CN110150727B - Preparation method of dried orange peel-flavor plant aroma-producing sheet suitable for heating non-combustible cigarettes - Google Patents
Preparation method of dried orange peel-flavor plant aroma-producing sheet suitable for heating non-combustible cigarettes Download PDFInfo
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- CN110150727B CN110150727B CN201910366877.5A CN201910366877A CN110150727B CN 110150727 B CN110150727 B CN 110150727B CN 201910366877 A CN201910366877 A CN 201910366877A CN 110150727 B CN110150727 B CN 110150727B
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B3/00—Preparing tobacco in the factory
- A24B3/14—Forming reconstituted tobacco products, e.g. wrapper materials, sheets, imitation leaves, rods, cakes; Forms of such products
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/10—Chemical features of tobacco products or tobacco substitutes
- A24B15/16—Chemical features of tobacco products or tobacco substitutes of tobacco substitutes
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/28—Treatment of tobacco products or tobacco substitutes by chemical substances
- A24B15/30—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P60/00—Technologies relating to agriculture, livestock or agroalimentary industries
- Y02P60/80—Food processing, e.g. use of renewable energies or variable speed drives in handling, conveying or stacking
- Y02P60/87—Re-use of by-products of food processing for fodder production
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Abstract
A preparation method of a pericarpium Citri Tangerinae-flavored plant aroma-producing sheet suitable for heating non-combustible cigarettes comprises the steps of pericarpium Citri Tangerinae pretreatment, pericarpium Citri Tangerinae ethanol extraction, tobacco stems and tobacco fragments water extraction, mixing the extractive solution with Glycyrrhrizae radix solution, organic acid, polyalcohol and fruit extractive solution, adding pericarpium Citri Tangerinae granule, mixing uniformly, coating onto a substrate, and oven drying to obtain pericarpium Citri Tangerinae-flavored plant aroma-producing sheet suitable for heating non-combustible cigarettes; the water content of the dried orange peel-flavor plant aroma-producing sheet suitable for heating the non-combustible cigarettes is 10-12%, and the coating amount of the coating liquid is 30-40%. The plant aroma producing sheet developed by the invention not only can be suitable for heating non-combustible cigarettes, but also can be applied to traditional cigarettes to play a role in enriching and coordinating the aroma of cigarettes.
Description
Technical Field
The invention relates to a preparation method of a dried orange peel-flavored plant aroma-producing sheet suitable for heating non-combustible cigarettes, and belongs to the technical field of novel tobacco preparation.
Background
In recent years, domestic tobacco enterprises are actively researching the tobacco sheet technology, and particularly, the research on the production and processing technology of paper-making reconstituted tobacco is quite great. Among them, many scholars and experts have studied the application of non-tobacco plants in reconstituted tobacco: for example, chinese patent CN104223346 a invented a method for preparing functional reconstituted tobacco from orange grass, wherein the orange grass is used for replacing wood pulp fibers, so that the reconstituted tobacco has orange aroma; the Chinese patent CN 103783650A discloses application of stevia rebaudiana in preparing reconstituted tobacco and application of stevia rebaudiana extract and/or stevia rebaudiana fiber in preparing reconstituted tobacco, wherein the application is respectively or jointly applied to preparing reconstituted tobacco, and special fragrance is given to the reconstituted tobacco; the invention of Chinese patent CN 101536811A discloses an application method of non-tobacco material lotus leaf in papermaking method sheet, which adds lotus leaf into tobacco powder according to a certain proportion to prepare tobacco sheet after mixing and extracting, thus alleviating the shortage problem of tobacco raw material and improving the moisture absorption performance of tobacco sheet.
