CN110339693A - A kind of plant type air deodorization agent of farm and preparation method thereof - Google Patents
A kind of plant type air deodorization agent of farm and preparation method thereof Download PDFInfo
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- CN110339693A CN110339693A CN201910638526.5A CN201910638526A CN110339693A CN 110339693 A CN110339693 A CN 110339693A CN 201910638526 A CN201910638526 A CN 201910638526A CN 110339693 A CN110339693 A CN 110339693A
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- wood vinegar
- ethyl alcohol
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
- B01D53/34—Chemical or biological purification of waste gases
- B01D53/46—Removing components of defined structure
- B01D53/48—Sulfur compounds
- B01D53/52—Hydrogen sulfide
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
- B01D53/34—Chemical or biological purification of waste gases
- B01D53/46—Removing components of defined structure
- B01D53/54—Nitrogen compounds
- B01D53/58—Ammonia
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
- B01D53/34—Chemical or biological purification of waste gases
- B01D53/74—General processes for purification of waste gases; Apparatus or devices specially adapted therefor
- B01D53/77—Liquid phase processes
- B01D53/78—Liquid phase processes with gas-liquid contact
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D2258/00—Sources of waste gases
- B01D2258/06—Polluted air
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- Engineering & Computer Science (AREA)
- Chemical & Material Sciences (AREA)
- Environmental & Geological Engineering (AREA)
- Health & Medical Sciences (AREA)
- Biomedical Technology (AREA)
- Analytical Chemistry (AREA)
- General Chemical & Material Sciences (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Disinfection, Sterilisation Or Deodorisation Of Air (AREA)
Abstract
The invention discloses plant type air deodorization agents of a kind of farm and preparation method thereof, are related to technical field of air purification, solve the problems, such as existing chemical deodorizing technology not environmentally and the deodoriging properties of galenical deodorizer are bad.The present invention is made of wood vinegar, ethyl alcohol, copper sulphate or ironic citrate, surfactant, plants essential oil and deionized water, and the parts by weight of the wood vinegar are 50~80 parts；The parts by weight of the ethyl alcohol are 5~10 parts；The parts by weight of the copper sulphate or ironic citrate are 1~5 part；The surfactant is the one of which in poly- sorb rouge 80, dodecyl dimethyl ammonium chloride or dodecyl dimethyl benzyl ammonium bromide, and parts by weight are 0.1~2 part；The plants essential oil is P-Cymene or Rosa Damascana, and parts by weight are 0.01~0.1 part；The parts by weight of the deionized water are 0~50 part.Primary raw material of the invention is that resulting wood vinegar after low-temperature carbonization is carried out by wheat stalk or wormwood, and harmless to people, animal, environmentally protective and deodorizing effect is significant.
Description
Technical field
The present invention relates to technical field of air purification, more particularly to a kind of plant type air deodorization of farm
Agent and preparation method thereof.
Background technique
As the improvement of people's living standards, the bring food pollution of industrial or agricultural economy ceaselessly high speed development, more next
It is more valued by people, the pernicious gas in farm derives from the decomposition of organic matter, as excretas such as pad grass, urine.They
Master Home is in sulfur-containing compound, nitrogenous compound, volatile fatty acid and class etc..Since these gases often mix,
So the smell for being difficult to distinguish farm is related with that specific gas on earth.Lead to farm's air pollution and smell
Predominant gas is generally ammonia (NH3) and hydrogen sulfide (H2S).Hydrogen sulfide gas has severe toxicity, and stench can make people, animal poisoning even
It is dead.The organs of vision of ammonia intense stimulus people, animal make people, animal be poisoned or suffocate, threaten the health of people, animal.
Tradition can not be inherently eliminated the presence of malodor molecules by the deodorant such as physical absorption and fragrance cover, smelly
Taste actually still remains, so deodorizing effect is unsatisfactory, chemical deodorizing is removed by chemicals such as chlorine dioxide, paracide
It is smelly, although deodorizing effect is relatively preferable, often cause secondary pollution, it is larger to the irritation of people, also not likable.Cause
This, research and development are environmentally friendly and are important difficulties urgently to be resolved in current air mass control to the New deodouring agent of person poultry harmless
Topic.
Summary of the invention
It is an object of the invention to: in order to solve existing chemical deodorizing technology not environmentally and the deodorization of galenical deodorizer
The bad problem of energy, the present invention provide a kind of plant type air deodorization agent and preparation method thereof of farm.
