CN110058350A - A kind of low-loss large effective area dispersion shifted single mode fiber and its manufacturing method - Google Patents

A kind of low-loss large effective area dispersion shifted single mode fiber and its manufacturing method Download PDF

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Publication number
CN110058350A
CN110058350A CN201910341229.4A CN201910341229A CN110058350A CN 110058350 A CN110058350 A CN 110058350A CN 201910341229 A CN201910341229 A CN 201910341229A CN 110058350 A CN110058350 A CN 110058350A
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optical fiber
dispersion
wavelength
effective area
less
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成煜
邓洪昌
徐荣辉
苑立波
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Guilin University of Electronic Technology
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Guilin University of Electronic Technology
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    • GPHYSICS
    • G02OPTICS
    • G02BOPTICAL ELEMENTS, SYSTEMS OR APPARATUS
    • G02B6/00Light guides; Structural details of arrangements comprising light guides and other optical elements, e.g. couplings
    • G02B6/02Optical fibres with cladding with or without a coating
    • G02B6/02004Optical fibres with cladding with or without a coating characterised by the core effective area or mode field radius
    • G02B6/02009Large effective area or mode field radius, e.g. to reduce nonlinear effects in single mode fibres
    • G02B6/02014Effective area greater than 60 square microns in the C band, i.e. 1530-1565 nm
    • GPHYSICS
    • G02OPTICS
    • G02BOPTICAL ELEMENTS, SYSTEMS OR APPARATUS
    • G02B6/00Light guides; Structural details of arrangements comprising light guides and other optical elements, e.g. couplings
    • G02B6/02Optical fibres with cladding with or without a coating
    • G02B6/02214Optical fibres with cladding with or without a coating tailored to obtain the desired dispersion, e.g. dispersion shifted, dispersion flattened
    • G02B6/02219Characterised by the wavelength dispersion properties in the silica low loss window around 1550 nm, i.e. S, C, L and U bands from 1460-1675 nm
    • G02B6/02276Dispersion shifted fibres, i.e. zero dispersion at 1550 nm
    • GPHYSICS
    • G02OPTICS
    • G02BOPTICAL ELEMENTS, SYSTEMS OR APPARATUS
    • G02B6/00Light guides; Structural details of arrangements comprising light guides and other optical elements, e.g. couplings
    • G02B6/02Optical fibres with cladding with or without a coating
    • G02B6/036Optical fibres with cladding with or without a coating core or cladding comprising multiple layers
    • G02B6/03616Optical fibres characterised both by the number of different refractive index layers around the central core segment, i.e. around the innermost high index core layer, and their relative refractive index difference
    • G02B6/03638Optical fibres characterised both by the number of different refractive index layers around the central core segment, i.e. around the innermost high index core layer, and their relative refractive index difference having 3 layers only
    • G02B6/03644Optical fibres characterised both by the number of different refractive index layers around the central core segment, i.e. around the innermost high index core layer, and their relative refractive index difference having 3 layers only arranged - + -

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  • Physics & Mathematics (AREA)
  • General Physics & Mathematics (AREA)
  • Optics & Photonics (AREA)
  • Chemical & Material Sciences (AREA)
  • Dispersion Chemistry (AREA)
  • Optical Communication System (AREA)

Abstract

The present invention is to provide a kind of low-loss large effective area dispersion shifted single mode fiber and its manufacturing methods.Its fibre core is adulterated using Ge and Cl, and the first and third covering is shallowly to mix F covering, and the second covering is Ge, F codope.The mode field diameter of optical fiber 1550nm is 9.6 ± 0.4 μm, and effective area is greater than 75 μm2, zero-dispersion wavelength be less than 1500nm, 1530nm~1625nm dispersion values in 2.0~8.0ps/nm/km range, chromatic dispersion gradient≤0.06ps/nm of 1550nm2The dispersion values of/km, 1550nm are 3.0ps/nm/km between 5.0ps/nm/km;Fiber cut off wavelength is less than 1500nm.In 1550nm bending loss, 1 circle is not more than 0.01dB under 16mm bending radius, and optical fiber is less than or equal to 0.185dB/km in the attenuation of 1550nm wavelength.