The invention discloses a heating non-combustion tobacco sheet and a preparation method thereof in Chinese patent CN 107692303A. The preparation method provided by the invention comprises the following steps: a) Biological treatment is carried out on tobacco leaves under the action of microorganisms, so that primary biological treatment tobacco leaves are obtained; microorganisms include bacillus and/or yeast; b) Mixing the primary biological treatment tobacco leaves with dried orange peel to obtain a mixture; c) Extracting and concentrating the mixture with water, and adding a complex enzyme preparation for biological treatment to obtain a secondary biological treatment concentrated solution; the complex enzyme preparation comprises two or more than two of cellulase, pectase, protease and glucolase; d) Mixing the secondary biological treatment concentrated solution with a modifier for Maillard reaction to obtain a coating material; e) And coating the coating material on the surface of the tobacco sheet base, and drying to obtain the heated non-combustible tobacco sheet. The method is characterized in that the protein is obtained after the water extraction of the mixture of tobacco leaves and dried orange peel, then the amino acid is obtained by biological treatment of the mixture by using a compound enzyme preparation, and the aroma substances are obtained after Maillard reaction, so that the water-insoluble aroma substances of the dried orange peel are not fully utilized.
The heating of the non-combustible tobacco is to bake the tobacco material at a relatively low temperature (generally lower than 350 ℃), so that the baked tobacco material emits tobacco aroma under the condition of not burning, thereby meeting the sensory requirements of tobacco smoking. However, the tobacco materials used in low-temperature non-combustible cigarettes at present are tobacco sheets developed based on traditional cigarettes, the form and quality of the materials cannot completely meet the quality requirements of low-temperature cigarettes, the identification degree of the product aroma is low, and the characteristic aroma of brands cannot be well highlighted.
Although research on preparing functional sheets by taking non-tobacco plants as raw material components has been reported, research on preparing characteristic aroma-producing materials meeting the quality characteristic requirements of low-temperature non-combustible cigarettes on the basis of plant raw materials with characteristic aroma has not been reported.
Disclosure of Invention
The invention aims to provide a preparation method of a dried orange peel-flavor plant aroma-producing sheet suitable for heating non-combustible cigarettes.
To achieve the above and other related objects, the present invention provides the following technical solutions: a preparation method of a dried orange peel-flavor plant aroma-producing sheet suitable for heating non-combustible cigarettes comprises the following steps:
step 1: soaking dried pericarpium Citri Tangerinae in water, decocting in boiling water for 4-5min, taking out pericarpium Citri Tangerinae, draining, and drying at 40-60deg.C until water content is 10-12%;
step 2: mixing tobacco stems and tobacco fragments uniformly, adding into water, extracting at 60-80deg.C for 20-40min, and performing solid-liquid separation to obtain mixed extractive solution of tobacco stems and tobacco fragments and first solid;
step 3: reflux-extracting pericarpium Citri Tangerinae obtained in step 1 with ethanol at 40-50deg.C for 20-30min, separating solid and liquid to obtain pericarpium Citri Tangerinae ethanol extractive solution and second solid, drying the second solid at 80-100deg.C, and grinding into 80-100 mesh to obtain pericarpium Citri Tangerinae granule;
step 4: grinding the first solid into slurry, adding plant fibers with the mass of 5-10% of that of the slurry for slurry preparation, adding the slurry and dried orange peel particles into a pre-papermaking pond together with the fiber slurry, mixing and stirring uniformly, and forming the substrate by net after slurry preparation;
step 5: mixing the mixed extract of tobacco stems and tobacco flakes obtained in the step 2 and the dried orange peel ethanol extract obtained in the step 3 after respective purification treatment to obtain a mixed solution, adding 1-2% of liquorice liquid, 0.1-0.5% of organic acid, 10-20% of polyalcohol and 1-5% of fruit extract into the mixed solution, uniformly mixing and concentrating to a density of 1.0-1.2 g/cm 3 The paste of (2) is coating liquid;
step 6: adding pericarpium Citri Tangerinae particles into the coating solution, mixing, coating onto the substrate, and oven drying to obtain pericarpium Citri Tangerinae-flavored plant aroma-producing sheet suitable for heating non-burnt cigarette; the water content of the dried orange peel-flavor plant aroma-producing sheet suitable for heating the non-combustible cigarettes is 10-12%, and the coating amount of the coating liquid is 30-40%.
The preferable technical scheme is as follows: the plant fiber is at least one of softwood pulp fiber, hardwood pulp fiber and tobacco stem.
The preferable technical scheme is as follows: the fruit extract is at least one of apricot extract, red date extract, fig extract, haw extract and plum extract.
The preferable technical scheme is as follows: the organic acid is at least one of malic acid, citric acid, lactic acid, acetic acid, tartaric acid and isovaleric acid.
