CN109946193A - A kind of inspection method for preparing extruding dregs porcelain granule and detecting clod content in the process - Google Patents
A kind of inspection method for preparing extruding dregs porcelain granule and detecting clod content in the process Download PDFInfo
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Abstract
The present invention relates to extruding dregs porcelain granule technical fields, and disclose a kind of inspection method for preparing extruding dregs porcelain granule and detecting clod content in the process, include the following steps, choose sample, X parts are chosen from the extruding dregs porcelain granule prepared, the Xn that is denoted as X1, X2, X3 ..., it is individually positioned in spare in container, weighing screening, X parts of extruding dregs porcelain granule samples are weighed into weight respectively, obtain weight and be recorded as N1, N2, N3 ... Nn, X parts of extruding dregs porcelain granule samples are put into screening plant respectively, it is screened using vibrating screen, removes fine powder.The inspection method of clod content is detected during the preparation extruding dregs porcelain granule, pass through filtering, it will be filtered in X part extruding dregs porcelain granule sample investment filter plant of immersion, it is persistently stirred in filtering, obtain X parts of extruding dregs porcelain granule sample filtering turbid solutions, the result that the result COMPREHENSIVE CALCULATING of multiple sample detection obtains is more accurate, eliminates the worry of user, the use for the person of being convenient to use.
Description
Technical field
The present invention relates to extruding dregs porcelain granule technical field, specially a kind of prepare is detected clod during extruding dregs porcelain granule and is contained
The inspection method of amount.
Background technique
Southwest China Panxi Diqu contains vanadium titano-magnetite extremely abundant, and the reserves verified are more than 10,000,000,000 tons, possess
About 3,400,000,000 tons of reserves, high-titanium blast furnace slag fails to utilize on a large scale, causes clinker bulk deposition idle, and slag tip occupies a large amount of soil
Ground not only pollutes environment, destroys ecology, but also wastes resource, causes huge economic losses, therefore, to high-titanium blast furnace slag
The research comprehensively utilized is found a kind of good processing approach for comprehensively utilizing high-titanium blast furnace slag, is had highly important
Scientific value and future in engineering applications, currently, the processing of high-titanium blast furnace slag and application method are two kinds of shapes of flush slag and dry slag
Formula, it is generally the case that flush slag is the blast furnace slag that impact fusion state is forced using high pressure water, makes its cooling rapidly, fragmentation,
Manufactured goods partial size cannot function as aggregate for building between 0.1-2.0mm, can only use as the blend composition of cement, dry slag
It is that high-temperature slag is directly put in ground natural cooling, by the processing such as excavating, being crushed, screen and be classified, can be partially used to build
Build material, but due to the various higher cost of its process, and its specific gravity does not meet lightweight and wants mostly between 1.8-2.5kg/cm3
Ask, therefore, solid waste of the high-titanium blast furnace slag as blast furnace process, use value by its subsequent product limitation, always
Since application range it is extremely limited, haydite is exactly as its name suggests the particle of ceramic, and the external appearance characteristic of haydite is largely rounded
Or oval-shaped ball, but be not round or ellipse sphere there are also imitative rubble haydite, and it is in irregular rubble shape, haydite shape
Shape is different because of technique difference, its surface is one layer of hard shell, this layer of shell is in ceramic or enamel, and there is water proof to protect gas
Effect, and assign haydite higher intensity, because there are many raw material of production haydite, the kind of haydite is also very much, thus color
Also just very much, the color for roasting haydite is mostly kermesinus and ember, there are also special kinds be lark, grey black,
Canescence and cinerous etc., baking-free ceramicite vary in color, generally grey black, surface does not have because solid waste used is different
Glossiness, it is smooth not as good as roasting haydite.
Chinese patent CN206692568U discloses a kind of extruding dregs porcelain granule production system, which provides one kind and can show
It writes and improves high-titanium blast furnace slag utilization rate, economize on resources, it is raw to the extruding dregs porcelain granule of the destruction of environment to reduce high-titanium blast furnace slag
Production system, system preparation production extruding dregs porcelain granule need to detect the clod content in extruding dregs porcelain granule, traditional inspection
Survey method detects the detection for not being suitable for extruding dregs porcelain granule, and testing result is more coarse, is not very accurate, so propose one kind
Prepare the method that extruding dregs porcelain granule detects clod content in the process.
