CN110484377A - A kind of safe and efficient UV resin detergent and its preparation process and application method - Google Patents
A kind of safe and efficient UV resin detergent and its preparation process and application method Download PDFInfo
- Publication number
- CN110484377A CN110484377A CN201910662370.4A CN201910662370A CN110484377A CN 110484377 A CN110484377 A CN 110484377A CN 201910662370 A CN201910662370 A CN 201910662370A CN 110484377 A CN110484377 A CN 110484377A
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- Prior art keywords
- resin
- ether
- mixing
- safe
- diethylene glycol
- Prior art date
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Links
- 239000011347 resin Substances 0.000 title claims abstract description 56
- 229920005989 resin Polymers 0.000 title claims abstract description 56
- 239000003599 detergent Substances 0.000 title claims abstract description 30
- 238000000034 method Methods 0.000 title claims abstract description 16
- 238000002360 preparation method Methods 0.000 title claims abstract description 7
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 claims abstract description 62
- DNIAPMSPPWPWGF-UHFFFAOYSA-N Propylene glycol Chemical compound CC(O)CO DNIAPMSPPWPWGF-UHFFFAOYSA-N 0.000 claims abstract description 57
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 claims abstract description 19
- 239000011734 sodium Substances 0.000 claims abstract description 19
- 229910052708 sodium Inorganic materials 0.000 claims abstract description 19
- 239000002994 raw material Substances 0.000 claims abstract description 10
- MTHSVFCYNBDYFN-UHFFFAOYSA-N diethylene glycol Chemical compound OCCOCCO MTHSVFCYNBDYFN-UHFFFAOYSA-N 0.000 claims description 46
- 238000004140 cleaning Methods 0.000 claims description 18
- 239000004615 ingredient Substances 0.000 claims description 17
- 238000002156 mixing Methods 0.000 claims description 16
- SBZXBUIDTXKZTM-UHFFFAOYSA-N diglyme Chemical compound COCCOCCOC SBZXBUIDTXKZTM-UHFFFAOYSA-N 0.000 claims description 15
- 239000007788 liquid Substances 0.000 claims description 10
- 238000004806 packaging method and process Methods 0.000 claims description 6
- 238000011010 flushing procedure Methods 0.000 claims description 3
- 238000004519 manufacturing process Methods 0.000 claims description 3
- 238000003756 stirring Methods 0.000 claims description 3
- 238000003860 storage Methods 0.000 claims description 3
- 239000008399 tap water Substances 0.000 claims description 3
- 235000020679 tap water Nutrition 0.000 claims description 3
- 238000004506 ultrasonic cleaning Methods 0.000 claims description 3
- 239000012459 cleaning agent Substances 0.000 abstract description 4
- KFZMGEQAYNKOFK-UHFFFAOYSA-N Isopropanol Chemical group CC(C)O KFZMGEQAYNKOFK-UHFFFAOYSA-N 0.000 description 16
- 238000009835 boiling Methods 0.000 description 8
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 5
- 230000002209 hydrophobic effect Effects 0.000 description 5
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 5
- 231100000053 low toxicity Toxicity 0.000 description 4
- 239000007787 solid Substances 0.000 description 4
- 238000012360 testing method Methods 0.000 description 4
- UHOVQNZJYSORNB-UHFFFAOYSA-N Benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 description 3
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 description 3
- 235000019441 ethanol Nutrition 0.000 description 3
- 239000000203 mixture Substances 0.000 description 3
- 239000002904 solvent Substances 0.000 description 3
- 238000009736 wetting Methods 0.000 description 3
- CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 description 2
- HEDRZPFGACZZDS-UHFFFAOYSA-N Chloroform Chemical compound ClC(Cl)Cl HEDRZPFGACZZDS-UHFFFAOYSA-N 0.000 description 2
- LCGLNKUTAGEVQW-UHFFFAOYSA-N Dimethyl ether Chemical compound COC LCGLNKUTAGEVQW-UHFFFAOYSA-N 0.000 description 2
- JUJWROOIHBZHMG-UHFFFAOYSA-N Pyridine Chemical compound C1=CC=NC=C1 JUJWROOIHBZHMG-UHFFFAOYSA-N 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 238000011056 performance test Methods 0.000 description 2
- 239000002574 poison Substances 0.000 description 2
- 231100000614 poison Toxicity 0.000 description 2
- 238000010146 3D printing Methods 0.000 description 1
- 239000004215 Carbon black (E152) Substances 0.000 description 1