The preferable technical scheme is as follows: the polyol is at least one of propylene glycol and glycerol.
The preferable technical scheme is as follows: the boiling water has a mass at least twice that of dried orange peel.
The preferable technical scheme is as follows: in the step 5, the concentration process conditions are that the temperature is 60-100 ℃, the vacuum degree is 0.02-0.08Mpa, and the treatment time is as follows: 30-60min.
Due to the application of the technical scheme, compared with the prior art, the invention has the advantages that:
1. according to the invention, the dried orange peel natural raw materials are selected for pretreatment, so that the traditional processing mode of reconstituted tobacco is broken, and meanwhile, the dried orange peel extracting solution and the tobacco extract are reacted to form the dried orange peel fragrance type coating solution with unique fragrance.
2. According to the invention, the raw materials of the dried orange peel are fully and comprehensively utilized, not only are effective aroma substances extracted, but also solid parts are respectively added in a pulp preparation link and a coating link, so that aroma characteristics of the dried orange peel are further supplemented, aroma loss is reduced, and finally, a flake with rich aroma of the dried orange peel is formed.
3. The plant aroma producing sheet developed by the invention not only can be suitable for heating non-combustible cigarettes, but also can be applied to traditional cigarettes to play a role in enriching and coordinating the aroma of cigarettes.
Detailed Description
Further advantages and effects of the present invention will be readily apparent to those skilled in the art from the following disclosure of the present invention by reference to the specific embodiments.
The terminology used herein is for the purpose of describing particular embodiments only and is not intended to be limiting of the invention. As used herein, the singular forms "a", "an" and "the" are intended to include the plural forms as well, unless the context clearly indicates otherwise.
In describing the preferred embodiment, specific terminology may be resorted to for the sake of clarity; however, the disclosure of the present specification is not intended to be limited to the specific terminology so selected; and it is to be understood that each specific element includes all equivalent techniques for performing the same function, operating in a similar manner, and achieving a similar effect.
Embodiment one: preparation method of dried orange peel-flavor plant aroma-producing sheet suitable for heating non-combustible cigarettes
The preparation method of the dried orange peel-flavored plant aroma-producing sheet suitable for heating the non-combustible cigarettes comprises the following specific preparation processes:
(1) Weighing 1000 g of dried orange peel, soaking the dried orange peel in deionized water to soften, heating to boil with twice more clean water than the raw materials, adding the dried orange peel, boiling for about 4-5 minutes, filtering, taking out the dried orange peel after water filtering, and drying at 40 ℃ in a baking room until the water content is 10% for later use.
(2) Uniformly mixing 1000 g of tobacco stems and 1000 g of tobacco fragments, extracting at 60 ℃ for 40 minutes, and then carrying out solid-liquid separation to obtain a mixed extract and solid of the tobacco stems and tobacco flakes;
(3) Extracting the dried orange peel raw material obtained in the step (1) by adopting ethanol under the condition of heating reflux at 40 ℃ for 30 minutes, carrying out solid-liquid separation after the extraction is finished, quickly drying the solid raw material at 80 ℃, and grinding the solid raw material into 80-mesh particles by adopting a ball mill;
(4) Grinding the solid obtained in the step (2) by adopting a disc mill to obtain mixed slurry, adding 5% of softwood pulp fibers according to the mass ratio of the slurry to carry out slurry preparation, adding half of the dried orange peel particles obtained in the step (3) into a pre-papermaking pond to be mixed with the fiber slurry, uniformly stirring, and carrying out net pulping and forming after slurry preparation to obtain a substrate; the process of making substrates (flakes) by papermaking is known in the art.
(5) Purifying the mixed tobacco extract and pericarpium Citri Tangerinae extract obtained in step (2) and step (3), respectively, and adding Glycyrrhrizae radix solution with an extract mass ratio of 1%, citric acid 0.1%, and Sansan 15%Mixing alcohol and 2% apple extract together, stirring, concentrating to density of 1.0-1.2 g/cm under vacuum pressure of 0.04MPa at 60deg.C in a reactor for 30min 3 Preparing a coating liquid from the paste of (a) and (b); the mixed tobacco extract and the dried orange peel extract are respectively purified, specifically filtered respectively, and filtrate is obtained.
