CN109966233A

CN109966233A - It is a kind of efficiently to nourish anti-wrinkle face mask liquid

Info

Publication number: CN109966233A
Application number: CN201910362366.6A
Authority: CN
Inventors: 陈清
Original assignee: Individual
Current assignee: Individual
Priority date: 2019-04-30
Filing date: 2019-04-30
Publication date: 2019-07-05

Abstract

Anti-wrinkle face mask liquid is efficiently nourished the invention discloses a kind of, belongs to cosmetic technical field.The present invention carries out hot-water soak to pigskin, generation microballoon is crosslinked under the action of reagent, Geniposide, it can be when being applied to skin of face, the effect for efficiently dredging moisture is provided, nano-scale fiber can also play the role of clearing up keratoderma, moistening effect is improved, the effect of active constituent is lockked, and then stablizes to provide and nourishes anti-wrinkle effect.Using chitosan and Nano-meter SiO_2₂It is blended with microcrystalline wax, it can helper activity facial blood circulation well, improve skin metabolism, Cucumber Extract cell, composite facial mask fluid base ingredients can be cooperated to increase skin hydration effect, infiltration subcutaneously reaches improvement local microcirculation, reaches the self-repairing capability of enhancing skin, the effect to smooth away wrinkles.The present invention solves at present the problem of common often relying on property of anti-wrinkle face mask liquid is strong, deactivates rear skin and easily loses vigor, and makes the self-regeneration function reduction of skin.

Description

It is a kind of efficiently to nourish anti-wrinkle face mask liquid

Technical field

The invention belongs to cosmetic technical fields, and in particular to a kind of efficiently to nourish anti-wrinkle face mask liquid.

Background technique

Facial mask beauty is one of cosmetic skin care methods of modern popular, is more and more had been favored by people, facial mask have paste, Gluey, powdery and model shape etc. are several, and after facial skin coats facial mask, moisture evaporation can generate tightening skin, stimulation face Sanguimotor effect, the facial mask with nutriment can promote Skin Cell directly to draw nutrition, and contain various upper Chinese herbal medicines Facial mask can also play preventive and therapeutic effect to pigment on the face, acne, freckle.It is excoriative that face can be eliminated when removing facial mask Cell, dirt, thus there are also cleaning skin, pore refining and wrinkle resistant effects for facial mask.

The reason of generating wrinkle mainly divides two major classes: chronological aging (natural aging) and external cause aging (light aging and smoking, Excessive drinking, bad diet etc.).It is generally believed that the skin of inboard arm reflects the progress of natural aging substantially；If skin on the face There is uneven, relaxation corrugation of the colour of skin etc., is all external cause aging bring than the bad luck of inboard arm skin in skin, especially it is sun-proof not Sufficient bring light aging, accounts for 80% or more.It's 30 years old has past woman, and fibroblastic quantity gradually decreases in human body, therefore Its collagen secreted and elastic fibers albumen are also gradually decreased, are broken because being oxidized, and skin corium starts thinning, skin bullet Property be deteriorated, wrinkle also starts gradually to generate.After the collagen of skin corium is oxidized, is broken, just to the supporting role of epidermis Disappear, thus cause it is inhomogenous collapse, such wrinkle just produces.

It is to make up makeup removing and the still insufficient cleaning that washes one's face that it is also most important purpose that facial mask is most basic, basic herein Upper realization other maintenance functions, such as replenishing water and preserving moisture, whitening and anti-aging etc..The principle of facial mask, exactly using being covered on face The of short duration time in portion is temporarily isolating extraneous air and pollution, improves skin temperature, and the pore expansion of skin promotes sweat gland point It secretes and metabolic, increase the oxygen content of skin, be conducive to product and accumulation that skin excludes epidermal cell metabolism Oil substances, the moisture in facial mask penetrate into the cuticula of epidermis, and skin becomes soft, and light is flexible naturally for skin.

The type of facial mask is divided according to quality, can be divided into face paste cloth type facial mask, tear-pull facial mask, blending paste film, cream Five big kinds of white type facial mask, fresh fruit self-made face pack etc..Wherein the utilization of face paste cloth type facial mask is the most extensive, is in this five big kinds of facial masks It sticks, take the simplest one kind off.Although face paste cloth type facial mask sticks, takes simplicity, face paste cloth type face off Maintenance product on film is all only attached on face paste cloth after all, and the ingredient of maintenance product in general above is one Sample, for being easy the position of long wrinkle at forehead and canthus, it is therefore desirable to especially carry out maintenance processing, general facial mask is not up to To the Level Of Maintenance of needs, it is therefore desirable to again plus some anti-wrinkle products are applied, but facial mask is bonded with face at this time, it is crease-resistant Product, which can only add, to be coated in outside facial mask, in this way, anti-wrinkle product needs to get to face by penetrating through facial mask itself, in this way Anti-wrinkle effect will have a greatly reduced quality.There are mainly two types of facial masks currently on the market, it is a kind of with chemical synthesis substance be mainly at Point, although effect is obvious, dependence is strong, and skin easily loses vigor after deactivating, and makes under the self-regeneration function of skin Drop；One kind is face mask of traditional Chinese medicine, many kinds of, but is had a single function, it has not been convenient to use simultaneously, be not suitable for the allegro city of modern Life style.