The present invention specifically uses following technical scheme to achieve the goals above:
A kind of plant type air deodorization agent of farm, by wood vinegar, ethyl alcohol, copper sulphate or ironic citrate, 1,3- fourth
Glycol or glycerine, surfactant, plants essential oil and deionized water composition,
The parts by weight of the wood vinegar are 50~80 parts；
The parts by weight of the ethyl alcohol are 5~10 parts；
The parts by weight of the copper sulphate or ironic citrate are 1~5 part；
The parts by weight of the 1,3-BDO or glycerine are 1~5 part
The surfactant is poly- sorb rouge 80, dodecyl dimethyl ammonium chloride or dodecyl dimethyl benzyl bromide
Change the one of which in ammonium, parts by weight are 0.1~2 part；
The plants essential oil is P-Cymene or Rosa Damascana, and parts by weight are 0.01~0.1 part；
The parts by weight of the deionized water are 0~50 part.
A kind of preparation method of the plant type air deodorization agent of farm comprising the steps of:
1) wood vinegar is made in wheat stalk or wormwood low-temperature carbonization；
2) wormwood essential oil or Rosa Damascana are added in ethyl alcohol, ultrasonic wave stirring 30min is mixed them thoroughly；
3) by one of, the described surface-active in copper sulphate or ironic citrate, ethyl alcohol, 1,3-BDO or glycerine
Agent and deionized water are added in wood vinegar, and ultrasonic wave stirring 30min dissolves it sufficiently under room temperature；
4) the resulting solution of step 2) is added in the resulting solution of step 3), is stirred with the speed mechanical of 100r/min
10min is uniformly mixed it.
Beneficial effects of the present invention are as follows:
1. primary raw material of the invention is to carry out resulting wood vinegar after low-temperature carbonization by wheat stalk or wormwood, obtained
Deodorant is that main Raw material processing forms with natural plant extraction liquid or natural plant extracts, is harmless to human body and animal
, it is nontoxic, harmless to soil, plant, and without flammability and explosivity, use is safe.
2. the effective component of wood vinegar, copper sulphate or ironic citrate as deodorization in deodorant, reaction equation HAc+
NH3=NH4Ac, CuSO4+H2S=CuS, and the phenols in wood vinegar can be with NH3It reacts；In addition, surfactant cooperation wood
Vinegar liquid and copper sulphate etc. play the role of sterilization and foul smell elimination；Rosa Damascana or wormwood essential oil can play the role of flavouring；Ethyl alcohol,
1,3-BDO or glycerine can be used as the solvent of dissolution plants essential oil.
3. being obtained according to experimental data, the present invention is 85%~90% to the removal rate of hydrogen sulfide, and the removal rate to ammonia is
90%~96%, in contrast to the plant type air deodorization agent of existing farm, removal rate to hydrogen sulfide and to ammonia
Removal rate 80% hereinafter, it can thus be appreciated that period clean-up effect of the invention promoted it is very significant.
Specific embodiment
In order to which those skilled in the art better understand the present invention, the present invention is made into one below with reference to following embodiment
Step detailed description.The range of claimed invention is not intended to limit to the detailed description of the embodiment of the present invention below,
But it is merely representative of selected embodiment of the invention.Based on the embodiments of the present invention, those of ordinary skill in the art are not having
Every other embodiment obtained under the premise of creative work is made, shall fall within the protection scope of the present invention.
Embodiment 1
The present embodiment provides plant type air deodorization agent of a kind of farm and preparation method thereof, deodorant each component
Inventory ratio are as follows:
Wheat stalk wood vinegar: ethyl alcohol: 1,3 butylene glycol: copper sulphate: poly- sorb rouge 80: P-Cymene: deionized water=
50:10:5:5:0.1:0.02:30。
Preparation process are as follows:
1) 50 parts of wood vinegar are made in wheat stalk low-temperature carbonization；
2) ultrasonic wave stirring 30min makes after taking 0.02 part of wormwood essential oil and 10 parts of ethyl alcohol, wormwood essential oil to be added in ethyl alcohol
It is uniformly mixed；
3) take 5 parts of copper sulphate, 5 parts of 1,3-BDOs, 0.1 part of poly- sorb rouge 80 and 30 parts of deionized waters that wood vinegar is added
In, ultrasonic wave stirring 30min dissolves it sufficiently under room temperature；
4) the resulting solution of step 2) is added in the resulting solution of step 3), is stirred with the speed mechanical of 100r/min
10min is uniformly mixed it, obtains the deodorant.
Embodiment 2
The present embodiment provides plant type air deodorization agent of a kind of farm and preparation method thereof, deodorant each component
Inventory ratio are as follows:
Wheat stalk wood vinegar: ethyl alcohol: 1,3 butylene glycol: ironic citrate: dodecyl dimethyl benzyl ammonium bromide: folium artemisiae argyi
Essential oil: deionized water=60:10:2:5:0.5:0.05:30.