(6) And (3) adding half of the dried orange peel particles remained in the step (4) into the coating liquid, fully mixing with the coating liquid, coating onto the substrate formed in the step (4), and drying to obtain the special sheet with strong dried orange peel fragrance, wherein the water content of the final product of the sheet is 10%, the coating rate is 30%, the width after shredding is 0.6mm, and the length is 1.5cm.
Embodiment two: preparation method of dried orange peel-flavor plant aroma-producing sheet suitable for heating non-combustible cigarettes
(1) Weighing 1000 g of dried orange peel, soaking the dried orange peel in deionized water to soften, heating to boil with twice more clean water than the raw materials, adding the dried orange peel, boiling for about 4-5 minutes, filtering, taking out the dried orange peel after water filtering, and drying at 60 ℃ in a baking room until the water content is 12% for later use.
(2) Uniformly mixing 1000 g of tobacco stems and 1000 g of tobacco fragments, extracting at 80 ℃ for 20 minutes, and then carrying out solid-liquid separation to obtain a mixed extract and a solid of the tobacco stems and the tobacco fragments;
(3) Extracting the dried orange peel raw material obtained in the step (1) by adopting ethanol under the condition of heating reflux at 50 ℃ for 20 minutes, carrying out solid-liquid separation after the extraction is finished, quickly drying the solid raw material at 100 ℃, and grinding the solid raw material into 100-mesh particles by adopting a ball mill;
(4) Grinding the solid obtained in the step (2) by adopting a disc mill to obtain mixed slurry, adding 5% of softwood pulp fibers and 5% of fibrilia according to the mass ratio of the slurry to prepare slurry, adding half of the dried orange peel particles obtained in the step (3) into a pre-papermaking pond to be mixed with the fiber slurry, uniformly stirring, and forming by net papermaking after slurry preparation to obtain a substrate;
(5) Mixing the tobacco extract obtained in the step (2) and the step (3)And respectively purifying pericarpium Citri Tangerinae extractive solution, adding Glycyrrhrizae radix solution 1% by mass, malic acid 0.2% by mass, propylene glycol 5% by mass, glycerol 15% by mass and fructus Pruni extractive solution 3% by mass, mixing, stirring, concentrating at 60deg.C under vacuum pressure of 0.04MPa for 30min to obtain a concentrated solution with density of 1.0-1.2 g/cm 3 Preparing a coating liquid from the paste of (a) and (b);
(6) And (3) adding half of the dried orange peel particles remained in the step (4) into the coating liquid, fully mixing with the coating liquid, coating onto the substrate formed in the step (4), and drying to obtain the special sheet with strong dried orange peel fragrance, wherein the water content of the final product of the sheet is 10%, the coating rate is 35%, the width after shredding is 0.8mm, and the length is 3.5cm.
Embodiment III: preparation method of dried orange peel-flavor plant aroma-producing sheet suitable for heating non-combustible cigarettes
A preparation method of a dried orange peel-flavor plant aroma-producing sheet suitable for heating non-combustible cigarettes comprises the following steps:
step 1: soaking dried pericarpium Citri Tangerinae in water, decocting in boiling water for 4.5min, taking out pericarpium Citri Tangerinae, draining, and drying at 50deg.C until water content is 11%;
step 2: mixing tobacco stems and tobacco fragments uniformly, adding the mixture into water, extracting for 30min at 70 ℃, and carrying out solid-liquid separation to obtain a mixed extract of the tobacco stems and the tobacco fragments and a first solid;
step 3: reflux-extracting pericarpium Citri Tangerinae obtained in step 1 with ethanol at 45deg.C for 25min, separating solid and liquid to obtain pericarpium Citri Tangerinae ethanol extractive solution and second solid, drying the second solid at 90deg.C, and grinding into 90 mesh to obtain pericarpium Citri Tangerinae granule;
step 4: grinding the first solid into slurry, adding plant fibers with the mass of 7.5% of that of the slurry for slurry preparation, adding the slurry and dried orange peel particles into a pre-papermaking pond together with the fiber slurry, mixing and stirring uniformly, and forming the substrate by net after slurry preparation;
step 5: mixing the mixed extractive solution of tobacco stalk and tobacco flake obtained in step 2 with pericarpium Citri Tangerinae obtained in step 3Respectively purifying the ethanol extract, mixing to obtain mixed solution, adding Glycyrrhrizae radix solution 1.5% by mass, organic acid 0.3% by mass, polyalcohol 15% by mass and fruit extract 3% by mass into the mixed solution, mixing uniformly, and concentrating to density of 1.1g/cm 3 The paste of (2) is coating liquid;
step 6: adding pericarpium Citri Tangerinae particles into the coating solution, mixing, coating onto the substrate, and oven drying to obtain pericarpium Citri Tangerinae-flavored plant aroma-producing sheet suitable for heating non-burnt cigarette; the dried orange peel-flavor plant aroma-producing sheet suitable for the heating non-combustible cigarettes has the water content of 11% and the coating amount of the coating liquid of 35%.