Summary of the invention

The technical problems to be solved by the invention: it is often quick for common anti-wrinkle face mask liquid at present, but dependence By force, it is anti-to provide a kind of efficiently nourishing for the problem of deactivating rear skin easily to lose vigor, and making the self-regeneration function reduction of skin Drawn grain film liquid.

In order to solve the above technical problems, the present invention is using technical solution as described below:

A kind of efficiently to nourish anti-wrinkle face mask liquid, including following component: 2 ~ 5 parts of lanolin, 1 ~ 4 part of potassium sorbate, 2 ~ 5 parts of spermaceti are hard Aliphatic radical glucoside, 3 ~ 7 parts of moisturizer, 2 ~ 5 parts of honey, 200 ~ 300 parts of water, 30 ~ 50 parts of composite facial mask liquid base materials, 15 ~ 30 parts of seas Mosanom active material.

Preferably, the efficient nourishing anti-wrinkle face mask liquid, including following component: 2 ~ 4 parts of lanolin, 1 ~ 3 part of potassium sorbate, 2 ~ 4 parts of cetearyl glucosides, 4 ~ 6 parts of moisturizer, 2 ~ 4 parts of honey, 220 ~ 280 parts of water, 35 ~ 45 parts of composite facial mask liquid-baseds Material, 18 ~ 28 parts of sodium alginate active materials.

Preferably, the efficient nourishing anti-wrinkle face mask liquid, including following component: 3 parts of lanolin, 2 parts of potassium sorbates, 3 parts Cetearyl glucoside, 5 parts of moisturizer, 3 parts of honey, 250 parts of water, 40 parts of composite facial mask liquid base materials, 23 parts of sodium alginates are living Property material.

Preferably, the preparation method of the composite facial mask liquid base material, includes the following steps:

(1) pigskin hot-water soak is taken, pulls pigskin washing out, refrigeration obtains pretreatment pigskin, 5 ~ 8:1:1 in mass ratio takes pretreatment Pigskin, tremella, Chinese yam mixing, smash homogenate to pieces, obtain slurry, collect slurry 1:20 in mass ratio ~ 35 and ethanol solution mixing is added, in 60 ~ 75 DEG C of refluxing extractions, obtain extract, extract are taken to be washed with dehydrated alcohol, collect washing lotion 3 ~ 6:25 in mass ratio and examination is added Agent mixing, is stirred in 65 ~ 80 DEG C, is stood, and is obtained albumen and is mixed liquid；

(2) in 20 ~ 33 DEG C, taking albumen to mix, span-80 is added in liquid 20 ~ 35:1 in mass ratio ~ 3:1, additive is mixed, and is added Albumen mixes the ethanol solution mixing of the Geniposide of liquid quality 15 ~ 25%, is warming up to 36 ~ 40 DEG C, and heat preservation mixing is centrifuged, collects It is centrifuged object freeze-drying, material must be lyophilized, takes freeze-drying material 10:2 ~ 5:1 in mass ratio that fermentation process material, sesame oil mixing is added, i.e., Obtain composite facial mask liquid base material.

Preferably, the reagent in the step (1): 1:10 ~ 14 take dehydrated alcohol, calcium chloride solution mixing in mass ratio, Up to reagent.

Preferably, the additive in the step (2): 1:4 ~ 7:2 in mass ratio take carboxylic acid methyl cellulose, casein, Lavender mixes to get additive.

Preferably, the fermentation process material in the step (2): according to parts by weight, 20 ~ 35 portions of brewex's grains, 4 ~ 7 parts of silks are taken Melon network, 1 ~ 3 part of saccharomycete powder, 1 ~ 3 part of bacillus licheniformis powder, 0.2 ~ 0.5 part of NaH₂PO₄, 6 ~ 10 parts of glycerol, 500 ~ 700 parts of water Mixing shakes shaking table in 25 ~ 32 DEG C, and discharging, insulated sterilizing, must sterilize material, takes sterilizing material centrifugation, collects upper suspension and subtract Pressure evaporation is to get fermentation process material.

