CN110507594B - Toning lotion and preparation method thereof - Google Patents
Toning lotion and preparation method thereof Download PDFInfo
- Publication number
- CN110507594B CN110507594B CN201910875117.7A CN201910875117A CN110507594B CN 110507594 B CN110507594 B CN 110507594B CN 201910875117 A CN201910875117 A CN 201910875117A CN 110507594 B CN110507594 B CN 110507594B
- Authority
- CN
- China
- Prior art keywords
- water
- polyethylene glycol
- lotion
- soluble
- mixing
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
Images
Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/64—Proteins; Peptides; Derivatives or degradation products thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/81—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions involving only carbon-to-carbon unsaturated bonds
- A61K8/8141—Compositions of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides or nitriles thereof; Compositions of derivatives of such polymers
- A61K8/8152—Homopolymers or copolymers of esters, e.g. (meth)acrylic acid esters; Compositions of derivatives of such polymers
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
- A61K8/86—Polyethers
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9706—Algae
- A61K8/9717—Rhodophycota or Rhodophyta [red algae], e.g. Porphyra
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9728—Fungi, e.g. yeasts
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9794—Liliopsida [monocotyledons]
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/98—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin
- A61K8/987—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin of species other than mammals or birds
- A61K8/988—Honey; Royal jelly, Propolis
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/48—Thickener, Thickening system
Landscapes
- Life Sciences & Earth Sciences (AREA)
- Health & Medical Sciences (AREA)
- Veterinary Medicine (AREA)
- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
- Public Health (AREA)
- Birds (AREA)
- Epidemiology (AREA)
- Engineering & Computer Science (AREA)
- Biotechnology (AREA)
- Microbiology (AREA)
- Mycology (AREA)
- Botany (AREA)
- Zoology (AREA)
- Dermatology (AREA)
- Cosmetics (AREA)
Abstract
The invention discloses a toning lotion and a preparation method thereof. The raw materials for preparing the toning lotion comprise the following components in percentage by weight based on the total weight of the toning lotion: 1.0-40 wt% of a water-soluble humectant; 0.01-0.5 wt% of a water-soluble thickener; 0.1-20 wt% polyethylene glycol; and 55-95 wt% water.
Description
Technical Field
The invention relates to the field of cosmetics, in particular to toning lotion and a preparation method thereof.
Background
With the increasing economic and living standards, the demand of consumers for skin care is higher and higher. The toning lotion is a basic step in the skin care process and has the functions of moisturizing, cleaning and enhancing the absorption of subsequent products.
The cosmetic field is full of fashion, and the product is required to have aesthetic characteristics including color, skin feel, odor, use feel, etc., which will determine whether the consumer will continue to use the product. At present, young people after 95 have gradually become the consumer force army of cosmetics, and are more easily attracted by interesting and novel products, and products with the emphasis on individualization and interest are more easily stimulated to buy. At present, regardless of the characters and different efficacies of the toning lotion, the use of the toning lotion is generally low in interestingness, for example, when a jelly-shaped skin care product prepared by a high polymer with poor ion resistance is used, the product is often high in consistency, and the water melting and bursting effects are not obvious; or W/O emulsion in critical stable state or W/SI water-out cream; or the addition of soft bead particles or suspended grease, etc. all have similar problems.
The water replenishing effect is one of the demands of consumers on the lotion, so that the visual water drop feeling is urgently needed to be provided in the field, and the lotion which is continuously exploded is applied, so that the moisturizing effect is brought to people, and the interestingness of the product can be increased.
Disclosure of Invention
The invention aims to provide novel toning lotion and a preparation method thereof.
In a first aspect of the present invention, there is provided a moisturizing lotion, comprising, based on the total weight of the lotion:
1.0-40 wt% of water-soluble humectant
0.01-0.5 wt% of water-soluble thickener
0.1-20 wt% of polyethylene glycol
55-95 wt% water.