Summary of the invention
(1) the technical issues of solving
In view of the deficiencies of the prior art, the present invention provides a kind of extruding dregs porcelain granules for preparing to detect clod content in the process
Inspection method has the advantages that testing result is accurate, solves traditional detection method detection and is not suitable for extruding dregs porcelain granule
Detection, testing result is more coarse, is not very accurate problem.
(2) technical solution
To realize above-mentioned testing result accurately purpose, the invention provides the following technical scheme: a kind of prepare extruding slag pottery
The inspection method of clod content is detected during grain, comprising the following steps:
1) sample is chosen, X parts, the Xn that is denoted as X1, X2, X3 ... are chosen from the extruding dregs porcelain granule prepared, is placed respectively
It is spare in container；
2) X parts of extruding dregs porcelain granule samples are weighed weight respectively, obtain weight and be recorded as N1, N2, N3 ... by weighing screening
X parts of extruding dregs porcelain granule samples are put into screening plant respectively, are screened using vibrating screen by Nn, remove fine powder；
3) it impregnates, the X part extruding dregs porcelain granule sample for removing fine powder is held into immersion respectively, soaking time is 12-20 hours,
Stirred three hours after immersion, after stirring by standing one hour, it is spare；
4) it filters, will be filtered in X part extruding dregs porcelain granule sample investment filter plant of immersion, persistently stir, obtain in filtering
Turbid solution is filtered to X parts of extruding dregs porcelain granule samples；
5) drying and dewatering in X parts of extruding dregs porcelain granule sample filtering turbid solution investment drying equipments is obtained X by drying and dewatering
The dry mud of part, takes out spare；
6) the dry mud of X part that step 5 obtains is placed on meausring apparatus and is weighed, obtained weight and be recorded as Y1, Y2, Y3 ...
Yn；
7) it calculates, calculates clod content Z in extruding dregs porcelain granule, in respect of Z1=Y1/N1*100%, Z2=Y2/N2*100%,
Z3=Y3/N3*100% ... Zn=Yn/Nn*100%, Z=(Z2+Z3 ...+Zn-1)/(n-2), Z are required extruding slag
Clod content in haydite.
Preferably, X described in step 1 parts of extruding dregs porcelain granule sample, X are more than or equal to 4, the weight of every part of extruding dregs porcelain granule sample
Not less than ten kilograms.
Preferably, X parts of extruding dregs porcelain granule samples are put into screening plant described in step 2 respectively, screening plant is set
Screen number is 80 mesh.
Preferably, the X part extruding dregs porcelain granule sample for removing fine powder is held into immersion described in step 3 respectively, impregnates extruding slag
The weight ratio of haydite sample and water is 1:1.5, and water is distilled water, and stirring frequency is 60 turns per minute, and container is sealing
Container.
Preferably, filtering turbid solution described in step 4 is 200 mesh using the filter hole mesh number of filter device.
Preferably, it requires thoroughly to clean before every use using each equipment in detection process, weighs unit and precisely arrive
Milligram, setting drying temperature is 80 degrees Celsius in drying and dewatering described in step 5.
(3) beneficial effect
Compared with prior art, the present invention provides a kind of inspections for preparing extruding dregs porcelain granule and detecting clod content in the process
Method, have it is following the utility model has the advantages that
1, the inspection method that clod content is detected during the preparation extruding dregs porcelain granule, it is by filtering, X part of immersion is swollen
Slugging haydite sample puts into filtering in filter plant, persistently stirs in filtering, and it is muddy to obtain X parts of extruding dregs porcelain granule sample filterings
Drying and dewatering in X parts of extruding dregs porcelain granule sample filtering turbid solution investment drying equipments is obtained X parts of dry mud by liquid, drying and dewatering,
It takes out spare, the dry mud of X part that step 5 obtains is placed on meausring apparatus and is weighed, weight is obtained and is recorded as Y1, Y2, Y3 ...