Description

A kind of low-loss large effective area dispersion shifted single mode fiber and its manufacturing method
(1) technical field
The present invention relates to a kind of low-loss large effective area dispersion shifted single mode fiber and its manufacturing method, main application In high-speed optical fibre for metropolitan area network communication transmission field.
(2) background technique
Always constantly improve, number of users continues is increasing the transmission capacity of fiber optic communication.Long-distance transmission line mainly solves Certainly be carrier network scale.But Metropolitan Area Network (MAN) is the high value traffic network of operator, includes high speed Internet access business, interaction Game service, government services business, network TV business, enterprise/community services business etc..
The Networks of Fiber Communications of establishing of MAN is one of operator's emphasis investment contents, requires price just to optical fiber Preferably, it is suitble to a variety of transmission plans.Therefore, a kind of low-loss dispersion shift large-effective area single mode fiber can satisfy this need It asks, main performance is to improve C+L band dispersion characteristics, it is made to be suitble to the transmission of SDH and DWDM in Metropolitan Area Network (MAN).Meanwhile it to drop Low network construction cost increases optical fiber in the effective area of 1550nm and reduces fibre loss, so that Metropolitan Area Network (MAN) is built less or do not built Relaying amplification, can be greatly lowered network cost, meet actual demand.
Document CN00815954.8 discloses a kind of dispersion shifted optical fiber that effective area is big, in 1470nm to 1625nm There are the dispersion values of 1.0ps/nm/km to 16.0ps/nm/km.It is greater than 70 μm in the effective area of 1550nm2, at 1550nm Attenuation is less than 0.20dB/km.The optical fiber is larger in the dispersion of C+L band, and chromatic dispersion gradient is big, needs special dispersion compensating fiber It is broadened to compensate long distance transmission bring pulse, but dispersion compensation brings the increase of system loss, and whole system is caused to be made The increase of valence.
A kind of dispersion shifted optical fiber of low-dispersion slope, 1530nm to 1625nm are disclosed in document CN02809096.9 There are the dispersion values of 2.5ps/nm/km to 8.6ps/nm/km.It is about 8.3 ± 0.6 μm in the mode field diameter of 1550nm, in 1550nm The attenuation at place is less than 0.22dB/km.In chromatic dispersion gradient≤0.05ps/nm of 1550nm2/km.This layout optimises dispersions, still It is smaller in the limited areal of 1550nm, less than 60 μm2, and Section Design is complicated, increases manufacturing cost.
A kind of super large effective area and low dispersion slope non-zero dispersion displacement optical fiber is disclosed in document CN03119080.4, it should Fiber design has the totally 6 layers of design of 5 core segments and 1 covering.Optical fiber 1550nm dispersion values 8ps/nm/km extremely Between 10ps/nm/km.It is greater than 95 μm in the effective area of 1550nm2, the attenuation at 1550nm is less than 0.22dB/km.? Chromatic dispersion gradient≤0.06ps/nm of 1550nm2/km.Dispersion values of the optical fiber in 1550nm are very big, reach 10ps/nm/km.
Dispersion shifted optical fiber always is disclosed in document CN03125581.7, zero dispersion point is very high, 1640nm with On.It has the dispersion values of -1.0ps/nm/km to -10.0ps/nm/km in 1530nm to 1625nm, in the effective area of 1550nm It is 40~70 μm2.This design causes effective area very small because zero-dispersion wavelength is very big.
A kind of dispersion shifted optical fiber is disclosed in document CN03823169.7, zero-dispersion wavelength is less than 1450nm, The effective area of 1550nm is greater than 60 μm2, in chromatic dispersion gradient≤0.07ps/nm of 1550nm2/km.Dispersion of the optical fiber in 1550nm Value is 4ps/nm/km between 10ps/nm/km.Its dispersion is larger, and when network construction needs dispersion compensation, and effective area is inclined It is small.
Disclose a kind of dispersion shifted optical fiber in document CN200410098270.7, the optical fiber in 1490nm to 1625nm Effective area be 45~120 μm2, chromatic dispersion gradient is 0.03~0.10ps/nm2/ km, but bending loss is 100dB/m, this The attenuation of sample optical fiber will be very big.