Preferably, the preparation of the sodium alginate active material: in 30 ~ 50 DEG C, 20 ~ 30:3 in mass ratio takes sodium alginate molten Liquid, ammonium chloride mixing, adjust pH, (N- amidino groups) dodecylacrylamide, sea of sodium alginate soln quality 35 ~ 55% are added The polyvinyl alcohol phosphate of solution of sodium alginate quality 15 ~ 25% is mixed, and obtains mixture, takes mixture in mass ratio 16 ~ 25: Calcium chloride, pretreatment chitosan mixing is added in 1:3, obtains mixture, takes mixture 1:8 in mass ratio ~ 12 that the poly- second of methoxyl group is added Glycol solution is mixed, and is evaporated under reduced pressure to get sodium alginate active material.

Preferably, the pretreatment chitosan: 1:20 ~ 30 take chitosan, acetic acid solution mixing in mass ratio, obtain chitosan Liquid takes chitosan liquid 15 ~ 25:0.1:3 in mass ratio ~ 7 that Nano-meter SiO_2 is added in 60 ~ 75 DEG C₂, microcrystalline wax mixing, heat preservation stirs It mixes, vacuumizes standing, filter, take Washing of Filter Cake, it is dry to get pretreatment chitosan.

Preferably, the moisturizer: 1:3 ~ 7:1 in mass ratio takes glycerol, birch juice, hyaluronic acid mixing to get moisturizing Agent.

The present invention is compared with other methods, and advantageous effects are:

(1) present invention carries out hot-water soak to pigskin, removes amount of grease, then smash homogenate to pieces with tremella, Chinese yam, refluxing extraction, Dissolve out protein, the macromoleculars nutritional ingredient such as polysaccharide, reagent, Geniposide ethanol solution under the action of crosslink production Raw microballoon, and multiple nutritional components are wrapped up wherein, good percutaneous mechanism can be played, and regulate and control in coating process The vigor of skin antioxidase, reduces damage of the free radical to skin, delay skin aging, in addition, with the brewex's grains of small particle, The mixed fermentations such as luffa, the ingredients such as dissolution nutritional ingredient such as tannic acid, polyphenol, provide antioxidant effect, and can divide after sterilization Smaller brewex's grains fiber, loofah fiber and bacteria cellulose through bacterial metabolism effect differentiation are separated out, face can be applied to It when portion's skin, provides and efficiently dredges the effect of moisture, nano-scale fiber can also play the role of clearing up keratoderma, and can be with Hydrogen bond is formed between the ingredients such as the alginic acid macromolecular of subsequent addition, so that macromolecular arranges closer, hydrophilic radical and hydrone It forms hydrogen bond and strand is made to generate reticular structure, be detained active material and moisture during face mask film, improve moistening effect, lock The firmly effect of active constituent, and then stablize to provide and nourish anti-wrinkle effect；

(2) present invention is activated with sodium alginate through ammonium chloride, then with the long chain with amidino groups by covalence graft, and with non- Covalent electrostatic interaction combines, and methoxy poly (ethylene glycol) is added and is modified, and can occurring to tangle in aqueous solution, it is netted to be formed Structure, this facial mask liquid is in application, its contained amidino groups with the effect of carbon dioxide stimuli responsive is stimulated by the breathing of people, from group Dress is linear or rod-shaped micelle vesica, morphologically can improve to different levels osmotic effect, the hydrophilic hydroxyl groups being rich in component, It can also contribute to form a film in face, the tightening effect of face skin improved, in addition, using chitosan and Nano-meter SiO_2₂And microlite Wax is blended, and moveing freely for its segment is hindered, and constitutes the macromolecular chain with larger space steric hindrance, is applied in this facial mask liquid During applying, helper activity facial blood circulation, improvement skin metabolism, Cucumber Extract cell it can cooperate multiple well It closes facial mask liquid base ingredients and increases skin hydration effect, infiltration subcutaneously reaches improvement local microcirculation, activates epidermal cell, reaches Enhance the self-repairing capability of skin, the effect to smooth away wrinkles；

(3) present invention is strong for common often relying on property of anti-wrinkle face mask liquid at present, and skin easily loses vigor after deactivating, and makes skin The problem of self-regeneration function reduction of skin, improvement is significant, has a good application prospect.

Specific embodiment

Moisturizer: 1:3 ~ 7:1 in mass ratio takes glycerol, birch juice, hyaluronic acid mixing to get moisturizer.

Pre-process chitosan: 1:20 ~ 30 take the second that chitosan, mass fraction that deacetylation is 95% are 8% in mass ratio Acid solution mixing, obtains chitosan liquid, in 60 ~ 75 DEG C, takes chitosan liquid 15 ~ 25:0.1:3 in mass ratio ~ 7 that Nano-meter SiO_2 is added₂、 Microcrystalline wax mixing, 1 ~ 3h of insulated and stirred vacuumize 1 ~ 2h of standing, filter, and after taking filter cake to wash 2 ~ 4 times with dehydrated alcohol, move To 60 ~ 75 DEG C of 5 ~ 8h of oven drying to get pretreatment chitosan.

