CN110448472A - 一种水油双相即时混合的面膜液及其制备方法 - Google Patents
一种水油双相即时混合的面膜液及其制备方法 Download PDFInfo
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Abstract
本发明提供了一种水油双相即时混合的面膜液及其制备方法,属于护肤品技术领域,所述面膜液包括水相和油相;所述水相和油相单独包装,使用时即时混合;所述水相和油相的混合质量比为(20~30):(2~5);所述水相包括保湿剂、增稠剂、水溶性功效添加剂、助剂和水,质量比为(0.1~20):(0.1~15):(0.1~15):(0.1~5):(45~99.5);所述油相包括润肤剂、油溶性功效添加剂和乳化剂,质量比为(80~100):(0.1~15):(0.1~5);本发明所述面膜液质地清爽温和不黏腻,不刺激皮肤,不加重皮肤负担。
Description
技术领域
本发明属于护肤品技术领域,尤其涉及一种水油双相即时混合的面膜液及其制备方法。
背景技术
护肤品种类繁多,面膜由于其即时效果明显一直倍受青睐,尤其受女性消费者喜爱。面膜起源早,且适用性较强,而面膜的形式,现在主要有泥膏型、撕拉型、冻胶型、湿纸巾型四种。随着人们生活水平的提高,消费者对皮肤护理的要求越来越高,市面上的产品多以水剂为主,而单一的水剂面膜液往往缺乏“滋润感”,而单纯的护肤油类产品,自然不够清爽,所以乳液往往成为对肤感要求较高的消费者的选择,而乳液油水混合的形式,油相和水相混合保存的状态,需要更多稳定剂和乳化剂的维持,对皮肤刺激较大,护肤效果并不理想。
发明内容
有鉴于此,本发明的目的在于提供一种水油双相即时混合的面膜液及其制备方法,将水相和油相单独包装,在使用时混合,能够即时乳化,质地清爽温和不黏腻,不会造成过敏刺激以及厚重、起皮等不良影响,也不会加重皮肤的负担。
为了实现上述发明目的,本发明提供了以下技术方案:
本发明提供了一种水油双相即时混合的面膜液,包括水相和油相;所述水相和油相单独包装,使用时即时混合;所述水相和油相的混合质量比为(20~30):(2~5);
所述水相包括保湿剂、增稠剂、水溶性功效添加剂、助剂和水;所述保湿剂、增稠剂、水溶性功效添加剂、助剂和水的质量比为(0.1~20):(0.1~15):(0.1~15):(0.1~5):(45~99.5);
所述油相包括润肤剂、油溶性功效添加剂和乳化剂;所述润肤剂、油溶性功效添加剂和乳化剂的质量比为(80~100):(0.1~15):(0.1~5)。
优选的,所述乳化剂选自PPG-13-癸基十四醇聚醚-24、PPG-20-癸基十四醇聚醚-10、PPG-6-癸基十四醇聚醚-12、PPG-6-癸基十四醇聚醚-20、PPG-6-癸基十四醇聚醚-30和PEG-60氢化蓖麻油中的一种或几种。
优选的,所述润肤剂选自辛酸/癸酸甘油三酯、棕榈酸乙基己酯、异十六烷、棕榈酸异丙酯、氢化聚癸烯、异十二烷、异壬酸异壬酯、氢化聚异丁烯、鲸蜡醇乙基己酸酯、角鲨烷、辛基十二醇、碳酸二辛酯、山梨坦辛酸酯中的一种或几种。
优选的,所述水溶性功效添加剂包括肌肽、乙酰基六肽-8、寡肽-1、九肽-1、胶原蛋白、胶原、酵母提取物、维生素C、传明酸、甘草黄酮、阿魏酸、精氨酸、赖氨酸、积雪草提取物、乳糖酸中的一种或几种;所述油溶性功效添加剂包括油溶性的虾青素、油菜甾醇类、山茶籽油、霍霍巴籽油、生育酚、氢化大豆磷脂、毛瑞榈果油、倒地铃花/叶/藤提取物、洋蓝蓟果油、向日葵籽油不皂化物、甜扁桃油、石栗籽油、牡丹籽油、卵磷脂中的一种或几种。
优选的,所述保湿剂选自丁二醇、丙二醇、二丙二醇、山梨醇、甘露糖醇、甜菜碱、透明质酸钠、海藻多糖、葡聚糖、赤藓醇、泛醇中的一种或几种。