- 206010019233 Headaches Diseases 0.000 description 1
- 206010028813 Nausea Diseases 0.000 description 1
- 206010047700 Vomiting Diseases 0.000 description 1
- 239000003945 anionic surfactant Substances 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 239000002537 cosmetic Substances 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 239000006185 dispersion Substances 0.000 description 1
- 238000004945 emulsification Methods 0.000 description 1
- 239000006260 foam Substances 0.000 description 1
- 239000007789 gas Substances 0.000 description 1
- 239000008233 hard water Substances 0.000 description 1
- 231100000869 headache Toxicity 0.000 description 1
- 229930195733 hydrocarbon Natural products 0.000 description 1
- 150000002430 hydrocarbons Chemical class 0.000 description 1
- 238000012423 maintenance Methods 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 238000005259 measurement Methods 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 230000008693 nausea Effects 0.000 description 1
- 239000003960 organic solvent Substances 0.000 description 1
- 238000000016 photochemical curing Methods 0.000 description 1
- 231100000572 poisoning Toxicity 0.000 description 1
- 230000000607 poisoning effect Effects 0.000 description 1
- 238000007639 printing Methods 0.000 description 1
- UMJSCPRVCHMLSP-UHFFFAOYSA-N pyridine Natural products COC1=CC=CN=C1 UMJSCPRVCHMLSP-UHFFFAOYSA-N 0.000 description 1
- 230000029058 respiratory gaseous exchange Effects 0.000 description 1
- 239000000344 soap Substances 0.000 description 1
- 230000000638 stimulation Effects 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 239000000606 toothpaste Substances 0.000 description 1
- 229940034610 toothpaste Drugs 0.000 description 1
- 230000008673 vomiting Effects 0.000 description 1
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B08—CLEANING
- B08B—CLEANING IN GENERAL; PREVENTION OF FOULING IN GENERAL
- B08B3/00—Cleaning by methods involving the use or presence of liquid or steam
- B08B3/04—Cleaning involving contact with liquid
- B08B3/08—Cleaning involving contact with liquid the liquid having chemical or dissolving effect
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B08—CLEANING
- B08B—CLEANING IN GENERAL; PREVENTION OF FOULING IN GENERAL
- B08B3/00—Cleaning by methods involving the use or presence of liquid or steam
- B08B3/04—Cleaning involving contact with liquid
- B08B3/10—Cleaning involving contact with liquid with additional treatment of the liquid or of the object being cleaned, e.g. by heat, by electricity or by vibration
- B08B3/12—Cleaning involving contact with liquid with additional treatment of the liquid or of the object being cleaned, e.g. by heat, by electricity or by vibration by sonic or ultrasonic vibrations
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/02—Anionic compounds
- C11D1/12—Sulfonic acids or sulfuric acid esters; Salts thereof
- C11D1/14—Sulfonic acids or sulfuric acid esters; Salts thereof derived from aliphatic hydrocarbons or mono-alcohols
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/20—Organic compounds containing oxygen
- C11D3/2003—Alcohols; Phenols
- C11D3/2041—Dihydric alcohols
- C11D3/2044—Dihydric alcohols linear
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/20—Organic compounds containing oxygen
- C11D3/2068—Ethers
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D2111/00—Cleaning compositions characterised by the objects to be cleaned; Cleaning compositions characterised by non-standard cleaning or washing processes
- C11D2111/40—Specific cleaning or washing processes
- C11D2111/44—Multi-step processes
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Health & Medical Sciences (AREA)
- Emergency Medicine (AREA)
- General Chemical & Material Sciences (AREA)
- Detergent Compositions (AREA)
Abstract
The present invention relates to detergent technology technical field, a kind of safe and efficient UV resin detergent and its preparation process and application method are disclosed, it is configured by the raw material of following weight percentage: mixing-in fat ether 30-80%；Propylene glycol 10-50%；Sodium cetanesulfonate 0.1-20%；The cleaning agent is nonflammable, safer, and performance is more excellent.