Additive: 1:4 ~ 7:2 in mass ratio takes carboxylic acid methyl cellulose, casein, Lavender mixing to get addition Agent.

Reagent: the calcium chloride solution that 1:10 ~ 14 take dehydrated alcohol in mass ratio, mass fraction is 18% mixes to get examination Agent.

Fermentation process material: according to parts by weight, brewex's grains, 4 ~ 7 portions of luffas, 1 ~ 3 part of 20 ~ 35 parts of 150 meshes of mistake are taken Saccharomycete powder, 1 ~ 3 part of bacillus licheniformis powder, 0.2 ~ 0.5 part of NaH₂PO₄, 6 ~ 10 parts of glycerol, 500 ~ 700 parts of water it is mixed in fermentor It closes, in 25 ~ 32 DEG C, with 180 ~ 220r/min concussion shaking table 5 ~ 8 days, discharging in 90 ~ 100 DEG C of 10 ~ 15min of insulated sterilizing, must go out Bacterium material, takes sterilizing material in centrifuge, is centrifuged 12 ~ 20min with 4000 ~ 7000r/min, collects upper suspension and is evaporated under reduced pressure to perseverance Weight is to get fermentation process material.

The preparation method of composite facial mask liquid base material, includes the following steps:

(1) it takes pigskin in 30 ~ 45 DEG C of hot water after 12 ~ 25min of water logging, pulls pigskin out and wash 2 ~ 4 times, it is cold to move to 2 ~ 5 DEG C of refrigerators 6 ~ 9h is hidden, pretreatment pigskin is obtained, 5 ~ 8:1:1 in mass ratio takes pretreatment pigskin, tremella, Chinese yam to mix in bruisher, smashs to pieces even 12 ~ 25min is starched, slurry is obtained, slurry 1:20 in mass ratio ~ 35 is collected and the ethanol solution mixing that volume fraction is 70% is added, in 60 ~ 75 DEG C of 2 ~ 4h of refluxing extraction, obtain extract, and extract is taken to be washed with 2 ~ 4 times of extract quality of dehydrated alcohol, collect washing lotion and press Reagent mixing is added in 3 ~ 6:25 of mass ratio, in 65 ~ 80 DEG C, with 400 ~ 700r/min, 40 ~ 60min of magnetic agitation, and it is stored at room temperature 2 ~ 4h obtains albumen and mixes liquid；

(2) it in 20 ~ 33 DEG C, takes albumen to mix liquid 20 ~ 35:1 in mass ratio ~ 3:1 and span-80, additive mixing is added, with 350 ~ 550r/min stirs 35 ~ 60min, and it is the ethanol solution of 1% Geniposide that albumen, which is added, and mixes the mass fraction of liquid quality 15 ~ 25% Mixing, is warming up to 36 ~ 40 DEG C, and heat preservation 30 ~ 50min of mixing moves to centrifuge with 3500 ~ 5500r/min and is centrifuged 12 ~ 20min, receives Collect centrifugation object in the dry 5 ~ 8h of -10 DEG C of freeze driers, material must be lyophilized, freeze-drying material 10:2 ~ 5:1 in mass ratio is taken to be added at fermentation Reason material, sesame oil mixing are to get composite facial mask liquid base material.

The preparation of sodium alginate active material: in 30 ~ 50 DEG C, it is 10% alginic acid that 20 ~ 30:3 in mass ratio, which takes mass fraction, Sodium solution, ammonium chloride mixing adjust pH to 7.5 ~ 7.8 with the ammonia spirit that concentration is 0.1mol/L, sodium alginate soln are added (N- amidino groups) dodecylacrylamide, the polyvinyl alcohol phosphate of sodium alginate soln quality 15 ~ 25% of quality 35 ~ 55% are mixed It closes, with 500 ~ 800r/min, 40 ~ 60min of magnetic agitation, obtains mixture, take mixture 16 ~ 25:1:3 in mass ratio that chlorination is added Calcium, pretreatment chitosan mixing, obtain mixture, take mixture 1:8 in mass ratio ~ 12 that the mixing of methoxy poly (ethylene glycol) solution is added 20 ~ 45min is stirred, the 20 ~ 35% of reduction vaporization to original volume are to get sodium alginate active material.

It is a kind of efficiently to nourish anti-wrinkle face mask liquid, according to parts by weight, including following component: 2 ~ 5 parts of lanolin, 1 ~ 4 part of mountain Potassium sorbate, 2 ~ 5 parts of cetearyl glucosides, 3 ~ 7 parts of moisturizer, 2 ~ 5 parts of honey, 200 ~ 300 parts of water, 30 ~ 50 parts of composite surfaces Film liquid base-material, 15 ~ 30 parts of sodium alginate active materials.

