CN110124349A - A kind of multifunction extracting device - Google Patents
A kind of multifunction extracting device Download PDFInfo
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- CN110124349A CN110124349A CN201910346059.9A CN201910346059A CN110124349A CN 110124349 A CN110124349 A CN 110124349A CN 201910346059 A CN201910346059 A CN 201910346059A CN 110124349 A CN110124349 A CN 110124349A
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- condenser
- tank body
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61J—CONTAINERS SPECIALLY ADAPTED FOR MEDICAL OR PHARMACEUTICAL PURPOSES; DEVICES OR METHODS SPECIALLY ADAPTED FOR BRINGING PHARMACEUTICAL PRODUCTS INTO PARTICULAR PHYSICAL OR ADMINISTERING FORMS; DEVICES FOR ADMINISTERING FOOD OR MEDICINES ORALLY; BABY COMFORTERS; DEVICES FOR RECEIVING SPITTLE
- A61J3/00—Devices or methods specially adapted for bringing pharmaceutical products into particular physical or administering forms
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D11/00—Solvent extraction
- B01D11/02—Solvent extraction of solids
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D11/00—Solvent extraction
- B01D11/02—Solvent extraction of solids
- B01D11/028—Flow sheets
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
- C11B9/022—Refining
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
- C11B9/025—Recovery by solvent extraction
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
- C11B9/027—Recovery of volatiles by distillation or stripping
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- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Life Sciences & Earth Sciences (AREA)
- Organic Chemistry (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Engineering & Computer Science (AREA)
- Health & Medical Sciences (AREA)
- Medicinal Chemistry (AREA)
- Pharmacology & Pharmacy (AREA)
- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
- Public Health (AREA)
- Veterinary Medicine (AREA)
- Extraction Or Liquid Replacement (AREA)
Abstract
The invention discloses a kind of extract equipments, comprising: the wall portion of extractor, including tank body, the tank body is equipped with collet；The tank body is adapted to fit into material and the mixed feed liquid of solvent, and is suitable for importing steam and heats to feed liquid, so that feed liquid is heated to Extracting temperature；The tank body is further adapted for importing air-compressed gas and stirs to feed liquid；The collet is suitable for being passed through circulating hot water after feed liquid is heated to Extracting temperature, so that feed liquid maintains Extracting temperature；And first condenser, it is connected to the tank body, the solvent vapo(u)r carried secretly when suitable for discharging to air-compressed gas condenses, so as to recycling design.Extract equipment of the invention, effective component, the extraction efficiency that can sufficiently extract material are high, and energy recycling design, can directly be concentrated and separated, settle at one go to extracting solution after obtaining extracting solution.In addition, extract equipment of the invention can also carry out distillation extraction to plant perfume and obtain sesame oil.
Description
Technical field
The present invention relates to Chinese herbal medicine extractive technique field more particularly to a kind of extract equipments.
Background technique
Currently, most of herbal pharmaceutical factories or Chinese herbal medicine product producer, extract Chinese herbal medicine application is still traditional extraction
Tank, and feed liquid is heated in such a way that extractor collet leads to steam, this heating method will lead to jacket temperature fluctuation
It is larger, it is unstable.Moreover, traditional extractor, the volume of tank body is larger, mostly 2m3~10m3, thus extracting solid material
When, be not suitable for mechanical agitation, be usually that the mode of the outer convection current of tank body is taken to make the slow convection current of feed liquid, be difficult to obtain stirring effect,
And time-consuming, and energy consumption is high, and extraction efficiency is low, and heat source consumption is big, and exhaust gas is escaped in extraction process, pollutes environment.Some producers
Mechanical agitation feed liquid is used to extractor, but during the extraction process, agitation paddle often occurs and gets stuck, thing liquid is turned round and round phenomenon, and effect is extracted
Fruit is low.In addition, traditional extractor, after material extracts, cannot effective recovered material absorption organic solvent, on the one hand
Cause the loss of solvent larger, the material that another aspect direct emission speckles with organic solvent will cause environmental pollution.
In addition, the abstraction function of above-mentioned traditional extractor is also relatively simple, the material variety of extraction is had certain limitations,
Extractible material variety is less.
Summary of the invention
For this purpose, the present invention provides a kind of extract equipment, to solve the problems, such as to exist above.