Description
Technical field
The present invention relates to detergent technical fields, and in particular to a kind of safe and efficient UV resin detergent and its preparation work
Skill and application method.
Background technique
Cleaning is that 3D printing industry has to one of problems faced.The daily cleaning maintenance of 3D printer is (including flat
Platform and various accessories etc.), the model that prints is both needed to clean up could normal use.
Nowadays commonly using cleaning agent on the market is isopropanol, but there are a variety of hidden danger for the use of isopropanol: 1. isopropanols
It is highly inflammable, should be far from other fire sources such as heat source, sparks, it cannot be used for supersonic wave cleaning machine, this will come pole to cleaning tape
It is big inconvenient；Although 2. a small amount of isopropanol be it is safe, headache will be will lead to by being above safety value, and sucking a large amount of isopropanols will
It can cause nausea, vomiting even breathing suffering may cause inhalation poisoning；3. isopropanol can not effectively decompose the institute in resin
Have material, can only play the role of it is diluted, this will reuse during reaches saturation, may have on cleaning objects residual
It stays, so that surface is muddy, can not have the function that cleaning.
Summary of the invention
In view of the deficiencies of the prior art, the present invention intends to provide a kind of safe and efficient UV resin detergent
And clean method, for isopropanol, the detergent is nonflammable, and safer, performance is more excellent.
To achieve the goals above, the invention provides the following technical scheme:
A kind of safe and efficient UV resin detergent, it is configured by the raw material of following weight percentage:
Mixing-in fat ether 30-80%；
Propylene glycol 10-50%；
Sodium cetanesulfonate 0.1-20%.
In the present invention, it is preferred to, the weight percent of each raw material are as follows:
Mixing-in fat ether 40-75%；
Propylene glycol 20-50%；
Sodium cetanesulfonate 1-10%.
In the present invention, it is preferred to, the weight percent of each raw material are as follows:
Mixing-in fat ether 65%；
Propylene glycol 30%；
Sodium cetanesulfonate 5%.
In the present invention, it is preferred to, the mixing-in fat ether by diethylene glycol ether and diethylene glycol dimethyl ether by volume
1:1~1:3 mixing composition.
In the present invention, it is preferred to, the mixing-in fat ether by diethylene glycol ether and diethylene glycol dimethyl ether by volume
1:1.5~1:2 mixing composition.
In the present invention, it is preferred to, the mixing-in fat ether by diethylene glycol ether and diethylene glycol dimethyl ether by volume
1:1.8 mixing composition.
A kind of application method of safe and efficient UV resin detergent, comprising the following steps:
It S1, in temperature is to be uniformly mixed detergent in 15-25 DEG C of environment；
S2, UV resin to be cleaned is immersed in 5-30min in detergent, and brushes away that remove the UV resin surface more with soft
Remaining resin；
S3, UV resin is immersed in supersonic cleaning machine carries out ultrasonic cleaning 5-15min again；
S4, UV resin is taken out from the supersonic cleaning machine, removes the extra liquid of UV resin surface using compressed air
Body；
S5, UV resin is solidified under 405nm LED light；
S6, last flushing UV resin under flowing tap water.
A kind of preparation process of safe and efficient UV resin detergent, comprising the following steps:
Stock: various raw materials needed for production of resins are sent to workshop；
Ingredient premixing: diethylene glycol ether is put into barrel, blender is opened, sequentially adds diethylene glycol under the low speed
Methyl ether, propylene glycol, sodium cetanesulfonate adjust impeller at a distance from bucket bottom, improve wheel speed, continue after mixing
Stirring；
Packaging: qualified resin finished product, metering, packaging, storage are examined.
