CN109930376A - Multi-functional printing and dyeing additive intermediate of one kind and preparation method thereof - Google Patents
Multi-functional printing and dyeing additive intermediate of one kind and preparation method thereof Download PDFInfo
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- CN109930376A CN109930376A CN201910209122.4A CN201910209122A CN109930376A CN 109930376 A CN109930376 A CN 109930376A CN 201910209122 A CN201910209122 A CN 201910209122A CN 109930376 A CN109930376 A CN 109930376A
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Abstract
The invention discloses a kind of multi-functional printing and dyeing additive intermediates and preparation method thereof, the multi-functional printing and dyeing additive intermediate being prepared has the multiple performances such as excellent hydrotropy, washing, infiltration, dispersion, chelating, efficient impurity removal is merged, deoils, removal floating color, go the multiple functions such as (water) hardness, concise, desizing, bleaching simultaneously, there is excellent using effect.
Description
Technical field
The present invention relates to the dyeing and finishing processing technique field of fabric, more particularly to a kind of multi-functional printing and dyeing additive
Intermediate and preparation method thereof.
Background technique
The pre-treatment and printing and dyeing post-processing of textile mainly include kiering, bleaching, desizing of fabric etc. and dyed fabric
It soaps the processes such as removal floating color, these manufacturing procedures include the effect of removal of impurities, as removed lignin, cotton wax, cotton on cotton fabric
Seed shell, weaving starching, pigment, not fixed dyestuff etc..
And in order to reach processing purpose, in above-mentioned various processes often need addition different function auxiliary agent, as bleeding agent,
Detergent, scouring agent, chelated dispersants, desizing agent, soaping agent etc., but can influence each other between different auxiliary agents, cause auxiliary agent
Function and effect decline, corresponding impurity-eliminating effect is not achieved.Also, existing auxiliary agent functionality is single, necessary in use process
It is used in conjunction with each other with other type auxiliary agents, to cause production process complicated for operation.Importantly, existing functionality helps
Agent using effect is unsatisfactory, so causing each production process that can not achieve the effect that removal of impurities.
Therefore it provides a kind of multi-functional printing and dyeing additive intermediate and preparation method thereof is that those skilled in the art need to solve
Certainly the problem of.
Summary of the invention
In view of this, being prepared the present invention provides a kind of multi-functional printing and dyeing additive intermediate and preparation method thereof
Multi-functional printing and dyeing additive intermediate there are the multiple performances such as excellent hydrotropy, washing, infiltration, dispersion, chelating, merge simultaneously
Efficient impurity removal deoils, removal floating color, goes the multiple functions such as (water) hardness, concise, desizing, bleaching, has excellent using effect.
To achieve the goals above, the present invention adopts the following technical scheme:
A kind of multi-functional printing and dyeing additive intermediate, which is characterized in that the component including following parts by weight: 20~40 parts
Water, 0.1~2 part of cheating components, 1~15 part of infiltration component, 5~25 parts of dispersion and emulgate ingredient, 5~20 parts net
Wash component, 10~20 parts of esters component and 5~15 parts of organic solvent constituent.
The beneficial effect of above-mentioned optimal technical scheme is: the present invention complements each other to form multi-functional printing and dyeing by each component
Additive intermediate, has excellent stability, and raw material selectivity is high, it is often more important that has excellent hydrotropy, washing, infiltration
Thoroughly, the multiple performances such as disperse, chelate, fusion efficient impurity removal, deoil, removal floating color, to go (water) hardness, concise, desizing, bleaching etc. more
Kind function.
Preferably, the water includes deionized water.
Preferably, the cheating components include one of citric acid, sodium citrate or sodium gluconate or a variety of mixed
Close object.
The beneficial effect of above-mentioned optimal technical scheme is: the cheating components that the present invention is added can reduce calcium and magnesium in printing and dyeing water
The problems such as content of the substances such as iron prevents uneven dyeing, and bleaching effect is bad.
