CN110315670A - Ceramic material surfaces negative angle micron form multi-process transfer method - Google Patents

Ceramic material surfaces negative angle micron form multi-process transfer method Download PDF

Info

Publication number
CN110315670A
CN110315670A CN201910612808.8A CN201910612808A CN110315670A CN 110315670 A CN110315670 A CN 110315670A CN 201910612808 A CN201910612808 A CN 201910612808A CN 110315670 A CN110315670 A CN 110315670A
Authority
CN
China
Prior art keywords
weight
parts
mold
negative angle
ceramic material
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
CN201910612808.8A
Other languages
Chinese (zh)
Other versions
CN110315670B (en
Inventor
徐杨
黄风立
聂曼
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Jiaxing University
Original Assignee
Jiaxing University
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Jiaxing University filed Critical Jiaxing University
Priority to CN201910612808.8A priority Critical patent/CN110315670B/en
Publication of CN110315670A publication Critical patent/CN110315670A/en
Application granted granted Critical
Publication of CN110315670B publication Critical patent/CN110315670B/en
Active legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
    • B29C—SHAPING OR JOINING OF PLASTICS; SHAPING OF MATERIAL IN A PLASTIC STATE, NOT OTHERWISE PROVIDED FOR; AFTER-TREATMENT OF THE SHAPED PRODUCTS, e.g. REPAIRING
    • B29C41/00—Shaping by coating a mould, core or other substrate, i.e. by depositing material and stripping-off the shaped article; Apparatus therefor
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
    • B29C—SHAPING OR JOINING OF PLASTICS; SHAPING OF MATERIAL IN A PLASTIC STATE, NOT OTHERWISE PROVIDED FOR; AFTER-TREATMENT OF THE SHAPED PRODUCTS, e.g. REPAIRING
    • B29C59/00—Surface shaping of articles, e.g. embossing; Apparatus therefor
    • B29C59/005—Surface shaping of articles, e.g. embossing; Apparatus therefor characterised by the choice of material
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
    • B29C—SHAPING OR JOINING OF PLASTICS; SHAPING OF MATERIAL IN A PLASTIC STATE, NOT OTHERWISE PROVIDED FOR; AFTER-TREATMENT OF THE SHAPED PRODUCTS, e.g. REPAIRING
    • B29C59/00—Surface shaping of articles, e.g. embossing; Apparatus therefor
    • B29C59/02—Surface shaping of articles, e.g. embossing; Apparatus therefor by mechanical means, e.g. pressing
    • B29C59/022—Surface shaping of articles, e.g. embossing; Apparatus therefor by mechanical means, e.g. pressing characterised by the disposition or the configuration, e.g. dimensions, of the embossments or the shaping tools therefor
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
    • B29D—PRODUCING PARTICULAR ARTICLES FROM PLASTICS OR FROM SUBSTANCES IN A PLASTIC STATE
    • B29D7/00—Producing flat articles, e.g. films or sheets
    • B29D7/01—Films or sheets
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B26/00—Compositions of mortars, concrete or artificial stone, containing only organic binders, e.g. polymer or resin concrete
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B28/00—Compositions of mortars, concrete or artificial stone, containing inorganic binders or the reaction product of an inorganic and an organic binder, e.g. polycarboxylate cements
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B41/00—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
    • C04B41/45—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements
    • C04B41/52—Multiple coating or impregnating multiple coating or impregnating with the same composition or with compositions only differing in the concentration of the constituents, is classified as single coating or impregnation
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B41/00—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
    • C04B41/60—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone of only artificial stone
    • C04B41/61—Coating or impregnation
    • C04B41/70—Coating or impregnation for obtaining at least two superposed coatings having different compositions
    • C04B41/71—Coating or impregnation for obtaining at least two superposed coatings having different compositions at least one coating being an organic material
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
    • B29C—SHAPING OR JOINING OF PLASTICS; SHAPING OF MATERIAL IN A PLASTIC STATE, NOT OTHERWISE PROVIDED FOR; AFTER-TREATMENT OF THE SHAPED PRODUCTS, e.g. REPAIRING
    • B29C59/00—Surface shaping of articles, e.g. embossing; Apparatus therefor
    • B29C59/02—Surface shaping of articles, e.g. embossing; Apparatus therefor by mechanical means, e.g. pressing
    • B29C59/022—Surface shaping of articles, e.g. embossing; Apparatus therefor by mechanical means, e.g. pressing characterised by the disposition or the configuration, e.g. dimensions, of the embossments or the shaping tools therefor
    • B29C2059/023—Microembossing
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2111/00—Mortars, concrete or artificial stone or mixtures to prepare them, characterised by specific function, property or use
    • C04B2111/00474—Uses not provided for elsewhere in C04B2111/00
    • C04B2111/00612—Uses not provided for elsewhere in C04B2111/00 as one or more layers of a layered structure