In another preferred embodiment, the water-soluble thickener is one or two or more selected from the group consisting of: carbomer, acrylic acid/C10-30 alkanol acrylate crosspolymer, hydroxyethyl acrylate/sodium acryloyldimethyl taurate copolymer, ammonium acryloyldimethyl taurate/VP copolymer, sodium polyacrylate, xanthan gum, hydroxyethyl cellulose, and cellulose gum.
In another preferred embodiment, the polyethylene glycol is selected from one or two or more of the following: polyethylene glycol-6, polyethylene glycol-8, polyethylene glycol-10, polyethylene glycol-32, polyethylene glycol-75, polyethylene glycol-14M, polyethylene glycol-20M, polyethylene glycol-90M, and polyethylene glycol-150.
In another preferred embodiment, the water-soluble humectant is selected from one or more of the following: glycerol, propylene glycol, 1, 3-propanediol, dipropylene glycol, 1, 3-butanediol, methylpropanediol, sorbitol, sodium hyaluronate, hydrolyzed sodium hyaluronate, trehalose, betaine, panthenol, glyceryl polyether-26, and PEG/PPG-17/6 copolymer.
In another preferred example, the raw materials further comprise:
0.1-10 wt% of a skin conditioner
0.01-0.4 wt% of pH regulator
0.05-1.0 wt% of solubilizer
0.001-0.5 wt% chelating agent
0.01-3.0 wt% preservative
0.001-1.0 wt% of essence.
In another preferred embodiment, the skin conditioning agent is selected from one or more of the following: chondrus crispus extract, Tremella fuciformis entity extract, Chinese yam extract, honey extract, oat kernel extract, inositol, acetyl tetrapeptide-5, schizosaccharomyces cerevisiae fermentation product lysate, and hydrolyzed wheat protein.
In another preferred embodiment, the pH adjusting agent is selected from one or two or more of the following: sodium hydroxide, potassium hydroxide, triethanolamine, tromethamine, aminomethyl propanol, and arginine.
In another preferred embodiment, the solubilizer is selected from one or more than two of the following: PEG-40 hydrogenated castor oil, PEG-60 hydrogenated castor oil, octyldodecanol polyether-16, polysorbate-20, PPG-26-Butanethol-26, polyglycerol-10 laurate, and PPG-13-decyltetradecanol polyether-24.
In another preferred embodiment, the chelating agent is selected from one or two of the following: disodium EDTA, tetrasodium EDTA, pentasodium pentetate, sodium phytate, and phytic acid.
In another preferred embodiment, the preservative is selected from one or more of the following: 1, 2-hexanediol, 1, 2-pentanediol, benzyl alcohol, phenoxyethanol, ethylhexyl glycerol, p-hydroxyacetophenone, octaethylene glycol, methylparaben, and chlorphenesin.
In another preferred embodiment, the water-soluble thickener is carbopol Ultrez 20; the polyethylene glycol is polyethylene glycol-90M and polyethylene glycol-75 or polyethylene glycol-150.
In another preferred embodiment, the raw materials comprise 0.01-0.05 wt% of polyethylene glycol-90M and 1-3 wt% of polyethylene glycol-75 or polyethylene glycol-150 based on the total weight of the cosmetic water.
In a second aspect of the present invention, there is provided a method for preparing the cosmetic water provided by the present invention as described above, the method comprising the steps of: the formula dosage of the water-soluble humectant, the water-soluble thickener, the water and the polyethylene glycol are mixed to obtain the toning lotion provided by the invention.
In another preferred example, the method comprises the steps of:
(1) mixing the water-soluble humectant, the water-soluble thickener, the chelating agent and water according to the formula dosage to obtain a solution 1
(2) Mixing the solution 1 with a pH regulator in a formula dosage to obtain a mixture 1; and
(3) and mixing the mixture 1 with polyethylene glycol, a skin conditioning agent, a solubilizer, a essence and a preservative in formula dosage to obtain the toning lotion provided by the invention.
In another preferred embodiment, the mixing in step (1) is carried out at 75-85 ℃.
In another preferred embodiment, the mixing in step (2) is carried out at 48-55 ℃.
In another preferred embodiment, the mixing in step (3) is carried out at 42-48 ℃.