Preferably, the infiltration component includes one of sodium secondary alkyl sulfonate, fast penetrant T or alkyl glycosides or more
The mixture of kind.
The beneficial effect of above-mentioned optimal technical scheme is: the infiltration component that the present invention is added can reduce fiber surface tension,
Swollen fiber increases permeability, and auxiliary agent dyestuff is enabled preferably to go deep into fibrous inside.
Preferably, the dispersion and emulgate ingredient include isomerous tridecanol polyoxyethylene ether, it is fatty alcohol polyoxyethylene ether, different
In structure tridecanol polyoxyethylene ether, tallow amine polyoxyethylene ether, fatty acid methyl ester ethoxylate or alkyl polyoxyethylene ether
One or more mixtures.
The beneficial effect of above-mentioned optimal technical scheme is: the dispersion and emulgate ingredient that the present invention is added can help fabric to move back
Slurry and oil removing in the liquid phase by the grease removed from fabric and pulp separation are easily removed.
Preferably, the washing component includes fatty alcohol-ether sodium sulfate, fatty acid methyl ester ethoxylate sulfonate, 12
One of sodium alkyl benzene sulfonate or lauryl sodium sulfate or a variety of mixtures.
The beneficial effect of above-mentioned optimal technical scheme is: the washing component that the present invention is added has concise and effect of soaping,
The impurity such as the hydrolised dye that fabric surface can be made to adhere to and the cured matter of grease are washed down, and increase cleanliness and the color jail of fabric
Degree.
Preferably, the esters component includes glycerin polyoxyethylene ether trioleate, Ergol, anhydrous sorbitol three
One of oleate, anhydrous sorbitol laurate or diglycol benzoic ether or a variety of mixtures.
The beneficial effect of above-mentioned optimal technical scheme is: the esters component that the present invention is added has swelling action, helps to help
Agent dyestuff enters fibrous inside, while reducing dyestuff dyeing rate, has the function of moving dye level dyeing.
Preferably, the organic solvent constituent includes in ethyl alcohol, isopropanol, ethylene glycol monobutyl ether or butyl cellosolve
One or more mixtures.
The beneficial effect of above-mentioned optimal technical scheme is: the solvent that the present invention is added has dissolves grease and dye to a certain degree
The function of material can make to form homogeneous system between intermediate different component convenient for removing, and increase water solubility, be easy to use.
The invention also discloses a kind of preparation methods of multi-functional printing and dyeing additive intermediate, specifically comprise the following steps:
(1) according to multi-functional printing and dyeing intermediate as disclosed above, each raw material for standby is weighed；
(2) it first warms the water to 40~60 DEG C, cheating components is added, then stir 15-30min to being uniformly mixed；
(3) it is then warming up to 60-70 DEG C, infiltration component, dispersion and emulgate ingredient, washing component are then added while stirring
With esters component, and in 60~70 DEG C of stirring 1-2h；
(4) it is eventually adding organic solvent constituent, is stirred evenly, is cooled to 40~50 DEG C, discharging obtains the Multifunctional Printing
Contaminate additive intermediate.
The beneficial effect of above-mentioned optimal technical scheme is: the preparation method technique of the printing and dyeing additive intermediate in the present invention
Simply, preparation is convenient, and the stability for the printing and dyeing additive intermediate being prepared is good.Wherein, it is first added in water soluble easily in water
Cheating components, stabilizing water quality；Then infiltration component, dispersion and emulgate ingredient, washing component and esters group are added after heating up
Point, the dissolubility mobility that said components can be improved is convenient uniformly mixed；Said components can be made more by being eventually adding organic solvent
Good is compatible, is uniformly mixed, forms homogeneous system.