Landscapes

  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Ceramic Engineering (AREA)
  • Materials Engineering (AREA)
  • Structural Engineering (AREA)
  • Organic Chemistry (AREA)
  • Mechanical Engineering (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Inorganic Chemistry (AREA)
  • Micromachines (AREA)
  • Compositions Of Oxide Ceramics (AREA)

Abstract

The present invention relates to ceramic material surfaces processing technology fields, and disclose ceramic material surfaces negative angle micron form multi-process transfer method, the multi-process transfer method is the following steps are included: S1: 50-100 parts by weight of deionized water, 50-70 parts by weight ceramics micron particles, 10-20 part by weight of metal micron particles, 5-15 parts by weight alloy microparticles, 1-5 parts by weight semiconductor microactuator rice grain, 1-5 parts by weight binder are successively put into ultrasonic stirrer, it is mixed evenly through ultrasonic wave, obtains semi-finished product slurry；S2: sequentially adding 3-7 parts by weight lubricant, 5-9 parts per weight dispersing agent and 1-3 parts by weight of plasticizer in the semi-finished product slurry that S1 is obtained, and continues ultrasonic wave and is mixed evenly, obtains finished product even dispersion slurry；S3: the finished product even dispersion slurry that S2 is obtained is filtered by two layers of strainer.The ceramic material surfaces negative angle micron form multi-process transfer method effectively increases the quality of ceramic material surfaces negative angle micron form multi-process transfer.