Moisturizer: 1:3:1 in mass ratio takes glycerol, birch juice, hyaluronic acid mixing to get moisturizer.

Pre-process chitosan: 1:20 in mass ratio takes the acetic acid that the chitosan that deacetylation is 95%, mass fraction are 8% molten Liquid mixing, obtains chitosan liquid, in 60 DEG C, takes chitosan liquid 15:0.1:3 in mass ratio that Nano-meter SiO_2 is added₂, microcrystalline wax mixing, Insulated and stirred 1h, vacuumizes and stands 1h, and filtering after taking filter cake to wash 2 times with dehydrated alcohol, moves to 60 DEG C of oven drying 5h, i.e., Chitosan must be pre-processed.

Additive: 1:4:2 in mass ratio takes carboxylic acid methyl cellulose, casein, Lavender mixing to get addition Agent.

Reagent: the calcium chloride solution that 1:10 in mass ratio takes dehydrated alcohol, mass fraction is 18% mixes to get reagent.

Fermentation process material: according to parts by weight, the brewex's grains, 4 portions of luffas, 1 part of saccharomycete of 20 parts of 150 meshes of mistake are taken Powder, 1 part of bacillus licheniformis powder, 0.2 part of NaH₂PO₄, 6 parts of glycerol, 500 parts of water mixed in fermentor, in 25 DEG C, with 180r/ Min shakes shaking table 5 days, and discharging, in 90 DEG C of insulated sterilizing 10min, must sterilize material, takes sterilizing material in centrifuge, with 4000r/min It is centrifuged 12min, upper suspension is collected and is evaporated under reduced pressure to constant weight to get fermentation process material.

(1) it takes pigskin in 30 DEG C of hot water after water logging 12min, pulls pigskin out and wash 2 times, move to 2 DEG C of refrigerator cold-storage 6h, obtain pre- place Pigskin is managed, 5:1:1 in mass ratio takes pretreatment pigskin, tremella, Chinese yam to mix in bruisher, and it smashs homogenate 12min to pieces, obtains slurry, It collects slurry 1:20 in mass ratio and the ethanol solution mixing that volume fraction is 70% is added, in 60 DEG C of refluxing extraction 2h, must extract Object takes extract to be washed with 2 times of extract quality of dehydrated alcohol, collects washing lotion 3:25 in mass ratio and reagent mixing is added, in 65 DEG C, with 400r/min magnetic agitation 40min, it is stored at room temperature 2h, albumen is obtained and mixes liquid；

(2) it in 20 DEG C, takes albumen to mix liquid 20:1:1 in mass ratio and span-80, additive mixing is added, stirred with 350r/min 35min is added the ethanol solution mixing that albumen mixes the mass fraction of liquid quality 15% as 1% Geniposide, is warming up to 36 DEG C, protects Temperature mixing 30min, moves to centrifuge with 3500r/min and is centrifuged 12min, collects centrifugation object in the dry 5h of -10 DEG C of freeze driers, Material must be lyophilized, take freeze-drying material 10:2:1 in mass ratio that fermentation process material, sesame oil mixing is added to get composite facial mask liquid base material.

The preparation of sodium alginate active material: in 30 DEG C, the sodium alginate that 20:3 in mass ratio takes mass fraction to be 10% is molten Liquid, ammonium chloride mixing adjust pH to 7.5 with the ammonia spirit that concentration is 0.1mol/L, sodium alginate soln quality 35% are added The polyvinyl alcohol phosphate mixing of (N- amidino groups) dodecylacrylamide, sodium alginate soln quality 15%, with 500r/min magnetic Power stirs 40min, obtains mixture, takes mixture 16:1:3 in mass ratio that calcium chloride, pretreatment chitosan mixing is added, must mix Object takes mixture 1:8 in mass ratio that methoxy poly (ethylene glycol) solution is added and 20min is mixed, is evaporated under reduced pressure to original volume 20% to get sodium alginate active material.

It is a kind of efficiently to nourish anti-wrinkle face mask liquid, according to parts by weight, including following component: 3 parts of lanolin, 2 parts of sorbic acids Potassium, 3 parts of cetearyl glucosides, 5 parts of moisturizer, 4 parts of honey, 250 parts of water, 40 parts of composite facial mask liquid base materials, 25 portions of seaweed Sour sodium active material.

Moisturizer: 1:5:1 in mass ratio takes glycerol, birch juice, hyaluronic acid mixing to get moisturizer.