Sodium cetanesulfonate: yellowish liquid is a kind of anionic surfactant of good water solubility, has in hard water
Good wetting, emulsification, dispersion, foam and dirt-removing power, biological degradability is good, stimulates human body small；Propylene glycol: low toxicity, with
Water, ethyl alcohol and a variety of immiscible organic solvents can be used as wetting with glycerol or sorbierite cooperation in cosmetics, toothpaste and perfumed soap
Agent；Diethylene glycol dimethyl ether: low toxicity, colourless liquid, -58 DEG C of fusing point (- 71 DEG C), 84 DEG C of boiling point, relative density 0.8665 (20/4
DEG C), index of refraction 1.3796 0 DEG C of flash-point, can be miscible with water, alcohol, is dissolved in hydrocarbon solvent, there is strong ethereal odor；Diethylene glycol second
Ether: the product are high boiling solvent, and micro- poison is miscible with water, acetone, benzene, chloroform, ethyl alcohol, ether, pyridine etc., are used as solvent.
Table 1 is the property parameters of cleaning agent of the invention:
Table 1
| Project | Index |
| Sodium cetanesulfonate | It is small to human body stimulation, 192-193 DEG C of boiling point |
| Propylene glycol | Low toxicity, 99 DEG C of flash-point, 187.3 DEG C of boiling point |
| Diethylene glycol dimethyl ether | Low toxicity, 93 DEG C of flash-point, 84 DEG C of boiling point |
| Diethylene glycol ether | Micro- poison, 82 DEG C of flash-point, 180-190 DEG C of boiling point |
Isopropanol flash-point is 12 DEG C, and boiling point is 82 DEG C, and cleaning agent of the invention compares isopropanol flash-point as can be seen from Table 1
Height, boiling point is high, meanwhile, it is smaller to the harm of staff.
Compared with prior art, the beneficial effects of the present invention are:
Detergent flash-point of the invention is low nonflammable, this makes its application more extensive, and safety is higher.The detergent is set
Meter changes the chemical structure of resin, so that the uncured resin on printer model surface emulsifies, makes mainly for uncured resin
It is dissolved in cleaning solution, then is rinsed with clear water, can quickly and effectively remove printing accessory and photocuring finished product in this way
In be cured UV photopolymerization resin, and will not leave behind muddy residue.
Specific embodiment
It is clearly and completely described below in conjunction with the technical solution in the embodiment of the present invention, it is clear that described reality
Applying example is only a part of the embodiment of the present invention, instead of all the embodiments.Based on the embodiments of the present invention, this field is general
Logical technical staff every other embodiment obtained without making creative work belongs to what the present invention protected
Range.
It should be noted that it can be directly on another component when component is referred to as " being fixed on " another component
Or there may also be components placed in the middle.When a component is considered as " connection " another component, it, which can be, is directly connected to
To another component or it may be simultaneously present component placed in the middle.When a component is considered as " being set to " another component, it
It can be and be set up directly on another component or may be simultaneously present component placed in the middle.Term as used herein is " vertical
", " horizontal ", "left", "right" and similar statement for illustrative purposes only.
Unless otherwise defined, all technical and scientific terms used herein and belong to technical field of the invention
The normally understood meaning of technical staff is identical.Term as used herein in the specification of the present invention is intended merely to description tool
The purpose of the embodiment of body, it is not intended that in the limitation present invention.Term " and or " used herein includes one or more phases
Any and all combinations of the listed item of pass.
A kind of safe and efficient UV resin preparation process, specifically includes the following steps:
Stock: various raw materials needed for production of resins are sent to workshop；
Ingredient premixing: diethylene glycol ether is put into barrel, blender is opened, sequentially adds diethylene glycol under the low speed
Methyl ether, propylene glycol, sodium cetanesulfonate adjust impeller at a distance from bucket bottom, improve wheel speed, continue after mixing
Stirring；
Packaging: qualified resin finished product, metering, packaging, storage are examined.
Embodiment 1: the concrete content for each ingredient being added in the ingredient pre-mixing process is as follows
Mixing-in fat ether includes that 1:1 is mixed by volume for diethylene glycol ether and diethylene glycol dimethyl ether；
Mixing-in fat ether 30%；
Propylene glycol 50%；
Sodium cetanesulfonate 20%.
Embodiment 2: the concrete content for each ingredient being added in the ingredient pre-mixing process is as follows
Mixing-in fat ether includes that 1:1 is mixed by volume for diethylene glycol ether and diethylene glycol dimethyl ether；
Mixing-in fat ether 80%；
Propylene glycol 10%；
Sodium cetanesulfonate 10%.
