CN110123720A - A kind of konjaku glucomannan care face cream and preparation method thereof - Google Patents

A kind of konjaku glucomannan care face cream and preparation method thereof Download PDF

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Publication number
CN110123720A
CN110123720A CN201910518572.1A CN201910518572A CN110123720A CN 110123720 A CN110123720 A CN 110123720A CN 201910518572 A CN201910518572 A CN 201910518572A CN 110123720 A CN110123720 A CN 110123720A
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konjaku glucomannan
care
content
face cream
glucomannan
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Inventor
庞杰
郑萍云
徐晓薇
陈晓涵
王唯佳
陈思杨
童彩玲
郭洋洋
林理专
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Fujian Agriculture and Forestry University
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Fujian Agriculture and Forestry University
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    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
    • A61K8/04—Dispersions; Emulsions
    • A61K8/042—Gels
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/34—Alcohols
    • A61K8/345—Alcohols containing more than one hydroxy group
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
    • A61K8/44—Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/64—Proteins; Peptides; Derivatives or degradation products thereof
    • A61K8/65—Collagen; Gelatin; Keratin; Derivatives or degradation products thereof
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/73—Polysaccharides
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/73—Polysaccharides
    • A61K8/731—Cellulose; Quaternized cellulose derivatives
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/73—Polysaccharides
    • A61K8/735—Mucopolysaccharides, e.g. hyaluronic acid; Derivatives thereof
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/73—Polysaccharides
    • A61K8/736—Chitin; Chitosan; Derivatives thereof
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9783—Angiosperms [Magnoliophyta]
    • A61K8/9794—Liliopsida [monocotyledons]
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00—Preparations for care of the skin
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00—Preparations for care of the skin
    • A61Q19/08—Anti-ageing preparations

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  • Gerontology & Geriatric Medicine (AREA)
  • Cosmetics (AREA)

Abstract

The present invention relates to a kind of konjaku glucomannan care face creams and preparation method thereof.During the preparation process, sodium carboxymethylcellulose is added to be conducive to thicken, water lock；Stearic acid can enhance water lock；The addition of hyaluronic acid be conducive to improve skin-nourishing metabolism, make skin it is tender, it is smooth, go wrinkle, increase elasticity, prevent aging；The more good moistening effect of the addition of aloe and glycerol.Meanwhile acetylated modification makes gel have preferable transparency and toughness, is easy to invest skin and is conducive to absorb, and the performances such as its moisturizing are significantly improved and improve.A kind of konjaku glucomannan of the invention takees good care of face cream, using konjaku glucomannan as carrier, and it is aided with other auxiliary agents, with excellent biological moisture-keeping, gelation, antibiotic property, manufactured konjaku glucomannan takees good care of face cream, have many advantages, such as that good moisture retention, pure natural skin care, non-stimulated, fully biodegradable, environmentally friendly low-carbon, materials are convenient, cheap, and simple production process.