According to an aspect of the invention, there is provided a kind of extract equipment, comprising: extractor, including tank body, the tank body
Wall portion be equipped with collet；The tank body is adapted to fit into material and the mixed feed liquid of solvent, and is suitable for importing steam and adds to feed liquid
Heat, so that feed liquid is heated to Extracting temperature；The tank body is further adapted for importing air-compressed gas and stirs to feed liquid；The collet is suitable
In being passed through circulating hot water after feed liquid is heated to Extracting temperature, so that feed liquid maintains Extracting temperature；And first condenser, with
The tank body connection, the solvent vapo(u)r carried secretly when suitable for discharging to air-compressed gas condenses, so as to recycling design.
Optionally, in extract equipment according to the present invention, the first air guide is respectively equipped at the top and bottom of the tank body
Pipe and the second gas-guide tube, to import steam and/or air-compressed gas into tank body.
Optionally, in extract equipment according to the present invention, further includes: liquid trap, respectively with first condenser and
Tank body connection；Solvent vapo(u)r flows into the liquid trap after condensing in the first condenser, and is back to the tank body by liquid trap
It is interior.
Optionally, in extract equipment according to the present invention, further includes: water tank is connected to the liquid trap；Described in inflow
The air-compressed gas of liquid trap goes out suitable for flowing through the water tank washing heel row.
Optionally, in extract equipment according to the present invention, the top of the tank body is equipped with exhaust outlet；The exhaust outlet with
It is connected with exhaust pipe between first condenser, is connected with water inlet pipe on the exhaust pipe；The exhaust pipe is close to the row
One end of port is equipped with filter net device.
Optionally, in extract equipment according to the present invention, the extractor further include: sieve plate is removably mounted to institute
It states in tank body, is suitable for placing plant perfume on the sieve plate；The tank base is suitable for importing steam, so as to fragrant to the plant
Material carries out distillation and forms distillation gas, and distillation gas is suitable for condensing to form distillate by first condenser.
Optionally, in extract equipment according to the present invention, further includes: oil water separator connects with first condenser
It is logical, and be suitable for carrying out water-oil separating to the distillate, to extract sesame oil.
Optionally, in extract equipment according to the present invention, the collet is equipped with inlet and outlet, the extraction
Equipment further include: water loop temperature controls machine, is connected to respectively with the inlet and outlet of the collet by hot-water line, so as to
Circulating hot water is passed through into the collet.
Optionally, in extract equipment according to the present invention, further includes: steam heater, by steam pipe respectively with institute
The first gas-guide tube and the connection of the second gas-guide tube are stated, to import steam into the tank body.
Optionally, in extract equipment according to the present invention, further includes: air reservoir, respectively with first gas-guide tube
It is connected to the second gas-guide tube, to be passed through air-compressed gas into the tank body；And air compressor machine, it is connect with the air reservoir,
The air compressor machine is suitable for compressed gas, is passed through in the air reservoir to form air-compressed gas.
Optionally, in extract equipment according to the present invention, further includes: fluid reservoir is suitable for storage extracting solution；Filter,
It is connect respectively with the tank body and fluid reservoir, enters the storage after flowing through the filter filtering from the tank body so as to extracting solution
Flow container.
Optionally, in extract equipment according to the present invention, further includes: inspissator is suitable for carrying out the extracting solution dense
Contracting, the inspissator are single-effect concentrator or Multi-effect concentration device.
Optionally, in extract equipment according to the present invention, the inspissator includes: heating room, is suitable for importing to be concentrated
Extracting solution and be suitable for being passed through steam and heating extracting solution；Vaporization chamber is connected to, to extract by circulation pipe with heating room
The vaporization chamber is flowed into after the heated room heating of liquid, and is separated into secondary steam and extracting solution, and mentioning after separation in vaporization chamber
Take liquid that can be back to heating room by the circulation pipe；Second condenser is connected to the vaporization chamber, to evaporate indoor two
Secondary steam is condensed into the second condenser；And receive flow container, be located at below second condenser and with second condenser
It is connected by conduit, receives flow container to import through the condensed liquid of the second condenser by the conduit.
Optionally, in extract equipment according to the present invention, the receipts flow container includes upper layer and lower layer, and upper layer and lower layer pass through
Catheter connection.
Optionally, in extract equipment according to the present invention, further includes: vacuum evacuation device connects with second condenser
It connects, to extract the gas flowed into the second condenser by the vaporization chamber.
Optionally, in extract equipment according to the present invention, the vacuum evacuation device includes: vacuum pump；Third condenser,
It is connect respectively by vacuum-pumping tube with second condenser and vacuum pump；And vacuum buffer tank, it is located at the third and condenses
It is connected to below device and with the third condenser；Wherein, the vacuum pump is suitable for the vaporization chamber, the second condenser and third
Condenser is evacuated；Enter the vacuum buffer tank through the condensed liquid of third condenser.