In another preferred embodiment, the cosmetic water provided by the invention as described above is obtained by filtering at 32-39 ℃ after mixing in step (3).
Therefore, the cosmetic water provided by the invention has visual water drop feeling when in use, and is applied with the cosmetic water which is continuously exploded, so that the moisturizing feeling is brought to people, and the interestingness of the product is increased.
Drawings
FIG. 1 is a hand effect graph of the lotion prepared in example 5 of the present invention; wherein the content of the first and second substances,
a is the condition that the lotion is just applied to the hands and is gently flapped;
b is the condition that water drops begin to burst after the toning lotion is lightly beaten;
c is the effect graph of the cosmetic water spurting water beads.
Detailed Description
The inventors have extensively and intensively studied and found that a lotion having a burst effect can be obtained by using a medium rheology, ion resistant polymer and a high molecular weight polyethylene glycol.
As used herein, "burst" refers to a condition in which the lotion on the skin will burst into water droplets after being gently tapped.
The invention provides a toning lotion with a water bursting effect, wherein the raw materials mainly comprise the following components in percentage by total weight of the toning lotion:
further, the method can also comprise the following steps:
the water-soluble humectant used in the present invention includes one or more of glycerin, propylene glycol, 1, 3-propanediol, dipropylene glycol, 1, 3-butanediol, methyl propanediol, sorbitol, sodium hyaluronate, sodium acetylhyaluronate, hydrolyzed sodium hyaluronate, trehalose, betaine, panthenol, glyceryl polyether-26, and PEG/PPG-17/6 copolymer; preferably one or more of glycerol, 1, 3-butanediol, trehalose, sodium hyaluronate, betaine, and panthenol; more preferred are glycerol, 1, 3-butanediol and trehalose.
The adding amount of the water-soluble humectant is 1-40 wt%, preferably 5-30 wt% based on the total weight of the toning lotion; when the addition amount of the water-soluble humectant is less than 1 wt%, the moisturizing performance of the obtained lotion is poor, and when the addition amount of the water-soluble humectant is more than 40 wt%, the prepared lotion is sticky and high in cost.
The water-soluble thickener used in the invention comprises one or more than two of carbomer, acrylic acid (ester)/C10-30 alkanol acrylate cross-linked polymer, hydroxyethyl acrylate/sodium acryloyldimethyl taurate copolymer, ammonium acryloyldimethyl taurate/VP copolymer, sodium polyacrylate, xanthan gum, hydroxyethyl cellulose and cellulose gum; preferably one or more of carbomer, sodium polyacrylate, xanthan gum and acrylic acid (ester)/C10-30 alkanol acrylate cross-linked polymer; more preferably acrylic/C10-30 alkanol acrylate crosspolymer.
The inventor finds that the acrylic acid (ester)/C10-30 alkanol acrylate cross-linked polymer has better ion resistance, has good thickening capability after being neutralized, and has moist skin feel; furthermore, the polymer with better ion resistance is more durable in wire drawing effect and water bursting effect compared with the polymer with slightly poorer ion resistance.
In one embodiment of the invention, carbomers used include, but are not limited to, carbopol 980 (i.e., homopolymer of 2-methylbutyric acid, CAS number 600-07-7), carbopol 981 (i.e., homopolymer of prop-2-enoic acid, CAS number 9063-87-0).
In one embodiment of the invention, the acrylic/C10-30 alkanol acrylate crosspolymer used includes, but is not limited to carbopol Ultrez 20, carbopol Ultrez 21; carbopol Ultrez 20 is preferred.
The addition amount of the water-soluble thickener is 0.01-0.5 wt%, preferably 0.08-0.35 wt% based on the total weight of the toning lotion; when the addition amount of the water-soluble thickener is less than 0.01 wt%, the obtained toning lotion has low consistency and poor wire drawing and water bursting effects, and when the addition amount of the water-soluble thickener is more than 0.5 wt%, the obtained toning lotion has high consistency and poor spreadability and water bursting effects.