The preferred embodiments are: the plant fiber is hardwood pulp fiber.
The preferred embodiments are: the fruit extract is fig extract.
The preferred embodiments are: the organic acid is lactic acid.
The preferred embodiments are: the polyol is propylene glycol and glycerol according to the following ratio of 1:1, and a mixture of the components in a mass ratio.
The preferred embodiments are: the boiling water has twice the mass of dried pericarpium Citri Tangerinae.
The preferred embodiments are: in the step 5, the concentration process conditions are that the temperature is 80 ℃, the vacuum degree is 0.05Mpa, and the treatment time is as follows: 45min.
Embodiment four: preparation method of dried orange peel-flavor plant aroma-producing sheet suitable for heating non-combustible cigarettes
A preparation method of a dried orange peel-flavor plant aroma-producing sheet suitable for heating non-combustible cigarettes comprises the following steps:
step 1: soaking dried pericarpium Citri Tangerinae in water, decocting in boiling water for 4min, taking out pericarpium Citri Tangerinae, draining, and drying at 60deg.C until water content is 10%;
step 2: mixing tobacco stems and tobacco fragments uniformly, adding the mixture into water, extracting for 40min at 60 ℃, and carrying out solid-liquid separation to obtain a mixed extract of the tobacco stems and the tobacco fragments and a first solid;
step 3: reflux-extracting pericarpium Citri Tangerinae obtained in step 1 with ethanol at 40deg.C for 30min, separating solid and liquid to obtain pericarpium Citri Tangerinae ethanol extractive solution and second solid, drying the second solid at 80deg.C, and grinding into 100 mesh to obtain pericarpium Citri Tangerinae granule;
step 4: grinding the first solid into slurry, adding plant fibers accounting for 5% of the mass of the slurry to prepare slurry, adding the slurry and dried orange peel particles into a pre-papermaking pond together with the fiber slurry, mixing and stirring uniformly, and forming on a net to obtain a substrate;
step 5: mixing the mixed extract of tobacco stems and tobacco flakes obtained in the step 2 and the dried orange peel ethanol extract obtained in the step 3 after purification treatment respectively to obtain a mixed solution, adding 1% of liquorice liquid, 0.1% of organic acid, 10% of polyalcohol and 1% of fruit extract into the mixed solution, uniformly mixing and concentrating to a density of 1.0g/cm 3 The paste of (2) is coating liquid;
step 6: adding pericarpium Citri Tangerinae particles into the coating solution, mixing, coating onto the substrate, and oven drying to obtain pericarpium Citri Tangerinae-flavored plant aroma-producing sheet suitable for heating non-burnt cigarette; the dried orange peel-flavor plant aroma-producing sheet suitable for the heating non-combustible cigarettes has the moisture content of 10% and the coating amount of the coating liquid of 30%.
The preferred embodiments are: the plant fiber is a mixture of softwood pulp fiber and hardwood pulp fiber according to the mass ratio of 1:2.
The preferred embodiments are: the fruit extract is apricot extract and red date extract according to the following ratio of 2:1, and a mixture of the components in a mass ratio.
The preferred embodiments are: the organic acid is malic acid and citric acid according to the following ratio of 1:1, and a mixture of the components in a mass ratio.
The preferred embodiments are: the polyol is propylene glycol.
The preferred embodiments are: the boiling water has a mass 2.1 times of that of dried pericarpium Citri Tangerinae.