Optionally, in extract equipment according to the present invention, further includes: extractor is connected to the inspissator.
According to the technique and scheme of the present invention, a kind of extract equipment is provided, it is direct to first pass through the importing steam into extractor
Feed liquid is directly heated, and is heated to Extracting temperature, so be passed through into the collet of extractor circulating hot water feed liquid is carried out it is auxiliary
Heating is helped, feed liquid is made to be stably maintained at Extracting temperature.Moreover, during the extraction process, also being imported to the top of tank body or bottom empty
Body of calming the anger stirs feed liquid, to keep feed liquid stirring more abundant, obtains higher extraction efficiency.Connected by setting and tank body
The first logical condenser can carry out condensing recovery to the solvent vapo(u)r for the air-compressed gas entrainment discharged in extraction process, and can be
Carry out condensing recovery to the solvent of material residue absorption after the completion of extraction avoids solvent direct so as to reduce the loss of solvent
It discharges and pollutes environment.In addition, extract equipment of the invention, places plant perfume by the way that dismountable sieve plate is arranged, and pass through
Vapor is imported to tank base, obtains sesame oil so as to carry out distillation extraction to plant perfume.Extract equipment of the invention
Further include inspissator, to can be directly concentrated and separated to extracting solution after obtaining extracting solution, settles at one go.
The above description is only an overview of the technical scheme of the present invention, in order to better understand the technical means of the present invention,
And it can be implemented in accordance with the contents of the specification, and in order to allow above and other objects of the present invention, feature and advantage can
It is clearer and more comprehensible, the followings are specific embodiments of the present invention.
Detailed description of the invention
To the accomplishment of the foregoing and related purposes, certain illustrative sides are described herein in conjunction with following description and drawings
Face, these aspects indicate the various modes that can practice principles disclosed herein, and all aspects and its equivalent aspect
It is intended to fall in the range of theme claimed.Read following detailed description in conjunction with the accompanying drawings, the disclosure it is above-mentioned
And other purposes, feature and advantage will be apparent.It is related to the disclosure, identical appended drawing reference generally refers to identical
Component or element.
Fig. 1 shows the structural schematic diagram of extract equipment 300 according to an embodiment of the invention；
Fig. 2 shows the Local maps of the extraction module 100 according to an embodiment of the present invention；
Fig. 3 shows the Local map of the extractor 110 according to an embodiment of the present invention；
Fig. 4 shows the Local map of the inspissator 200 according to an embodiment of the present invention.
Specific embodiment
Exemplary embodiments of the present disclosure are described in more detail below with reference to accompanying drawings.Although showing the disclosure in attached drawing
Exemplary embodiment, it being understood, however, that may be realized in various forms the disclosure without should be by embodiments set forth here
It is limited.On the contrary, these embodiments are provided to facilitate a more thoroughly understanding of the present invention, and can be by the scope of the present disclosure
It is fully disclosed to those skilled in the art.
As it was noted above, being used for the extract equipment of Chinese herbal medicine in the prior art, more or less there are one in use
Fixed functional defect, therefore the invention proposes a kind of more optimized extract equipments 300 of performance.Fig. 1 shows of the invention mention
Take the structural schematic diagram of equipment 300.
As shown in Figure 1, extract equipment 300 include suitable for extract material extraction module 100, extraction module 100 be suitable for pair
Material is extracted with the mixed feed liquid of solvent, to form extracting solution and store.It should be noted that the material in the present invention
Such as can be Chinese herbal medicine etc., but not limited to this.Extracting solvent used by material can be pure water or tap water, be also possible to
Methanol solution or ethanol solution, but not limited to this.
According to one embodiment, as shown in Figure 1, extraction module 100 includes extractor 110 and is connected to extractor 110
The first condenser 120.Extractor 110 includes tank body 111, is adapted to fit into material and the mixed feed liquid of solvent in tank body 110,
The wall portion of tank body 111 is equipped with collet 112.The top and bottom of tank body 111 are respectively equipped with the first gas-guide tube 113 and the second gas-guide tube
114, the first gas-guide tube 113, the second gas-guide tube 114 are connect with steam pipe and pneumatics tracheae respectively, and steam pipe and compressed air
Valve is respectively equipped on pipe, thus by the switch control steam of control valve, air-compressed gas to the first gas-guide tube 113, second
Gas-guide tube 114 imports, and steam and/or compressed air are imported into tank body 111 from the first gas-guide tube 113 and the second gas-guide tube 114
Body.In addition, first gas-guide tube 113 at the top of tank body 111 is additionally provided with air jet pipe 119, air jet pipe 119 from the first gas-guide tube 113 to
Under extend to the lower part of tank body 111, so that the steam or air-compressed gas that are imported by the first gas-guide tube 113, can pass through air jet pipe 119
It is flowed into tank body 111 from the lower part of tank body 111.
