CN110124595A - A kind of lens monomer reaction kettle high-efficiency condensation device - Google Patents

A kind of lens monomer reaction kettle high-efficiency condensation device Download PDF

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Publication number
CN110124595A
CN110124595A CN201910510735.1A CN201910510735A CN110124595A CN 110124595 A CN110124595 A CN 110124595A CN 201910510735 A CN201910510735 A CN 201910510735A CN 110124595 A CN110124595 A CN 110124595A
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CN
China
Prior art keywords
inner shell
reaction kettle
shell
rotary shaft
monomer reaction
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CN201910510735.1A
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Chinese (zh)
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CN110124595B (en
Inventor
钱军
戴双汉
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JIANGSU KOC OPTICAL MATERIAL TECHNOLOGY Co Ltd
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JIANGSU KOC OPTICAL MATERIAL TECHNOLOGY Co Ltd
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Publication of CN110124595A publication Critical patent/CN110124595A/en
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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D5/00Condensation of vapours; Recovering volatile solvents by condensation
    • B01D5/0057Condensation of vapours; Recovering volatile solvents by condensation in combination with other processes
    • B01D5/0072Condensation of vapours; Recovering volatile solvents by condensation in combination with other processes with filtration
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D5/00Condensation of vapours; Recovering volatile solvents by condensation
    • B01D5/0078Condensation of vapours; Recovering volatile solvents by condensation characterised by auxiliary systems or arrangements
    • B01D5/009Collecting, removing and/or treatment of the condensate
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D50/00Combinations of methods or devices for separating particles from gases or vapours
    • B01D50/20Combinations of devices covered by groups B01D45/00 and B01D46/00
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D53/00Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
    • B01D53/002Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by condensation
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D53/00Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
    • B01D53/14Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by absorption
    • B01D53/1487Removing organic compounds
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0053Details of the reactor
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/18Stationary reactors having moving elements inside
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049Controlling or regulating processes
    • B01J2219/00051Controlling the temperature
    • B01J2219/00121Controlling the temperature by direct heating or cooling
    • B01J2219/0013Controlling the temperature by direct heating or cooling by condensation of reactants

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  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Analytical Chemistry (AREA)
  • General Chemical & Material Sciences (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Physical Or Chemical Processes And Apparatus (AREA)
  • Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)

Abstract

The invention proposes a kind of lens monomer reaction kettle high-efficiency condensation devices, including the condenser ontology by support feet station twelve Earthly Branches support;Condenser ontology is made of the double Shell that outer shell and inner shell are constituted, and inner shell lower end and upper end are respectively equipped with air inlet pipe and an air outlet pipe, and the upper end of air inlet pipe passes through porous plate and is connected with processing section;Vertically go deep into one rotary shaft of bottom at the top of from inner shell, is fixed with spiral blade in rotary shaft;The multiple filtration plate tilted upward is symmetrically arranged on inner shell two sidewalls, filter plate end is close with spiral blade but does not connect;The present invention constitutes the helical intake that air-flow rises in condenser using rotary shaft and the spiral blade that is arranged thereon, by gas solid granule and some drop impurity absorptions on spiral blade and filter plate, it is integrated with cooling down to realize filtering.

