CN110506976A - A kind of full particle low temperature fuming liquids - Google Patents

A kind of full particle low temperature fuming liquids Download PDF

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Publication number
CN110506976A
CN110506976A CN201810486814.9A CN201810486814A CN110506976A CN 110506976 A CN110506976 A CN 110506976A CN 201810486814 A CN201810486814 A CN 201810486814A CN 110506976 A CN110506976 A CN 110506976A
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China
Prior art keywords
low temperature
fuming liquids
particles inside
temperature fuming
full particle
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Granted
Application number
CN201810486814.9A
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Chinese (zh)
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CN110506976B (en
Inventor
陈潜
谭超
范红梅
金勇�
李克
易建华
杜文
谭海风
王诗太
喻赛波
刘琦
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China Tobacco Hunan Industrial Co Ltd
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China Tobacco Hunan Industrial Co Ltd
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Publication date
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Priority to CN201810486814.9A priority Critical patent/CN110506976B/en
Priority to PCT/CN2019/078652 priority patent/WO2019223411A1/en
Priority to KR1020207036581A priority patent/KR102583754B1/en
Priority to US17/057,598 priority patent/US20210401030A1/en
Priority to JP2020563970A priority patent/JP7029553B2/en
Priority to EP19808374.3A priority patent/EP3797602A4/en
Publication of CN110506976A publication Critical patent/CN110506976A/en
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Publication of CN110506976B publication Critical patent/CN110506976B/en
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    • AHUMAN NECESSITIES
    • A24TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24BMANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
    • A24B15/00Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
    • A24B15/10Chemical features of tobacco products or tobacco substitutes
    • A24B15/16Chemical features of tobacco products or tobacco substitutes of tobacco substitutes

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  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Manufacture Of Tobacco Products (AREA)

Abstract

The present invention relates to a kind of full particle low temperature fuming liquids, are the smoker particles inside of 20-45 mesh including partial size;The low temperature fuming liquids are formed by smoker particles inside curing molding, have cavity structure in the low temperature fuming liquids.The present invention, which provides full particle low temperature fuming liquids, has special cavity structure, it can be achieved that surrounding and center are heated simultaneously, keeps smoke rapider;Smoker particles inside atomized inside agent of the invention and tobacco extract are evenly distributed, and smoke stability and uniformity are more preferable.Smoker particles inside surface of the invention has offal layer and outer shell, has largely blocked particle internal component and external contact, has more conducively stored, while largely having solved liquid object leakage problems.

