CN110055376A - A kind of preparation method of high-strength pipe pile PC rod iron wire rod - Google Patents

A kind of preparation method of high-strength pipe pile PC rod iron wire rod Download PDF

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Publication number
CN110055376A
CN110055376A CN201910474369.9A CN201910474369A CN110055376A CN 110055376 A CN110055376 A CN 110055376A CN 201910474369 A CN201910474369 A CN 201910474369A CN 110055376 A CN110055376 A CN 110055376A
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CN
China
Prior art keywords
temperature
wire rod
preparation
pipe pile
iron wire
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201910474369.9A
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Chinese (zh)
Inventor
杨鲁明
吕刚
赵晓敏
白月琴
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Baotou Iron and Steel Group Co Ltd
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Baotou Iron and Steel Group Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Baotou Iron and Steel Group Co Ltd filed Critical Baotou Iron and Steel Group Co Ltd
Priority to CN201910474369.9A priority Critical patent/CN110055376A/en
Publication of CN110055376A publication Critical patent/CN110055376A/en
Pending legal-status Critical Current

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Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B21MECHANICAL METAL-WORKING WITHOUT ESSENTIALLY REMOVING MATERIAL; PUNCHING METAL
    • B21BROLLING OF METAL
    • B21B1/00Metal-rolling methods or mills for making semi-finished products of solid or profiled cross-section; Sequence of operations in milling trains; Layout of rolling-mill plant, e.g. grouping of stands; Succession of passes or of sectional pass alternations
    • B21B1/16Metal-rolling methods or mills for making semi-finished products of solid or profiled cross-section; Sequence of operations in milling trains; Layout of rolling-mill plant, e.g. grouping of stands; Succession of passes or of sectional pass alternations for rolling wire rods, bars, merchant bars, rounds wire or material of like small cross-section
    • CCHEMISTRY; METALLURGY
    • C21METALLURGY OF IRON
    • C21CPROCESSING OF PIG-IRON, e.g. REFINING, MANUFACTURE OF WROUGHT-IRON OR STEEL; TREATMENT IN MOLTEN STATE OF FERROUS ALLOYS
    • C21C5/00Manufacture of carbon-steel, e.g. plain mild steel, medium carbon steel or cast steel or stainless steel
    • C21C5/28Manufacture of steel in the converter
    • CCHEMISTRY; METALLURGY
    • C21METALLURGY OF IRON
    • C21CPROCESSING OF PIG-IRON, e.g. REFINING, MANUFACTURE OF WROUGHT-IRON OR STEEL; TREATMENT IN MOLTEN STATE OF FERROUS ALLOYS
    • C21C7/00Treating molten ferrous alloys, e.g. steel, not covered by groups C21C1/00 - C21C5/00
    • CCHEMISTRY; METALLURGY
    • C21METALLURGY OF IRON
    • C21CPROCESSING OF PIG-IRON, e.g. REFINING, MANUFACTURE OF WROUGHT-IRON OR STEEL; TREATMENT IN MOLTEN STATE OF FERROUS ALLOYS
    • C21C7/00Treating molten ferrous alloys, e.g. steel, not covered by groups C21C1/00 - C21C5/00
    • C21C7/0006Adding metallic additives
    • CCHEMISTRY; METALLURGY
    • C21METALLURGY OF IRON
    • C21CPROCESSING OF PIG-IRON, e.g. REFINING, MANUFACTURE OF WROUGHT-IRON OR STEEL; TREATMENT IN MOLTEN STATE OF FERROUS ALLOYS
    • C21C7/00Treating molten ferrous alloys, e.g. steel, not covered by groups C21C1/00 - C21C5/00
    • C21C7/04Removing impurities by adding a treating agent
    • C21C7/06Deoxidising, e.g. killing

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  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Metallurgy (AREA)
  • Organic Chemistry (AREA)
  • Mechanical Engineering (AREA)
  • Manufacturing & Machinery (AREA)
  • Refinement Of Pig-Iron, Manufacture Of Cast Iron, And Steel Manufacture Other Than In Revolving Furnaces (AREA)