A kind of dispersion shifted optical fiber of low decaying is disclosed in document CN200680051445.6, zero-dispersion wavelength is less than 1450nm is greater than 50 μm in the effective area of 1550nm2, in chromatic dispersion gradient≤0.06ps/nm of 1550nm2/km.Optical fiber exists The dispersion values of 1550nm are 5ps/nm/km between 15ps/nm/km.The optical fiber is less than 0.19dB/km 1550nm's.Its color Dissipate larger, when network construction needs dispersion compensation.
Dispersion shifted optical fiber is disclosed in document CN200910203954.1, dispersion values of the optical fiber in 1550nm are less than 12ps/nm/km, effective area are greater than 50 μm2, and cutoff wavelength is less than 1600nm.This design causes fiber cut off wavelength high, Effective single mode transport is not can guarantee, and effective area is very small.
201110034823.2 disclose a kind of dispersion shifted optical fiber of short cutoff wavelength in document CN, which exists The dispersion values of 1550nm are 3ps/nm/km between 14ps/nm/km, and effective area is greater than 55 μm2, and cutoff wavelength is less than 1150nm.The bending loss of this design optical fiber is big, and effective area is less than normal.
Dispersion shifted optical fiber is disclosed in document CN201110035625.8, which is 3ps/ in the dispersion values of 1550nm For nm/km between 14ps/nm/km, effective area is greater than 95 μm2, in chromatic dispersion gradient≤0.11ps/nm of 1550nm2/ km, and cut Only wavelength is less than 1530nm.Its dispersion is larger, and when network construction needs dispersion compensation, and the document do not disclose manufacturing method or Other technical characteristics.
Dispersion shifted optical fiber is disclosed in document CN200820166463.5, dispersion of the optical fiber in 1530nm~1625nm Value is 2.5ps/nm/km between 12ps/nm/km, 70~75 μm of effective area2, 1550nm chromatic dispersion gradient≤ 0.073ps/nm2/ km, zero-dispersion wavelength is less than 1500nm, and cutoff wavelength is less than 1530nm.It is small in the optical fiber attenuation of 1550nm In 0.22dB/km.The dispersion of the optical fiber and chromatic dispersion gradient are larger, and without disclosing manufacture formula and method.
In conclusion the large effective area dispersion shifted single mode fiber for developing a kind of low dispersion values of low attenuation closes very much Key.In order to which the long-distance optical fiber communication of establishing of MAN must be single mode transport, dispersion and the chromatic dispersion gradient of C+L band are reduced, together The effective area of Shi Zeng great 1550nm reduces optical fiber in the attenuation of 1550nm, and improves the bend loss properties of optical fiber, can be effective Reduce network construction cost.Meanwhile selecting a kind of suitable technique manufacturing method to manufacture the optical fiber, the doping skill including fibre core Art is also a urgent problem to be solved.
(3) summary of the invention
The purpose of the present invention is to provide a kind of low-loss, low dispersion values, the dispersion shifted optical fiber of large effective area and its Preparation method.
It is involved term in the present invention below:
Relative fefractive index difference: outermost one layer of optical fiber is defined as surrounding layer, and absolute index of refraction is defined as nSiO2, past from a left side Right i-th of step (referring to attached drawing 1) is defined as i-th layer, if i is outermost one layer, absolute index of refraction is exactly nSiO2
I-th layer of relative fefractive index difference is defined as:
The effective area Aeff of optical fiber is defined by following formula:
Wherein E is and propagates the associated electric field of light in optical fiber, and r is the radius of optical fiber.
Cable cut-off wavelength: being that optical signal is transmitted in a fiber after 22 meters according to the cable cut-off wavelength that IEC is defined It is not re-used as the wavelength that single mode signal is propagated.It needs to obtain by testing after looping to optical fiber in test.