Description

A kind of lens monomer reaction kettle high-efficiency condensation device
Technical field
The present invention relates to a kind of lens monomer reaction kettle high-efficiency condensation devices.
Background technique
Currently, eyeglass on the market is other than using organic glass, using the synthesis with excellent optical characteristics Resin is constantly developing as the exploitation of lens materials;Resin lens have light-weight, transparency compared with unorganic glass Height does the features such as impact, easy processing;Allyl alcohol etc. is had in reaction kettle in existing resin lens synthetic reaction equipment production process Gasification product or in which the liquid or solid impurity particle swept along generate, subsequent to need to install additional condensing plant to recycle, but at present The general condensation efficiency of condensing plant it is slower, and do not have filtering function, the impurity being mingled in the liquid condensed out easily blocks Air inlet pipe, and lead to the yield losses of condensed product, it is improved therefore, it is necessary to further to the prior art.
Summary of the invention
The purpose of the present invention is to solve the above the deficiencies in the prior art, and it is efficient to provide a kind of lens monomer reaction kettle use Condensing unit, including the condenser ontology for support with standing by support leg;The condenser ontology by outer shell and The double Shell composition that inner shell is constituted, the interior inner shell is condensation process area;The condensation process area includes logical Cross the superposed treatment region that a porous plate separates and the conical liquid recovery area positioned at lower part;
Inner shell lower end and upper end are respectively equipped with air inlet pipe and an air outlet pipe, the upper end of the air inlet pipe pass through porous plate with Processing section is connected;Vertically go deep into one rotary shaft of bottom at the top of from inner shell, is fixed with spiral blade in the rotary shaft;
The multiple filtration plate tilted upward, the filter plate end and the spiral shell are symmetrically arranged on inner shell two sidewalls Rotation shape blade is close but does not connect;The upper and lower ends of the outer shell are respectively equipped with refrigerant exit and refrigerant inlet;
The condensing unit further includes the wash spray circulatory system, and the wash cycle system includes fluid reservoir, follows Ring water pump and the spray head that rotary shaft two sides are protruded into inner shell and be located at from inner shell upper end;The taper liquid Body recovery area is connected by an outlet tube with fluid reservoir, and the fluid reservoir passes through the water circulating pump and the spray head phase Connection;
Preferably, the spray head is rotary nozzle.
Preferably, the filter plate is equipped with 3-5 layers.
Preferably, the filter plate tilt angle is 30-45 °.
Preferably, the liquid storage pot bottom is equipped with tapping valve.
Rise in condenser the utility model has the advantages that the present invention constitutes air-flow with the spiral blade being arranged thereon using rotary shaft Helical intake, by gas solid granule and some drop impurity absorptions on rotating vane and filter plate, realize Filtering is integrated with cooling, meanwhile, the time of contact of gas Yu spiral blade and filter plate is increased, condensation is effectively improved The yield of product;In addition, carrying out spray and further condensation enrichment to gas using the liquid to get off by preliminary condensation, system is realized The recycling of organic gas, high production efficiency in system.
Detailed description of the invention
Fig. 1 is the lens monomer reaction kettle high-efficiency condensation apparatus structure schematic diagram in the present invention.
In figure, 1- condenser ontology, 11- outer shell, 12- inner shell, 13- condensation process area, 131- treatment region, 132- conical liquid recovery area, 14- porous plate, 15- air inlet pipe, 16- escape pipe, 17- rotary shaft, 18- support leg, 19- filtering Plate, 171- spiral blade, the 2- wash spray circulatory system, 21- fluid reservoir, 22- water circulating pump, 23- spray head, 24- go out liquid Pipe, 25- tapping valve, 3- refrigerant exit, 4- refrigerant inlet.
Specific embodiment
As shown in Figure 1, the present embodiment provides a kind of lens monomer reaction kettle high-efficiency condensation devices, including pass through support leg 18 carry out the condenser ontology 1 supported with standing;The condenser ontology 1 is made of double outer shell 11 and inner shell 12 Layer shell composition, the interior inner shell 12 is condensation process area 13;The condensation process area 13 includes passing through a porous plate The 14 superposed treatment regions 131 separated and the conical liquid recovery area 132 positioned at lower part;
12 lower end of inner shell and upper end are respectively equipped with air inlet pipe 15 and escape pipe 16, and the upper end of the air inlet pipe 15 passes through Porous plate 14 is connected with processing section 131;Vertically go deep into one rotary shaft 17 of bottom, the rotary shaft 17 from 12 top of inner shell On be fixed with spiral blade 171;
Be symmetrically arranged with the multiple filtration plate 19 tilted upward on 12 two sidewalls of inner shell, 19 end of filter plate with The spiral blade 171 is close but does not connect;The upper and lower ends of the outer shell 11 are respectively equipped with refrigerant exit 3 and refrigerant Entrance 4.
The condensing unit further includes the wash spray circulatory system 2, the wash cycle system include fluid reservoir 21, Water circulating pump 22 and the spray head 23 that 17 two sides of rotary shaft are protruded into inner shell 12 and be located at from 12 upper end of inner shell; The conical liquid recovery area 132 is connected by an outlet tube 24 with fluid reservoir 21, and the fluid reservoir 21 passes through described Water circulating pump 22 is connected with the spray head 23;
In the above-mentioned technical solutions, the spray head 23 is rotary nozzle.
In the above-mentioned technical solutions, the filter plate 19 is equipped with 3-5 layers.
In the above-mentioned technical solutions, 19 tilt angle of filter plate is 30-45 °.
In the above-mentioned technical solutions, 21 bottom of fluid reservoir is equipped with tapping valve 25.
The foregoing is merely illustrative of the preferred embodiments of the present invention, is not intended to limit the invention, all in essence of the invention Within mind and principle, any modification, equivalent replacement, improvement and so on be should all be included in the protection scope of the present invention.