Abstract

The invention discloses a kind of preparation method of high-strength pipe pile PC rod iron wire rod, mass percent carbon content 0.06-0.15%, the phosphorus content 0.011-0.020% of converter terminal molten steel, 1630-1650 DEG C of tapping temperature;1504-1581 DEG C of temperature in place of the refining of LF furnace, 1557-1605 DEG C of temperature of offing normal;Degree of superheat control is between 20-32 DEG C in continuous casting;Bringing-up section temperature: upper 1050-1200 DEG C of heating, heating is 980--1180 DEG C lower;1000-1200 DEG C in soaking, 980--1180 DEG C under soaking, keep steel billet poker temperature uniform, for start rolling temperature in the range of 960 DEG C-1000 DEG C, wire rod laying temperature is 900-950 DEG C.The present invention is generated under the premise of not changing process route using the crackle that the heating process of design, rolling mill practice avoid finished product wire rod.

Description

A kind of preparation method of high-strength pipe pile PC rod iron wire rod
Technical field
The present invention relates to metal material field, especially a kind of preparation method of high-strength pipe pile PC rod iron wire rod.
Background technique
Although traditional 30MnSi avoids it from being easy delayed fracture as far as possible by fining production control, low by its intensity Influence, gradually replaced by high-intensitive 30Si2Mn, which is a kind of to have higher-strength, toughness and shock resistance Middle low-carbon alloy steel, gren rod through pulling enhancing and modulation heat treatment after be mainly used in production harbour pipe of concrete Stake, tall building foundation concrete tubular pile etc..
Since 30Si2Mn belongs to high silicon steel, the thermal conductivity of silicon is poor, conducts heat in steel bad, therefore quickly heating or chilling Steel billet easily is cracked, is especially produced in severe winter, is easier to crack, therefore the production gets up to have certain hardly possible Degree.
Summary of the invention
In order to solve the above-mentioned technical problem, the object of the present invention is to provide a kind of preparations of high-strength pipe pile PC rod iron wire rod Method, this method is reliable and stable, easy to operate, low in cost, and submersed nozzle inner wall temperature can be improved, and reduces inner wall folder Sundries absorption further mitigates wadding steel incidence, reduces production cost.
In order to solve the above technical problems, the present invention adopts the following technical scheme:
A kind of preparation method of high-strength pipe pile PC rod iron wire rod, comprising:
S1, converter producing
To guarantee product quality and for refined molten steel ingredient, for the requirement of converter molten iron: phosphorus content is less than by weight percent Equal to 0.12%, sulfur content is less than or equal to 0.05%;The slag making auxiliary materials such as lime, dolomite are added in converter steelmaking process, out It is required that ferrosilicon, silicomanganese and aluminium silicomanganese progress deoxidation alloying is added according to finished product 30Si2Mn composition of steel during steel;
The carbon content of converter terminal molten steel, phosphorus content and tapping temperature are as follows:
1630-1650 DEG C of tapping temperature;Carbon content 0.06-0.15%;Phosphorus content 0.011-0.020%;
The production of S2, LF furnace
1504-1581 DEG C of temperature in place of the refining of LF furnace;Refining is offed normal 1557-1605 DEG C of temperature,;Refining treatment time 30- 56min;
S3, continuous casting
Degree of superheat control is between 20-32 DEG C in continuous casting, and pulling rate is between 2m/min-2.2m/min;
S4, high speed wire rolling