The preferred embodiments are: in the step 5, the concentration process condition is that the temperature is 60 ℃, the vacuum degree is 0.02Mpa, and the treatment time is 60min.
Fifth embodiment: preparation method of dried orange peel-flavor plant aroma-producing sheet suitable for heating non-combustible cigarettes
A preparation method of a dried orange peel-flavor plant aroma-producing sheet suitable for heating non-combustible cigarettes comprises the following steps:
step 1: soaking dried pericarpium Citri Tangerinae in water, decocting in boiling water for 5min, taking out pericarpium Citri Tangerinae, draining, and drying at 40deg.C until water content is 10%;
step 2: mixing tobacco stems and tobacco fragments uniformly, adding the mixture into water, extracting for 20min at 80 ℃, and carrying out solid-liquid separation to obtain a mixed extract of the tobacco stems and the tobacco fragments and a first solid;
step 3: reflux-extracting pericarpium Citri Tangerinae obtained in step 1 with ethanol at 50deg.C for 20min, separating solid and liquid to obtain pericarpium Citri Tangerinae ethanol extractive solution and second solid, drying the second solid at 80deg.C, and grinding into 80 mesh to obtain pericarpium Citri Tangerinae granule;
step 4: grinding the first solid into slurry, adding plant fibers accounting for 10% of the mass of the slurry to prepare slurry, adding the slurry and dried orange peel particles into a pre-papermaking pond together with the fiber slurry, mixing and stirring uniformly, and forming on a net to obtain a substrate;
step 5: mixing the mixed extract of tobacco stems and tobacco flakes obtained in the step 2 and the dried orange peel ethanol extract obtained in the step 3 after respective purification treatment to obtain a mixed solution, adding 2% of liquorice liquid, 0.5% of organic acid, 20% of polyalcohol and 5% of fruit extract into the mixed solution, uniformly mixing, and concentrating to a density of 1.2g/cm 3 The paste of (2) is coating liquid;
step 6: adding pericarpium Citri Tangerinae particles into the coating solution, mixing, coating onto the substrate, and oven drying to obtain pericarpium Citri Tangerinae-flavored plant aroma-producing sheet suitable for heating non-burnt cigarette; the dried orange peel-flavor plant aroma-producing sheet suitable for the heating non-combustible cigarettes has the moisture content of 12% and the coating amount of the coating liquid of 40%.
The preferred embodiments are: the plant fiber is tobacco stalk.
The preferred embodiments are: the fruit extract is a haw extract.
The preferred embodiments are: the organic acid is tartaric acid.
The preferred embodiments are: the polyol is glycerol.
The preferred embodiments are: the boiling water has a mass 2.5 times of that of dried pericarpium Citri Tangerinae.
The preferred embodiments are: in the step 5, the concentration process condition is that the temperature is 100 ℃, the vacuum degree is 0.08Mpa, and the treatment time is 60min.
The foregoing description of the preferred embodiment of the invention is not intended to be limiting in any way, but rather, it is intended to cover all modifications or variations of the invention which fall within the spirit and scope of the invention.