The polyethylene glycol used in the invention comprises one or more than two of polyethylene glycol-6, polyethylene glycol-8, polyethylene glycol-10, polyethylene glycol-32, polyethylene glycol-75, polyethylene glycol-14M, polyethylene glycol-20M, polyethylene glycol-90M and polyethylene glycol-150; one or two of polyethylene glycol-90M, polyethylene glycol-32, polyethylene glycol-75, polyethylene glycol-150, polyethylene glycol-14M, and polyethylene glycol-8 are preferable.
In one embodiment of the present invention, a polyethylene glycol having a repeating unit number of ethylene glycol of 20 to 200000, preferably a repeating unit number of ethylene glycol of 50 to 100000, such as a repeating unit number of ethylene glycol of 75, 100, 120, 150, 1000-9000, 10000-90000 and the like, for example, one or more of polyethylene glycol-90M, polyethylene glycol-75 and polyethylene glycol-150, more preferably polyethylene glycol-75 or a combination of polyethylene glycol-150 and polyethylene glycol-90M is used.
The addition amount of the polyethylene glycols is 0.1-20 wt%, preferably 1-10 wt%, based on the total weight of the lotion. When the addition amount of the polyethylene glycols is less than 0.1 wt%, the prepared lotion has low moisturizing performance and poor wire drawing durability; when the addition amount of the polyethylene glycol is more than 20 wt%, the obtained astringent has strong stringiness and sticky skin feel.
Skin conditioning agents useful in the present invention include: one or more of Chondrus crispus extract, Tremella fuciformis fruiting body extract, rhizoma Dioscoreae extract, Mel extract, herba Avenae Fatuae kernel extract, inositol, acetyl tetrapeptide-5, Schizosaccharomyces cerevisiae fermentation product lysate, and hydrolyzed wheat protein. These substances can be prepared by the methods disclosed, and are commercially available, for example, but not limited to, Chondrus crispus extract (trade name: Seamolitent) from BASF of Germany, Tremella fuciformis fruiting body extract (trade name: WSK) from Hippocampus GmbH, and Mel extract (trade name: Mel extract) from Bailander Biochemical Co.
Preferably one or two of Tremella fuciformis fruiting body extract, Mel extract, and Chondrus crispus extract.
The addition amount of the skin conditioning agent is 0.1-10 wt%, preferably 0.3-5 wt% based on the total weight of the toning lotion; when the skin conditioner is added in an amount of less than 0.1 wt%, the prepared lotion has poor effect of conditioning the skin.
The pH regulator used in the invention comprises one or more than two of sodium hydroxide, potassium hydroxide, triethanolamine, tromethamine, aminomethyl propanol and arginine; preferably one of triethanolamine, tromethamine and arginine.
The addition amount of the pH regulator is 0.01-0.4 wt% based on the total weight of the toning lotion. Preferably 0.05-0.3 wt%, when the amount of the pH regulator added is less than 0.01 wt%, the pH of the resulting lotion is too low, and when the amount of the pH regulator added is more than 0.4 wt%, the pH of the lotion is too high, and the skin irritation is easily caused by too high or too low pH.
The solubilizer used in the invention comprises one or more than two of PEG-40 hydrogenated castor oil, PEG-60 hydrogenated castor oil, octyl dodecanol polyether-16, polysorbate-20, PPG-26-butanol polyether-26, polyglycerol-10 laurate and PPG-13-decyl tetradecanol polyether-24; preferably one or two of octyldodecanol polyether-16, PEG-60 hydrogenated castor oil, and polysorbate-20.
The addition amount of the solubilizer is 0.05-1 wt% based on the total weight of the toning lotion. Preferably 0.1 to 0.5 wt%; when the addition amount of the solubilizer is less than 0.05% by weight, the solubilization ability of the resulting lotion is poor, and the transparency is poor, and when the addition amount of the solubilizer is more than 1% by weight, the resulting lotion is more irritating.
The chelating agent used in the invention comprises one or two of disodium EDTA, tetrasodium EDTA, pentasodium pentetate, sodium phytate and phytic acid; one or two of disodium EDTA, sodium phytate and pentasodium pentetate are preferred.