Pre-process chitosan: 1:25 in mass ratio takes the acetic acid that the chitosan that deacetylation is 95%, mass fraction are 8% molten Liquid mixing, obtains chitosan liquid, in 70 DEG C, takes chitosan liquid 20:0.1:5 in mass ratio that Nano-meter SiO_2 is added₂, microcrystalline wax mixing, Insulated and stirred 2h is vacuumized and is stood 1.5h, and filtering after taking filter cake to wash 3 times with dehydrated alcohol, moves to 70 DEG C of oven drying 7h, Up to pretreatment chitosan.

Additive: 1:5:2 in mass ratio takes carboxylic acid methyl cellulose, casein, Lavender mixing to get addition Agent.

Reagent: the calcium chloride solution that 1:12 in mass ratio takes dehydrated alcohol, mass fraction is 18% mixes to get reagent.

Fermentation process material: according to parts by weight, the brewex's grains, 5 portions of luffas, 2 parts of saccharomycete of 25 parts of 150 meshes of mistake are taken Powder, 2 parts of bacillus licheniformis powder, 0.3 part of NaH₂PO₄, 8 parts of glycerol, 600 parts of water mixed in fermentor, in 28 DEG C, with 200r/ Min shakes shaking table 7 days, and discharging, in 95 DEG C of insulated sterilizing 12min, must sterilize material, takes sterilizing material in centrifuge, with 5500r/min It is centrifuged 16min, upper suspension is collected and is evaporated under reduced pressure to constant weight to get fermentation process material.

(1) it takes pigskin in 40 DEG C of hot water after water logging 18min, pulls pigskin out and wash 3 times, move to 4 DEG C of refrigerator cold-storage 8h, obtain pre- place Pigskin is managed, 6:1:1 in mass ratio takes pretreatment pigskin, tremella, Chinese yam to mix in bruisher, and it smashs homogenate 18min to pieces, obtains slurry, It collects slurry 1:30 in mass ratio and the ethanol solution mixing that volume fraction is 70% is added, in 70 DEG C of refluxing extraction 3h, must extract Object takes extract to be washed with 3 times of extract quality of dehydrated alcohol, collects washing lotion 5:25 in mass ratio and reagent mixing is added, in 70 DEG C, with 550r/min magnetic agitation 50min, it is stored at room temperature 3h, albumen is obtained and mixes liquid；

(2) it in 26 DEG C, takes albumen to mix liquid 25:2:1 in mass ratio and span-80, additive mixing is added, stirred with 450r/min 47min is added the ethanol solution mixing that albumen mixes the mass fraction of liquid quality 20% as 1% Geniposide, is warming up to 38 DEG C, protects Temperature mixing 40min, moves to centrifuge with 4500r/min and is centrifuged 16min, collects centrifugation object in the dry 7h of -10 DEG C of freeze driers, Material must be lyophilized, take freeze-drying material 10:4:1 in mass ratio that fermentation process material, sesame oil mixing is added to get composite facial mask liquid base material.

The preparation of sodium alginate active material: in 40 DEG C, the sodium alginate that 25:3 in mass ratio takes mass fraction to be 10% is molten Liquid, ammonium chloride mixing adjust pH to 7.6 with the ammonia spirit that concentration is 0.1mol/L, sodium alginate soln quality 45% are added The polyvinyl alcohol phosphate mixing of (N- amidino groups) dodecylacrylamide, sodium alginate soln quality 20%, with 650r/min magnetic Power stirs 50min, obtains mixture, takes mixture 20:1:3 in mass ratio that calcium chloride, pretreatment chitosan mixing is added, must mix Object takes mixture 1:10 in mass ratio that methoxy poly (ethylene glycol) solution is added and 30min is mixed, is evaporated under reduced pressure to original volume 30% to get sodium alginate active material.

It is a kind of efficiently to nourish anti-wrinkle face mask liquid, according to parts by weight, including following component: 3 parts of lanolin, 2 parts of sorbic acids Potassium, 3 parts of cetearyl glucosides, 5 parts of moisturizer, 3 parts of honey, 250 parts of water, 40 parts of composite facial mask liquid base materials, 23 portions of seaweed Sour sodium active material.

Moisturizer: 1:7:1 in mass ratio takes glycerol, birch juice, hyaluronic acid mixing to get moisturizer.

Pre-process chitosan: 1:30 in mass ratio takes the acetic acid that the chitosan that deacetylation is 95%, mass fraction are 8% molten Liquid mixing, obtains chitosan liquid, in 75 DEG C, takes chitosan liquid 25:0.1:7 in mass ratio that Nano-meter SiO_2 is added₂, microcrystalline wax mixing, Insulated and stirred 3h, vacuumizes and stands 2h, and filtering after taking filter cake to wash 4 times with dehydrated alcohol, moves to 75 DEG C of oven drying 8h, i.e., Chitosan must be pre-processed.

Additive: 1:7:2 in mass ratio takes carboxylic acid methyl cellulose, casein, Lavender mixing to get addition Agent.