Claims (6)
1. A preparation method of a dried orange peel-flavor plant aroma-producing sheet suitable for heating non-combustible cigarettes is characterized by comprising the following steps of: comprises the following steps:
step 1: soaking dried pericarpium Citri Tangerinae in water, decocting in boiling water for 4-5min, taking out pericarpium Citri Tangerinae, draining, and drying at 40-60deg.C until water content is 10-12%;
step 2: mixing tobacco stems and tobacco fragments uniformly, adding into water, extracting at 60-80deg.C for 20-40min, and performing solid-liquid separation to obtain mixed extractive solution of tobacco stems and tobacco fragments and first solid;
step 3: reflux-extracting pericarpium Citri Tangerinae obtained in step 1 with ethanol at 40-50deg.C for 20-30min, separating solid and liquid to obtain pericarpium Citri Tangerinae ethanol extractive solution and second solid, drying the second solid at 80-100deg.C, and grinding into 80-100 mesh to obtain pericarpium Citri Tangerinae granule;
step 4: grinding the first solid into slurry, adding plant fibers with the mass of 5-10% of that of the slurry for slurry preparation, adding the slurry and dried orange peel particles into a pre-papermaking pond together with the fiber slurry, mixing and stirring uniformly, and forming the substrate by net after slurry preparation;
step 5: mixing the mixed extract of tobacco stems and tobacco flakes obtained in the step 2 and the dried orange peel ethanol extract obtained in the step 3 after respective purification treatment to obtain a mixed solution, adding 1-2% of liquorice liquid, 0.1-0.5% of organic acid, 10-20% of polyalcohol and 1-5% of fruit extract into the mixed solution, uniformly mixing and concentrating to a density of 1.0-1.2 g/cm 3 The paste of (2) is coating liquid; the polyalcohol is at least one of propylene glycol and glycerol;
step 6: adding pericarpium Citri Tangerinae particles into the coating solution, mixing, coating onto the substrate, and oven drying to obtain pericarpium Citri Tangerinae-flavored plant aroma-producing sheet suitable for heating non-burnt cigarette; the water content of the dried orange peel-flavor plant aroma-producing sheet suitable for heating the non-combustible cigarettes is 10-12%, and the coating amount of the coating liquid is 30-40%.
2. The method for preparing the dried orange peel-flavor plant aroma-producing sheet suitable for heating non-combustible cigarettes according to claim 1, wherein the method comprises the following steps: the plant fiber is at least one of softwood pulp fiber, hardwood pulp fiber and tobacco stem.
3. The method for preparing the dried orange peel-flavor plant aroma-producing sheet suitable for heating non-combustible cigarettes according to claim 1, wherein the method comprises the following steps: the fruit extract is at least one of apricot extract, red date extract, fig extract, haw extract and plum extract.
4. The method for preparing the dried orange peel-flavor plant aroma-producing sheet suitable for heating non-combustible cigarettes according to claim 1, wherein the method comprises the following steps: the organic acid is at least one of malic acid, citric acid, lactic acid, acetic acid, tartaric acid and isovaleric acid.
5. The method for preparing the dried orange peel-flavor plant aroma-producing sheet suitable for heating non-combustible cigarettes according to claim 1, wherein the method comprises the following steps: the boiling water has a mass at least twice that of dried orange peel.
6. The method for preparing the dried orange peel-flavor plant aroma-producing sheet suitable for heating non-combustible cigarettes according to claim 1, wherein the method comprises the following steps: in the step 5, the concentration process conditions are that the temperature is 60-100 ℃, the vacuum degree is 0.02-0.08Mpa, and the treatment time is as follows: 30-60min.
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|---|---|---|---|---|
| RU2352205C1 (en) * | 2008-05-15 | 2009-04-20 | Олег Иванович Квасенков | Method of production reconstituted tobacco |
| CN104223346B (en) * | 2014-10-17 | 2016-08-24 | 安徽中烟再造烟叶科技有限责任公司 | The method of functional type reconstituted tobacco prepared by Fructus Citri tangerinae grass |
| CN104382219A (en) * | 2014-10-17 | 2015-03-04 | 安徽中烟再造烟叶科技有限责任公司 | Method for manufacturing reconstituted tobaccos through pericarpium citri reticulatae and chrysanthemums |
| CN104687233B (en) * | 2014-12-30 | 2017-10-10 | 广东中烟工业有限责任公司 | The preparation method and orange flavor reconstituted tobacco of a kind of orange flavor reconstituted tobacco |
| CN104886754B (en) * | 2015-04-20 | 2016-04-13 | 广州神韵香料科技发展有限公司 | A kind of preparation method of the reconstituted tobacoo containing vetiver and application thereof |
| CN107183778A (en) * | 2017-07-03 | 2017-09-22 | 中烟施伟策（云南）再造烟叶有限公司 | A kind of papermaking-method reconstituted tobaccos preparation method of the natural plant powder containing ultra micro |
| CN109007956A (en) * | 2018-06-01 | 2018-12-18 | 云南中烟工业有限责任公司 | A kind of preparation method and purposes of cigarette fruit solid fragrance |
| CN109567254B (en) * | 2018-12-20 | 2021-07-30 | 陕西科技大学 | Tobacco sheet, preparation method thereof, substrate of tobacco sheet and preparation method of coating liquid |
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