The addition amount of the chelating agent is 0.001-0.5 wt% based on the total weight of the lotion. Preferably 0.01 to 0.3 wt%; when the added amount of the chelating agent is less than 0.001 wt%, the ability to chelate metal ions is weak, and when the added amount of the chelating agent is more than 0.5 wt%, the pH of the resulting lotion is too high or too low, easily causing skin irritation.
Preservatives and perfumes are also useful in the present invention. The preservative comprises one or more than two of 1, 2-hexanediol, 1, 2-pentanediol, benzyl alcohol, phenoxyethanol, ethylhexyl glycerol, p-hydroxyacetophenone, caprylyl glycol, methylparaben and chlorphenesin; preferably one or more of 1, 2-hexanediol, p-hydroxyacetophenone, phenoxyethanol, and ethylhexylglycerin.
The addition amount of the preservative is 0.01-3.0 wt%, preferably 0.05-2.0 wt% based on the total weight of the toning lotion; the addition amount of the essence is 0.001-1 wt%, preferably 0.01-0.05 wt%.
The water used in the present invention may be one commonly used in the cosmetic field, such as, but not limited to, deionized water. The adding amount of the deionized water in the toning lotion provided by the invention is 55-95 wt%, preferably 60-90 wt% based on the total weight of the toning lotion.
The present invention provides a method for preparing a cosmetic lotion, the method comprising the steps of:
firstly, adding a water-soluble humectant, a water-soluble thickener and a chelating agent into deionized water, stirring and heating to 75-85 ℃ for complete dissolution;
secondly, cooling to 48-55 ℃, adding a pH regulator, and uniformly stirring and dispersing;
and thirdly, cooling to 42-48 ℃, adding polyethylene glycol, a skin conditioner, a solubilizer, essence and a preservative, and uniformly stirring to obtain the toning lotion.
In one embodiment of the invention, the above steps are carried out in a reaction vessel.
In one embodiment of the invention, the temperature is reduced to 32-39 ℃ after the uniform stirring, and the toning lotion provided by the invention is obtained by filtering. The filtration may be carried out according to methods conventional in the art, such as, but not limited to, suction filtration.
The features mentioned above with reference to the invention, or the features mentioned with reference to the embodiments, can be combined arbitrarily. All the features disclosed in this specification may be combined in any combination, and each feature disclosed in this specification may be replaced by alternative features serving the same, equivalent or similar purpose. Thus, unless expressly stated otherwise, the features disclosed are merely generic examples of equivalent or similar features.
The main advantages of the invention are:
the toning lotion provided by the invention has a lasting wire drawing effect along with slight flapping of hands when being used, and meanwhile, generates visible particle water globules for a long time, and after being used, the skin has soft and silky touch feeling, is fresh and not sticky.
Embodiments of the present invention will be described in detail below with reference to examples, but it will be understood by those skilled in the art that the following examples are only illustrative of the present invention and should not be construed as limiting the scope of the present invention. The examples, in which specific conditions are not specified, were conducted under conventional conditions or conditions recommended by the manufacturer. The reagents or instruments used are not indicated by the manufacturer, and are all conventional products commercially available.
In an embodiment of the present invention,
the carbomer # 1 manufacturer is lubrizol, product designation: carbopol 980;
the carbomer 2# manufacturer is lubrizol, product designation: carbopol 981;
the manufacturer of acrylic acid/C10-30 alkanol acrylate crosspolymer # 1 is lubrizol, product designation: carbopol Ultrez 20;
the manufacturer of acrylic acid/C10-30 alkanol acrylate crosspolymer No. 2 is lubrizol, product designation: carbopol Ultrez 21;
preparation examples
Lotions were prepared according to the contents (parts) of the components of examples 1 to 5 and comparative examples 1 to 2 in the following table 1, according to the following procedures.
The preparation method comprises the following steps:
step 1: putting deionized water into a reaction vessel, adding a water-soluble humectant, a water-soluble thickener and a chelating agent, stirring and heating to 78 ℃ for complete dissolution;
and 2, step: cooling to 50 ℃, adding a pH regulator into the reaction vessel, and stirring and dispersing uniformly;
and step 3: cooling to 45 deg.C, adding polyethylene glycol, skin conditioner, solubilizer, essence, and antiseptic into a reaction container, and stirring;
and 4, step 4: cooling to 35 deg.C, and filtering to obtain astringent with water burst effect.