Solution before is built using G.655 optical fiber cooperation erbium-doped fiber amplifier (EDFA) and dispersion compensation module If Metropolitan Area Network (MAN).G.655 optical fiber is 12ps/nm/km in the dispersion representative value of 1550nm, and attenuation representative value is 0.22dB/km.This hair Bright another thinking solved the problems, such as that proposes: a kind of dispersion shifted optical fiber of low dispersion values is designed, builds it in Metropolitan Area Network (MAN) If dispersion compensation module is not necessarily in.Increase the effective area of optical fiber, improves injected optical power, while reducing the loss of optical fiber, it can To effectively improve span length, erbium-doped fiber amplifier is not necessarily in establishing of MAN.
The present invention is by solving the problems, such as the technical solution set forth above taken are as follows: the fuse radius r1 of optical fiber be 2.5~ 3.5 μm, sandwich layer relative fefractive index difference △ n1 is+0.45%~+0.55%, and sandwich layer is doped to Cl and Ge;First cladding radius r2 It is 4.0~5.0 μm, relative fefractive index difference △ n2 is -0.08%~-0.11%, and first is clad doped for F doping;Second covering Radius r3 is 7.5~9 μm, and relative fefractive index difference △ n3 is+0.12%~+0.17%, and second is clad doped for Ge, F codope; Third cladding radius r4 is 10~12 μm, and relative fefractive index difference △ n4 is -0.03%~-0.05%, and third is clad doped to mix for F It is miscellaneous;Outermost layer is pure silicon dioxide, and radius is 62.5 μm.The center relative refractive index difference of fiber design is larger, is because in this way Dispersion shift purpose may be implemented.Unlike bibliography, the core design that the present invention is adulterated using Cl and Ge, because of Cl The refractive index of sandwich layer can be effectively increased but the rayleigh scattering coefficient of optical fiber can be reduced, it in this way can be in high-speed wire-drawing Effectively reduce fibre loss.Fibre core does not mix alkali metal K in the present invention, is because fibre core is doped with more GeO2,GeO2In glass It is also network body in glass network, but its bond energy and SiO2Difference is big, therefore effectively reduces the viscosity of network body, inherently may be used To match the temperature field of wire drawing.Secondly, present invention employs two to mix the recessed covering of F, the purpose is to reduce the cut-off wave of optical fiber Long and reduction bending loss.
Doped with the GeO of 8.5-10.5mol% in fuse2Cl with 0.5wt%-0.8wt% is to reach the opposite folding of design It is poor to penetrate rate, and it is this doped be conducive to matching inside of optical fibre stress therefore use design of the invention can be with high-speed wire-drawing condition The lower attenuation by optical fiber 1550nm is reduced to 0.185dB/km or less.Its drawing speed can be from 600m/min to 1800m/ min。
Sandwich layer, the first covering, the second covering and third covering are prepared using PCVD technique, center core layer, the first covering, the Two coverings and third covering are in PCVD technique according to the SiCl of calculating4Flow, GeCl4Flow quantitatively evaporates and C2F6、O2Flow It is uniformly mixed in pipeline, is then delivered to plasma area and is chemically reacted, generate required waveguiding structure.
Sandwich layer is the viscosity in order to match inside of optical fibre with the main purpose designed of adulterating of the first, second and third covering, favorably In reduce optical fiber 1550nm attenuation.
Prefabricated rods after the completion of deposition are lifted to melt and carry out being collapsed into solid mandrel in contracting equipment, finally according to pure the two of calculating Silica carries out wire drawing after covering pipe sleeve outside the prefabricated rods.