Embodiment 3: the concrete content for each ingredient being added in the ingredient pre-mixing process is as follows
Mixing-in fat ether includes that 1:1 is mixed by volume for diethylene glycol ether and diethylene glycol dimethyl ether；
Mixing-in fat ether 65%；
Propylene glycol 30%；
Sodium cetanesulfonate 5%.
Embodiment 4: the concrete content for each ingredient being added in the ingredient pre-mixing process is as follows
Mixing-in fat ether includes that 1:1.5 is mixed by volume for diethylene glycol ether and diethylene glycol dimethyl ether；
Mixing-in fat ether 65%；
Propylene glycol 30%；
Sodium cetanesulfonate 5%.
Embodiment 5: the concrete content for each ingredient being added in the ingredient pre-mixing process is as follows
Mixing-in fat ether includes that 1:1.8 is mixed by volume for diethylene glycol ether and diethylene glycol dimethyl ether；
Mixing-in fat ether 65%；
Propylene glycol 30%；
Sodium cetanesulfonate 5%.
Embodiment 6: the concrete content for each ingredient being added in the ingredient pre-mixing process is as follows
Mixing-in fat ether includes that 1:2 is mixed by volume for diethylene glycol ether and diethylene glycol dimethyl ether；
Mixing-in fat ether 65%；
Propylene glycol 30%；
Sodium cetanesulfonate 5%.
Embodiment 7: the concrete content for each ingredient being added in the ingredient pre-mixing process is as follows
Mixing-in fat ether includes that 1:3 is mixed by volume for diethylene glycol ether and diethylene glycol dimethyl ether；
Mixing-in fat ether 65%；
Propylene glycol 30%；
Sodium cetanesulfonate 5%.
The UV resin clean hydrophobicity made to embodiment 1- embodiment 7 is tested, and test result is as shown in table 1,
Wherein using contact angle tester test, (contact angle refers to solution-air circle made by gas, liquid, solid three-phase point of intersection to hydrophobic performance
The tangent line in face, this tangent line are the measurements of wetness degree in the angle theta between solid-liquid boundary line of one side of liquid；If θ < 90 °,
Then the surface of solids is hydrophilic, i.e., liquid is easier to wetting solid, and angle is smaller, indicates that wetability is better；If θ > 90 °, Gu
Body surface face be it is hydrophobic, i.e., liquid is not easily wetted by solid, be easy move on the surface), droplet size be 2 μ L.
2. hydrophobic performance test result of table
| Project | Embodiment 1 | Embodiment 2 | Embodiment 3 | Embodiment 4 | Embodiment 5 | Embodiment 6 | Embodiment 7 |
| Contact angle | 130° | 125° | 140° | 135° | 150° | 145° | 130° |
Embodiment 1- embodiment 3 is compared, the contact angle that embodiment 3 measures it can be seen from the data in table 2
Numerical value is maximum, is 140 °, it is known that the detergent hydrophobic performance in embodiment 3 is preferable；Embodiment 3- embodiment 7 is compared,
The numerical value for the contact angle that embodiment 5 measures is maximum, is 150 °, it is known that the cleaning hydrophobic performance in embodiment 5 is optimal.
The UV resin clean-up performance made to embodiment 1- embodiment 7 is tested, and test result is as shown in table 3, wherein
Self-cleaning performance test method, comprising the following steps:
It S1, in temperature is to be uniformly mixed detergent in 25 DEG C of environment；
S2, UV resin to be cleaned is immersed in 20min in detergent, and brushes away that remove the UV resin surface extra with soft
Resin；
S3, UV resin is immersed in supersonic cleaning machine carries out ultrasonic cleaning 10min again；
S4, UV resin is taken out from the supersonic cleaning machine, removes the extra liquid of UV resin surface using compressed air
Body；
S5, UV resin is solidified under 405nm LED light；
S6, last flushing UV resin under flowing tap water.
The test of 3. clean-up performance of table
Embodiment 1- embodiment 3 is compared, embodiment 3 measures the cleaning of UV resin it can be seen from the data in table 3
Degree is maximum, is 95%, it is known that the content of each component is optimal proportion in embodiment 3, so that the cleaning effect of detergent is preferable；
Embodiment 3- embodiment 7 is compared, it is 99%, it is known that embodiment 5 is mixed that embodiment 5, which measures UV resin clean-up performance maximum,
Closing ether is optimal proportion, and the cleaning effect of detergent is best.