Description

A kind of full particle low temperature fuming liquids
Technical field
The present invention relates to a kind of full particle low temperature fuming liquids more particularly to a kind of full particle low temperature hairs with cavity structure Smoke belongs to low temperature cigarette field.
Background technique
Generally raising with scientific and technological progress and people to health perception, new tobacco products present blowout hair Exhibition.The low temperature cigarette that do not burn is particularly subject to the attention of major research institution and enterprise as one type major product.Currently, city Low temperature on field do not burn cigarette product mainly using in special electric heater unit fill tobacco-containing material such as cigarette, pipe tobacco or Smoked sheet etc. evaporates the flue gas in tobacco fill material by electric heating, so that obtaining smoker is similar to conventional smoke The suction impression of grass.And the generally existing amount of smoke of low temperature fuming liquids of this form is insufficient, and front and back is uneven and suction oral account is few etc. Problem.Meanwhile existing low temperature smoking set is generally surrounding heating or center heating, the heat transfer rate of cigarette causes smoke fast more slowly Degree is also relatively slow, causes consumer experience sense poor.
Chinese patent CN201610232919 provides a kind of column of smoke suitable for low temperature cigarette, by tobacco particle, thermally conductive Component is molded with after mixing with adhesive, tobacco essence and humectant, which has smoke amount speed fast and more, is taken out Inhale smooth advantage, even if defect be the column of smoke be dried after it is still more damp, be unfavorable for storing, the strong easy to leak of hygroscopicity, sternly Ghost image rings its availability, its smoke stability and front and back homogeneity is all poor, while nicotine content excessively high irritation when sucking It is larger.
Summary of the invention
Present invention solves the technical problem that being, low temperature does not burn in the prior art, and cigarette smoke amount is insufficient, and fuming rate is slow, Puff number is few, and smoke stability and front and back homogeneity are poor, and fuming liquids permeability phenomenon easily occur when placing.
In order to solve the above-mentioned technical problem, technical scheme is as follows: a kind of full particle low temperature fuming liquids, including grain Diameter is the smoker particles inside of 20-45 mesh;The low temperature fuming liquids are formed by smoker particles inside curing molding, tool in the low temperature fuming liquids There is cavity structure.
In the present invention, low temperature fuming liquids are formed by the smoker particles inside curing molding with certain partial size, and low temperature fuming liquids are real Contain a large amount of gaps between the particle of center portion point, it is ensured that the flue gas that smoker particles inside generates is walked by smooth suction;Cavity structure Design, on the one hand can reduce the resistance to suction of full particle fuming liquids, guarantee suck it is more smooth, on the other hand, can centered on heat Protruding into for piece provides space, and the heating of low temperature fuming liquids surrounding and center heating can be achieved at the same time, promote fuming rate, guarantee smoke Body each section smoker particles inside obtains effective smoke and utilizes.
The low temperature fuming liquids are column, and cavity structure extends along low temperature fuming liquids length direction.
Further, the cross section of cavity structure is one of round, oval, rectangular, diamond shape, star.
Smoker particles inside has core-shell structure, and kernel includes carrier, smoke object, and shell is by the material with adhesive force It is made.Smoke object in this way is carried on carrier, so that being evenly distributed tobacco extract and Alevaire in kernel, guarantees smoke Amount promotes puff number;By the setting of coatings, smoke object can be effectively isolated from the outside, solve leakage problems.
Further, offal layer is equipped between kernel and shell.
The quality of smoker particles inside shell is the 0.1-5% of smoker particles inside gross mass, it is ensured that reduction pair while molding bonded Suck the influence of flavor.
The carrier includes tobacco-containing material and non-tobacco material, and the mass ratio of the two is 100:20-100.
Further, the tobacco-containing material and the partial size of non-tobacco material are 80-150 mesh.
Further, the non-tobacco material include microcrystalline cellulose, tealeaves, sugarcane fibre, ramie pulp fiber, bamboo fibre, At least one of cocoanut fiber, pre-gelatinized starch, coffee shell, dried peppermint leaf.The use of non-tobacco material can play dilution tobacco The effect of material, nicotine content is greatly reduced when making to suck, and reduces irritation;The use of some materials simultaneously, helps to be granulated The control of process or imparting smoker particles inside particularly suck flavor.