Description

A kind of konjaku glucomannan care face cream and preparation method thereof
Technical field
The present invention relates to a kind of face creams and preparation method thereof, and in particular to a kind of konjaku glucomannan care face cream and its system Preparation Method belongs to daily necessities technical field.
Background technique
Face cream in the market is many kinds of, and the face cream for being added to various chemical components is even more that can be found everywhere, and stability is poor, very The multipair irritant effect of skin, practical moistening effect is poor, therefore, that is, has used face cream, the skin quality that can also generate face is dry, Coarse dark yellow phenomenon.
Patent of invention " a kind of face cream and preparation method thereof of naturally moistening " (Shen that number of patent application is 201810553593.2 Please day: 2018.05.30), using plant extract components such as a variety of Chinese herbal medicines, production has transdermal facilitation, can keep Face moistens, and reduces the natural moist face cream of fat secretion, and property is mild, and securely and reliably, but its material composition is more, has and is partially Compounding agent, additive, to skin, there are certain stimulations.
Patent of invention " a kind of moisturizing condensation face cream and preparation method thereof " (Shen that number of patent application is 201810416911.0 Please day: 2018.05.03) use the objects such as a certain proportion of water, aloe extract, SIMMONDSIA CHINENSIS SEED OIL, dimethyl silicone polymer, essence Matter is made, and can carry out moistening moisturizing to skin, and prevention has dry skin, improvement skin quality, but its raw material SIMMONDSIA CHINENSIS SEED OIL cost It is higher, it is unable to satisfy the demand of economical and practical modern society.
With economic development, continuous improvement of people's living standards more payes attention to the maintenance to facial skin quality, recent years Makeup, beauty and skin care, it is even more like a raging fire.But it makes up compared with the later period to people's state of mind and aesthetic feeling, carries out skin care maintenance and be only At all.And commercially available face cream contains that chemical component, skin effect are poor, and therefore, it is necessary to a pure natural care face creams more.
Summary of the invention
To solve the above-mentioned problems, the object of the present invention is to provide a kind of konjaku glucomannan care face cream and its preparation sides Method.The present invention using its biologic antibiosis, gelation, moisture retention and is aided with other lifes using konjaku glucomannan as main material Object moisturizer is made that moisture retention is good, and natural skin care, non-stimulated konjaku glucomannan take good care of face cream.
The purpose of the present invention is achieved through the following technical solutions.
A kind of preparation method of konjaku glucomannan care face cream of the present invention, it is characterised in that preparation step is as follows:
(1) it prepares aloe liquid: aloe being cleaned, being cut into small pieces is ground into paste, the deionized water with quality such as aloes is added, with The revolving speed of 300rpm/min stirs 9-11min, obtains aloe liquid, spare；
(2) it prepares konjaku glucomannan mixed liquor: preparing content of konjak glucomannan and be 1~2% aqueous solution, and it is poly- that shell is added Sugar, amino acid, glycerol and gelatin, chitosan content is 2~3%, amino acid content is 5~6%, glycerol content is 7.5 ~ 9%, Gelatine content is 4% ~ 5%, with the Ca (OH) of mass concentration 0.2%2PH to 8 ~ 10 is adjusted, thick colloid is made；What is obtained In colloid add 0.2% ~ 0.3% sodium carboxymethylcellulose, 0.05% ~ 0.06% stearic acid, 0.1% ~ 0.15% hyaluronic acid Aloe liquid with 2 ~ 3%, stirs 1.5-2h in the magnetic stirring apparatus of 1000r/min, obtains konjaku glucomannan mixed liquor, spare； Percentage shared by the chitosan, glycerol, amino acid and gelatin be each raw material and konjaku glucomannan mass percent (under Together), percentage shared by konjaku glucomannan, Ca (OH) 2, hyaluronic acid and aloe liquid is each raw material and konjak portuguese gansu polyose syrup The mass percent (similarly hereinafter) of solution；
(3) it deaerates: the konjaku glucomannan mixed liquor of step (2) is placed in a centrifuge, 3000r/min centrifugation, deaerate 15- 25min obtains konjaku glucomannan mixed gel, spare；
(4) it dispenses: the konjaku glucomannan mixed gel in step (3) being weighed into packing, as konjaku glucomannan takees good care of face White product.
Wherein, aloe liquid, mixing time 10min are prepared described in step (1).
Step (2) the konjaku glucomannan mixed liquor for preparing: preparing the aqueous solution that content of konjak glucomannan is 1%, Addition chitosan, amino acid, glycerol and gelatin, chitosan content 2%, amino acid content 5%, glycerol content 7.5%, Gelatine content is 4%, with 0.2% Ca (OH)2Adjust pH to 10；Due to the deacetylation of konjaku glucomannan, it has been made viscous Thick shape colloid.0.2% sodium carboxymethylcellulose, 0.05% stearic acid, 0.1% hyaluronic acid are added in obtained colloid Aloe liquid with 2%, stirs 1.5h in the magnetic stirring apparatus of 1000r/min.
Step (3) described degassing, centrifugation degassing time are 15min.