Preparation process are as follows:
1) 50 parts of wood vinegar are made in wheat stalk low-temperature carbonization；
2) ultrasonic wave stirring 30min makes after taking 0.05 part of wormwood essential oil and 10 parts of ethyl alcohol, wormwood essential oil to be added in ethyl alcohol
It is uniformly mixed；
3) take 5 parts of ironic citrates, 2 parts of 1,3-BDOs, 0.5 part of dodecyl dimethyl benzyl ammonium bromide and 30 parts go from
Sub- water is added in wood vinegar, and ultrasonic wave stirring 30min dissolves it sufficiently under room temperature；
4) the resulting solution of step 2) is added in the resulting solution of step 3), is stirred with the speed mechanical of 100r/min
10min is uniformly mixed it, obtains the deodorant.
Embodiment 3
The present embodiment provides plant type air deodorization agent of a kind of farm and preparation method thereof, deodorant each component
Inventory ratio are as follows:
Wheat stalk wood vinegar: ethyl alcohol: glycerine: copper sulphate: dodecyl dimethyl ammonium chloride: P-Cymene: go from
Sub- water=80:5:2:5:0.2:0.02:10.
Preparation process are as follows:
1) 80 parts of wood vinegar are made in wheat stalk low-temperature carbonization；
2) ultrasonic wave stirring 30min makes it after taking 0.02 part of wormwood essential oil and 5 parts of ethyl alcohol, wormwood essential oil to be added in ethyl alcohol
It is uniformly mixed；
3) take 5 parts of copper sulphate, 2 parts of glycerine, 0.2 part of dodecyl dimethyl ammonium chloride and 10 parts of deionized waters that wood is added
In vinegar liquid, ultrasonic wave stirring 30min dissolves it sufficiently under room temperature；
4) the resulting solution of step 2) is added in the resulting solution of step 3), is stirred with the speed mechanical of 100r/min
10min is uniformly mixed it, obtains the deodorant.
Embodiment 4
The present embodiment provides plant type air deodorization agent of a kind of farm and preparation method thereof, deodorant each component
Inventory ratio are as follows:
Wheat stalk wood vinegar: ethyl alcohol: glycerine: ironic citrate: dodecyl dimethyl benzyl ammonium bromide: rhodamine toner
Oil: deionized water=80:10:5:5:0.8:0.05:30.
Preparation process are as follows:
1) 80 parts of wood vinegar are made in wheat stalk low-temperature carbonization；
2) ultrasonic wave stirring 30min makes after taking 0.05 part of Rosa Damascana and 10 parts of ethyl alcohol, Rosa Damascana to be added in ethyl alcohol
It is uniformly mixed；
3) 5 parts of ironic citrates, 5 parts of glycerine, 0.8 part of dodecyl dimethyl benzyl ammonium bromide and 30 parts of deionized waters are taken
It is added in wood vinegar, ultrasonic wave stirring 30min dissolves it sufficiently under room temperature；
4) the resulting solution of step 2) is added in the resulting solution of step 3), is stirred with the speed mechanical of 100r/min
10min is uniformly mixed it, obtains the deodorant.
Comparative example 1
Existing deodorant preparation process is as follows:
1) high temperature pyrolysis distillation of the discarded jujube core at 130 DEG C is taken, is precipitating obtained wood vinegar after the gas condensation of generation；
2) the mainly kitchen castoff 30kg based on food is collected, brown sugar 10kg and water 100kg is added, is fermented 3 months
More than, environmental protection ferment is made in the brown liquid of filtering arrived；
3) roseleaf is first mixed into (mass ratio 1:4) with clear water, in the pressure of 2.5Mpa, when temperature is 50 DEG C, into
Row steam distillation 2.5 hours, obtain oil water mixture.Carry out water-oil separating；Rose extracting solution is obtained after being set layering.
After taking 50 parts of wood vinegar, in mass ratio 1:1 to be diluted with water under stirring, the environmentally friendly ferment after being diluted with water is added
The mass ratio of element, environmental protection ferment and water is 1:2, after being sufficiently mixed with wood vinegar, precipitates 24 hours, reinjects plant extraction liquid,
It is uniformly mixed and obtains deodorant.
By deodorant obtained by feed ratios different in Examples 1 to 4, deodorant comparison is made further according to the prior art
Example, different deodorant is sprayed on 5~7 days chicken manures of sealing and fermenting, wherein the quality of deodorant is chicken manure quality
10%, the hydrogen sulfide gas and ammonia data in the air of different deodorant uses front and backs are collected, table 1 is made.
