S4, adding volatile oil (mixed by thyme volatile oil and apricot volatile oil in equal ratio) into the filtrate, mixing for 3-5 minutes, and finally sealing and packaging to complete the production of the electronic cigarette oil.
Example 3
The nicotine salt is prepared from 55 parts by weight of organic acid and 65 parts by weight of nicotine, wherein the organic acid comprises sorbic acid, glycolic acid, ascorbic acid, glycyrrhizic acid, citric acid, tartaric acid and gluconic acid. In specific implementation, the organic acid comprises the following components in percentage by mass: wherein, the content of sorbic acid is 20 percent, the content of glycolic acid is 3 percent, the content of ascorbic acid is 5 percent, the content of glycyrrhizic acid is 4 percent, the content of citric acid is 20 percent, the content of tartaric acid is 1 percent, and the content of gluconic acid is 47 percent.
the electronic cigarette oil comprises, by mass, 2-10 parts of the nicotine salt, 50-100 parts of propylene glycol, 50-100 parts of glycerol and 1-5 parts of volatile oil. When the electronic cigarette liquid is produced, the method comprises the following steps:
S1, weighing and preparing nicotine salt (10 parts), propylene glycol (100 parts), glycerol (100 parts) and volatile oil (5 parts) according to the mass ratio;
S2, preparing nicotine salt: firstly, uniformly mixing sorbic acid, citric acid and gluconic acid in a heating and stirring tank, heating while mixing (the heating temperature is kept at 55-85 ℃, and the stirring speed is kept at 60-80rpm), preheating ascorbic acid, glycyrrhizic acid, tartaric acid and glycolic acid, then sequentially putting the ascorbic acid, the glycyrrhizic acid, the tartaric acid, the glycolic acid and nicotine into the heating and stirring tank for full reaction, and crushing the reacted solid to obtain nicotine salt;
S3, placing the mixture of propylene glycol and glycerol into a stirring tank, then placing the nicotine salt obtained in the step S2 into the stirring tank to be stirred, continuously stirring, mixing and dissolving for 1-3 hours at the temperature of 25-50 ℃, and then filtering through filter cloth (the aperture of the filter cloth is set to be 80-120 meshes) at the room temperature environment to obtain pure filtrate;
S4, adding the volatile oil (licorice root volatile oil) into the filtrate, mixing for 3-5 minutes, and finally sealing and packaging to complete the production of the electronic cigarette oil.
Comparative data for three sets of examples are as follows:
in summary, the following steps: sorbic acid in the nicotine salt has an antibacterial effect, and the sorbic acid is the same as natural fatty acid, participates in the metabolism process in a human body, is digested and absorbed by the human body, generates carbon dioxide and water, and has the effect of moistening the lung; meanwhile, a small amount of ascorbic acid, glycyrrhizic acid and glycolic acid is added into the nicotine salt, so that the nicotine salt has the effects of resisting tumors and fungi, preventing fungal infection, improving immunity and playing a role in protecting the lung; according to the invention, the garlic volatile oil, the wild yam volatile oil, the licorice root volatile oil, the thyme volatile oil and the apricot volatile oil are added into the electronic cigarette oil, so that the electronic cigarette oil can be selected and combined according to the taste and the medicinal value requirements, has the effects of moistening throat, moistening lung and relieving asthma, can remove free radicals, improves the immunity, has the effect of relieving nerves, and improves the enjoyment of the electronic cigarette oil in use. The electronic cigarette oil has simple production process and easy implementation, and is suitable for mass production.
Finally, it should be noted that: although the present invention has been described in detail with reference to the foregoing embodiments, it will be apparent to those skilled in the art that modifications may be made to the embodiments or portions thereof without departing from the spirit and scope of the invention.
Claims (10)
1. a nicotine salt characterized by: the raw materials of the nicotine salt comprise 35-55 parts of organic acid and 15-65 parts of nicotine by weight, wherein the organic acid comprises sorbic acid, glycolic acid, ascorbic acid, glycyrrhizic acid, citric acid, tartaric acid and gluconic acid.
2. A nicotine salt according to claim 1, wherein: the organic acid comprises the following components in percentage by mass: wherein, the sorbic acid accounts for 15 to 25 percent, the glycolic acid accounts for 2 to 4 percent, the ascorbic acid accounts for 3 to 6 percent, the glycyrrhizic acid accounts for 2 to 5 percent, the citric acid accounts for 20 to 35 percent, the tartaric acid accounts for 1 to 2 percent and the grape acid accounts for 35 to 55 percent.