Advantages of the present invention: a kind of konjaku glucomannan of the invention takees good care of face cream, using konjaku glucomannan as carrier, and It is aided with other auxiliary agents, there is excellent biological moisture-keeping, gelation, antibiotic property, manufactured konjaku glucomannan takees good care of face cream Moisture retention is good, pure natural skin care, non-stimulated.Use konjaku glucomannan as the main material of face cream, good, the natural nothing with moisture retention Stimulation, fully biodegradable, environmentally friendly low-carbon, materials are convenient, cheap, and the advantages that simple production process.
During preparing konjaku glucomannan care face cream, sodium carboxymethylcellulose is added and is conducive to thicken, water lock； Stearic acid can enhance water lock；The addition of hyaluronic acid be conducive to improve skin-nourishing metabolism, make skin it is tender, it is smooth, go wrinkle, Increase elasticity, prevent aging, is good skin penetration enhancer again while moisturizing；Amino acid is day in keratoderma So ingredient of the wetting factor, can make the skin of aging and hardening restore hydrability；The more good guarantor of the addition of aloe and glycerol Wet effect.Meanwhile acetylated modification makes gel have preferable transparency and toughness, is easy to invest skin and is conducive to absorb, and The performances such as its moisturizing are significantly improved and improve.Therefore, konjaku glucomannan care face cream, which has, preferably improves skin Skin state, anti-aging, performance of keeping humidity, performance test are as follows:
(1) moisture retention
Care face cream and tradition are smeared in skin, makees 30min humidity-preserving type and compares
(2) skin improving gloss degree
Care face cream and tradition are smeared in skin, makees 30min skin improving gloss and compares
(3) skin skin quality improves degree
Care face cream and tradition are smeared in skin, makees the improvement of 30min skin skin quality and compares.
Konjaku glucomannan care face cream of the invention and commercially available common face cream properties comparison result are as shown in table 1.
Table 1 konjaku glucomannan care face cream and commercially available common face cream properties comparison result of the invention
Type performance Konjaku glucomannan takees good care of face cream Commercially available common face cream
Moisture retention Very well It is poor
Skin improving gloss degree Preferably It is general or poor
Skin skin quality improves degree Preferably It is poor
Excellent with care face cream properties of the invention by the above contrast test, index is more than commercially available common face cream, It is consumer's better choice.
Specific embodiment
Invention is further described in detail combined with specific embodiments below.
A kind of preparation method of the konjaku glucomannan of embodiment 1 care face cream, comprising the following steps:
(1) it prepares aloe liquid: aloe being cleaned, being cut into small pieces is ground into paste, the deionized water with quality such as aloes is added, with The revolving speed stirring 10min of 300rpm/min is spare to get aloe liquid；
(2) it prepares konjaku glucomannan mixed liquor: preparing the aqueous solution that content of konjak glucomannan is 1%, chitosan, ammonia is added Base acid, glycerol and gelatin, chitosan content 2%, amino acid content 5%, glycerol content 7.5%, gelatine content 4%, With the Ca (OH) of mass concentration 0.2%2Adjust pH to 10；Due to the deacetylation of konjaku glucomannan, thick glue has been made Body.Added in obtained colloid 0.2% sodium carboxymethylcellulose, 0.05% stearic acid, 0.1% hyaluronic acid and 2% Aloe liquid stirs 1.5h in the magnetic stirring apparatus of 1000r/min, and konjaku glucomannan mixed liquor is made, spare；
(3) it deaerates: the konjaku glucomannan mixed liquor of step (2) is placed in a centrifuge, 3000r/min centrifugation, degassing 15min obtains konjaku glucomannan mixed gel, spare；
(4) it dispenses: the konjaku glucomannan mixed gel in step (3) is weighed into packing.
Care face cream manufactured in the present embodiment can be used as the use of the care moisturizing face cream in daily skin care.
A kind of preparation method of the konjaku glucomannan of embodiment 2 care face cream, comprising the following steps:
(1) it prepares aloe liquid: aloe being cleaned, being cut into small pieces is ground into paste, the deionized water with quality such as aloes is added, with The revolving speed of 300rpm/min stirs 11min, obtains aloe liquid, spare；
(2) it prepares konjaku glucomannan mixed liquor: preparing the aqueous solution that content of konjak glucomannan is 2%, chitosan, ammonia is added Base acid, glycerol and gelatin, chitosan content 3%, amino acid content 5%, glycerol content 9%, gelatine content 5% are used The Ca (OH) of mass concentration 0.2%2Adjust pH to 8；Due to the deacetylation of konjaku glucomannan, thick colloid has been made. 0.3% sodium carboxymethylcellulose, 0.06% stearic acid, 0.15% hyaluronic acid and 3% reed are added in obtained colloid Luxuriant growth liquid stirs 2h in the magnetic stirring apparatus of 1000r/min, and konjaku glucomannan mixed liquor is made, spare；
(3) it deaerates: by the konjaku glucomannan mixed liquor of step (2), being placed in a centrifuge 3000r/min centrifugation, degassing 25min obtains konjaku glucomannan mixed gel, spare；
(4) it dispenses: the konjaku glucomannan mixed gel in step (3) is weighed into packing.
Care face cream manufactured in the present embodiment can be used as the use of the care moisturizing face cream in daily skin care.
The foregoing is merely presently preferred embodiments of the present invention, all equivalent changes done according to scope of the present invention patent with Modification, is all covered by the present invention.