TABLE 1
Effects of the embodiment
The moisturizing lotions i to v prepared in examples 1 to 5 and the moisturizing lotions vi to vii prepared in comparative examples 1 to 2 were used for tests of consumer experience, and evaluated with 30 consumers of average age of 26 years. The evaluation method is to select the acceptance (whether the description is met) of each item in 1-5 points. The effect corresponding to each score is described as follows:
the test results are shown in Table 2
TABLE 2
Test results show that the use experience of the toning lotion provided by the embodiment of the application on the water bursting effect is obviously superior to that of the toning lotion provided by a comparative example. By comparing the toning lotion prepared by the polymers with different rheologies and ion resistances, the comprehensive performance of the toning lotion prepared by the ion-resistant polymer is good, and the use experience of the water bursting effect is relatively medium rheologies. By comparing the combination use of the polyethylene glycol polymers with different molecular weights, the comprehensive performance of the toning lotion prepared by using the combination of the polyethylene glycol polymers with relatively high molecular weights is good in the use experience of the water bursting effect.
The foregoing is merely a preferred embodiment of the invention and is not intended to limit the scope of the invention, which is defined by the claims appended hereto, and any other technical entity or method that is encompassed by the claims as broadly defined herein, or equivalent variations thereof, is contemplated as being encompassed by the claims.
Claims (6)
1. The moisturizing astringent is characterized in that raw materials for preparing the astringent comprise the following components in percentage by weight:
1.0-40 wt% of water-soluble humectant
0.01-0.5 wt% of water-soluble thickener
0.1-20 wt% of polyethylene glycol
55-95 wt% water;
the water-soluble thickener is acrylic acid (ester)/C10-30 alkanol acrylate cross-linked polymer, and the acrylic acid (ester)/C10-30 alkanol acrylate cross-linked polymer is carbopol Ultrez 20;
the polyethylene glycol is 0.01-0.05 wt% of polyethylene glycol-90M and 1-3 wt% of polyethylene glycol-75 or polyethylene glycol-150.
2. The astringent of claim 1, wherein the water-soluble humectant is selected from one or more of the following: glycerol, propylene glycol, 1, 3-propanediol, dipropylene glycol, 1, 3-butanediol, methylpropanediol, sorbitol, sodium hyaluronate, sodium acetylhyaluronate, hydrolyzed sodium hyaluronate, trehalose, betaine, panthenol, glyceryl polyether-26, and PEG/PPG-17/6 copolymer.
3. The lotion of claim 1, wherein the raw materials further comprise:
0.1-10 wt% of a skin conditioner
0.01-0.4 wt% of pH regulator
0.05-1.0 wt% of solubilizer
0.001-0.5 wt% of a chelating agent
0.01-3.0 wt% preservative
0.001-1.0 wt% of essence.
4. A method for preparing a lotion according to claim 1 or 2, characterized in that it comprises the steps of: mixing a formula amount of a water-soluble humectant, a water-soluble thickener, water and polyethylene glycol to obtain the lotion according to claim 1 or 2.
5. A method for preparing the lotion according to claim 3, characterized in that it comprises the steps of:
(1) mixing the water-soluble humectant, the water-soluble thickener, the chelating agent and water according to the formula dosage to obtain a solution 1
(2) Mixing the solution 1 with a pH regulator in a formula dosage to obtain a mixture 1;
(3) mixing mixture 1 with formula amounts of polyethylene glycol, skin conditioning agents, solubilizers, fragrances and preservatives to obtain the lotion according to claim 3.