3. A nicotine salt according to claim 1, wherein: the organic acid comprises the following components in percentage by mass: wherein, the content of sorbic acid is 20 percent, the content of glycolic acid is 3 percent, the content of ascorbic acid is 5 percent, the content of glycyrrhizic acid is 4 percent, the content of citric acid is 20 percent, the content of tartaric acid is 1 percent, and the content of gluconic acid is 47 percent.
4. A nicotine salt according to claim 2, wherein: the organic acid also comprises 0-1% of pseudolaric acid by mass percent.
5. A nicotine salt according to claim 4, wherein: the organic acid comprises the following components in percentage by mass: wherein, the content of sorbic acid is 22 percent, the content of glycolic acid is 2 percent, the content of ascorbic acid is 4 percent, the content of glycyrrhizic acid is 3 percent, the content of citric acid is 28 percent, the content of tartaric acid is 2 percent, the content of gluconic acid is 38 percent, and the content of pseudolaric acid is 1 percent.
6. An electronic cigarette liquid, which is characterized in that: the nicotine salt according to any one of claims 1-3, which comprises 2-10 parts by weight of nicotine salt, 50-100 parts by weight of propylene glycol, 50-100 parts by weight of glycerol and 1-5 parts by weight of volatile oil.
7. The electronic cigarette liquid of claim 6, wherein: the volatile oil is one or two of Bulbus Allii volatile oil, rhizoma Dioscoreae volatile oil, Glycyrrhrizae radix volatile oil, herba Thymi volatile oil, and fructus Pruni volatile oil.
8. The process for producing the electronic cigarette liquid of claim 6, comprising the steps of:
s1, weighing and preparing nicotine salt, propylene glycol, glycerol and volatile oil according to the mass ratio;
S2, preparing nicotine salt: firstly, uniformly mixing sorbic acid, citric acid and gluconic acid in a heating and stirring tank, heating while mixing, preheating ascorbic acid, glycyrrhizic acid, tartaric acid and glycolic acid, sequentially putting the ascorbic acid, the glycyrrhizic acid, the tartaric acid, the glycolic acid and nicotine into the heating and stirring tank for full reaction, and crushing the reacted solid to obtain nicotine salt;
s3, placing the mixture of propylene glycol and glycerol into a stirring tank, then placing the nicotine salt obtained in the step S2 into the stirring tank to be stirred, continuously stirring, mixing and dissolving for 1-3 hours at the temperature of 25-50 ℃, and then filtering through filter cloth at room temperature to obtain pure filtrate;
and S4, adding the volatile oil into the filtrate, mixing for 3-5 minutes, and finally sealing and packaging to finish the production of the electronic cigarette oil.
9. the process of claim 8, wherein the step of preparing the electronic cigarette liquid comprises: and during heating and stirring in the S2, the heating temperature is kept at 55-85 ℃, and the stirring speed is kept at 60-80 rpm.
10. The process of claim 8, wherein the step of preparing the electronic cigarette liquid comprises: the aperture of the filter cloth in the S3 is set to be 80-120 meshes.
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| CN201910926105.2A CN110537724A (en) | 2019-09-27 | 2019-09-27 | Nicotine salt, electronic cigarette oil and production process thereof |
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| CN201910926105.2A CN110537724A (en) | 2019-09-27 | 2019-09-27 | Nicotine salt, electronic cigarette oil and production process thereof |
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Cited By (4)
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| CN111419726A (en) * | 2020-04-30 | 2020-07-17 | 云南风联科技有限公司 | Plant dried orange peel tobacco-flavored oral cavity atomized liquid and preparation method thereof |
| CN112715555A (en) * | 2020-12-18 | 2021-04-30 | 湖北和诺生物工程股份有限公司 | Synthetic method and application of nicotine salt |
| CN112841709A (en) * | 2021-01-20 | 2021-05-28 | 深圳市艾普生物科技有限公司 | Preparation method and application of nicotine salt |
| CN113912585A (en) * | 2021-11-09 | 2022-01-11 | 深圳萨特瓦生物科技有限公司 | Composite nicotine salt, preparation method and application thereof, electronic cigarette oil and electronic cigarette |
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| CN113912585A (en) * | 2021-11-09 | 2022-01-11 | 深圳萨特瓦生物科技有限公司 | Composite nicotine salt, preparation method and application thereof, electronic cigarette oil and electronic cigarette |
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