During the extraction process, it first passes through the first gas-guide tube 113 or the second gas-guide tube 114 imports steam and directly carries out to feed liquid
Heating, and feed liquid is heated to Extracting temperature, to extract to obtain extracting solution to feed liquid in Extracting temperature.It needs to illustrate
It is that extracting solution is to stir feed liquid by continuing through air-compressed gas under Extracting temperature, mixes material sufficiently, uniformly with solvent
Afterwards, the effective component in material is extracted to obtained extraction solution in solvent.Wherein, Extracting temperature, heating time etc. join
Number can be by those skilled in the art's self-setting, and the present invention is without limitation.
In turn, after feed liquid is heated to Extracting temperature by steam, stop importing steam, and to the folder of extractor 110
Circulation is passed through the hot water of predetermined temperature in set 112, and the feed liquid auxiliary heating to making in tank body 111 makes to maintain stable extraction
Temperature.In this way, after steam is directly heated to Extracting temperature to feed liquid, by circulating hot water to the collet 112 of extractor 110 into
Row auxiliary heating, is conducive to steadily control Extracting temperature, and save energy.It should be pointed out that during heating, also passing through
First gas-guide tube 113 imports air-compressed gas from the top of tank body 110, or by the second gas-guide tube 114 from the bottom of tank body 110
Air-compressed gas is imported, feed liquid is stirred by importing air-compressed gas, to keep the space temperature of feed liquid uniform, while making to mention
Take effective component in material well into extracting solution, obtaining higher extraction efficiency.
Specifically, extract equipment 300 includes steam heater 160, and steam heater 160 is by steam pipe respectively with first
Gas-guide tube 113, the connection of the second gas-guide tube 114 provide heat to import steam into tank body 111 for feed liquid.Steam heater
160 can be electrothermal furnace.
As shown in Figure 1, extract equipment 300 further include water loop temperature control machine 170, collet 112 be equipped with water inlet and
Water outlet.Water loop temperature control machine 170 is connected to the inlet and outlet of collet 112 respectively by hot-water line, thus shape
At the heating systems of sealing circulation, it is passed through circulating hot water into collet 112, auxiliary heating is carried out to the intracorporal feed liquid of tank, makes to expect
Liquid is in stable Extracting temperature.Water loop temperature control machine 170 can be micro-control numeralization heating equipment, can be on demand
Be arranged water temperature and water loop temperature control machine 170 be equipped with digitlization display inflow temperature, leaving water temperature, current water temperature degree with
And setting coolant-temperature gage, so as to auto-control heating temperature or stop heating.Optionally, water loop temperature controls machine 170
Heating temperature-control range is 25~98 DEG C.
Extract equipment 300 further includes air reservoir 140 and air compressor machine 145, and air compressor machine 145 is connect with air reservoir 145, empty
Press 145 is suitable for compressed gas, is passed into air reservoir with to form air-compressed gas and is stored.Air reservoir 140 passes through compressed air
Pipe is connected to the first gas-guide tube 113, the second gas-guide tube 114 respectively, so that the air-compressed gas exported by pneumatics tracheae can be by
One gas-guide tube 113 or the second gas-guide tube 114 are directed into tank body 111.Air-compressed gas may include air, nitrogen, inert gas etc..
Further, air reservoir 140 is also connected with air oil water separator 141.Due to 145 compressed air meeting of air compressor machine
Oily waste water is generated, by the way that air oil water separator 141 is arranged, the air-compressed gas entrainment of the output of air reservoir 140 can be filtered
Oily waste water, to purify air-compressed gas, raising is passed through to the degree of purity of the air-compressed gas in tank body 111.
In addition, as shown in Figures 2 and 3, the bottom of tank body 111 is equipped with slag-drip opening 101, it is equipped at slag-drip opening 101 and is suitable for envelope
The deslagging lid 102 of stifled slag-drip opening.According to a kind of embodiment, extractor 110 further includes pneumatic device 105, and is suitable for passing through
The pneumatic device 105 control deslagging lid 102 opens or closes, and the source of turning on the power of deslagging lid 102 is air-compressed gas.