优选的,所述增稠剂选自羟乙基纤维素、羟丙基甲基纤维素、聚丙烯酸酯交联聚合物-6、黄原胶、结冷胶、卡波姆、聚丙烯酸钠、聚丙烯酰胺、甘油聚丙烯酸酯中的一种或几种。
优选的,所述助剂选自防腐剂、抗敏感剂、芳香剂、pH调节剂中的一种或多种。
优选的,所述抗敏感剂选自甘草酸二钾、红没药醇、马齿苋提取物、尿囊素、粉防己甲素、辣蓼提取物、白薇提取物、艾叶提取物中的一种或多种。
优选的,所述pH调节剂选自氨甲基丙醇、酒石酸、柠檬酸、三乙醇胺、柠檬酸钠中的一种或多种。
本发明提供了所述面膜液的制备方法,包括以下步骤:
1)将所述水相的组分混合制备获得水相;
2)将所述油相的组分混合制备获得油相。
本发明的有益效果:本发明提供的水油双相即时混合的面膜液,包括水相和油相;所述水相和油相单独包装,使用时即时混合,得到即时乳化的乳液型面膜液,即时乳化的乳液型面膜液与成品乳液或乳状面膜液相比,乳化剂的使用量少,对皮肤的刺激更小。
进一步的,本发明所述的面膜液优选的采用乳化剂PPG-13-癸基十四醇聚醚-24,在使用时,将所述水相和油相混合,能够实现即时乳化,由于PPG-13-癸基十四醇聚醚-24独特的增容能力和肤感,仅需要极少量即可达到乳化效果,使油相变得清爽,使水相变得滋润。
本发明提供的水油双相即时混合的面膜液,在使用时,质地清爽温和不黏腻,不会造成过敏刺激、厚重、起皮等不良影响,不会增加皮肤的负担;本发明所述的水相和油相,可以作为功效物载体,可将各类功效活性物加入到水相或者油相,增强单一水剂面膜液的滋润感,又将油溶性活性物有效的即时乳化,更便于皮肤吸收,非常灵活。
具体实施方式
本发明提供了一种水油双相即时混合的面膜液,包括水相和油相;所述水相和油相单独包装,使用时即时混合;所述水相和油相的混合质量比为(20~30):(2~5);所述水相包括保湿剂、增稠剂、水溶性功效添加剂、助剂和水;所述保湿剂、增稠剂、水溶性功效添加剂、助剂和水的质量比为(0.1~20):(0.1~15):(0.1~15):(0.1~5):(45~99.5);所述油相包括润肤剂、油溶性功效添加剂和乳化剂;所述润肤剂、油溶性功效添加剂和乳化剂的质量比为(80~100):(0.1~15):(0.1~5)。
在本发明中,所述水相和油相的混合质量比优选为(22~28):(3~4),更优选为(24~26):3。
在本发明中,所述保湿剂、增稠剂、水溶性功效添加剂、助剂和水的质量比优选为(0.1~20):(0.1~15):(0.1~15):(0.1~5):(45~99.5),更优选为(3~13):(0.15~0.3):(0.5~12):(0.3~4):(80~90)。
在本发明中,所述乳化剂选自PPG-13-癸基十四醇聚醚-24、PPG-20-癸基十四醇聚醚-10、PPG-6-癸基十四醇聚醚-12、PPG-6-癸基十四醇聚醚-20、PPG-6-癸基十四醇聚醚-30和PEG-60氢化蓖麻油中的一种或几种,优选的为PPG-13-癸基十四醇聚醚-24,所述PPG-13-癸基十四醇聚醚-24具有高极性,增溶能力强且肤感不黏腻;采用所述PPG-13-癸基十四醇聚醚-24作为乳化剂添加量少,能够实现即时乳化,乳化效果好。
在本发明中,所述润肤剂选自辛酸/癸酸甘油三酯、棕榈酸乙基己酯、异十六烷、棕榈酸异丙酯、氢化聚癸烯、异十二烷、异壬酸异壬酯、氢化聚异丁烯、鲸蜡醇乙基己酸酯、角鲨烷、辛基十二醇、碳酸二辛酯、山梨坦辛酸酯中的一种或几种。
在本发明中,所述水溶性功效添加剂包括水溶性的美白剂、抗衰老剂、防蓝光剂、抗皱剂、消炎剂和修复剂中的一种或几种;所述油溶性功效添加剂包括油溶性的美白剂、抗衰老剂、防蓝光剂、抗皱剂、消炎剂和修复剂中的一种或几种。本发明对所述水溶性功效添加剂和油溶性功效添加剂的具体种类没有特殊限定,具有美白、抗衰老、防蓝光、抗皱、消炎、去黑眼圈、***和修复等功效的成分均可以。