6. The method of claim 5, wherein the toning lotion according to claim 3 is obtained by filtering at 32 to 39 ℃ after mixing in step (3).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201910875117.7A CN110507594B (en) | 2019-09-17 | 2019-09-17 | Toning lotion and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201910875117.7A CN110507594B (en) | 2019-09-17 | 2019-09-17 | Toning lotion and preparation method thereof |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN110507594A CN110507594A (en) | 2019-11-29 |
| CN110507594B true CN110507594B (en) | 2022-06-17 |
Family
ID=68632607
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201910875117.7A Active CN110507594B (en) | 2019-09-17 | 2019-09-17 | Toning lotion and preparation method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN110507594B (en) |
Families Citing this family (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP4247322A1 (en) * | 2020-11-20 | 2023-09-27 | L'Oreal | Composition for caring for a keratin material |
| CN113318029A (en) * | 2021-06-17 | 2021-08-31 | 广东柏俐臣生物科技有限公司 | Moisturizing lotion and preparation method thereof |
Citations (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106619306A (en) * | 2017-01-03 | 2017-05-10 | 广州科玛生物科技股份有限公司 | Whitening, nourishing and moisturizing water and preparation method thereof |
| CN107184474A (en) * | 2017-06-12 | 2017-09-22 | 广州劳莎生物科技有限公司 | A kind of Wrinkle-eliminating cosmetics and preparation method thereof |
| CN107949369A (en) * | 2014-12-10 | 2018-04-20 | 莱雅公司 | Cleasing compositions based on polyethylene glycol, polyether ester and polymer suspending agent |
| CN108348410A (en) * | 2015-09-02 | 2018-07-31 | 爱茉莉太平洋股份有限公司 | A kind of high interior phase water-in-oil type cosmetic constituent |
| CN109288724A (en) * | 2018-10-12 | 2019-02-01 | 上海中翊日化有限公司 | Aqua product, method and the application of fountain type appearance are presented when beating |
| CN109330954A (en) * | 2018-12-26 | 2019-02-15 | 广州市科能化妆品科研有限公司 | Whitening skin lightening water and preparation method thereof and tyrosinase inhibitor |
| CN109512744A (en) * | 2018-12-29 | 2019-03-26 | 广州博科健康科技集团有限公司 | A kind of eyelashes growth-promoting media and preparation method thereof |
| CN109820769A (en) * | 2019-03-14 | 2019-05-31 | 上海新高姿化妆品有限公司 | A kind of toner and preparation method thereof for having effects that moisturizing and releiving |
| CN110169944A (en) * | 2019-04-25 | 2019-08-27 | 上海百雀羚生物科技有限公司 | A kind of ageing-resistant skin care composition, its preparation process and application |
Family Cites Families (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US20050238595A1 (en) * | 2004-04-21 | 2005-10-27 | Qing Stella | Personal care compositions that deposit sunless tanning benefit agents |
| US8105996B2 (en) * | 2007-03-30 | 2012-01-31 | The Procter & Gamble Company | Multiphase personal care composition comprising a structuring |
| DE102015219712A1 (en) * | 2015-10-12 | 2017-04-13 | Henkel Ag & Co. Kgaa | Thickened skin care product |
| CN108904323A (en) * | 2018-08-03 | 2018-11-30 | 花安堂生物科技集团有限公司 | A kind of compound with unique wire-drawing effect and its application in cosmetics |
-
2019
- 2019-09-17 CN CN201910875117.7A patent/CN110507594B/en active Active
Patent Citations (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107949369A (en) * | 2014-12-10 | 2018-04-20 | 莱雅公司 | Cleasing compositions based on polyethylene glycol, polyether ester and polymer suspending agent |
| CN108348410A (en) * | 2015-09-02 | 2018-07-31 | 爱茉莉太平洋股份有限公司 | A kind of high interior phase water-in-oil type cosmetic constituent |
| CN106619306A (en) * | 2017-01-03 | 2017-05-10 | 广州科玛生物科技股份有限公司 | Whitening, nourishing and moisturizing water and preparation method thereof |