According to one embodiment, as shown in Figure 1, the top of tank body 111 is equipped with exhaust outlet 115, the sky imported in tank body 111
Cognition of calming the anger is discharged by exhaust outlet 115.It is connected with exhaust pipe 117 between the exhaust outlet 115 and the first condenser 120, thus,
First condenser 120 is connected to tank body 111 by the exhaust pipe 117.Since air-compressed gas understands entrapment solvent steam in discharge,
By the way that the first condenser 120 being connected to tank body 111 is arranged, the solvent vapo(u)r of air-compressed gas and entrainment is made to pass through exhaust pipe
117 enter the first condenser 120, and by the first condenser 120 to recycling after solvent vapo(u)r condensation, so as to prevent extractor
Solvent loss in 110.
Further, as shown in Figure 1, the lower section of the first condenser 120 is equipped with liquid trap 125.The top of liquid trap 125
The bottom (liquid outlet) of (inlet) and condenser Guan Liantong, liquid trap 125 are connected to tank body 111.Air-compressed gas entrainment
After solvent vapo(u)r condenses in the first condenser 120, recycling in liquid trap 125 can be flowed into, and can be from the liquid outlet of liquid trap 125
It is back in tank body 111 and extracts material.In this way, can be utilized again with the solvent that air-compressed gas discharges, on the one hand reduce molten
The loss of agent, on the other hand prevents solvent discharge from polluting environment into atmosphere.
As shown in Figure 1, extraction module 100 further includes water tank 130, water tank 130 is connected to liquid trap 125.It is cold without first
The air-compressed gas and the uncooled solvent vapo(u)r of small part that condenser 120 condenses will continue to flow through after entering liquid trap 125
Water tank 130 is discharged after washing, and solvent vapo(u)r is further prevented to be directly discharged to pollute environment in atmosphere.
In addition, the water inlet pipe is equipped with hand-operated valve, as shown in Figure 1, being also connected with water inlet pipe on exhaust pipe 117 to lead to
After crossing hand-operated valve control water inlet pipe unlatching, it can be passed through water flow into exhaust pipe 117, so that the material cleaned in exhaust pipe 117 is residual
Slag.In addition, one end on exhaust pipe 117 close to exhaust outlet 115 is additionally provided with filter net device 116, filter net device 116 can intercept pneumatics
The material particles that gas is carried secretly when discharging prevent material particles from entering in the first condenser 120 with air-compressed gas.
It should be noted that can also continue to import air-compressed gas into tank body 111 and water steam after the completion of being extracted to feed liquid
Gas, air-compressed gas and vapor can form resultant force, and the solvent for carrying away the absorption of material residue is discharged from exhaust outlet 115, goes forward side by side
Enter the condensation of the first condenser 120, condensed solvent enters liquid trap 125, after uncooled gas then flows through the washing of water tank 130
Discharge.The solvent of material residue absorption is recycled in this way, being able to achieve, the loss of solvent is reduced, it is direct to also avoid solvent
It discharges and pollutes environment.
According to one embodiment, extract equipment 300 of the invention can also extract sesame oil by the way of distillation from plant perfume.
Plant perfume for example can be plant petals, plant leaf, root skin etc., but not limited to this.Specifically, extractor 110 further includes
Sieve plate 118, sieve plate 118 are removably installed in tank body 111.When needing to extract sesame oil from plant perfume by the way of distillation
When, by the way that sieve plate 118 to be mounted in tank body 111, the plant perfume to be extracted is placed on sieve plate 118.Pass through the second air guide
Pipe 114 imports steam from the bottom of tank body 111, thus, the effective component in plant perfume forms distillation gas with steam distillation, real
Distillation extraction now is carried out to the effective component in plant perfume.
Further, as shown in Figure 1 to Figure 3, extraction module 100 further includes oil water separator 160, oil water separator 160
It is connected to the first condenser 120.The distillation gas that effective component in plant perfume is formed with steam distillation is flowed by exhaust pipe 117
First condenser 120, and distillate is formed by the condensation of the first condenser 120, in turn, distillate flows into oil water separator 160,
And water-oil separating is carried out in oil water separator 160, to extract sesame oil.In addition, being additionally provided with oil outlet on oil water separator 160
161, so that the sesame oil of extraction be exported from oil outlet 161.
It should be noted that the first gas-guide tube can also be passed through when extracting sesame oil from plant perfume by the way of distillation
113 or second gas-guide tube 114 import air-compressed gas into tank body 111, thus air-compressed gas and vapor can be formed resultant force, help
In more rapidly, fully carrying out distillation extraction to the effective component in plant perfume.