Description

Ceramic material surfaces negative angle micron form multi-process transfer method
Technical field
The present invention relates to ceramic material surfaces processing technology fields, specially ceramic material surfaces negative angle micron form multiplexing Sequence transfer method.
Background technique
Micro nano transfer printing technology is simply and efficiently to carry out micro nano structure as a kind of non-traditional micro-nano processing technology Production with device improves an effective means, ceramics as novel engineering material with its unique compression strength, very High surface hardness and excellent wear-resisting property are used widely in engineering field, micro- to ceramic material surfaces negative angle at present Rice form multi-process transfers quality that is ineffective, and then influencing the transfer of ceramic material surfaces negative angle micron form multi-process.
Summary of the invention
(1) the technical issues of solving
In view of the deficiencies of the prior art, the present invention provides ceramic material surfaces negative angle micron form multi-process transfer sides Method has the good advantage of ceramic material surfaces negative angle micron form multi-process transfer quality, solves in the prior art, ceramic material Expect the ineffective problem of surface negative angle micron form multi-process transfer.
(2) technical solution
To realize that the good purpose of above-mentioned ceramic material surfaces negative angle micron form multi-process transfer quality, the present invention provide such as Lower technical solution: ceramic material surfaces negative angle micron form multi-process transfer method, which includes following step It is rapid:
S1: by 50-100 parts by weight of deionized water, 50-70 parts by weight ceramics micron particles, 10-20 part by weight of metal micron Particle, 5-15 parts by weight alloy microparticles, 1-5 parts by weight semiconductor microactuator rice grain, 1-5 parts by weight binder successively put into super It in Sound Wave Mixer, is mixed evenly through ultrasonic wave, obtains semi-finished product slurry；
S2: 3-7 parts by weight lubricant, 5-9 parts per weight dispersing agent and 1-3 are sequentially added in the semi-finished product slurry that S1 is obtained Parts by weight of plasticizer continues ultrasonic wave and is mixed evenly, obtains finished product even dispersion slurry；
S3: the finished product even dispersion slurry that S2 is obtained is filtered by two layers of strainer；
S4: the filtered finished product even dispersion slurry of S3 is added in casting machine, through the tape casting, obtains slurry film；
S5: based on the slurry film that S4 is obtained, it is cast macromolecule monofilm in upper and lower surface, more Material claddings are made Film；
S6: taking one piece of silicon mother matrix, carries out photoetching on silicon mother matrix by litho machine, obtains mold mother matrix, and pass through coating machine Surface coating processing is carried out to mold mother matrix；
S7: high molecular material slurry is added on the mold mother matrix after S6 coating film treatment, and is turned in vacuum environment Print can form mold after high molecular material solidification；
S8: photoetching is carried out on the mold that S7 is obtained by litho machine, obtains photoetching mold；
S9: the photoetching mold that S8 is obtained is placed on more Material cladding films that S5 is obtained, and enterprising in more Material cladding films Row plane coining rolls transfer, forms the micro-nano form for having negative angle.
Preferably, the ultrasonic wave mixing time in the step S1 is 25min.
Preferably, the ultrasonic wave mixing time in the step S2 is 5min.
Preferably, two layers of strainer is respectively 40um and 10um in the step S3.
Preferably, the mold formed after the step S7 solidification is plane mould or cylinder mold.
Preferably, litho machine makes the micro-nano shape that section is triangle or cuboid by lithography on mold in the step S8 State.
(3) beneficial effect
Compared with prior art, the present invention provides ceramic material surfaces negative angle micron form multi-process transfer method, tools It is standby following the utility model has the advantages that
1, the ceramic material surfaces negative angle micron form multi-process transfer method is cooperated viscous by various powder micron particles Agent, lubricant, dispersing agent and plasticizer are tied, is mixed evenly to form even dispersion slurry via ultrasonic wave, paddle body passes through stream More Material cladding films are made in the method for prolonging, and photoetching mold carries out plane coining on more Material cladding films or rolls transfer, and formation has The micro-nano form of negative angle, the synthesis of multiple material component and its proportion can be largely fixed the quality of paddle body, component and Not mutually coordinated, beneficial effect brought by single component is matched, can even be eliminated by other components abatement, when serious, Different component mutually contradicts, and does not have whole synthesis effect, turns to influence ceramic material surfaces negative angle micron form multi-process The quality of print.The present invention passes through the optimal component and proportion for constantly debugging a variety of materials, so that various ingredients combine, phase Mutually coordinate, effectively improves the quality of ceramic material surfaces negative angle micron form multi-process transfer.
Specific embodiment
Below in conjunction with the embodiment of the present invention, technical scheme in the embodiment of the invention is clearly and completely described, Obviously, described embodiments are only a part of the embodiments of the present invention, instead of all the embodiments.Based in the present invention Embodiment, every other embodiment obtained by those of ordinary skill in the art without making creative efforts, all Belong to the scope of protection of the invention.
Embodiment 1
Present embodiments provide ceramic material surfaces negative angle micron form multi-process transfer method, the multi-process transfer method The following steps are included:
S1: by 50 parts by weight of deionized water, 50 parts by weight ceramics micron particles, 10 part by weight of metal micron particles, 5 weight Part alloy microparticles, 1 parts by weight semiconductor microactuator rice grain, 2 parts by weight binder are successively put into ultrasonic stirrer, through super Sound wave is mixed evenly, and obtains semi-finished product slurry；
S2: 3 parts by weight lubricants, 5 parts per weight dispersing agents and 1 parts by weight are sequentially added in the semi-finished product slurry that S1 is obtained Plasticizer continues ultrasonic wave and is mixed evenly, obtains finished product even dispersion slurry；
S3: the finished product even dispersion slurry that S2 is obtained is filtered by two layers of strainer；
S4: the filtered finished product even dispersion slurry of S3 is added in casting machine, through the tape casting, obtains slurry film；
S5: based on the slurry film that S4 is obtained, it is cast macromolecule monofilm in upper and lower surface, more Material claddings are made Film；
S6: taking one piece of silicon mother matrix, carries out photoetching on silicon mother matrix by litho machine, obtains mold mother matrix, and pass through coating machine Surface coating processing is carried out to mold mother matrix；
S7: high molecular material slurry is added on the mold mother matrix after S6 coating film treatment, and is turned in vacuum environment Print can form mold after high molecular material solidification；
S8: photoetching is carried out on the mold that S7 is obtained by litho machine, obtains photoetching mold；
S9: the photoetching mold that S8 is obtained is placed on more Material cladding films that S5 is obtained, and enterprising in more Material cladding films Row plane coining rolls transfer, forms the micro-nano form for having negative angle.
Embodiment 2
Present embodiments provide ceramic material surfaces negative angle micron form multi-process transfer method, the multi-process transfer method The following steps are included:
S1: by 60 parts by weight of deionized water, 55 parts by weight ceramics micron particles, 15 part by weight of metal micron particles, 10 weights Amount part alloy microparticles, 5 parts by weight semiconductor microactuator rice grains, 3 parts by weight binder are successively put into ultrasonic stirrer, are passed through Ultrasonic wave is mixed evenly, and obtains semi-finished product slurry；
S2: 5 parts by weight lubricants, 7 parts per weight dispersing agents and 2 parts by weight are sequentially added in the semi-finished product slurry that S1 is obtained Plasticizer continues ultrasonic wave and is mixed evenly, obtains finished product even dispersion slurry；
S3: the finished product even dispersion slurry that S2 is obtained is filtered by two layers of strainer；
S4: the filtered finished product even dispersion slurry of S3 is added in casting machine, through the tape casting, obtains slurry film；
S5: based on the slurry film that S4 is obtained, it is cast macromolecule monofilm in upper and lower surface, more Material claddings are made Film；
S6: taking one piece of silicon mother matrix, carries out photoetching on silicon mother matrix by litho machine, obtains mold mother matrix, and pass through coating machine Surface coating processing is carried out to mold mother matrix；
S7: high molecular material slurry is added on the mold mother matrix after S6 coating film treatment, and is turned in vacuum environment Print can form mold after high molecular material solidification；
S8: photoetching is carried out on the mold that S7 is obtained by litho machine, obtains photoetching mold；
S9: the photoetching mold that S8 is obtained is placed on more Material cladding films that S5 is obtained, and enterprising in more Material cladding films Row plane coining rolls transfer, forms the micro-nano form for having negative angle.
Embodiment 3
Present embodiments provide ceramic material surfaces negative angle micron form multi-process transfer method, the multi-process transfer method The following steps are included:
S1: by 80 parts by weight of deionized water, 60 parts by weight ceramics micron particles, 20 part by weight of metal micron particles, 10 weights Amount part alloy microparticles, 5 parts by weight semiconductor microactuator rice grains, 3 parts by weight binder are successively put into ultrasonic stirrer, are passed through Ultrasonic wave is mixed evenly, and obtains semi-finished product slurry；
S2: 6 parts by weight lubricants, 7 parts per weight dispersing agents and 1 parts by weight are sequentially added in the semi-finished product slurry that S1 is obtained Plasticizer continues ultrasonic wave and is mixed evenly, obtains finished product even dispersion slurry；
S3: the finished product even dispersion slurry that S2 is obtained is filtered by two layers of strainer；
S4: the filtered finished product even dispersion slurry of S3 is added in casting machine, through the tape casting, obtains slurry film；
S5: based on the slurry film that S4 is obtained, it is cast macromolecule monofilm in upper and lower surface, more Material claddings are made Film；
S6: taking one piece of silicon mother matrix, carries out photoetching on silicon mother matrix by litho machine, obtains mold mother matrix, and pass through coating machine Surface coating processing is carried out to mold mother matrix；
S7: high molecular material slurry is added on the mold mother matrix after S6 coating film treatment, and is turned in vacuum environment Print can form mold after high molecular material solidification；
S8: photoetching is carried out on the mold that S7 is obtained by litho machine, obtains photoetching mold；
S9: the photoetching mold that S8 is obtained is placed on more Material cladding films that S5 is obtained, and enterprising in more Material cladding films Row plane coining rolls transfer, forms the micro-nano form for having negative angle.
Embodiment 4
Present embodiments provide ceramic material surfaces negative angle micron form multi-process transfer method, the multi-process transfer method The following steps are included:
S1: by 90 parts by weight of deionized water, 60 parts by weight ceramics micron particles, 20 part by weight of metal micron particles, 15 weights Amount part alloy microparticles, 2 parts by weight semiconductor microactuator rice grains, 4 parts by weight binder are successively put into ultrasonic stirrer, are passed through Ultrasonic wave is mixed evenly, and obtains semi-finished product slurry；
S2: 5 parts by weight lubricants, 8 parts per weight dispersing agents and 2 parts by weight are sequentially added in the semi-finished product slurry that S1 is obtained Plasticizer continues ultrasonic wave and is mixed evenly, obtains finished product even dispersion slurry；
S3: the finished product even dispersion slurry that S2 is obtained is filtered by two layers of strainer；
S4: the filtered finished product even dispersion slurry of S3 is added in casting machine, through the tape casting, obtains slurry film；
S5: based on the slurry film that S4 is obtained, it is cast macromolecule monofilm in upper and lower surface, more Material claddings are made Film；
S6: taking one piece of silicon mother matrix, carries out photoetching on silicon mother matrix by litho machine, obtains mold mother matrix, and pass through coating machine Surface coating processing is carried out to mold mother matrix；
S7: high molecular material slurry is added on the mold mother matrix after S6 coating film treatment, and is turned in vacuum environment Print can form mold after high molecular material solidification；
S8: photoetching is carried out on the mold that S7 is obtained by litho machine, obtains photoetching mold；
S9: the photoetching mold that S8 is obtained is placed on more Material cladding films that S5 is obtained, and enterprising in more Material cladding films Row plane coining rolls transfer, forms the micro-nano form for having negative angle.
Embodiment 5
Present embodiments provide ceramic material surfaces negative angle micron form multi-process transfer method, the multi-process transfer method The following steps are included:
S1: by 100 parts by weight of deionized water, 70 parts by weight ceramics micron particles, 20 part by weight of metal micron particles, 15 weights Amount part alloy microparticles, 5 parts by weight semiconductor microactuator rice grains, 5 parts by weight binder are successively put into ultrasonic stirrer, are passed through Ultrasonic wave is mixed evenly, and obtains semi-finished product slurry；
S2: 7 parts by weight lubricants, 9 parts per weight dispersing agents and 3 parts by weight are sequentially added in the semi-finished product slurry that S1 is obtained Plasticizer continues ultrasonic wave and is mixed evenly, obtains finished product even dispersion slurry；
S3: the finished product even dispersion slurry that S2 is obtained is filtered by two layers of strainer；
S4: the filtered finished product even dispersion slurry of S3 is added in casting machine, through the tape casting, obtains slurry film；
S5: based on the slurry film that S4 is obtained, it is cast macromolecule monofilm in upper and lower surface, more Material claddings are made Film；
S6: taking one piece of silicon mother matrix, carries out photoetching on silicon mother matrix by litho machine, obtains mold mother matrix, and pass through coating machine Surface coating processing is carried out to mold mother matrix；
S7: high molecular material slurry is added on the mold mother matrix after S6 coating film treatment, and is turned in vacuum environment Print can form mold after high molecular material solidification；
S8: photoetching is carried out on the mold that S7 is obtained by litho machine, obtains photoetching mold；
S9: the photoetching mold that S8 is obtained is placed on more Material cladding films that S5 is obtained, and enterprising in more Material cladding films Row plane coining rolls transfer, forms the micro-nano form for having negative angle.
In conclusion the ceramic material surfaces negative angle micron form multi-process transfer method, passes through various powder microns Grain cooperation binder, lubricant, dispersing agent and plasticizer, are mixed evenly to form even dispersion slurry, paddle via ultrasonic wave More Material cladding films are made by the tape casting in body, and photoetching mold carries out plane coining on more Material cladding films or rolls transfer, The micro-nano form for having negative angle is formed, the synthesis of multiple material component and its proportion can be largely fixed the matter of paddle body Amount, component and not mutually coordinated, the beneficial effect brought by single component of proportion can even be eliminated, sternly by other components abatement When weight, different component is mutually contradicted, and whole synthesis effect is not had, to influence ceramic material surfaces negative angle micron form The quality of multi-process transfer.The present invention passes through the optimal component and proportion for constantly debugging a variety of materials, so that various ingredients are comprehensive Together, mutually coordinated, effectively improve the quality of ceramic material surfaces negative angle micron form multi-process transfer.
It should be noted that the terms "include", "comprise" or its any other variant are intended to the packet of nonexcludability Contain, so that the process, method, article or equipment for including a series of elements not only includes those elements, but also including Other elements that are not explicitly listed, or further include for elements inherent to such a process, method, article, or device. In the absence of more restrictions, the element limited by sentence "including a ...", it is not excluded that including the element Process, method, article or equipment in there is also other identical elements.
It although an embodiment of the present invention has been shown and described, for the ordinary skill in the art, can be with A variety of variations, modification, replacement can be carried out to these embodiments without departing from the principles and spirit of the present invention by understanding And modification, the scope of the present invention is defined by the appended.