Further, the material with adhesive force includes hydroxypropyl methyl cellulose, hydroxypropyl cellulose, poly- dimension One of ketone, sodium carboxymethylcellulose, microcrystalline cellulose, polyethylene glycol, polyvinyl alcohol are a variety of, on the one hand, can partially hinder Exhausted particle atomized inside agent and tobacco extract externally leak, and make particle and have better appearance and mobility, while it this Body has adhesive force, and when subsequent processing can make quick molding bonded between smoker particles inside.
The smoke object includes tobacco extract and Alevaire, and the mass ratio of the two is 1-15:5-30.
Further, the Alevaire is the mixture of glycerol, propylene glycol, glycerine, and mass ratio is (0-10): (0-20): (0-30).
The preparation method of the smoker particles inside includes the following steps:
(1) in parts by mass, 0-200 parts of carrier 12,6-45 parts of smoke object, 0-25 parts of wetting agent are weighed, is uniformly mixed, is granulated, Obtain soft profit particle;
(2) using the material with adhesive force as raw material, the soft profit particle obtained to step (1) is coated processing, is sent out Smoke particle.
Further, further include the steps that wrapping up offal layer in soft profit particle surface, i.e., wrap up grain in soft profit particle surface Diameter is the offal of 80-150 mesh.Further, the mass ratio of offal layer and soft profit particle is 5-25:100.Soft profit particle surface packet Wrap up in offal after-fume grain color it is more attractive, close to tobacco true qualities, while offal can partially block the agent of particle atomized inside and cigarette Careless extract externally leaks.
Further, the wetting agent is water or alcohol, and suitable wetting agent can guarantee that smoker particles inside preferably forms.
Further, smoker particles inside is spherical or subsphaeroidal.
Moisture content is 8-20wt% in the smoker particles inside.Suitable moisture, which exists, to be conducive to excite smoke when subsequent processing The adhesive force of particle surface coating material enables quick molding bonded.
The partial size of smoker particles inside is 20-45 mesh.The too small then fuming liquids internal breathability of partial size is inadequate, influences smoke and sucks Feel;Not beautiful enough the fuming rate simultaneously of the excessive then fuming liquids appearance of partial size is slack-off.
The low temperature fuming liquids are by smoker particles inside microwave or heat cure obtained by molding.Microwave or heat cure processing make smoke Particle internal moisture is quickly volatilized, and fuming liquids moisture content on the one hand can be made to be down to reasonable level, and another aspect moisture evaporation seeps During out can excitating surface coating material adhesive force, so that good bond between smoker particles inside is shaped to the smoke of suitable shape Body.
Moisture content is 6-12wt% in the full particle low temperature fuming liquids.
The effecive porosity of the solid section of the full particle low temperature fuming liquids is 40-80%.Effecive porosity appropriate can Guarantee fuming liquids internal breathability, keeps its suction more easily smooth, smoke is more rapidly.
The low temperature fuming liquids can be used for surrounding heating, center heating or the two simultaneously both with low temperature smoking set.
Compared with prior art, beneficial effects of the present invention are as follows:
1, the present invention, which provides full particle low temperature fuming liquids, has special cavity structure, it can be achieved that surrounding and center are heated simultaneously, makes Smoke is rapider;
2, smoker particles inside atomized inside agent of the invention and tobacco extract are evenly distributed, and smoke stability and uniformity are more preferable.
3, smoker particles inside surface of the invention has offal layer and outer shell, has largely blocked particle internal component It with external contact, more conducively stores, while largely solving liquid object leakage problems.
4, smoker particles inside of the invention uses, and there is adhesive force material to be coated processing formation shell, very cleverly sharp With its isolation capacity and adhesive force, subsequent processing is not necessarily to be glued again, more conducively industrialized mass production.
Detailed description of the invention
Fig. 1 is the cross-sectional structure schematic diagram of low temperature fuming liquids in embodiment 1.
Fig. 2 is the cross-sectional structure schematic diagram of low temperature fuming liquids in embodiment 2.
Fig. 3 is the cross-sectional structure schematic diagram of low temperature fuming liquids in embodiment 3.
Specific embodiment
Below with reference to embodiment, the present invention will be described in detail.
Following embodiment is intended to illustrate summary of the invention, rather than further limits to the scope of the present invention.
Embodiment 1
In the present embodiment, low temperature fuming liquids the preparation method is as follows:
1) tobacco powder of 100 parts of 100-200 mesh, the microcrystalline cellulose of 50 parts of 100-200 mesh in parts by mass, are taken, takes 6 parts Tobacco extract, 5 parts of glycerol, 10 parts of glycerine, 12 part of 95% alcohol are sprayed in above-mentioned offal and mix after being mixed uniformly It closes uniform, extruding pelletization and obtains soft profit smoker particles inside;2) tobacco powder of 10 parts of 150-200 mesh is taken to be mixed with round as a ball, sieving takes 10-40 mesh particle, 50 DEG C dry to obtain smoker particles inside semi-finished product;3) 0.3 part of sodium carboxymethylcellulose is taken to be dissolved in 20 parts of water, to aforementioned Smoker particles inside semi-finished product are coated processing, and control smoker particles inside needed for finished particle moisture 15% obtains;4) certain mass is weighed Smoker particles inside be placed in special cylindrical empty cavity mould, mold center is oval solid post, suitably presses and is brought rapidly up To 100 DEG C, it is 10% or so that held for some time, which controls particle internal moisture, quickly cooling to room temperature, and smoker particles inside has been glued in mold Form stick, takes out up to required full particle low temperature fuming liquids, which is oblong cavity.The low temperature fuming liquids can be straight Connect and be filled in the low temperature cigarette smoking set of the heating of corresponding surrounding and/or center heating and suck material, also can cigarette used at cigarette shape In sucking, fuming rate is fast when sucking, and amount of smoke is sufficient and front and back uniformity is good, and puff number is more, and aroma quality is good.Fuming liquids are horizontal Schematic cross-section is as shown in Figure 1.
Embodiment 2
In the present embodiment, low temperature fuming liquids the preparation method is as follows:
1) tobacco powder of 100 parts of 120-200 mesh, the tea-leaf power of 0 part of 100-200 mesh in parts by mass, are taken, 12 parts of cigarettes are taken Careless extract, 10 parts of glycerol, 5 parts of propylene glycol, 10 parts of glycerine, 15 parts of water are sprayed in above-mentioned offal after being mixed uniformly And be uniformly mixed, extruding pelletization obtains soft profit particle;2) it takes the tobacco powder of 20 parts of 150-200 mesh to be mixed with round as a ball, sieving to take 10-40 mesh particle, 50 DEG C dry to obtain smoker particles inside semi-finished product;3) 1 part of povidone, 0.5 part of polyethylene glycol is taken to be dissolved in 20 parts of water, it is right Aforementioned smoker particles inside semi-finished product are coated processing, and control smoker particles inside needed for finished particle moisture 18% obtains;4) it weighs certain The smoker particles inside of quality is placed in special cylindrical cavity mold, and mold center is cuboid solid post, at appropriate pressure and microwave 45s is managed, quickly cooling to room temperature, smoker particles inside has been bonded to stick in mold, takes out up to required low temperature fuming liquids, in the fuming liquids The heart is rectangular cavity.The fillable low temperature cigarette in the heating of corresponding surrounding and/or center heating of the low temperature fuming liquids Smoking set, also can cigarette at cigarette shape for sucking, fuming rate is fast when sucking, and amount of smoke is sufficient and front and back uniformity is good, suction Mouth number is more, and aroma quality is good and has light tea perfume.Fuming liquids cross-sectional view is as shown in Figure 2.
Embodiment 3
In the present embodiment, low temperature fuming liquids the preparation method is as follows:
1) tobacco powder of 100 parts of 120-200 mesh, ramie pulp fiber, 20 part of 150 mesh of 30 parts of 100-200 mesh in parts by mass, are taken Starch, take 12 parts of tobacco extracts, 10 parts of glycerol, 5 parts of propylene glycol, 10 parts of glycerine, 15 parts of water, be mixed uniformly after spray It spills in above-mentioned offal and is uniformly mixed, extruding pelletization obtains soft profit particle;2) tobacco powder of 20 parts of 150-200 mesh is taken to mix therewith It closes round as a ball, sieving and takes 10-40 mesh particle, 50 DEG C dry to obtain smoker particles inside semi-finished product;3) 1 part of povidone, 0.5 part of polyethylene glycol are taken 20 parts of water are dissolved in, processing is coated to aforementioned smoker particles inside semi-finished product, and control smoke needed for finished particle moisture 18% obtains Grain;4) smoker particles inside for weighing certain mass is placed in special cylindrical cavity mold, and mold center is cylindrical, massive column, suitably Press simultaneously microwave treatment 45s, quickly cooling to room temperature, and smoker particles inside has been bonded to stick in mold, takes out up to required low temperature smoke Body, the fuming liquids center are circular cavity.
The fillable low temperature cigarette smoking set in the heating of corresponding surrounding and/or center heating of the low temperature fuming liquids, also Can cigarette at cigarette shape for sucking, fuming rate is fast when sucking, and amount of smoke is sufficient and front and back uniformity is good, and puff number is more, Aroma quality is good, and the moderate irritation of nicotine content is reduced.Fuming liquids cross-sectional view is as shown in Figure 3.
The content that above-described embodiment illustrates should be understood as that these embodiments are only used for being illustrated more clearly that the present invention, without For limiting the scope of the invention, after the present invention has been read, those skilled in the art are to various equivalent forms of the invention Modification each fall within the application range as defined in the appended claims.