Table 1
| Deodorant dosage | Hydrogen sulfide removal rate | Ammonia removal rate | |
| Embodiment 1 | 10% | 85% | 96% |
| Embodiment 2 | 10% | 90% | 95% |
| Embodiment 3 | 10% | 88% | 93% |
| Embodiment 4 | 10% | 87% | 91% |
| Comparative example 1 | 10% | 80% | 40% |
Conclusion:
It can be obtained by table 1, the hydrogen sulfide removal rate after the deodorant private in Examples 1 to 4 in air reaches 85% or more,
The removal rate of ammonia reaches 90% or more, compares the odor purification effect of existing plant type air deodorization agent, the present invention is to cultivation
Odor purification effect in is significant.
The above, only presently preferred embodiments of the present invention, are not intended to limit the invention, patent protection model of the invention
It encloses and is subject to claims, it is all to change with equivalent structure made by description of the invention, similarly should all include
Within the scope of the present invention.
Claims (2)
1. the plant type air deodorization agent of a kind of farm, by wood vinegar, ethyl alcohol, copper sulphate or ironic citrate, 1,3- fourth two
Alcohol or glycerine, surfactant, plants essential oil and deionized water composition,
The parts by weight of the wood vinegar are 50~80 parts；
The parts by weight of the ethyl alcohol are 5~10 parts；
The parts by weight of the copper sulphate or ironic citrate are 1~5 part；
The 1,3-BDO or glycerine parts by weight are 1~5 part
The surfactant is poly- sorb rouge 80, dodecyl dimethyl ammonium chloride or dodecyl dimethyl benzyl ammonium bromide
In one of which, parts by weight be 0.1~2 part；
The plants essential oil is P-Cymene or Rosa Damascana, and parts by weight are 0.01~0.1 part；
The parts by weight of the deionized water are 0~50 part.
2. a kind of preparation method of the plant type air deodorization agent of farm comprising the steps of:
1) wood vinegar is made in wheat stalk or wormwood low-temperature carbonization；
2) wormwood essential oil or Rosa Damascana are added in ethyl alcohol, ultrasonic wave stirring 30min is mixed them thoroughly；
3) by copper sulphate or ironic citrate, ethyl alcohol, 1,3-BDO or glycerine one of, the described surfactant and
Deionized water is added in wood vinegar, and ultrasonic wave stirring 30min dissolves it sufficiently under room temperature；
4) the resulting solution of step 2) is added in the resulting solution of step 3), 10min is stirred with the speed mechanical of 100r/min
It is uniformly mixed it, obtains the deodorant.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
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| CN201910638526.5A CN110339693A (en) | 2019-07-16 | 2019-07-16 | A kind of plant type air deodorization agent of farm and preparation method thereof |
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| CN201910638526.5A CN110339693A (en) | 2019-07-16 | 2019-07-16 | A kind of plant type air deodorization agent of farm and preparation method thereof |
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Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111202095A (en) * | 2020-03-10 | 2020-05-29 | 广东省农业科学院植物保护研究所 | Composition for preventing and treating bacterial leaf streak of rice as well as preparation method and application thereof |
| CN112999397A (en) * | 2021-03-23 | 2021-06-22 | 铜陵金基科技有限公司 | Environment-friendly deodorization medicament and preparation method thereof |
| CN113069915A (en) * | 2020-01-03 | 2021-07-06 | 湖南巨高屾科技发展有限公司 | Multifunctional deodorant for treating odor of farm |
| CN113975962A (en) * | 2021-11-02 | 2022-01-28 | 湖南德邦生物科技有限公司 | Amino acid chelate deodorant and preparation method thereof |
| CN114950103A (en) * | 2021-02-22 | 2022-08-30 | 蓝星(北京)化工机械有限公司 | Wood vinegar deodorant |
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| JPH01277565A (en) * | 1988-04-28 | 1989-11-08 | Teruzou Murai | Deodorizing composition |
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Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113069915A (en) * | 2020-01-03 | 2021-07-06 | 湖南巨高屾科技发展有限公司 | Multifunctional deodorant for treating odor of farm |
| CN111202095A (en) * | 2020-03-10 | 2020-05-29 | 广东省农业科学院植物保护研究所 | Composition for preventing and treating bacterial leaf streak of rice as well as preparation method and application thereof |
| CN114950103A (en) * | 2021-02-22 | 2022-08-30 | 蓝星(北京)化工机械有限公司 | Wood vinegar deodorant |
| CN112999397A (en) * | 2021-03-23 | 2021-06-22 | 铜陵金基科技有限公司 | Environment-friendly deodorization medicament and preparation method thereof |
| CN113975962A (en) * | 2021-11-02 | 2022-01-28 | 湖南德邦生物科技有限公司 | Amino acid chelate deodorant and preparation method thereof |
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Application publication date: 20191018 |