Claims (6)

1. ceramic material surfaces negative angle micron form multi-process transfer method, it is characterised in that: the multi-process transfer method includes Following steps:
S1: by 50-100 parts by weight of deionized water, 50-70 parts by weight ceramics micron particles, 10-20 part by weight of metal micron Grain, 5-15 parts by weight alloy microparticles, 1-5 parts by weight semiconductor microactuator rice grain, 1-5 parts by weight binder successively put into ultrasound It in wave blender, is mixed evenly through ultrasonic wave, obtains semi-finished product slurry；
S2: 3-7 parts by weight lubricant, 5-9 parts per weight dispersing agent and 1-3 weight are sequentially added in the semi-finished product slurry that S1 is obtained Part plasticizer continues ultrasonic wave and is mixed evenly, obtains finished product even dispersion slurry；
S3: the finished product even dispersion slurry that S2 is obtained is filtered by two layers of strainer；
S4: the filtered finished product even dispersion slurry of S3 is added in casting machine, through the tape casting, obtains slurry film；
S5: based on the slurry film that S4 is obtained, it is cast macromolecule monofilm in upper and lower surface, more Material cladding films are made；
S6: taking one piece of silicon mother matrix, and photoetching is carried out on silicon mother matrix by litho machine, obtains mold mother matrix, and by coating machine to mould Have mother matrix and carries out surface coating processing；
S7: high molecular material slurry being added on the mold mother matrix after S6 coating film treatment, and is transferred in vacuum environment, high Mold can be formed after molecular material solidification；
S8: photoetching is carried out on the mold that S7 is obtained by litho machine, obtains photoetching mold；
S9: the photoetching mold that S8 is obtained being placed on more Material cladding films that S5 is obtained, and is carried out on more Material cladding films flat Face pressure print rolls transfer, forms the micro-nano form for having negative angle.
2. ceramic material surfaces negative angle micron form multi-process transfer method according to claim 1, it is characterised in that: institute Stating the ultrasonic wave mixing time in step S1 is 25min.
3. ceramic material surfaces negative angle micron form multi-process transfer method according to claim 1, it is characterised in that: institute Stating the ultrasonic wave mixing time in step S2 is 5min.
4. ceramic material surfaces negative angle micron form multi-process transfer method according to claim 1, it is characterised in that: institute Stating two layers of strainer in step S3 is respectively 40um and 10um.
5. ceramic material surfaces negative angle micron form multi-process transfer method according to claim 1, it is characterised in that: institute Stating the mold formed after step S7 solidification is plane mould or cylinder mold.
6. ceramic material surfaces negative angle micron form multi-process transfer method according to claim 1, it is characterised in that: institute It states litho machine in step S8 and makes the micro-nano form that section is triangle or cuboid by lithography on mold.
CN201910612808.8A 2019-07-09 2019-07-09 Ceramic material surface negative angle micron form multi-process transfer printing method Active CN110315670B (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201910612808.8A CN110315670B (en) 2019-07-09 2019-07-09 Ceramic material surface negative angle micron form multi-process transfer printing method