Yn is calculated, and clod content Z in extruding dregs porcelain granule is calculated, in respect of Z1=Y1/N1*100%, Z2=Y2/N2*100%, Z3=Y3/
N3*100% ... Zn=Yn/Nn*100%, Z=(Z2+Z3 ...+Zn-1)/(n-2), Z are in required extruding dregs porcelain granule
Clod content, the result that the result COMPREHENSIVE CALCULATING of multiple sample detection obtains is more accurate, eliminates the worry of user, convenient
The use of user.
2, the inspection method that clod content is detected during the preparation extruding dregs porcelain granule, by choosing sample, from preparing
Extruding dregs porcelain granule in choose X part, the Xn that is denoted as X1, X2, X3 ..., be individually positioned in spare in container, weighing is screened, by X parts
Extruding dregs porcelain granule sample weighs weight respectively, obtains weight and be recorded as N1, N2, N3 ... Nn, by X parts of extruding dregs porcelain granule samples point
It Tou Ru not be screened using vibrating screen in screening plant, remove fine powder, impregnated, the X part extruding dregs porcelain granule sample that will remove fine powder divides
Do not hold immersion, soaking time is 12-20 hours, stirred three hours after immersion, after stirring by standing one hour,
Extruding dregs porcelain granule screening sample is taken out mud powder and other impurities by user, clod impregnate in it is soluble in water, stir so that clod
Dissolution it is more thorough, further facilitated the use of user.
Specific embodiment
Below in conjunction with the embodiment of the present invention, technical solution in the embodiment of the present invention is clearly and completely retouched
It states, it is clear that described embodiments are only a part of the embodiments of the present invention, instead of all the embodiments.Based on the present invention
In embodiment, every other implementation obtained by those of ordinary skill in the art without making creative efforts
Example, shall fall within the protection scope of the present invention.
A kind of embodiment one: inspection method for preparing extruding dregs porcelain granule and detecting clod content in the process, comprising the following steps:
1) sample is chosen, X parts, the Xn that is denoted as X1, X2, X3 ... are chosen from the extruding dregs porcelain granule prepared, is placed respectively
It is spare in container；
2) X parts of extruding dregs porcelain granule samples are weighed weight respectively, obtain weight and be recorded as N1, N2, N3 ... by weighing screening
X parts of extruding dregs porcelain granule samples are put into screening plant respectively, are screened using vibrating screen by Nn, remove fine powder；
3) it impregnates, the X part extruding dregs porcelain granule sample for removing fine powder is held into immersion respectively, soaking time is 12-20 hours,
Stirred three hours after immersion, after stirring by standing one hour, it is spare；
4) it filters, will be filtered in X part extruding dregs porcelain granule sample investment filter plant of immersion, persistently stir, obtain in filtering
Turbid solution is filtered to X parts of extruding dregs porcelain granule samples；
5) drying and dewatering in X parts of extruding dregs porcelain granule sample filtering turbid solution investment drying equipments is obtained X by drying and dewatering
The dry mud of part, takes out spare；
6) the dry mud of X part that step 5 obtains is placed on meausring apparatus and is weighed, obtained weight and be recorded as Y1, Y2, Y3 ...
Yn；
7) it calculates, calculates clod content Z in extruding dregs porcelain granule, in respect of Z1=Y1/N1*100%, Z2=Y2/N2*100%,
Z3=Y3/N3*100% ... Zn=Yn/Nn*100%, Z=(Z2+Z3 ...+Zn-1)/(n-2), Z are required extruding slag
Clod content in haydite.
1X parts of extruding dregs porcelain granule samples of step, X are more than or equal to 4, and the weight of every part of extruding dregs porcelain granule sample is not less than 10,000
Gram.
Step 2 puts into X parts of extruding dregs porcelain granule samples in screening plant respectively, and the screen number that screening plant is arranged is eight
Ten mesh.
The X part extruding dregs porcelain granule sample for removing fine powder is held immersion by step 3 respectively, impregnates extruding dregs porcelain granule sample and water
Weight ratio be 1:1.5, water is distilled water, and stirring frequency is 60 turns per minute, and container is sealing container.
It is 200 mesh that step 4, which filters turbid solution using the filter hole mesh number of filter device,.
It requires thoroughly to clean before every use using each equipment in detection process, weighs unit and precisely arrive milligram, walk
It is 80 degrees Celsius that drying temperature is arranged in rapid 5 drying and dewatering.