Claims (5)

1. a kind of lens monomer reaction kettle high-efficiency condensation device, which is characterized in that including support with standing by support leg Condenser ontology;The condenser ontology is made of the double Shell that outer shell and inner shell are constituted, and described is interior It is condensation process area in floor shell;The condensation process area by a porous plate is divided into the treatment region on top and positioned at lower part Conical liquid recovery area;
Inner shell lower end and upper end are respectively equipped with air inlet pipe and an air outlet pipe, and the upper end of the air inlet pipe passes through porous plate and processing Section is connected;Vertically go deep into one rotary shaft of bottom at the top of from inner shell, is fixed with spiral blade in the rotary shaft;
The multiple filtration plate tilted upward, the filter plate end and the helical form are symmetrically arranged on inner shell two sidewalls Blade is close but does not connect;The upper and lower ends of the outer shell are respectively equipped with refrigerant exit and refrigerant inlet;
The condensing unit further includes the wash spray circulatory system, and the wash cycle system includes fluid reservoir, recirculated water Pump and the spray head that rotary shaft two sides are protruded into inner shell and be located at from inner shell upper end;The conical liquid returns It receives area to be connected by an outlet tube with fluid reservoir, the fluid reservoir is connected by the circulating pump with the spray head.
2. a kind of lens monomer reaction kettle high-efficiency condensation device according to claim 1, which is characterized in that the spray Head is rotary nozzle.
3. a kind of lens monomer reaction kettle high-efficiency condensation device according to claim 1, which is characterized in that the mistake Filter plate is equipped with 3-5 layers.
4. a kind of lens monomer reaction kettle high-efficiency condensation device according to claim 1, which is characterized in that the mistake Inclination of filtering plate angle is 30-45 °.
5. a kind of lens monomer reaction kettle high-efficiency condensation device according to claim 1, which is characterized in that the storage Flow container bottom is equipped with tapping valve.
CN201910510735.1A 2019-06-13 2019-06-13 Lens monomer is high-efficient condensing equipment for reation kettle Active CN110124595B (en)

Priority Applications (1)

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CN201910510735.1A CN110124595B (en) 2019-06-13 2019-06-13 Lens monomer is high-efficient condensing equipment for reation kettle

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CN110124595B CN110124595B (en) 2024-04-30

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Citations (22)

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SU704641A1 (en) * 1977-03-05 1979-12-25 Казанский Химико-Технологический Институт Им. С.М.Кирова Mass-exchange apparatus
JP2000225394A (en) * 1999-02-04 2000-08-15 Ishikawajima Harima Heavy Ind Co Ltd Solid-liquid separating apparatus
CN101851520A (en) * 2010-04-29 2010-10-06 江苏中容电气有限公司 Sludge pyrolysis gas fractional condensation method for recycling biological oil
CN201802593U (en) * 2010-10-11 2011-04-20 吉首大学 Separator demisting device of compressor
CN202052448U (en) * 2011-05-19 2011-11-30 韦志锋 Rotary fume filter
DE202012002963U1 (en) * 2012-03-14 2012-04-03 Raimund Rerucha separators
CN102532825A (en) * 2011-12-14 2012-07-04 江苏可奥熙光学材料科技有限公司 Preparation method for high-stability resin monomer
CN104383714A (en) * 2014-11-30 2015-03-04 重庆市天星寨粉葛食品有限公司 Food extraction device capable of recycling solvent
CN105084320A (en) * 2015-08-14 2015-11-25 长沙金马冶金设备有限公司 Condenser for recycling sulfur and condensing technology
CN204815749U (en) * 2015-07-06 2015-12-02 安徽圣诺贝化学科技有限公司 Solvent recovery unit in tail gas
CN204891276U (en) * 2015-06-29 2015-12-23 安徽广信农化股份有限公司 Toluene recovery unit is used in production of 3, 4 - dichlorophenyl isocyanate
CN205391787U (en) * 2016-02-29 2016-07-27 广东衡光化工有限公司 Condenser that producing building emulsion was used
CN205613263U (en) * 2016-05-04 2016-10-05 山东鲁抗中和环保科技有限公司 Reation kettle tail gas processing apparatus
CN205699538U (en) * 2016-04-29 2016-11-23 淮安市赛利化工有限公司 A kind of glycol recovery device
CN205925356U (en) * 2016-08-03 2017-02-08 南京钟腾化工有限公司 Cis -butenedioic anhydride waste gas recovery device
WO2017081625A1 (en) * 2015-11-12 2017-05-18 Green Solutions Sp. Z O.O. A method for receiving, fractioning and condensing gas mixtures, particularly hydrocarbon formed during thermo-catalytic degradation of plastics and a set of devices for implementing the method
CN107008111A (en) * 2017-05-22 2017-08-04 朱强 Organic exhaust gas multistage cold washing condensation recycling and processing device and method
WO2017219623A1 (en) * 2016-06-23 2017-12-28 华南理工大学 Online cyclic regeneration organic waste gas treatment method and device
CN206853170U (en) * 2017-05-27 2018-01-09 建滔(番禺南沙)石化有限公司 A kind of condenser for resin recovery
CN208465226U (en) * 2018-04-26 2019-02-05 浙江龙安环保工程有限公司 A kind of waste gas condensation device in sewage disposal process
CN208959593U (en) * 2018-09-28 2019-06-11 王钰淇 A kind of environment-friendly type industrial waste-gas purifier
CN210303614U (en) * 2019-06-13 2020-04-14 江苏可奥熙光学材料科技有限公司 Lens monomer is high-efficient condensing equipment for reation kettle