In addition, fluid reservoir 150 is suitable for storage as shown in Figure 1, extraction module 100 further includes fluid reservoir 150 and filter 155
Deposit the extracting solution after the completion of extracting.Specifically, the bottom of tank body 111, which is connected with, extracts liquid pipe 151, and by extracting liquid pipe 151
It is connected to the inlet of filter 155, the liquid outlet of filter 155 is connected to fluid reservoir 150.In this way, filter 155 respectively with
Tank body 111 and fluid reservoir 150 connect, and after the completion of the feed liquid in tank body 111 is extracted, extract liquid pipe 151 by opening, will extract
Liquid exports out of tank body 111 and enters filter 155 and filters, and in turn, filtered extracting solution imports fluid reservoir 150 again.
According to one embodiment, extract equipment 300 further includes inspissator 200, and inspissator 200 is suitable for carrying out extracting solution dense
Contracting.Optionally, inspissator 200 is single-effect concentrator or Multi-effect concentration device.
According to a kind of embodiment, as shown in Figure 1, inspissator 200 is single-effect concentrator, which includes heating
Room 210, vaporization chamber 220, the second condenser 230 and receipts flow container 240.
Wherein, heating room 210 can be connected to fluid reservoir 150, so that the extracting solution in fluid reservoir 150 can import heating room
It in 210, and heats room 210 and is connect by steam pipe with steam heater 160, so that steam can be passed through to extraction by heating room 210
Liquid is heated.It should be noted that being also possible to disconnected separate state, liquid storage between heating room 210 and fluid reservoir 150
Extracting solution in tank 150 can be pumped into heating room 210 by medical fluid, and is heated in heating room 210 by steam.
In addition, the top of heating room 210 passes through circulation pipe with lower part respectively and is connected to vaporization chamber 220, the top of vaporization chamber 220
Portion is connected to the second condenser 230, is received flow container 240 and is located at 230 lower section of the second condenser and passes through conduit with the second condenser 230
Connection.In this way, the heated room 210 of extracting solution is heated, and flows into vaporization chamber 220 from the circulation pipe on top by external force is vacuumized,
And secondary steam and extracting solution are separated into vaporization chamber 220.Extracting solution after the separation of vaporization chamber 220 can pass through the circulation of lower part
Pipe flows back into heating room 210, flows into vaporization chamber 220 after heated room 210 is heated again, forms the circulating-heating to extracting solution
And evaporation, realize the concentration of extracting solution.And the secondary steam after the separation of vaporization chamber 220 can enter the second condenser 230 and condense
For liquid, and is imported and received in flow container 240 by conduit.
According to a kind of embodiment, as shown in figure 4, receiving flow container 240 as double-layer structure, including upper layer and lower layer, and upper and lower two
Layer is connected to by catheter 245, and the liquid for receiving 240 upper layer of flow container can be directed into lower layer by catheter 245, on catheter 245
Equipped with valve.In this way, 245 valve of catheter can be closed when lower liquid is collected into a certain amount of, the liquid of lower layer is discharged,
And then valve is opened again, make the upper layer and lower layer connection for receiving flow container 240, supernatant liquid can be directed into lower layer by catheter 245 again.
As it can be seen that the present invention can constantly evaporate the solvent in extracting solution by inspissator 200 and in condensing recovery to receipts flow container 240, into
And realize the concentration lasting to extracting solution.
As shown in Figure 1, the wall portion of vaporization chamber 220 also is provided with vaporization chamber collet 222, the vaporization chamber collet 222 and water are recycled
Temperature controller 170 is connected to also by hot-water line, to be vaporization chamber by being passed through circulating hot water into vaporization chamber collet 222
Extracting solution in 220 after separation provides heat, guarantees the extracting solution temperature with higher for being recycled into heating room 210, improves
Thickening efficiency.
In addition, as shown in Figure 1, extract equipment 300 further includes vacuum evacuation device 250, vacuum evacuation device 250 and the second condensation
Device 230 connects, and can extract the gas evaporated in vaporization chamber 220.In other words, it is cold that the gas evaporated in vaporization chamber 220 flows into second
In condenser 230, and it is evacuated device 250 and takes away.Specifically, vacuum evacuation device 250 is slow including third condenser 251, vacuum
Tank 252 and vacuum pump 253 are rushed, vacuum pump 253 can be water ring vacuum pump, but not limited to this.Third condenser 251 passes through respectively
Vacuum-pumping tube is connect with the second condenser 230 and vacuum pump 253.Vacuum buffer tank 252 be located at the lower section of third condenser 251 and with
Third condenser 251 is connected to.In this way, the gas that evaporated in vaporization chamber 220 (can be passed through the second condenser by vacuum pump 253
230) it extracts and is further condensed into third condenser 251, and gas uncooled in third condenser 251 is taken away；Through
The condensed liquid of three condenser 251 then enters in vacuum buffer tank 252.
