CN109971422A - A kind of aerospace composite polycrystal-diamond lapping liquid - Google Patents

A kind of aerospace composite polycrystal-diamond lapping liquid Download PDF

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Publication number
CN109971422A
CN109971422A CN201910254509.1A CN201910254509A CN109971422A CN 109971422 A CN109971422 A CN 109971422A CN 201910254509 A CN201910254509 A CN 201910254509A CN 109971422 A CN109971422 A CN 109971422A
Authority
CN
China
Prior art keywords
lapping liquid
diamond
composite polycrystal
suspension
aerospace
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201910254509.1A
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Chinese (zh)
Inventor
李花蕾
薛飞
李闯
张怡虎
张丰丰
刘花
王森林
王庆丰
李双霞
李德柱
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
HENAN FAMOUS DIAMOND INDUSTRIAL Co Ltd
Original Assignee
HENAN FAMOUS DIAMOND INDUSTRIAL Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by HENAN FAMOUS DIAMOND INDUSTRIAL Co Ltd filed Critical HENAN FAMOUS DIAMOND INDUSTRIAL Co Ltd
Priority to CN201910254509.1A priority Critical patent/CN109971422A/en
Publication of CN109971422A publication Critical patent/CN109971422A/en
Pending legal-status Critical Current

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Classifications

    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09GPOLISHING COMPOSITIONS; SKI WAXES
    • C09G1/00Polishing compositions
    • C09G1/02Polishing compositions containing abrasives or grinding agents
    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09KMATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
    • C09K3/00Materials not provided for elsewhere
    • C09K3/14Anti-slip materials; Abrasives
    • C09K3/1454Abrasive powders, suspensions and pastes for polishing
    • C09K3/1463Aqueous liquid suspensions

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Finish Polishing, Edge Sharpening, And Grinding By Specific Grinding Devices (AREA)

Abstract

The invention discloses a kind of aerospace composite polycrystal-diamond lapping liquid, the lapping liquid is 0-5 by polycrystalline diamond micro mist, deionized water, dispersing agent, the sticky dose of suspension formed, the PH of the suspension.The application's has the beneficial effect that the composite polycrystal-diamond surface grinding for being mainly used for having cambered surface, and the lapping liquid of the application is thick suspension, is substantially shorter milling time using the lapping liquid of the invention, improves working efficiency, saves grinding cost.It can guarantee to grind stable state for a long time, the processing stage of composite polycrystal-diamond, easy to clean, energy conservation and environmental protection are judged convenient for visual inspection.

Description

A kind of aerospace composite polycrystal-diamond lapping liquid
Technical field
The present invention relates to a kind of aerospace composite polycrystal-diamond lapping liquids, belong to diamond processing techniques neck Domain.
Background technique
Aerospace composite polycrystal-diamond such as guided missile pod etc. generally has arcwall face, and requires high saturating Photosensitiveness and best bright finish, thus aerospace also needed after deposition modeling with composite polycrystal-diamond using lapping liquid into Row grinding.Because of its hardness height, most of lapping liquids on the market cannot be ground it at present.
Summary of the invention
In order to overcome drawbacks described above, the present invention provides a kind of aerospace composite polycrystal-diamond lapping liquids.
To achieve the goals above, the technical solution of the present invention is as follows: a kind of aerospace is ground with composite polycrystal-diamond Grinding fluid, the lapping liquid is by polycrystalline diamond micro mist, deionized water, dispersing agent, the sticky dose of suspension formed, the suspension PH be 0-5.
Preferably, the granularity of the diadust is≤2 microns.
Preferably, the dispersing agent is one or more of sulfate, quaternary ammonium salt, PEO derivative, lactone, dispersing agent Have the function of adjusting PH and dispersed material.
Preferably, described sticky dose is food thickening agent.Food thickening agent generally selects gelatin, casein sodium, I Primary glue, tamarind seed polysaccharide glue, sesbania gum, agar, sodium alginate (sodium alginate, phycocolloid), carragheen, pectin, xanthan gum, β- Cyclodextrine, sodium carboxymethylcellulose (CMC-Na), starch phosphate sodium (sodium starch phosphate), sodium carboxymethyl starch, hydroxypropyl It is one or more in the substances such as starch and propylene glycol alginate (PGA) to add.
Preferably, the lapping liquid is made of raw material from the following weight: 10-20 parts of polycrystalline diamond micro mists, 70-100 The deionized water of part, 2-5 parts of dispersing agents, 0.2-2 parts sticky dose.
The application is mainly used to that suspension is made to form sticky, satiny state using food thickening agent, convenient for carrying out arc The aerospace in face can keep the adhesion in face to be processed when being processed with composite polycrystal-diamond, lapping liquid is kept to add Action time on work face.
The application's has the beneficial effect that the composite polycrystal-diamond surface grinding for being mainly used for having cambered surface, the application's Lapping liquid is thick suspension, using polycrystalline diamond micro mist, improves grinding efficiency and does not hurt workpiece, saves grinding cost.It can Stable state is ground with long-term guarantee, the processing stage of composite polycrystal-diamond is judged convenient for visual inspection, easy to clean, section It can environmental protection.
Specific embodiment
Technical solution of the present invention will be clearly and completely described below, it is clear that described embodiment is this hair Bright a part of the embodiment, instead of all the embodiments.Based on the embodiments of the present invention, those of ordinary skill in the art are not having Every other embodiment obtained under the premise of creative work is made, shall fall within the protection scope of the present invention.
Embodiment 1
A kind of aerospace composite polycrystal-diamond lapping liquid, the lapping liquid are made of raw material from the following weight: 20 Part polycrystalline diamond micro mist, 100 parts of deionized water, 4 parts of dispersing agents, the 1 part sticky dose suspension for stirring evenly composition, it is described The PH of suspension is 4.The granularity of diadust is≤2 microns.
Dispersing agent selects sulfate and quaternary ammonium salt, for dispersing and adjusting PH, sticky dose of selection sodium carboxymethylcellulose (CMC-Na) it is used to increase the viscosity of suspension.
After tested, the suspension viscosity of the present embodiment is 762cps, and polycrystalline diamond micro mist without obvious sediment, divides for a long time Cloth is uniform.It is processed for the aerospace of arcwall face with composite polycrystal-diamond, is 321g/cm2 in polish pressure, it is main Disk rotating speed is 80rmp, grinds flow quantity: 4ml/min, polishing time 30min, composite polycrystal-diamond rough surface before polishing 28.1628nm is spent, light transmittance 68%, composite polycrystal-diamond surface roughness 1.102nm after polishing, light transmittance 72%(70% are For qualification).And it in process obviously can mobility status be observed on composite polycrystal-diamond by polishing fluid The processing stage and surface defect of composite polycrystal-diamond.
Embodiment 2
A kind of aerospace composite polycrystal-diamond lapping liquid, the lapping liquid are made of raw material from the following weight: 10 Part polycrystalline diamond micro mist, 70 parts of deionized water, 2 parts of dispersing agents, the 0.5 part sticky dose suspension for stirring evenly composition, institute The PH for stating suspension is 3.The granularity of diadust is≤2 microns.
Dispersing agent selects sulfate, quaternary ammonium salt, PEO derivative, and for dispersing and adjusting PH, sticky dose of selection carboxymethyl is fine It ties up plain sodium (CMC-Na) and hydroxypropul starch is used to increase the viscosity of suspension.
After tested, the suspension viscosity of the present embodiment is 843cps, and polycrystalline diamond micro mist without obvious sediment, divides for a long time Cloth is uniform.It is processed for the aerospace of arcwall face with composite polycrystal-diamond, is 296g/cm2 in polish pressure, it is main Disk rotating speed is 80rmp, grinds flow quantity: 3ml/min, polishing time 40min, composite polycrystal-diamond rough surface before polishing Spend 28.1628nm, light transmittance 68%, composite polycrystal-diamond surface roughness 1.003nm after polishing, light transmittance 74%(technology It is required that 70% is qualification).And it can obviously be flowed emotionally on composite polycrystal-diamond by polishing fluid in process Condition observes the processing stage and surface defect of composite polycrystal-diamond.
The limitation that technical solution of the present invention is not limited to the above specific embodiments, it is all to do according to the technique and scheme of the present invention Technology deformation out, falls within the scope of protection of the present invention.