| CN107184474A (en) * | 2017-06-12 | 2017-09-22 | 广州劳莎生物科技有限公司 | A kind of Wrinkle-eliminating cosmetics and preparation method thereof |
| CN109288724A (en) * | 2018-10-12 | 2019-02-01 | 上海中翊日化有限公司 | Aqua product, method and the application of fountain type appearance are presented when beating |
| CN109330954A (en) * | 2018-12-26 | 2019-02-15 | 广州市科能化妆品科研有限公司 | Whitening skin lightening water and preparation method thereof and tyrosinase inhibitor |
| CN109512744A (en) * | 2018-12-29 | 2019-03-26 | 广州博科健康科技集团有限公司 | A kind of eyelashes growth-promoting media and preparation method thereof |
| CN109820769A (en) * | 2019-03-14 | 2019-05-31 | 上海新高姿化妆品有限公司 | A kind of toner and preparation method thereof for having effects that moisturizing and releiving |
| CN110169944A (en) * | 2019-04-25 | 2019-08-27 | 上海百雀羚生物科技有限公司 | A kind of ageing-resistant skin care composition, its preparation process and application |
Non-Patent Citations (3)
| Title |
|---|
| 我的心机 玻尿酸雪藻保湿化妆水;东莞市捷司特化妆品有限公司;《网址：http://ftba.nmpa.gov.cn:8181/ftban/itownet/hzp_ba/fw/pz.jsp?processid=20160919145204otxyi&nid=20160919145204otxyi》;20160929;第1页 * |
| 爆水神器、爆水科技的出水霜都是水货？;佚名;《网址：https://www.truebuty.com/baoshui.html》;20160705;第1-4页 * |
| 百雀羚水光弹润弹力水（第2代）;上海百雀羚日用化学有限公司;《网址：http://ftba.nmpa.gov.cn:8181/ftban/itownet/hzp_ba/fw/pz.jsp?processid=201908131014170kh5v&nid=201908131014170kh5v》;20190814;第1页 * |
Also Published As
| Publication number | Publication date |
|---|---|
| CN110507594A (en) | 2019-11-29 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| US3485915A (en) | Thickened hydroxypropyl cellulose compositions | |
| EP2024476B1 (en) | Compositions comprising low-dp polymerized surfactants and methods of use thereof | |
| EP2611412B1 (en) | Crosslinked acrylic copolymers | |
| EP2585174B1 (en) | Low-irritating, clear cleansing compositions with relatively low ph | |
| CN110507594B (en) | Toning lotion and preparation method thereof | |
| JPS63185438A (en) | Stable and rapidly separable oil in water type emulsion | |
| EP0893117B2 (en) | Use of cationic copolymers as hair conditioning agents | |
| US10952953B2 (en) | Skin cleansing composition | |
| US20170224604A1 (en) | Cationic/cationogenic comb copolymer compositions and personal care products containing the same | |
| CN113181080A (en) | Transparent oil solution of phosphorylcholine polymer and its preparation method and use | |
| EP1967233B1 (en) | Aqueous external preparation for the treatment of scalp | |
| JPH06503566A (en) | Gel-type composition with improved oil control properties | |
| CN108473634A (en) | Including the flavor delivery composition of the copolymer of acryl lactam and alkyl methacrylate, preparation method and its application method | |
| CN101433504A (en) | Composition for protecting hair and shaping hair | |
| US11154476B2 (en) | Synergistic effects of alkanolamine alkylamides and other moisturizing agents | |
| CN108495615B (en) | Use of alkanolamine alkylamides as humectants | |
| KR102593543B1 (en) | Cosmetic Composition Capable of Phase-Inversion on Skin | |
| CN113348196A (en) | Alkylene oxide derivative, antifoaming agent, lubricant, cosmetic base material, and cosmetic, hair cleanser composition and body cleanser composition containing the cosmetic base material | |
| CN115040463A (en) | Anti-wrinkle whitening composition | |
| JPH0952814A (en) | Skin cosmetic composition | |
| JP6938105B2 (en) | Hair treatment composition and hair treatment mist cosmetics | |
| JP2002275027A (en) | Cosmetic and cosmetic impregnated in nonwoven fabric | |
| JPH09301838A (en) | Liquid hairdressing | |
| CN106333872A (en) | Hair styling compositions comprising maltodextrin/NVP copolymer | |
| JP4056948B2 (en) | Gel-like composition |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| GR01 | Patent grant | ||
| GR01 | Patent grant |