It should be appreciated that vaporization chamber 220, the second condenser 230 and third condenser 251 can be pumped into very by vacuum pump 253
Dummy status.The gas evaporated in vaporization chamber 220 is extracted by vacuum evacuation device 250, can be made in inspissator 200 in negative pressure ring
Border makes extracting solution reach concentration more quickly under subnormal ambient and requires.In addition, passing through setting third condenser 251 and vacuum
Surge tank 252 further condenses uncooled gas in the second condenser 230, to make to reach stable in inspissator 200
Vacuum degree, and the pressure difference inside and outside concentration tank can be buffered, it prevents from flowing backward.
According to one embodiment, extractor (not shown) can also be arranged in extract equipment 300, by by extractor with
Inspissator 200 is connected to, specifically can with the outlet of heating room 210, thus, extracting solution in inspissator 200, which is concentrated, to be completed
Afterwards, by pressurizeing to inspissator 200 or to extractor decompression, making to generate pressure difference between inspissator 200 and extractor, from
And convenient for importing the concentrating streams in inspissator 200 in extractor, and concentrate is extracted in extractor.
In the description of this specification unless specifically defined or limited otherwise, term " connection ", " fixation " etc. should all be done extensively
Reason and good sense solution.In addition, the orientation or positional relationship of the instructions such as term " on ", "lower", "inner", "outside", "top", "bottom" is based on attached drawing
Shown in orientation or positional relationship, be merely for convenience of description of the present invention and simplification of the description, rather than indication or suggestion is signified
Equipment or unit must have specific direction, be constructed and operated in a specific orientation, it is thus impossible to be interpreted as to of the invention
Limitation.
In the description of this specification, the description of term " one embodiment ", " some embodiments ", " specific embodiment " etc.
Mean that particular features, structures, materials, or characteristics described in conjunction with this embodiment or example are contained at least one reality of the invention
It applies in example or example.In the present specification, schematic expression of the above terms are not necessarily referring to identical embodiment or show
Example.Moreover, description particular features, structures, materials, or characteristics can in any one or more of the embodiments or examples with
Suitable mode combines.
In the instructions provided here, numerous specific details are set forth.It is to be appreciated, however, that implementation of the invention
Example can be practiced without these specific details.In some instances, well known method, knot is not been shown in detail
Structure and technology, so as not to obscure the understanding of this specification.
Claims (17)
1. a kind of extract equipment, comprising:
The wall portion of extractor, including tank body, the tank body is equipped with collet；
The tank body is adapted to fit into material and the mixed feed liquid of solvent, and is suitable for importing steam and heats to feed liquid, so that feed liquid
It is heated to Extracting temperature；The tank body is further adapted for importing air-compressed gas and stirs to feed liquid；
The collet is suitable for being passed through circulating hot water after feed liquid is heated to Extracting temperature, so that feed liquid maintains Extracting temperature；With
And
First condenser is connected to the tank body, and the solvent vapo(u)r carried secretly when suitable for discharging to air-compressed gas condenses, so as to
Recycling design.
2. extract equipment as described in claim 1, in which:
The first gas-guide tube and the second gas-guide tube are respectively equipped at the top and bottom of the tank body, to import steam into tank body
And/or air-compressed gas.
3. extract equipment as described in claim 1, wherein further include:
Liquid trap is connected to first condenser and tank body respectively；
Solvent vapo(u)r flows into the liquid trap after condensing in the first condenser, and is back in the tank body by liquid trap.
4. extract equipment as claimed in claim 3, wherein further include:
Water tank is connected to the liquid trap；
The air-compressed gas for flowing into the liquid trap goes out suitable for flowing through the water tank washing heel row.
5. extract equipment as described in claim 1, in which:
The top of the tank body is equipped with exhaust outlet；
It is connected with exhaust pipe between the exhaust outlet and first condenser, is connected with water inlet pipe on the exhaust pipe；
The exhaust pipe is equipped with filter net device close to one end of the exhaust outlet.
6. extract equipment as described in claim 1, wherein the extractor further include:
Sieve plate is removably mounted in the tank body, is suitable for placing plant perfume on the sieve plate；
The tank base is suitable for importing steam, forms distillation gas to carry out distillation to the plant perfume, distillation gas is suitable for
It condenses to form distillate by first condenser.
7. extract equipment as claimed in claim 6, wherein further include:
Oil water separator is connected to first condenser, and is suitable for carrying out water-oil separating to the distillate, to extract perfume (or spice)
Oil.