It is 200 mesh that turbid solution, which is filtered, using the filter hole mesh number of filter device, and the filter hole of 200 mesh can prevent extruding
Non- mud particle in dregs porcelain granule is mixed into, and testing result is avoided to be affected.
A kind of embodiment two: inspection method for preparing extruding dregs porcelain granule and detecting clod content in the process, comprising the following steps:
1) sample is chosen, X parts, the Xn that is denoted as X1, X2, X3 ... are chosen from the extruding dregs porcelain granule prepared, is placed respectively
It is spare in container；
2) X parts of extruding dregs porcelain granule samples are weighed weight respectively, obtain weight and be recorded as N1, N2, N3 ... by weighing screening
X parts of extruding dregs porcelain granule samples are put into screening plant respectively, are screened using vibrating screen by Nn, remove fine powder；
3) it impregnates, the X part extruding dregs porcelain granule sample for removing fine powder is held into immersion respectively, soaking time is 12-20 hours,
Stirred three hours after immersion, after stirring by standing one hour, it is spare；
4) it filters, will be filtered in X part extruding dregs porcelain granule sample investment filter plant of immersion, persistently stir, obtain in filtering
Turbid solution is filtered to X parts of extruding dregs porcelain granule samples；
5) drying and dewatering in X parts of extruding dregs porcelain granule sample filtering turbid solution investment drying equipments is obtained X by drying and dewatering
The dry mud of part, takes out spare；
6) the dry mud of X part that step 5 obtains is placed on meausring apparatus and is weighed, obtained weight and be recorded as Y1, Y2, Y3 ...
Yn；
7) it calculates, calculates clod content Z in extruding dregs porcelain granule, in respect of Z1=Y1/N1*100%, Z2=Y2/N2*100%,
Z3=Y3/N3*100% ... Zn=Yn/Nn*100%, Z=(Z2+Z3 ...+Zn-1)/(n-2), Z are required extruding slag
Clod content in haydite.
1X parts of extruding dregs porcelain granule samples of step, X are more than or equal to 4, and the weight of every part of extruding dregs porcelain granule sample is not less than 10,000
Gram.
Step 2 puts into X parts of extruding dregs porcelain granule samples in screening plant respectively, and the screen number that screening plant is arranged is eight
Ten mesh.
The X part extruding dregs porcelain granule sample for removing fine powder is held immersion by step 3 respectively, impregnates extruding dregs porcelain granule sample and water
Weight ratio be 1:1.5, water is distilled water, and stirring frequency is 60 turns per minute, and container is sealing container.
It is 200 mesh that step 4, which filters turbid solution using the filter hole mesh number of filter device,.
It requires thoroughly to clean before every use using each equipment in detection process, weighs unit and precisely arrive milligram, walk
It is 80 degrees Celsius that drying temperature is arranged in rapid 5 drying and dewatering.
X parts of extruding dregs porcelain granule samples, X are more than or equal to 4, and the weight of every part of extruding dregs porcelain granule sample is not less than ten kilograms, inspection
Test sample is originally more, and testing result is more accurate, and detection sample weight is bigger, and testing result is more accurate.
A kind of embodiment three: inspection method for preparing extruding dregs porcelain granule and detecting clod content in the process, comprising the following steps:
1) sample is chosen, X parts, the Xn that is denoted as X1, X2, X3 ... are chosen from the extruding dregs porcelain granule prepared, is placed respectively
It is spare in container；
2) X parts of extruding dregs porcelain granule samples are weighed weight respectively, obtain weight and be recorded as N1, N2, N3 ... by weighing screening
X parts of extruding dregs porcelain granule samples are put into screening plant respectively, are screened using vibrating screen by Nn, remove fine powder；
3) it impregnates, the X part extruding dregs porcelain granule sample for removing fine powder is held into immersion respectively, soaking time is 12-20 hours,
Stirred three hours after immersion, after stirring by standing one hour, it is spare；
4) it filters, will be filtered in X part extruding dregs porcelain granule sample investment filter plant of immersion, persistently stir, obtain in filtering
Turbid solution is filtered to X parts of extruding dregs porcelain granule samples；
5) drying and dewatering in X parts of extruding dregs porcelain granule sample filtering turbid solution investment drying equipments is obtained X by drying and dewatering
The dry mud of part, takes out spare；
6) the dry mud of X part that step 5 obtains is placed on meausring apparatus and is weighed, obtained weight and be recorded as Y1, Y2, Y3 ...