The temperature of wire drawing be 1900 DEG C to 2000 DEG C, delivery speed be 4.5~10mm/min, drawing speed be 1200~ 1800m/min, optical fiber is by high-temperature region, and behind annealed zone and cooling zone, into a double application system, interlayer coatings and outer layer are applied Expect while multiple solidification equipments carry out interlayer coatings and outer layer coating solidifies simultaneously coated in then passing through outside bare optical fiber.Light Fibre is by high-temperature region, behind annealed zone and cooling zone, can also enter first of applicator and solidify, after coating diameter be 185~ It 200 μm, then enters back into second applicator and solidifies, diameter is 242~252 μm after coating.Optical fiber designed by the present invention Because bending loss is smaller, the added losses applied after stranding are also smaller, are suitble to multiple use such as Metropolitan Area Network (MAN) or residence network, Meanwhile optical fiber is smaller and flat in the dispersion of C+L band, can be applied to a variety of transmission modes without dispersion compensation.Meanwhile this The designed optical fiber of invention is greater than 75 μm in 1550nm effective area2, the nonlinear factor of optical fiber is increased, can be injected bigger The signal light of power, loss of the optical fiber in 1550nm are less than or equal to 0.185dB/km, increase the signal-to-noise ratio of network, can be substantially Degree improves transmission range, reduces the bit error rate of system design, can reduce the construction cost of the networks such as communication Metropolitan Area Network (MAN).Meanwhile Using each layer doping formula of optical fiber of the invention, low-loss large effective area dispersion position can be obtained under the conditions of high-speed wire-drawing Single mode optical fiber is moved, fiber manufacturing cost is reduced.The optical fiber property of test is as follows: the mode field diameter of 1550nm is 9.78 μm, is had 75 μm of area of effect2, zero-dispersion wavelength 1485nm is 2.3ps/nm/km to 7.9ps/nm/ in the dispersion values of 1530nm~1625nm Between km, the chromatic dispersion gradient of 1550nm is 0.06ps/nm2/ km, fiber cut off wavelength 1485nm.Exist in 1550nm bending loss 1 circle is 0.008dB under 16mm bending radius.
(4) Detailed description of the invention
Fig. 1 is low-loss large effective area dispersion shifted single mode fiber diagrammatic cross-section, and r1 represents fiber core radius, opposite Refringence is indicated with Δ n1 on the diagram;R2 represents first and shallowly mixes F cladding radius, and relative fefractive index difference uses Δ n2 on the diagram It indicates;R3 represents second layer cladding radius, and relative fefractive index difference is indicated with Δ n3 on the diagram;R4 represents second and shallowly mixes F packet Layer radius, relative fefractive index difference are indicated with Δ n4 on the diagram;R5 is exactly pure silicon dioxide cladding radius, and usually 62.5 μm.
Fig. 2 is the dispersion curve figure of low-loss large effective area dispersion shifted single mode fiber.Zero-dispersion wavelength is 1491.2nm, the dispersion values at 1550nm are 3.26ps/nm/km, and the chromatic dispersion gradient of this wavelength is 0.06ps/nm2/ km, Dispersion values at 1625nm are 7.96ps/nm/km.
(5) specific embodiment
The embodiment illustrated in further detail below.
Silicon tetrachloride, oxygen and carbon hexa fluoride are passed first into using PCVD method and are deposited on quartz reaction inside pipe wall formation third Covering then passes to silicon tetrachloride, germanium tetrachloride, oxygen and carbon hexa fluoride and deposits to form the second covering, then be passed through silicon tetrachloride, Oxygen and carbon hexa fluoride deposit to form the first covering, then are passed through silicon tetrachloride, germanium tetrachloride, oxygen and carbon hexa fluoride and deposit to be formed Sandwich layer is formed, the deposition flow proportional of sandwich layer is by special optimization to increase sandwich layer Cl content.After the completion of deposition, it will have The reaction tube collapsing in heart hole obtains solid preform.
Design fibre profile of the invention and parameter are as shown in table 1:
Test optical fiber data of the invention are as shown in table 2:
Infuse *: the unit of dispersion is ps/nm/km, and the unit of chromatic dispersion gradient is ps/nm2/km;
Test optical fiber data of the invention are as shown in table 3:
Design parameter in above embodiments is although preferably, above-described embodiment also retouch in detail to the present invention It states, but those skilled in the art is, it will be observed that without departing from the spirit and scope of the present invention can also be in form Or a variety of variations are made in details.