在本发明中,所述保湿剂选自丁二醇、丙二醇、二丙二醇、山梨醇、甘露糖醇、甜菜碱、透明质酸钠、海藻多糖、葡聚糖、赤藓醇、泛醇中的一种或几种;所述增稠剂选自羟乙基纤维素、羟丙基甲基纤维素、聚丙烯酸酯交联聚合物-6、黄原胶、结冷胶、卡波姆、聚丙烯酸钠、聚丙烯酰胺、甘油聚丙烯酸酯中的一种或几种。
在本发明中,所述助剂选自防腐剂、抗敏感剂、芳香剂、pH调节剂中的一种或多种。所述抗敏感剂优选的选自甘草酸二钾、红没药醇、马齿苋提取物、尿囊素、粉防己甲素、辣蓼提取物、白薇提取物、艾叶提取物中的一种或几种;所述pH调节剂优选的选自氨甲基丙醇、酒石酸、柠檬酸、三乙醇胺、柠檬酸钠中的一种或多种。
本发明对上述原料的来源没有特殊限定,采用本领域常规的市售产品即可。
本发明还提供了所述面膜液的制备方法,包括以下步骤:1)将所述水相的组分混合制备获得水相;2)将所述油相的组分混合制备获得油相。本发明对步骤1)和步骤2)中所述的混合的方法没有特殊限定,采用本领域常规的方法即可。在本发明中,所述水相和油相单独包装;在使用时,优选的将所述油相加入到水相中,实现即时乳化,然后使用。本发明中,所述面膜液可以直接涂抹使用,也可以浸泡面膜纸后使用。
下面结合实施例对本发明提供的技术方案进行详细的说明,但是不能把它们理解为对本发明保护范围的限定。
实施例1
一种水油双相即时混合的面膜液
水相:
油相:
PEG-60氢化蓖麻油 1.00%,
生育酚(维生素E) 0.50%,
辛酸/癸酸甘油三酯 余量。
其中,面膜液中水相质量为25g,油相质量为3g;水相和油相单独包装,使用时即时混合。
实施例2
一种水油双相即时混合的面膜液
水相:
油相:
PPG-20-癸基十四醇聚醚-10 1.00%,
生育酚(维生素E) 0.50%,
辛酸/癸酸甘油三酯 余量。
其中,面膜液中水相质量为25g,油相质量为3g;水相和油相单独包装,使用时即时混合。
实施例3
一种水油双相即时混合的面膜液
水相:
油相:
PPG-13-癸基十四醇聚醚-24 1.00%,
生育酚(维生素E) 0.50%,
辛酸/癸酸甘油三酯 余量。
其中,面膜液中水相质量为25g,油相质量为3g;水相和油相单独包装,使用时即时混合。
对比测试:
30名志愿者左右脸分别对比A样品与C样品,同时左右臂比较B样品与C样品,其中:A样品为实施例1的产品;B样品为实施例2的产品;C样品为实施例3的产品。
经过统计,对比A样品与C样品的30名志愿者中,27名志愿者认为A样品比C样品黏腻,3人无明显差异感。30名志愿者认为B样品与C样品无明显肤感差异,但混合后C样品外观更白更细腻,乳化状态优于B样品。
由统计结果可以看出,实施例3的产品体验感优于实施例1和实施例2;这是因为实施例3中使用乳化剂PPG-13-癸基十四醇聚醚-24具有高极性,增溶能力强且肤感不黏腻的特点。
实施例4
一种水油双相即时混合的面膜液
水相:
油相:
其中,面膜液中水相质量为30g,油相质量为3g;水相和油相单独包装,使用时即时混合。
实施例5
一种水油双相即时混合的面膜液
水相:
油相:
其中,面膜液中水相质量为25g,和油相质量为3g。
实施例6
一种水油双相即时混合的面膜液
水相:
油相:
PPG-13-癸基十四醇聚醚-24 1.00%,
生育酚(维生素E) 0.50%,
辛酸/癸酸甘油三酯 余量。
其中,面膜液中水相质量为20g,油相质量为5g,水相和油相单独包装,使用时即时混合。
对比测试:
比较实施例3-6的产品,对其体验感和安全性进行评价,并统计志愿者经受试者反馈。体验评价分最高为5分,表示非常喜欢非常棒,最低为0分,表示有不适感。根据30位志愿者的评分,统计平均分以及产品的安全性。经受试者反馈,实施例3-实施例6的产品体验感平均分为4.2~4.8,无人有不适感,详见表1。结果表明,本发明的面膜贴体验感较好,安全性较高,具有开发潜力。