Above description is the detailed description for the present invention preferably possible embodiments, but embodiment is not limited to this hair
Bright patent claim, it is all the present invention suggested by technical spirit under completed same changes or modifications change, should all belong to
In the covered the scope of the patents of the present invention.
Claims (8)
1. a kind of safe and efficient UV resin detergent, which is characterized in that it be by following weight percentage raw material configuration and
At:
Mixing-in fat ether 30-80%；
Propylene glycol 10-50%；
Sodium cetanesulfonate 0.1-20%.
2. a kind of safe and efficient UV resin detergent according to claim 1, which is characterized in that the weight of each raw material
Measure percentage are as follows:
Mixing-in fat ether 40-75%；
Propylene glycol 20-50%；
Sodium cetanesulfonate 1-10%.
3. a kind of safe and efficient UV resin detergent according to claim 1, which is characterized in that the weight of each raw material
Measure percentage are as follows:
Mixing-in fat ether 65%；
Propylene glycol 30%；
Sodium cetanesulfonate 5%.
4. a kind of safe and efficient UV resin detergent according to any one of claim 1-3, which is characterized in that described
Mixing-in fat ether is made of diethylene glycol ether and diethylene glycol dimethyl ether 1:1~1:3 mixing by volume.
5. a kind of safe and efficient UV resin detergent according to claim 4, which is characterized in that the mixing-in fat ether
It is made of the 1:1.5~1:2 mixing by volume of diethylene glycol ether and diethylene glycol dimethyl ether.
6. a kind of safe and efficient UV resin detergent according to claim 4, which is characterized in that the mixing-in fat ether
It is made of the 1:1.8 mixing by volume of diethylene glycol ether and diethylene glycol dimethyl ether.
7. a kind of application method of safe and efficient UV resin detergent, which comprises the following steps:
It S1, in temperature is to be uniformly mixed detergent in 15-25 DEG C of environment；
S2, UV resin to be cleaned is immersed in 5-30min in detergent, and brushes away that remove the UV resin surface extra with soft
Resin；
S3, UV resin is immersed in supersonic cleaning machine carries out ultrasonic cleaning 5-15min again；
S4, UV resin is taken out from the supersonic cleaning machine, removes the extra liquid of UV resin surface using compressed air；
S5, UV resin is solidified under 405nm LED light；
S6, last flushing UV resin under flowing tap water.
8. a kind of preparation process of safe and efficient UV resin detergent, which comprises the following steps:
Stock: various raw materials needed for production of resins are sent to workshop；
Ingredient premixing: diethylene glycol ether is put into barrel, blender is opened, sequentially adds diethylene glycol first under the low speed
Ether, propylene glycol, sodium cetanesulfonate adjust impeller at a distance from bucket bottom, improve wheel speed, persistently stir after mixing
It mixes；
Packaging: qualified resin finished product, metering, packaging, storage are examined.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201910662370.4A CN110484377B (en) | 2019-07-22 | 2019-07-22 | UV resin cleaning agent and preparation process and use method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201910662370.4A CN110484377B (en) | 2019-07-22 | 2019-07-22 | UV resin cleaning agent and preparation process and use method thereof |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN110484377A true CN110484377A (en) | 2019-11-22 |
| CN110484377B CN110484377B (en) | 2021-03-23 |
Family
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|---|---|---|---|
| CN201910662370.4A Active CN110484377B (en) | 2019-07-22 | 2019-07-22 | UV resin cleaning agent and preparation process and use method thereof |