Claims (5)

1. a kind of aerospace composite polycrystal-diamond lapping liquid, it is characterised in that: the lapping liquid is by polycrystalline diamond Micro mist, deionized water, dispersing agent, the sticky dose of suspension formed, the PH of the suspension are 0-5.
2. aerospace according to claim 1 composite polycrystal-diamond lapping liquid, it is characterised in that: the Buddha's warrior attendant The granularity of stone micro mist is≤2 microns.
3. aerospace according to claim 2 composite polycrystal-diamond lapping liquid, it is characterised in that: the dispersion Agent is one or more of sulfate, quaternary ammonium salt, PEO derivative, lactone.
4. aerospace according to claim 3 composite polycrystal-diamond lapping liquid, it is characterised in that: described sticky Agent is food thickening agent.
5. aerospace according to claim 1 to 4 composite polycrystal-diamond lapping liquid, it is characterised in that: institute It states lapping liquid to be made of raw material from the following weight: 10-20 parts of polycrystalline diamond micro mists, 70-100 parts of deionized water, 2-5 parts Dispersing agent, 0.2-2 parts sticky dose.
CN201910254509.1A 2019-03-31 2019-03-31 A kind of aerospace composite polycrystal-diamond lapping liquid Pending CN109971422A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201910254509.1A CN109971422A (en) 2019-03-31 2019-03-31 A kind of aerospace composite polycrystal-diamond lapping liquid

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201910254509.1A CN109971422A (en) 2019-03-31 2019-03-31 A kind of aerospace composite polycrystal-diamond lapping liquid

Publications (1)

Publication Number Publication Date
CN109971422A true CN109971422A (en) 2019-07-05

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Family Applications (1)

Application Number Title Priority Date Filing Date
CN201910254509.1A Pending CN109971422A (en) 2019-03-31 2019-03-31 A kind of aerospace composite polycrystal-diamond lapping liquid

Country Status (1)

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CN (1) CN109971422A (en)

Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103013345A (en) * 2012-12-21 2013-04-03 清华大学 Oily diamond grinding liquid and preparation method thereof
CN106147617A (en) * 2015-04-28 2016-11-23 天津诺邦科技有限公司 A kind of water base polishing fluid of polycrystalline diamond and preparation method thereof

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103013345A (en) * 2012-12-21 2013-04-03 清华大学 Oily diamond grinding liquid and preparation method thereof
CN106147617A (en) * 2015-04-28 2016-11-23 天津诺邦科技有限公司 A kind of water base polishing fluid of polycrystalline diamond and preparation method thereof

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Application publication date: 20190705

RJ01 Rejection of invention patent application after publication