8. extract equipment as described in claim 1, wherein the collet is equipped with inlet and outlet, and the extraction is set
It is standby further include:
Water loop temperature controls machine, is connected to respectively with the inlet and outlet of the collet by hot-water line, so as to described
Circulating hot water is passed through in collet.
9. extract equipment as claimed in claim 2, wherein further include:
Steam heater is connected to first gas-guide tube and the second gas-guide tube respectively by steam pipe, so as to the tank body
Interior importing steam.
10. extract equipment as claimed in claim 2, wherein further include:
Air reservoir is connected to first gas-guide tube and the second gas-guide tube respectively, to be passed through compressed air into the tank body
Body；And
Air compressor machine is connect with the air reservoir, and the air compressor machine is suitable for compressed gas, so as to formed air-compressed gas be passed through it is described
In air reservoir.
11. extract equipment as described in claim 1, wherein further include:
Fluid reservoir is suitable for storage extracting solution；
Filter is connect with the tank body and fluid reservoir respectively, so that extracting solution flows through the filter filtering from the tank body
Enter the fluid reservoir afterwards.
12. extract equipment as described in claim 1, wherein further include:
Inspissator, suitable for the extracting solution is concentrated, the inspissator is single-effect concentrator or Multi-effect concentration device.
13. extract equipment as claimed in claim 12, wherein the inspissator includes:
Room is heated, extracting solution is heated suitable for importing extracting solution to be concentrated and being suitable for being passed through steam；
Vaporization chamber is connected to heating room by circulation pipe, flows into the vaporization chamber after heating so as to the heated room of extracting solution, and
Vaporization chamber is separated into secondary steam and extracting solution, and the extracting solution after separation can be back to heating room by the circulation pipe；
Second condenser is connected to the vaporization chamber, is condensed to evaporate indoor secondary steam into the second condenser；And
Flow container is received, be located at below second condenser and is connect with second condenser by conduit, so as to cold through second
The condensed liquid of condenser is imported by the conduit and receives flow container.
14. extract equipment as claimed in claim 13, in which:
The receipts flow container includes upper layer and lower layer, and upper layer and lower layer are connected to by catheter.
15. extract equipment as claimed in claim 13, wherein further include:
Vacuum evacuation device is connect with second condenser, to extract the gas flowed into the second condenser by the vaporization chamber
Body.
16. extract equipment as claimed in claim 15, wherein the vacuum evacuation device includes:
Vacuum pump；
Third condenser is connect by vacuum-pumping tube with second condenser and vacuum pump respectively；And
Vacuum buffer tank is located at below the third condenser and is connected to the third condenser；
Wherein, the vacuum pump is suitable for for the vaporization chamber, the second condenser and third condenser being evacuated；It is condensed through third
The condensed liquid of device enters the vacuum buffer tank.
17. extract equipment as claimed in claim 12, wherein further include:
Extractor is connected to the inspissator.
Priority Applications (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201910346059.9A CN110124349A (en) | 2019-04-26 | 2019-04-26 | A kind of multifunction extracting device |
| PCT/CN2019/087195 WO2020215407A1 (en) | 2019-04-26 | 2019-05-16 | Multifunctional extraction device |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201910346059.9A CN110124349A (en) | 2019-04-26 | 2019-04-26 | A kind of multifunction extracting device |
Publications (1)
| Publication Number | Publication Date |
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| CN110124349A true CN110124349A (en) | 2019-08-16 |
Family
ID=67575189
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201910346059.9A Pending CN110124349A (en) | 2019-04-26 | 2019-04-26 | A kind of multifunction extracting device |
Country Status (2)
| Country | Link |
|---|---|
| CN (1) | CN110124349A (en) |
| WO (1) | WO2020215407A1 (en) |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112266826A (en) * | 2020-10-23 | 2021-01-26 | 海南红塔卷烟有限责任公司 | Production equipment and method for extracting and concentrating agilawood spice for cigarettes by heating and pressurizing |
| CN113057246A (en) * | 2021-03-26 | 2021-07-02 | 广安万豪生物技术有限公司 | Method for extracting selenoprotein from selenium-enriched edible fungi |
| CN114854494A (en) * | 2022-05-31 | 2022-08-05 | 郑州科达机械仪器设备有限公司 | Essential oil extractor |
Families Citing this family (1)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN112494984B (en) * | 2020-12-09 | 2022-04-08 | 安庆医药高等专科学校 | Continuous dynamic extraction and separation production process for traditional Chinese medicine |
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| WO2020215407A1 (en) | 2020-10-29 |
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Application publication date: 20190816 |