Yn；
7) it calculates, calculates clod content Z in extruding dregs porcelain granule, in respect of Z1=Y1/N1*100%, Z2=Y2/N2*100%,
Z3=Y3/N3*100% ... Zn=Yn/Nn*100%, Z=(Z2+Z3 ...+Zn-1)/(n-2), Z are required extruding slag
Clod content in haydite.
1X parts of extruding dregs porcelain granule samples of step, X are more than or equal to 4, and the weight of every part of extruding dregs porcelain granule sample is not less than 10,000
Gram.
Step 2 puts into X parts of extruding dregs porcelain granule samples in screening plant respectively, and the screen number that screening plant is arranged is eight
Ten mesh.
The X part extruding dregs porcelain granule sample for removing fine powder is held immersion by step 3 respectively, impregnates extruding dregs porcelain granule sample and water
Weight ratio be 1:1.5, water is distilled water, and stirring frequency is 60 turns per minute, and container is sealing container.
It is 200 mesh that step 4, which filters turbid solution using the filter hole mesh number of filter device,.
It requires thoroughly to clean before every use using each equipment in detection process, weighs unit and precisely arrive milligram, walk
It is 80 degrees Celsius that drying temperature is arranged in rapid 5 drying and dewatering.
The weight ratio for impregnating extruding dregs porcelain granule sample and water is 1:1.5, and water is distilled water, and stirring frequency is per minute 60
Turn, container is sealing container, and sufficient water guarantees that clod is dissolved in water and will not be saturated precipitating, and distilled water free from admixture will not shadow
Testing result is rung, sealing container avoids introduced contaminants from being mixed into.
The beneficial effects of the present invention are: detecting the inspection method of clod content during the preparation extruding dregs porcelain granule, pass through
Filtering will filter in X part extruding dregs porcelain granule sample investment filter plant of immersion, persistently stir in filtering, obtain X parts of extruding slags
Haydite sample filters turbid solution, and drying and dewatering is de- by drying in X parts of extruding dregs porcelain granule sample filtering turbid solution investment drying equipments
Water obtains X parts of dry mud, and taking-up is spare, and the dry mud of X part that step 5 obtains is placed on meausring apparatus and is weighed, and obtains weight record
It for Y1, Y2, Y3 ... Yn, calculates, clod content Z in extruding dregs porcelain granule is calculated, in respect of Z1=Y1/N1*100%, Z2=Y2/
N2*100%, Z3=Y3/N3*100% ... Zn=Yn/Nn*100%, Z=(Z2+Z3 ...+Zn-1)/(n-2), Z are institute
The clod content in extruding dregs porcelain granule is sought, the result that the result COMPREHENSIVE CALCULATING of multiple sample detection obtains is more accurate, eliminates
The worry of user, the use for the person of being convenient to use choose X parts, note by choosing sample from the extruding dregs porcelain granule prepared
For X1, X2, X3 ... Xn, it is individually positioned in spare in container, weighing screening weighs X part extruding dregs porcelain granule samples again respectively
Amount, obtains weight and is recorded as N1, N2, N3 ... Nn, X parts of extruding dregs porcelain granule samples are put into screening plant respectively, use vibration
Dynamic sieve screening, removes fine powder, impregnates, the X part extruding dregs porcelain granule sample for removing fine powder is held immersion respectively, soaking time is
12-20 hours, stirred three hours after immersion, after stirring by standing one hour, user is by extruding dregs porcelain granule sample
Mud powder and other impurities are taken out in this screening, clod impregnate in it is soluble in water, stir so that the dissolution of clod is more thorough, further
The use for the person of being convenient to use solves the detection that traditional detection method detection is not suitable for extruding dregs porcelain granule, testing result
It is more coarse, it is not very accurate problem.