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| CN (1) | CN110484377B (en) |
Citations (12)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH09208992A (en) * | 1996-01-29 | 1997-08-12 | Daicel Chem Ind Ltd | Resin composition for cleaning |
| JPH11116993A (en) * | 1997-10-21 | 1999-04-27 | Uni Charm Corp | Detergent composition and fiber sheet impregnated therewith |
| US20030059708A1 (en) * | 2000-06-09 | 2003-03-27 | Tetsuya Yamamura | Resin composition and three-dimensional object |
| CN1418942A (en) * | 2001-11-14 | 2003-05-21 | 金元振 | Detergent for high molecular synthetic resin spectacle lens and moulding die |
| KR20090088578A (en) * | 2008-02-15 | 2009-08-20 | 주식회사 케이알씨 | Resin composition su khem characteristic scale removal tax administration me |
| CN103119105A (en) * | 2010-09-27 | 2013-05-22 | 伊士曼化工公司 | Polymeric or monomeric compositions comprising at least one mono-amide and/or at least one diamide for removing substances from substrates and methods of using the same |
| CN105039022A (en) * | 2015-06-05 | 2015-11-11 | 柳州立洁科技有限公司 | Resin cleaning agent |
| CN105039025A (en) * | 2015-06-04 | 2015-11-11 | 宁夏共享化工有限公司 | Cleaning agent for cleaning 3D-type sand printing head and preparation method of cleaning agent |
| CN105062706A (en) * | 2015-08-14 | 2015-11-18 | 上海奈拓化工科技有限公司 | High-precision ultrasonic cleaning agent for glass mould used in resin optical lens mold closing |
| CN106475521A (en) * | 2016-08-01 | 2017-03-08 | 苏州聚复高分子材料有限公司 | A kind of metal casting part preparation method based on 3D printing technique |
| CN108048233A (en) * | 2017-12-29 | 2018-05-18 | 广东铁科灌浆科技有限公司 | Epoxy resin cleaning agent and preparation method thereof |
| CN109054071A (en) * | 2018-07-20 | 2018-12-21 | 宁波市石生科技有限公司 | A kind of aftertreatment technology of 3D printing part |
-
2019
- 2019-07-22 CN CN201910662370.4A patent/CN110484377B/en active Active
Patent Citations (12)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH09208992A (en) * | 1996-01-29 | 1997-08-12 | Daicel Chem Ind Ltd | Resin composition for cleaning |
| JPH11116993A (en) * | 1997-10-21 | 1999-04-27 | Uni Charm Corp | Detergent composition and fiber sheet impregnated therewith |
| US20030059708A1 (en) * | 2000-06-09 | 2003-03-27 | Tetsuya Yamamura | Resin composition and three-dimensional object |
| CN1418942A (en) * | 2001-11-14 | 2003-05-21 | 金元振 | Detergent for high molecular synthetic resin spectacle lens and moulding die |
| KR20090088578A (en) * | 2008-02-15 | 2009-08-20 | 주식회사 케이알씨 | Resin composition su khem characteristic scale removal tax administration me |
| CN103119105A (en) * | 2010-09-27 | 2013-05-22 | 伊士曼化工公司 | Polymeric or monomeric compositions comprising at least one mono-amide and/or at least one diamide for removing substances from substrates and methods of using the same |
| CN105039025A (en) * | 2015-06-04 | 2015-11-11 | 宁夏共享化工有限公司 | Cleaning agent for cleaning 3D-type sand printing head and preparation method of cleaning agent |
| CN105039022A (en) * | 2015-06-05 | 2015-11-11 | 柳州立洁科技有限公司 | Resin cleaning agent |
| CN105062706A (en) * | 2015-08-14 | 2015-11-18 | 上海奈拓化工科技有限公司 | High-precision ultrasonic cleaning agent for glass mould used in resin optical lens mold closing |
| CN106475521A (en) * | 2016-08-01 | 2017-03-08 | 苏州聚复高分子材料有限公司 | A kind of metal casting part preparation method based on 3D printing technique |
| CN108048233A (en) * | 2017-12-29 | 2018-05-18 | 广东铁科灌浆科技有限公司 | Epoxy resin cleaning agent and preparation method thereof |
| CN109054071A (en) * | 2018-07-20 | 2018-12-21 | 宁波市石生科技有限公司 | A kind of aftertreatment technology of 3D printing part |
Non-Patent Citations (2)
| Title |
|---|
| 王洪福: "气质联用技术在3D打印材料国产化中的应用", 《中国测试》 * |
| 陆其明: "异丙醇的毒性及卫生标准研究", 《职业医学》 * |
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