CN1102206A - Method for preparing edible smoked perfumery - Google Patents
Method for preparing edible smoked perfumery Download PDFInfo
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- CN1102206A CN1102206A CN 93115174 CN93115174A CN1102206A CN 1102206 A CN1102206 A CN 1102206A CN 93115174 CN93115174 CN 93115174 CN 93115174 A CN93115174 A CN 93115174A CN 1102206 A CN1102206 A CN 1102206A
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- essence
- smoked
- extracting method
- retort
- edible smoked
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Abstract
The present invention relates to a method for extracting edible smoked essence from hawthorn kernel, belonging to the field of food additive. Said method uses the hawthorn kernels as raw material, and makes them pass through such processes of dry distillation and smoking vapour condensation at constant temp. of 100-150 deg.C so as to obtain an oil-like material, and then the oil-like material is filtered, and then a matter specific gravity separation method is used for separating the obtained filtrate at normal temp. and ordinary pressure, and then the separated super-liquor is passed through the process of syphon separation, so that the invented product can be obtained. Said method has the advantages of simplified technological process, low investment, and economizing energy source.
Description
The present invention is a kind of method of extracting edible cigarette perfume material from Semen Crataegi, belongs to technical field of food additives.
State Patent Office was on July 16th, 1986, a kind of " extracting liq fumigating agent and medical relaxing are dripped smart method from Semen Crataegi " (application number 85100470) disclosed, this method has overcome conventional smoke and has smoked the problem that easily produces carcinogenic substance and atmosphere pollution in the method, the spices extraction process process of this new technology is: Semen Crataegi under 90～450 ℃ of temperature through destructive distillation, its smog is collected, be condensed into dry distillation liquid, dry distillation liquid separates spices through rectifying tower again.Though this method advantage is more outstanding, in technology, adopt the investment of dry distillation liquid rectifying very big, consumes energy, and also equipment is installed and execute-in-place is also cumbersome.
The objective of the invention is at the problems referred to above, employing material hydrometer method replaces the loaded down with trivial details rectifying in the former technology, to reach the simplification technical process, reduces the purpose of investment save energy.
The present invention is achieved in that a kind of extracting method of edible cigarette perfume material, be to adopt the Semen Crataegi destructive distillation, get the process of the sootiness vapor condensation under its 100-150 ℃ constant temperature, its technical essential is: condensed oily matter is imported its filtrate in the jar, under normal temperature, condition of normal pressure after filtration then, adopt the material density separation, it is upper and lower two-layer that filtrate is divided into, and upper strata liquid separates through siphon, can obtain this product.
Now concrete operational process of craft and the processing condition with this method are summarized as follows: the Semen Crataegi that will clean after drying is put in the retort, is that termite carries out the external-heat destructive distillation under 220-230 ℃ of condition with fire coal.Material is the intermittently effect of whipping appts in retort, material is heated evenly, when temperature of charge reaches more than 80 ℃, there is a spot of steam to emerge, mainly be the moisture content in the Semen Crataegi, under 100-150 ℃ of constant temperature, constantly emit smoke fumigation vapour, steam is isolated yellow oil through condenser, oily matter leaches impurity such as miscellaneous carbon ash through 80-120 order filter cloth filter, and filtrate is statically placed in the jar, under normal temperature and pressure (or low temperature), be divided into upper and lower two-layerly, the upper strata is the red-brown transparent liquid, and siphon is this product after separating.
Be save energy, with the incoagulability inflammable gas that sootiness steam is discharged through condenser, be circulated to retort at the bottom of heating combustion-supporting.
The embodiment of the invention:
Retort adopts cast iron materials; Batch mixer adopts reducing motor to drive in the still; The strainer filter cloth adopts 100 target standards.
The present invention has the following advantages than prior art:
1, material is heated evenly in the retort, and the pyrolysis temperature terminal point is significantly less than the temperature of the disclosed 450 ℃ of heating upper limits of prior art at 220-230 ℃, has saved the energy.
2, through condensed incoagulability fuel gas, it is combustion-supporting to be circulated to the retort heating, has namely reduced air pollution, again energy savings.
3, this law adopts the material density separation, replaces the distillation process in the former technology, has simplified technological process, has saved investment.
4, owing to the Heating temperature of heating up in a steamer still is lower, the Semen Crataegi after the charing can further activate becomes gac.
5, the yield of the spices that extracts through this method is more than 20% of dry Semen Crataegi weight.
Claims (4)
1, a kind of extracting method of edible smoked essence, be to adopt the Semen Crataegi destructive distillation, get the sootiness vapor condensation process under its 100-150 ℃ constant temperature, it is characterized in that condensed oily matter after filtration, then with in its filtrate input jar, under normal temperature, condition of normal pressure, adopt the material density separation, it is upper and lower two-layer that filtrate is divided into, and upper strata liquid separates through siphon, can obtain this product.
2, according to the extracting method of the described edible smoked essence of claim 1, it is characterized in that the retort fire coal is that termite carries out the external-heat destructive distillation, intermittently whipping appts of machinery is housed in the still.
3,, it is characterized in that strainer adopts 80-120 order filter cloth according to the extracting method of the described edible smoked essence of claim 1.
4, according to the extracting method of the described edible smoked essence of claim 1, it is characterized in that the incoagulability inflammable gas that sootiness steam is discharged through condenser, be circulated to retort at the bottom of heating combustion-supporting.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 93115174 CN1102206A (en) | 1993-10-26 | 1993-10-26 | Method for preparing edible smoked perfumery |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 93115174 CN1102206A (en) | 1993-10-26 | 1993-10-26 | Method for preparing edible smoked perfumery |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN1102206A true CN1102206A (en) | 1995-05-03 |
Family
ID=4990853
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN 93115174 Pending CN1102206A (en) | 1993-10-26 | 1993-10-26 | Method for preparing edible smoked perfumery |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN1102206A (en) |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP1295603A4 (en) * | 2000-06-16 | 2009-05-27 | Yi Shi | The process of extracting from haw-pit by dry distillation and its device |
| CN101999618A (en) * | 2010-11-09 | 2011-04-06 | 合肥工业大学 | Method for preparing liquid smoking spice for meat from pecan shells |
| CN103103018A (en) * | 2012-11-13 | 2013-05-15 | 苏州谷力生物科技有限公司 | Compound plant spice and preparation method |
| CN109549110A (en) * | 2018-11-30 | 2019-04-02 | 中国肉类食品综合研究中心 | A kind of smoke solution and the preparation method and application thereof |
-
1993
- 1993-10-26 CN CN 93115174 patent/CN1102206A/en active Pending
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP1295603A4 (en) * | 2000-06-16 | 2009-05-27 | Yi Shi | The process of extracting from haw-pit by dry distillation and its device |
| CN101999618A (en) * | 2010-11-09 | 2011-04-06 | 合肥工业大学 | Method for preparing liquid smoking spice for meat from pecan shells |
| CN103103018A (en) * | 2012-11-13 | 2013-05-15 | 苏州谷力生物科技有限公司 | Compound plant spice and preparation method |
| CN103103018B (en) * | 2012-11-13 | 2014-03-19 | 苏州谷力生物科技有限公司 | Compound plant spice and preparation method |
| CN109549110A (en) * | 2018-11-30 | 2019-04-02 | 中国肉类食品综合研究中心 | A kind of smoke solution and the preparation method and application thereof |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| C01 | Deemed withdrawal of patent application (patent law 1993) | ||
| WD01 | Invention patent application deemed withdrawn after publication |