Claims (5)

1. a kind of preparation method of konjaku glucomannan care face cream, it is characterised in that preparation step is as follows:
(1) it prepares aloe liquid: aloe being cleaned, being cut into small pieces is ground into paste, the deionized water with quality such as aloes is added, with The revolving speed of 300rpm/min stirs 9-11min, obtains aloe liquid, spare；
(2) it prepares konjaku glucomannan mixed liquor: preparing content of konjak glucomannan and be 1~2% aqueous solution, and it is poly- that shell is added Sugar, amino acid, glycerol and gelatin, chitosan content is 2~3%, amino acid content is 5~6%, glycerol content is 7.5 ~ 9%, Gelatine content is 4% ~ 5%；With the Ca (OH) of mass concentration 0.2%2PH to 8 ~ 10 is adjusted, thick colloid is made；What is obtained In colloid add 0.2% ~ 0.3% sodium carboxymethylcellulose, 0.05% ~ 0.06% stearic acid, 0.1% ~ 0.15% hyaluronic acid Aloe liquid with 2 ~ 3%, stirs 1.5-2h in the magnetic stirring apparatus of 1000r/min, obtains konjaku glucomannan mixed liquor, spare； Percentage shared by the chitosan, glycerol, amino acid and gelatin is the mass percent of each raw material and konjaku glucomannan, evil spirit Percentage shared by taro Glucomannan, Ca (OH) 2, hyaluronic acid and aloe liquid is each raw material and konjak portuguese gansu polyose sugar aqueous solution Mass percent；
(3) it deaerates: the konjaku glucomannan mixed liquor of step (2) is placed in a centrifuge, 3000r/min centrifugation, deaerate 15- 25min obtains konjaku glucomannan mixed gel, spare；
(4) it dispenses: the konjaku glucomannan mixed gel in step (3) being weighed into packing, as konjaku glucomannan takees good care of face White product.
2. a kind of preparation method of konjaku glucomannan care face cream according to claim 1, it is characterised in that step (1) Described prepares aloe liquid, mixing time 10min.
3. a kind of preparation method of konjaku glucomannan care face cream according to claim 1, it is characterised in that step (2) The konjaku glucomannan mixed liquor for preparing: preparing the aqueous solution that content of konjak glucomannan is 1%, and chitosan, amino is added Acid, glycerol and gelatin, chitosan content 2%, amino acid content 5%, glycerol content 7.5%, gelatine content 4%；With The Ca (OH) of mass concentration 0.2%2PH to 10 is adjusted, thick colloid is made；The carboxymethyl of addition 0.2% in obtained colloid Sodium cellulosate, 0.05% stearic acid, 0.1% hyaluronic acid and 2% aloe liquid, stirred in the magnetic stirring apparatus of 1000r/min Mix 1.5h.
4. a kind of preparation method of konjaku glucomannan care face cream according to claim 1, it is characterised in that step (3) The degassing, centrifugation degassing time are 15min.
5. the konjaku glucomannan that either as described in claim 1-4 prepared by method takees good care of face cream.
CN201910518572.1A 2019-06-15 2019-06-15 A kind of konjaku glucomannan care face cream and preparation method thereof Pending CN110123720A (en)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN112618455A (en) * 2020-12-31 2021-04-09 重庆知翔科技有限公司 Moisture mask and preparation method thereof

Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103405350A (en) * 2013-07-16 2013-11-27 福建农林大学 Granular glucomannan moisturizing mask and preparation method thereof
CN103462850A (en) * 2013-09-26 2013-12-25 陈理敬 Moisturizing cream formula
CN105287292A (en) * 2015-11-18 2016-02-03 陈洁娣 Whitening moisture-retention face cream and preparation method thereof
CN105496906A (en) * 2016-01-29 2016-04-20 福建农林大学 Aloe and konjac glucomannan facial mask and preparation method thereof
KR20170133134A (en) * 2016-05-25 2017-12-05 엠제이바이오 주식회사 Hydrogel composition comprising hot water extract of soybean, preparation method thereof and cosmetic composition comprising the same
CN108403548A (en) * 2018-04-20 2018-08-17 安徽怡人生物科技有限公司 A kind of skin-whitening frost and preparation method thereof

Patent Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103405350A (en) * 2013-07-16 2013-11-27 福建农林大学 Granular glucomannan moisturizing mask and preparation method thereof
CN103462850A (en) * 2013-09-26 2013-12-25 陈理敬 Moisturizing cream formula
CN105287292A (en) * 2015-11-18 2016-02-03 陈洁娣 Whitening moisture-retention face cream and preparation method thereof
CN105496906A (en) * 2016-01-29 2016-04-20 福建农林大学 Aloe and konjac glucomannan facial mask and preparation method thereof
KR20170133134A (en) * 2016-05-25 2017-12-05 엠제이바이오 주식회사 Hydrogel composition comprising hot water extract of soybean, preparation method thereof and cosmetic composition comprising the same
CN108403548A (en) * 2018-04-20 2018-08-17 安徽怡人生物科技有限公司 A kind of skin-whitening frost and preparation method thereof

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN112618455A (en) * 2020-12-31 2021-04-09 重庆知翔科技有限公司 Moisture mask and preparation method thereof

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Application publication date: 20190816