Heating time is greater than 2 hours steel billet in heating furnace, bringing-up section temperature: upper 1050-1200 DEG C of heating, under heating 980--1180 DEG C, guarantee that the bringing-up section time is no less than 1 hour;1000-1200 DEG C in soaking, 980--1180 DEG C under soaking, protect The card soaking zone time is no less than 1 hour, keeps steel billet poker temperature uniform;
For steel billet start rolling temperature at 960 DEG C -1000 DEG C, wire rod laying temperature is 900--950 DEG C.
Further, tapping temperature is 1638 DEG C in the S1.
Further, carbon content is 0.11% in the S1.
Further, phosphorus content is 0.16% in the S1.
Further, it is 1519 DEG C that LF furnace, which refines temperature in place, in the S2, and refining temperature of offing normal is 1564 DEG C.
Further, the refining treatment time is 40min in the S2.
Further, stelmo line insulation cover and blower are turned off in the S4.
Compared with prior art, advantageous effects of the invention:
The present invention finds out production under the premise of not changing process route, using the heating process and rolling mill practice of design Technique avoids the generation of the crack defect of finished product wire rod by most economical and the simplest method.
Specific embodiment
Commerical test production technology is summarized as follows:
Converter smelting-(LF) ladle furnace refining-continuous small-billet casting (150mm × 150mm)-high speed wire rolling.
THE INDUSTRIAL TRIAL 10 furnace steel, specific process parameter control are as follows:
1) converter producing
It is added lime 4000-5000kg when converter smelting according to the actual situation, dolomite 800-1200kg, in tapping process Ferrosilicon 2000kg, silicomangan 1000kg, aluminium silicomanganese 200kg is added.
The carbon content of converter terminal molten steel, phosphorus content (mass percent) and tapping temperature are as shown in table 1.
The ingredient and temperature of 1 converter tapping of table
2) LF furnace produces
The refining of LF furnace carries out plus auxiliary material slag making according to molten steel composition and temperature change, and adduction gold is finely adjusted and heats up behaviour Make.Be added lime 400-500kg, fluorite 200kg, alumina 150-200kg, calcium carbide 50kg, alloy according to refine ingredient in place into Row fine tuning manganese iron 300-500kg, ferrosilicon 300-500kg, feed silicon-calcium wire 150m.
Table 2 refines the control of LF furnace temperature
3) continuous casting
In continuous casting the degree of superheat control between 20-32 DEG C, pulling rate between 2m/min-2.2m/min, molten steel at Divide (mass percent) control as shown in table 3.
3 finished product ingredient (%) of table
4) Rolling production
Heating time is greater than 2 hours steel billet in heating furnace, bringing-up section temperature: upper 1050-1200 DEG C of heating, under heating 980--1180 DEG C, guarantee that the bringing-up section time is no less than 1 hour;1000-1200 DEG C in soaking, 980--1180 DEG C under soaking, protect The card soaking zone time is no less than 1 hour, keeps steel billet poker temperature uniform.Steel billet start rolling temperature steel billet start rolling temperature 960 DEG C- In the range of 1000 DEG C, cool controlled rolling is carried out to wire rod, laying temperature is 900-950 DEG C, stelmo line insulation cover and blower It is turned off.
5) service check
4 performance test results of table
By table 4 as it can be seen that 10 furnace steel mechanical properties of test fully meet the performance requirement of wire rod.
6) surface quality
The defects of not finding face crack fully meets the surface quality requirements of wire rod.
Embodiment described above is only that preferred embodiment of the invention is described, and is not carried out to the scope of the present invention It limits, without departing from the spirit of the design of the present invention, those of ordinary skill in the art make technical solution of the present invention Various changes and improvements, should all fall into claims of the present invention determine protection scope in.