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201910612808.8A CN110315670B (en) 2019-07-09 2019-07-09 Ceramic material surface negative angle micron form multi-process transfer printing method

Publications (2)

Publication Number Publication Date
CN110315670A true CN110315670A (en) 2019-10-11
CN110315670B CN110315670B (en) 2021-04-16

Family

ID=68123054

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201910612808.8A Active CN110315670B (en) 2019-07-09 2019-07-09 Ceramic material surface negative angle micron form multi-process transfer printing method

Country Status (1)

Country Link
CN (1) CN110315670B (en)

Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101101441A (en) * 2007-08-07 2008-01-09 山东大学 Large area periodic array three-dimensional microstructure preparation method
CN106365635A (en) * 2016-08-17 2017-02-01 南方科技大学 Functional ceramic material surface patterning method

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101101441A (en) * 2007-08-07 2008-01-09 山东大学 Large area periodic array three-dimensional microstructure preparation method
CN106365635A (en) * 2016-08-17 2017-02-01 南方科技大学 Functional ceramic material surface patterning method

Non-Patent Citations (3)

* Cited by examiner, † Cited by third party
Title
李垚等: "《新型功能材料制备原理与工艺》", 31 August 2017, 哈尔滨工业大学出版社 *
邹建新等: "《钒钛功能材料》", 31 March 2019, 冶金工业出版社 *
陈光文等: "高聚物/陶瓷复合膜的制备及性能表征", 《化工学报》 *

Also Published As

Publication number Publication date
CN110315670B (en) 2021-04-16

Similar Documents

Publication Publication Date Title
CN109909445B (en) Ceramic shell for inhibiting sand sticking on surface of high-temperature alloy turbine blade and preparation method thereof
CA2419115A1 (en) Microparticles, and method and apparatus for forming same
CN110093588B (en) Fine-grain aluminum-scandium alloy target material and preparation method and application thereof
JP2008251735A (en) Magnetic-sheet manufacturing method
JPH05345835A (en) Porous form with open cell, its production and pressureized casting mold for pottery using the same
US6866803B1 (en) Mold for use in slip casting method, and method of manufacturing open porous body for use in mold
CN108747856A (en) A kind of resin wheel, preparation method and application for piezoelectric ceramics grinding
CN105950114B (en) A kind of outer membrane mixing diamond spherical abrasive material and preparation method thereof
CN110315670A (en) Ceramic material surfaces negative angle micron form multi-process transfer method
CN109261890A (en) The preparation method of ceramic core printed material and preparation method thereof and ceramic core
CN104084586B (en) Filter-pressing preparation method for soft-magnetic composite material
CN108788003A (en) A kind of powdered mold release agents and preparation method thereof and application method
CN107214343A (en) A kind of preparation method of gradient nozzle
CN110253021A (en) The micro-nano form roller/plane transfer method of ceramic material surfaces
CN112777987B (en) Iron tailing foam concrete and preparation method thereof
JP6461463B2 (en) Silica-coated magnetic material particles and method for producing the same
CN208308711U (en) Porous membrane green body and porous membrane presoma
JP2010110770A (en) Parting agent for casting lattice body for electrode plate of lead battery
JPS6391208A (en) Manufacture of molding tool
CN100386363C (en) High suspension force water soluble anti-rust grinding liquid
CN110871257A (en) Preparation method and application of graphite activated ceramic surface layer slurry
CN107382343A (en) A kind of AlON BN diphase ceramic materials and preparation method thereof, application
JPH03106984A (en) Manufacture of abrasive composition
JP2006150500A (en) Resin bonded abrasive wheel and semiconductor chip manufacturing method using the same
JPH11114403A (en) Molding method for ceramic powder

Legal Events

Date Code Title Description
PB01 Publication
PB01 Publication
SE01 Entry into force of request for substantive examination
SE01 Entry into force of request for substantive examination
GR01 Patent grant
GR01 Patent grant