表1.体验感和安全性评价统计
选项 | 体验平均分 | 安全刺激性 | 比例% |
实施例3 | 4.8 | 0 | 0 |
实施例4 | 4.2 | 0 | 0 |
实施例5 | 4.6 | 0 | 0 |
实施例6 | 4.5 | 0 | 0 |
由上述实施例可知,本发明所述的面膜液,在使用时,将所述水相和油相混合,能够实现即时乳化,采用PPG-13-癸基十四醇聚醚-24作为乳化剂,仅需要极少量即可达到乳化效果,使油相变得清爽,使水相变得滋润;质地清爽温和不黏腻,不会造成过敏刺激、厚重、起皮等不良影响,不会增加皮肤的负担。
以上所述仅是本发明的优选实施方式,应当指出,对于本技术领域的普通技术人员来说,在不脱离本发明原理的前提下,还可以做出若干改进和润饰,这些改进和润饰也应视为本发明的保护范围。
Claims (10)
1.一种水油双相即时混合的面膜液,其特征在于,包括水相和油相;所述水相和油相单独包装,使用时即时混合;所述水相和油相的混合质量比为(20~30):(2~5);
所述水相包括保湿剂、增稠剂、水溶性功效添加剂、助剂和水;所述保湿剂、增稠剂、水溶性功效添加剂、助剂和水的质量比为(0.1~20):(0.1~15):(0.1~15):(0.1~5):(45~99.5);
所述油相包括润肤剂、油溶性功效添加剂和乳化剂;所述润肤剂、油溶性功效添加剂和乳化剂的质量比为(80~100):(0.1~15):(0.1~5)。
2.根据权利要求1所述的面膜液,其特征在于,所述乳化剂选自PPG-13-癸基十四醇聚醚-24、PPG-20-癸基十四醇聚醚-10、PPG-6-癸基十四醇聚醚-12、PPG-6-癸基十四醇聚醚-20、PPG-6-癸基十四醇聚醚-30和PEG-60氢化蓖麻油中的一种或几种。
3.根据权利要求1或2所述的面膜液,其特征在于,所述润肤剂选自辛酸/癸酸甘油三酯、棕榈酸乙基己酯、异十六烷、棕榈酸异丙酯、氢化聚癸烯、异十二烷、异壬酸异壬酯、氢化聚异丁烯、鲸蜡醇乙基己酸酯、角鲨烷、辛基十二醇、碳酸二辛酯、山梨坦辛酸酯中的一种或几种。
4.根据权利要求1所述的面膜液,其特征在于,所述水溶性功效添加剂包括肌肽、乙酰基六肽-8、寡肽-1、九肽-1、胶原蛋白、胶原、酵母提取物、维生素C、传明酸、甘草黄酮、阿魏酸、精氨酸、赖氨酸、积雪草提取物、乳糖酸中的一种或几种;所述油溶性功效添加剂包括油溶性的虾青素、油菜甾醇类、山茶籽油、霍霍巴籽油、生育酚、氢化大豆磷脂、毛瑞榈果油、倒地铃花/叶/藤提取物、洋蓝蓟果油、向日葵籽油不皂化物、甜扁桃油、石栗籽油、牡丹籽油、卵磷脂中的一种或几种。
5.根据权利要求1所述的面膜液,其特征在于,所述保湿剂选自丁二醇、丙二醇、二丙二醇、山梨醇、甘露糖醇、甜菜碱、透明质酸钠、海藻多糖、葡聚糖、赤藓醇、泛醇中的一种或几种。
6.根据权利要求1所述的面膜液,其特征在于,所述增稠剂选自羟乙基纤维素、羟丙基甲基纤维素、聚丙烯酸酯交联聚合物-6、黄原胶、结冷胶、卡波姆、聚丙烯酸钠、聚丙烯酰胺、甘油聚丙烯酸酯中的一种或几种。
7.根据权利要求1所述的面膜液,其特征在于,所述助剂选自防腐剂、抗敏感剂、芳香剂、pH调节剂中的一种或多种。
8.根据权利要求7所述的面膜液,其特征在于,所述抗敏感剂选自甘草酸二钾、红没药醇、马齿苋提取物、尿囊素、粉防己甲素、辣蓼提取物、白薇提取物、艾叶提取物中的一种或多种。
9.根据权利要求7或8所述的面膜液,其特征在于,所述pH调节剂选自氨甲基丙醇、酒石酸、柠檬酸、三乙醇胺、柠檬酸钠中的一种或多种。
10.权利要求1~9任意一项所述面膜液的制备方法,包括以下步骤:
1)将所述水相的组分混合制备获得水相;
2)将所述油相的组分混合制备获得油相。
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