Patent Citations (22)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
SU704641A1 (en) * 1977-03-05 1979-12-25 Казанский Химико-Технологический Институт Им. С.М.Кирова Mass-exchange apparatus
JP2000225394A (en) * 1999-02-04 2000-08-15 Ishikawajima Harima Heavy Ind Co Ltd Solid-liquid separating apparatus
CN101851520A (en) * 2010-04-29 2010-10-06 江苏中容电气有限公司 Sludge pyrolysis gas fractional condensation method for recycling biological oil
CN201802593U (en) * 2010-10-11 2011-04-20 吉首大学 Separator demisting device of compressor
CN202052448U (en) * 2011-05-19 2011-11-30 韦志锋 Rotary fume filter
CN102532825A (en) * 2011-12-14 2012-07-04 江苏可奥熙光学材料科技有限公司 Preparation method for high-stability resin monomer
DE202012002963U1 (en) * 2012-03-14 2012-04-03 Raimund Rerucha separators
CN104383714A (en) * 2014-11-30 2015-03-04 重庆市天星寨粉葛食品有限公司 Food extraction device capable of recycling solvent
CN204891276U (en) * 2015-06-29 2015-12-23 安徽广信农化股份有限公司 Toluene recovery unit is used in production of 3, 4 - dichlorophenyl isocyanate
CN204815749U (en) * 2015-07-06 2015-12-02 安徽圣诺贝化学科技有限公司 Solvent recovery unit in tail gas
CN105084320A (en) * 2015-08-14 2015-11-25 长沙金马冶金设备有限公司 Condenser for recycling sulfur and condensing technology
WO2017081625A1 (en) * 2015-11-12 2017-05-18 Green Solutions Sp. Z O.O. A method for receiving, fractioning and condensing gas mixtures, particularly hydrocarbon formed during thermo-catalytic degradation of plastics and a set of devices for implementing the method
CN205391787U (en) * 2016-02-29 2016-07-27 广东衡光化工有限公司 Condenser that producing building emulsion was used
CN205699538U (en) * 2016-04-29 2016-11-23 淮安市赛利化工有限公司 A kind of glycol recovery device
CN205613263U (en) * 2016-05-04 2016-10-05 山东鲁抗中和环保科技有限公司 Reation kettle tail gas processing apparatus
WO2017219623A1 (en) * 2016-06-23 2017-12-28 华南理工大学 Online cyclic regeneration organic waste gas treatment method and device
CN205925356U (en) * 2016-08-03 2017-02-08 南京钟腾化工有限公司 Cis -butenedioic anhydride waste gas recovery device
CN107008111A (en) * 2017-05-22 2017-08-04 朱强 Organic exhaust gas multistage cold washing condensation recycling and processing device and method
CN206853170U (en) * 2017-05-27 2018-01-09 建滔(番禺南沙)石化有限公司 A kind of condenser for resin recovery
CN208465226U (en) * 2018-04-26 2019-02-05 浙江龙安环保工程有限公司 A kind of waste gas condensation device in sewage disposal process
CN208959593U (en) * 2018-09-28 2019-06-11 王钰淇 A kind of environment-friendly type industrial waste-gas purifier
CN210303614U (en) * 2019-06-13 2020-04-14 江苏可奥熙光学材料科技有限公司 Lens monomer is high-efficient condensing equipment for reation kettle

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