Claims (7)

1. a kind of preparation method of high-strength pipe pile PC rod iron wire rod characterized by comprising
S1, converter producing
To guarantee product quality and for refined molten steel ingredient, for the requirement of converter molten iron: phosphorus content is less than or equal to by weight percent 0.12%, sulfur content is less than or equal to 0.05%;The slag making auxiliary materials such as lime, dolomite are added in converter steelmaking process, tapped It is required that ferrosilicon, silicomanganese and aluminium silicomanganese progress deoxidation alloying is added according to finished product 30Si2Mn composition of steel in journey;
The carbon content of converter terminal molten steel, phosphorus content and tapping temperature are as follows:
1630-1650 DEG C of tapping temperature;Carbon content 0.06-0.15%;Phosphorus content 0.011-0.020%;
The production of S2, LF furnace
1504-1581 DEG C of temperature in place of the refining of LF furnace;Refining is offed normal 1557-1605 DEG C of temperature,;Refining treatment time 30- 56min;
S3, continuous casting
Degree of superheat control is between 20-32 DEG C in continuous casting, and pulling rate is between 2m/min-2.2m/min;
S4, high speed wire rolling
Heating time is greater than 2 hours steel billet in heating furnace, bringing-up section temperature: upper 1050-1200 DEG C of heating, heating lower 980-- 1180 DEG C, guarantee that the bringing-up section time is no less than 1 hour;1000-1200 DEG C in soaking, 980--1180 DEG C under soaking, guarantee equal The hot arc time is no less than 1 hour, keeps steel billet poker temperature uniform;
For steel billet start rolling temperature at 960 DEG C -1000 DEG C, wire rod laying temperature is 900--950 DEG C.
2. the preparation method of high-strength pipe pile PC rod iron wire rod according to claim 1, which is characterized in that go out in the S1 Steel temperature is 1638 DEG C.
3. the preparation method of high-strength pipe pile PC rod iron wire rod according to claim 1, which is characterized in that carbon in the S1 Content is 0.11%.
4. the preparation method of high-strength pipe pile PC rod iron wire rod according to claim 3, which is characterized in that phosphorus in the S1 Content is 0.16%.
5. the preparation method of high-strength pipe pile PC rod iron wire rod according to claim 1, which is characterized in that LF in the S2 It is 1519 DEG C that furnace, which refines temperature in place, and refining temperature of offing normal is 1564 DEG C.
6. the preparation method of high-strength pipe pile PC rod iron wire rod according to claim 1 or 5, which is characterized in that the S2 The middle refining treatment time is 40min.
7. the preparation method of high-strength pipe pile PC rod iron wire rod according to claim 1, which is characterized in that this in the S4 Tai Ermo line insulation cover and blower are turned off.
CN201910474369.9A 2019-06-03 2019-06-03 A kind of preparation method of high-strength pipe pile PC rod iron wire rod Pending CN110055376A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201910474369.9A CN110055376A (en) 2019-06-03 2019-06-03 A kind of preparation method of high-strength pipe pile PC rod iron wire rod

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201910474369.9A CN110055376A (en) 2019-06-03 2019-06-03 A kind of preparation method of high-strength pipe pile PC rod iron wire rod

Publications (1)

Publication Number Publication Date
CN110055376A true CN110055376A (en) 2019-07-26

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Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN113699309A (en) * 2021-07-28 2021-11-26 邯郸钢铁集团有限责任公司 Steelmaking method for improving fluidity of molten PC steel
CN114101368A (en) * 2021-10-12 2022-03-01 包头钢铁(集团)有限责任公司 Production method of high-silicon prestressed steel bar
CN114875203A (en) * 2022-04-25 2022-08-09 盐城市联鑫钢铁有限公司 Preparation method of 30MnSi steel billet

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102703804A (en) * 2012-06-11 2012-10-03 首钢水城钢铁(集团)有限责任公司 Production method of wire rod for high-strength prestressed steel bar
CN104526285A (en) * 2014-12-23 2015-04-22 内蒙古包钢钢联股份有限公司 High silicon manganese steel wire rod production method
CN105970082A (en) * 2016-05-31 2016-09-28 内蒙古包钢钢联股份有限公司 Production method of steel wire rod used for high-strength prestressed concrete steel bars

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102703804A (en) * 2012-06-11 2012-10-03 首钢水城钢铁(集团)有限责任公司 Production method of wire rod for high-strength prestressed steel bar
CN104526285A (en) * 2014-12-23 2015-04-22 内蒙古包钢钢联股份有限公司 High silicon manganese steel wire rod production method
CN105970082A (en) * 2016-05-31 2016-09-28 内蒙古包钢钢联股份有限公司 Production method of steel wire rod used for high-strength prestressed concrete steel bars

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN113699309A (en) * 2021-07-28 2021-11-26 邯郸钢铁集团有限责任公司 Steelmaking method for improving fluidity of molten PC steel
CN114101368A (en) * 2021-10-12 2022-03-01 包头钢铁(集团)有限责任公司 Production method of high-silicon prestressed steel bar
CN114875203A (en) * 2022-04-25 2022-08-09 盐城市联鑫钢铁有限公司 Preparation method of 30MnSi steel billet

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Application publication date: 20190726