It although an embodiment of the present invention has been shown and described, for the ordinary skill in the art, can be with
A variety of variations, modification, replacement can be carried out to these embodiments without departing from the principles and spirit of the present invention by understanding
And modification, the scope of the present invention is defined by the appended.
Claims (6)
1. a kind of inspection method for preparing extruding dregs porcelain granule and detecting clod content in the process, which comprises the following steps:
1) sample is chosen, X parts, the Xn that is denoted as X1, X2, X3 ... are chosen from the extruding dregs porcelain granule prepared, is individually positioned in appearance
It is spare in device；
2) X parts of extruding dregs porcelain granule samples are weighed weight respectively, obtain weight and be recorded as N1, N2, N3 ... Nn by weighing screening,
X parts of extruding dregs porcelain granule samples are put into screening plant respectively, are screened using vibrating screen, fine powder is removed；
3) it impregnates, the X part extruding dregs porcelain granule sample for removing fine powder is held into immersion respectively, soaking time is 12-20 hours, is impregnated
After stir three hours, after stirring by standing one hour, it is spare；
4) it filters, will be filtered in X part extruding dregs porcelain granule sample investment filter plant of immersion, persistently stirred in filtering, obtain X parts
Extruding dregs porcelain granule sample filters turbid solution；
5) drying and dewatering in X parts of extruding dregs porcelain granule sample filtering turbid solution investment drying equipments is obtained X parts and done by drying and dewatering
Mud takes out spare；
6) the dry mud of X part that step 5 obtains is placed on meausring apparatus and is weighed, obtain weight and be recorded as Y1, Y2, Y3 ... Yn；
7) it calculates, clod content Z in extruding dregs porcelain granule is calculated, in respect of Z1=Y1/N1*100%, Z2=Y2/N2*100%, Z3=
Y3/N3*100% ... Zn=Yn/Nn*100%, Z=(Z2+Z3 ...+Zn-1)/(n-2), Z are required extruding dregs porcelain granule
In clod content.
2. a kind of inspection method for preparing extruding dregs porcelain granule and detecting clod content in the process according to claim 1, special
Sign is: X described in step 1 parts of extruding dregs porcelain granule sample, and X is more than or equal to 4, and the weight of every part of extruding dregs porcelain granule sample is not less than ten
Kilogram.
3. a kind of inspection method for preparing extruding dregs porcelain granule and detecting clod content in the process according to claim 1, special
Sign is: putting into screening plant X parts of extruding dregs porcelain granule samples respectively described in step 2, the screen number of screening plant is arranged
For 80 mesh.
4. a kind of inspection method for preparing extruding dregs porcelain granule and detecting clod content in the process according to claim 1, special
Sign is: described in step 3 the X part extruding dregs porcelain granule sample for removing fine powder being held immersion respectively, impregnates extruding dregs porcelain granule sample
Weight ratio with water is 1:1.5, and water is distilled water, and stirring frequency is 60 turns per minute, and container is sealing container.
5. a kind of inspection method for preparing extruding dregs porcelain granule and detecting clod content in the process according to claim 1, special
Sign is: filtering turbid solution described in step 4 is 200 mesh using the filter hole mesh number of filter device.
6. a kind of inspection method for preparing extruding dregs porcelain granule and detecting clod content in the process according to claim 1, special
Sign is: requiring thoroughly to clean before every use using each equipment in detection process, weighs unit and precisely arrive milligram, step
It is 80 degrees Celsius that drying temperature is arranged in 5 drying and dewaterings.
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN117607469A (en) * | 2024-01-19 | 2024-02-27 | 陕西延长石油压裂材料有限公司 | Automatic detection method for quality of finished ceramsite sand |
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| 中国国家标准化管理委员会: "《GB/T 17431.2-2010 轻集料及其试验方法 第2部分：轻集料试验方法》", 26 September 2010 * |
| 廖林清等: "《机械设计方法学》", 31 August 1996 * |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN117607469A (en) * | 2024-01-19 | 2024-02-27 | 陕西延长石油压裂材料有限公司 | Automatic detection method for quality of finished ceramsite sand |
| CN117607469B (en) * | 2024-01-19 | 2024-04-02 | 陕西延长石油压裂材料有限公司 | Automatic detection method for quality of finished ceramsite sand |
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