Reagent: the calcium chloride solution that 1:14 in mass ratio takes dehydrated alcohol, mass fraction is 18% mixes to get reagent.

Fermentation process material: according to parts by weight, the brewex's grains, 7 portions of luffas, 3 parts of saccharomycete of 35 parts of 150 meshes of mistake are taken Powder, 3 parts of bacillus licheniformis powder, 0.5 part of NaH₂PO₄, 10 parts of glycerol, 700 parts of water mixed in fermentor, in 32 DEG C, with 220r/ Min shakes shaking table 8 days, and discharging, in 100 DEG C of insulated sterilizing 15min, must sterilize material, takes sterilizing material in centrifuge, with 7000r/ Min is centrifuged 20min, collects upper suspension and is evaporated under reduced pressure to constant weight to get fermentation process material.

(1) it takes pigskin in 45 DEG C of hot water after water logging 25min, pulls pigskin out and wash 4 times, move to 5 DEG C of refrigerator cold-storage 9h, obtain pre- place Pigskin is managed, 8:1:1 in mass ratio takes pretreatment pigskin, tremella, Chinese yam to mix in bruisher, and it smashs homogenate 25min to pieces, obtains slurry, It collects slurry 1:35 in mass ratio and the ethanol solution mixing that volume fraction is 70% is added, in 75 DEG C of refluxing extraction 4h, must extract Object takes extract to be washed with 4 times of extract quality of dehydrated alcohol, collects washing lotion 6:25 in mass ratio and reagent mixing is added, in 80 DEG C, with 700r/min magnetic agitation 60min, it is stored at room temperature 4h, albumen is obtained and mixes liquid；

(2) it in 33 DEG C, takes albumen to mix liquid 35:3:1 in mass ratio and span-80, additive mixing is added, stirred with 550r/min 60min is added the ethanol solution mixing that albumen mixes the mass fraction of liquid quality 25% as 1% Geniposide, is warming up to 40 DEG C, protects Temperature mixing 50min, moves to centrifuge with 5500r/min and is centrifuged 20min, collects centrifugation object in the dry 8h of -10 DEG C of freeze driers, Material must be lyophilized, take freeze-drying material 10:5:1 in mass ratio that fermentation process material, sesame oil mixing is added to get composite facial mask liquid base material.

The preparation of sodium alginate active material: in 50 DEG C, the sodium alginate that 30:3 in mass ratio takes mass fraction to be 10% is molten Liquid, ammonium chloride mixing adjust pH to 7.8 with the ammonia spirit that concentration is 0.1mol/L, sodium alginate soln quality 55% are added The polyvinyl alcohol phosphate mixing of (N- amidino groups) dodecylacrylamide, sodium alginate soln quality 25%, with 800r/min magnetic Power stirs 60min, obtains mixture, takes mixture 25:1:3 in mass ratio that calcium chloride, pretreatment chitosan mixing is added, must mix Object takes mixture 1:12 in mass ratio that methoxy poly (ethylene glycol) solution is added and 45min is mixed, is evaporated under reduced pressure to original volume 35% to get sodium alginate active material.

Comparative example 1: it is essentially identical with the preparation method of embodiment 1, it has only the difference is that lacking composite facial mask liquid base material.

Comparative example 2: it is essentially identical with the preparation method of embodiment 1, it has only the difference is that lacking sodium alginate active material.

Comparative example 3: the efficient nourishing anti-wrinkle face mask liquid of company, Shenzhen production.

Embodiment is tested with efficient nourishing anti-wrinkle face mask liquid obtained by comparative example according to QB/T2872-2007, is tested The results are shown in Table 1:

Table 1:

Test item

Embodiment 1

Embodiment 2

Embodiment 3

Comparative example 1

Comparative example 2

Comparative example 3

30 days skin elasticity increase rate/%

75.3

78.4

80.1

72.3

69.1

65.3

Use skin average moisture content/% after 20min

28.65

30.25

35.21

25.32

23.01

18.52

Self-regeneration function

Generally

It is relatively strong

Generally

It is weaker

15 days skin conditions

There is microgroove at canthus

It is substantially wrinkle-free line, smooth

It is substantially wrinkle-free line, smooth, moist

There is microgroove at canthus

There is many places wrinkle

In summary, the resulting efficient nourishing anti-wrinkle face mask quick permeation of the present invention, good absorbing, delaying skin cell ageing are crease-resistant Effect is preferable, after use color spot obviously desalinate, skin it is more fine and smooth pale, self-repairing capability is strong.Compared to commercial product Effect is more preferable, is worth promoting.

The foregoing is merely preferred modes of the invention, are not intended to limit the invention, all in spirit and original of the invention Within then, any modification, equivalent replacement, improvement and so on be should all be included in the protection scope of the present invention.