Claims (10)

1. a kind of full particle low temperature fuming liquids, which is characterized in that be the smoker particles inside of 20-45 mesh including partial size;The low temperature hair Smoke is formed by smoker particles inside curing molding, has cavity structure in the low temperature fuming liquids.
2. full particle low temperature fuming liquids according to claim 1, which is characterized in that the low temperature fuming liquids are column, empty Cavity configuration extends along low temperature fuming liquids length direction.
3. full particle low temperature fuming liquids according to claim 1, which is characterized in that the cross section of cavity structure be it is round, One of oval, rectangular, diamond shape.
4. full particle low temperature fuming liquids according to claim 1, which is characterized in that smoker particles inside has core-shell structure, Kernel includes carrier, smoke object, and shell is made of the material with adhesive force.
5. full particle low temperature fuming liquids according to claim 4, which is characterized in that the carrier includes tobacco-containing material and non- Tobacco-containing material, the mass ratio of the two are 100:20-100.
6. full particle low temperature fuming liquids according to claim 4, which is characterized in that the smoke object includes tobacco extract And Alevaire, the mass ratio of the two are 1-15:5-30.
7. according to the described in any item full particle low temperature fuming liquids of claim 4-6, which is characterized in that the system of the smoker particles inside Preparation Method includes the following steps:
(1) in parts by mass, 0-200 parts of carrier 12,6-45 parts of smoke object, 0-25 parts of wetting agent are weighed, is uniformly mixed, is granulated, Obtain soft profit particle;
(2) using the material with adhesive force as raw material, the soft profit particle obtained to step (1) is coated processing, is sent out Smoke particle.
8. full particle low temperature fuming liquids according to claim 1, which is characterized in that moisture content is in the smoker particles inside 8-20wt%。
9. full particle low temperature fuming liquids according to claim 1, which is characterized in that water in the full particle low temperature fuming liquids Dividing content is 6-12wt%.
10. -9 described in any item full particle low temperature fuming liquids according to claim 1, which is characterized in that the full particle low temperature The effecive porosity of the solid section of fuming liquids is 40-80%.
CN201810486814.9A 2018-05-21 2018-05-21 Full-particle low-temperature smoke generator Active CN110506976B (en)

Priority Applications (6)

Application Number Priority Date Filing Date Title
CN201810486814.9A CN110506976B (en) 2018-05-21 2018-05-21 Full-particle low-temperature smoke generator
PCT/CN2019/078652 WO2019223411A1 (en) 2018-05-21 2019-03-19 Low-temperature smoking body and preparation method therefor
KR1020207036581A KR102583754B1 (en) 2018-05-21 2019-03-19 Low-temperature smoking body and method of manufacturing the same
US17/057,598 US20210401030A1 (en) 2018-05-21 2019-03-19 Low-temperature smoking body and preparation method thereof
JP2020563970A JP7029553B2 (en) 2018-05-21 2019-03-19 Low temperature smoker and its manufacturing method
EP19808374.3A EP3797602A4 (en) 2018-05-21 2019-03-19 Low-temperature smoking body and preparation method therefor

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Application Number Priority Date Filing Date Title
CN201810486814.9A CN110506976B (en) 2018-05-21 2018-05-21 Full-particle low-temperature smoke generator

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CN110506976A true CN110506976A (en) 2019-11-29
CN110506976B CN110506976B (en) 2022-02-08

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Cited By (4)

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CN111150108A (en) * 2020-01-17 2020-05-15 深圳新火瑞升技术有限公司 Functional barrier sheet for heating non-combustible cigarettes and preparation method and application thereof
CN112273706A (en) * 2020-10-19 2021-01-29 深圳波顿香料有限公司 Particle for heating non-combustible smoke and preparation method and application thereof
CN113502692A (en) * 2021-06-11 2021-10-15 云南中烟工业有限责任公司 Method for preparing material for heating cigarette to reduce temperature by adopting papermaking method
CN113545514A (en) * 2020-04-23 2021-10-26 云南中烟工业有限责任公司 Heating cigarette with self-bonding function

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CN107594634A (en) * 2017-09-27 2018-01-19 武汉市腾宁新材料科技有限公司 A kind of Electromagnetic Heating new type low temperature cigarette and preparation method and heating means

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Cited By (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111150108A (en) * 2020-01-17 2020-05-15 深圳新火瑞升技术有限公司 Functional barrier sheet for heating non-combustible cigarettes and preparation method and application thereof
CN111150108B (en) * 2020-01-17 2023-02-28 深圳新火瑞升技术有限公司 Functional barrier sheet for heating non-combustible cigarettes and preparation method and application thereof
CN113545514A (en) * 2020-04-23 2021-10-26 云南中烟工业有限责任公司 Heating cigarette with self-bonding function
CN112273706A (en) * 2020-10-19 2021-01-29 深圳波顿香料有限公司 Particle for heating non-combustible smoke and preparation method and application thereof
CN112273706B (en) * 2020-10-19 2022-08-12 深圳波顿香料有限公司 Particle for heating non-combustible smoke and preparation method and application thereof
CN113502692A (en) * 2021-06-11 2021-10-15 云南中烟工业有限责任公司 Method for preparing material for heating cigarette to reduce temperature by adopting papermaking method
CN113502692B (en) * 2021-06-11 2022-11-18 云南中烟工业有限责任公司 Method for preparing material for heating cigarette to reduce temperature by adopting papermaking method

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