Claims (9)

1. a kind of low-loss large effective area dispersion shifted single mode fiber, the fiber core radius r1 of optical fiber is 2.5~3.5 μm, sandwich layer Relative fefractive index difference △ n1It is+0.45%~+0.55%, sandwich layer is doped to Cl and Ge;First cladding radius r2 is 4.0~5.0 μ M, relative fefractive index difference △ n2It is -0.08%~-0.11%, first is clad doped for F doping;Second cladding radius r3 is 7.5 ~9 μm, relative fefractive index difference △ n3 is+0.12%~+0.17%, and second is clad doped for Ge, F codope;Third covering half Diameter r4 is 10~12 μm, and relative fefractive index difference △ n4 is -0.03%~-0.05%, and third is clad doped to be adulterated for F;Outermost layer For pure silicon dioxide.
2. optical fiber according to claim 1 is manufactured using PCVD technique, it is Si respectively that fibre core, which includes four kinds of elements, O, Ge and Cl;Wherein the weight ratio of Cl accounts for 0.5% to 0.8%, GeO of glass of fiber core weight2Molar ratio account for the 8.5% of fibre core and arrive 10.5%.
3. optical fiber according to claim 1, it is characterised in that: the zero-dispersion wavelength of optical fiber is less than 1500nm.
4. optical fiber according to claim 1, it is characterised in that: optical fiber 1550nm dispersion values in 3~5ps/nm/km range It is interior;It is 2.0ps/nm/km between 8.0ps/nm/km in the dispersion values of 1530nm~1625nm, the chromatic dispersion gradient of 1550nm≤ 0.06ps/nm2/km。
5. optical fiber according to claim 1, it is characterised in that: optical fiber is 9.6 ± 0.4 μm in the mode field diameter of 1550nm, is had It imitates area and is greater than 75 μm2
6. optical fiber according to claim 1, it is characterised in that: optical fiber is less than or equal in the attenuation of 1550nm wavelength 0.185dB/km。
7. optical fiber according to claim 1, it is characterised in that: drawing speed of optical fiber is greater than 1200m/min, preferred wire drawing speed Degree is 1600m/min.
8. optical fiber according to claim 1, it is characterised in that: the cutoff wavelength of the optical fiber is less than or equal to 1500nm.
9. optical fiber according to claim 1, it is characterised in that: the bending loss of the optical fiber at 1550nm wavelength, with The circle of 16mm bending radius 1 is then less than or equal to 0.01dB.
CN201910341229.4A 2019-04-25 2019-04-25 A kind of low-loss large effective area dispersion shifted single mode fiber and its manufacturing method Pending CN110058350A (en)

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Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2000162462A (en) * 1998-11-23 2000-06-16 Alcatel Dispersion compensating fiber for wavelength-divided multiple optical fiber transmission system using dispersion shift type line fiber
JP2003075674A (en) * 2001-08-31 2003-03-12 Hitachi Cable Ltd Low-nonlinearity low-dispersion slope optical fiber
CN1434309A (en) * 2002-01-22 2003-08-06 株式会社藤仓 Optical fibre and transmission path
CN1667437A (en) * 2004-03-09 2005-09-14 株式会社藤仓 Dispersion compensating fiber module and optical fiber transmission line
CN107247305A (en) * 2017-07-04 2017-10-13 长飞光纤光缆股份有限公司 Low decay single-mode fiber and preparation method thereof

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2000162462A (en) * 1998-11-23 2000-06-16 Alcatel Dispersion compensating fiber for wavelength-divided multiple optical fiber transmission system using dispersion shift type line fiber
JP2003075674A (en) * 2001-08-31 2003-03-12 Hitachi Cable Ltd Low-nonlinearity low-dispersion slope optical fiber
CN1434309A (en) * 2002-01-22 2003-08-06 株式会社藤仓 Optical fibre and transmission path
CN1667437A (en) * 2004-03-09 2005-09-14 株式会社藤仓 Dispersion compensating fiber module and optical fiber transmission line
CN107247305A (en) * 2017-07-04 2017-10-13 长飞光纤光缆股份有限公司 Low decay single-mode fiber and preparation method thereof

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