Claims

1. a kind of efficiently nourish anti-wrinkle face mask liquid, according to parts by weight, including following component: 2 ~ 5 parts of lanolin, 1 ~ 4 portion of sorb Sour potassium, 2 ~ 5 parts of cetearyl glucosides, 3 ~ 7 parts of moisturizer, 2 ~ 5 parts of honey, 200 ~ 300 parts of water, which is characterized in that also wrap It includes: 30 ~ 50 parts of composite facial mask liquid base materials, 15 ~ 30 parts of sodium alginate active materials.

2. a kind of according to claim 1 efficiently nourish anti-wrinkle face mask liquid, which is characterized in that according to parts by weight, the height Effect nourishes anti-wrinkle face mask liquid, including following component: 2 ~ 4 parts of lanolin, 1 ~ 3 part of potassium sorbate, 2 ~ 4 parts of cetearyl glucose Glycosides, 4 ~ 6 parts of moisturizer, 2 ~ 4 parts of honey, 220 ~ 280 parts of water, 35 ~ 45 parts of composite facial mask liquid base materials, 18 ~ 28 parts of sodium alginates are living Property material.

3. a kind of according to claim 1 efficiently nourish anti-wrinkle face mask liquid, which is characterized in that according to parts by weight, the height Effect nourishes anti-wrinkle face mask liquid, including following component: 3 parts of lanolin, 2 parts of potassium sorbates, 3 parts of cetearyl glucosides, 5 parts of guarantors Humectant, 3 parts of honey, 250 parts of water, 40 parts of composite facial mask liquid base materials, 23 parts of sodium alginate active materials.

4. a kind of according to claim 1 efficiently nourish anti-wrinkle face mask liquid, which is characterized in that the composite facial mask liquid base material Preparation method includes the following steps:

5. a kind of according to claim 4 efficiently nourish anti-wrinkle face mask liquid, which is characterized in that the reagent in the step (1): 1:10 ~ 14 take dehydrated alcohol, calcium chloride solution mixing to get reagent in mass ratio.

6. a kind of according to claim 4 efficiently nourish anti-wrinkle face mask liquid, which is characterized in that the addition in the step (2) Agent: 1:4 ~ 7:2 in mass ratio takes carboxylic acid methyl cellulose, casein, Lavender mixing to get additive.

7. a kind of according to claim 4 efficiently nourish anti-wrinkle face mask liquid, which is characterized in that the fermentation in the step (2) Processing material: according to parts by weight, 20 ~ 35 portions of brewex's grains, 4 ~ 7 portions of luffas, 1 ~ 3 part of saccharomycete powder, 1 ~ 3 part of lichens brood cell's bar are taken Bacterium powder, 0.2 ~ 0.5 part of NaH₂PO₄, 6 ~ 10 parts of glycerol, 500 ~ 700 parts of water mixing in 25 ~ 32 DEG C shake shaking table, discharge, heat preservation Sterilizing, must sterilize material, take sterilizing material centrifugation, collect upper suspension and be evaporated under reduced pressure to get fermentation process material.

8. a kind of according to claim 1 efficiently nourish anti-wrinkle face mask liquid, which is characterized in that the sodium alginate active material Preparation: in 30 ~ 50 DEG C, 20 ~ 30:3 in mass ratio takes sodium alginate soln, ammonium chloride mixing, adjusts pH, it is molten that sodium alginate is added The polyvinyl alcohol phosphate of (N- amidino groups) dodecylacrylamide of liquid quality 35 ~ 55%, sodium alginate soln quality 15 ~ 25% It is mixed, obtains mixture, take mixture 16 ~ 25:1:3 in mass ratio that calcium chloride, pretreatment chitosan mixing is added, must mix Object takes mixture 1:8 in mass ratio ~ 12 that methoxy poly (ethylene glycol) solution is added and is mixed, is evaporated under reduced pressure to get sodium alginate Active material.

9. a kind of according to claim 8 efficiently nourish anti-wrinkle face mask liquid, which is characterized in that the pretreatment chitosan: press Mass ratio 1:20 ~ 30 take chitosan, acetic acid solution mixing, obtain chitosan liquid, in 60 ~ 75 DEG C, take chitosan liquid in mass ratio 15 ~ 25:0.1:3 ~ 7 are added Nano-meter SiO_2₂, microcrystalline wax mixing, insulated and stirred vacuumizes standings, filters, takes Washing of Filter Cake, dry, Up to pretreatment chitosan.

10. a kind of according to claim 1 efficiently nourish anti-wrinkle face mask liquid, which is characterized in that the moisturizer: in mass ratio 1:3 ~ 7:1 takes glycerol, birch juice, hyaluronic acid mixing to get moisturizer.