It can be seen via above technical scheme that compared with prior art, the present disclosure provides a kind of multi-functional printing and dyeing
Additive intermediate and preparation method thereof, has the following beneficial effects:
(1) multi-functional printing and dyeing additive intermediate disclosed by the invention has excellent hydrotropy, washing, infiltration, dispersion, chela
The multiple performances such as conjunction, while merging efficient impurity removal, deoil, removal floating color, remove a variety of function such as (water) hardness, concise, desizing, bleaching
Can, there is excellent using effect；
(2) multi-functional printing and dyeing additive intermediate disclosed by the invention by be used alone or with other auxiliary agent synergistic applications
It can effectively realize or strengthen the desizing of fabric, processing effect that is concise, multiple links such as bleaching, soap；
(3) multi-functional printing and dyeing additive intermediate disclosed by the invention can not only be realized one multi-purpose, it is often more important that
The fusion perforation for realizing each process is pursued, a variety of processing purposes are completed with a kind of process, reach raising working efficiency, reduce life
Cost is produced, realizes the effect of energy-saving and emission-reduction；
(4) preparation method disclosed by the invention is simple to operate, is easy to carry out industrialized production.
Specific embodiment
The technical scheme in the embodiments of the invention will be clearly and completely described below, it is clear that described implementation
Example is only a part of the embodiment of the present invention, instead of all the embodiments.Based on the embodiments of the present invention, this field is common
Technical staff's every other embodiment obtained without making creative work belongs to the model that the present invention protects
It encloses.
The embodiment of the invention discloses a kind of multi-functional printing and dyeing additive intermediate, the components including following parts by weight: 20
~40 parts of water, 0.1~2 part of cheating components, 1~15 part of infiltration component, 5~25 parts of dispersion and emulgate ingredient, 5~20
The washing component, 10~20 parts of esters component and 5~15 parts of organic solvent constituent of part.
For further optimisation technique scheme, the water includes deionized water.
For further optimisation technique scheme, the cheating components include citric acid, sodium citrate or sodium gluconate
One of or a variety of mixtures.
For further optimisation technique scheme, the infiltration component includes sodium secondary alkyl sulfonate, fast penetrant T or alkane
One of base glucosides or a variety of mixtures.
For further optimisation technique scheme, it is described dispersion and emulgate ingredient include isomerous tridecanol polyoxyethylene ether,
Fatty alcohol polyoxyethylene ether, isomerous tridecanol polyoxyethylene ether, tallow amine polyoxyethylene ether, fatty acid methyl ester ethoxylate or
One of alkyl polyoxyethylene ether or a variety of mixtures.
For further optimisation technique scheme, the washing component includes fatty alcohol-ether sodium sulfate, fatty acid methyl ester second
One of oxygroup compound sulfonate, neopelex or lauryl sodium sulfate or a variety of mixtures.
For further optimisation technique scheme, the esters component includes glycerin polyoxyethylene ether trioleate, benzene first
One of acid benzyl ester, sorbitan trioleate, anhydrous sorbitol laurate or diglycol benzoic ether or
A variety of mixtures.
For further optimisation technique scheme, the organic solvent constituent includes ethyl alcohol, isopropanol, ethylene glycol monobutyl ether
Or one of butyl cellosolve or a variety of mixtures.
The embodiment of the invention also provides a kind of preparation methods of multi-functional printing and dyeing additive intermediate, specifically include as follows
Step:
(1) according to multi-functional printing and dyeing intermediate as described above, each raw material for standby is weighed；
(2) it first warms the water to 40~60 DEG C, cheating components is added, then stir 15-30min to being uniformly mixed；
(3) it is then warming up to 60-70 DEG C, infiltration component, dispersion and emulgate ingredient, washing component are then added while stirring
With esters component, and 1-2h is stirred under the conditions of 60~70 DEG C；
(4) it is eventually adding organic solvent constituent, is stirred evenly, is cooled to 40~50 DEG C, discharging obtains the Multifunctional Printing
Contaminate additive intermediate.
Embodiment 1
The embodiment of the present invention 1 discloses a kind of multi-functional printing and dyeing additive intermediate, the component including following parts by weight: 40
The water, 1 part of cheating components, 10 parts of infiltration component, 19 parts of dispersion and emulgate ingredient of part, 15 parts of washing component, 10 parts
Esters component and 5 parts of organic solvent constituent.
Wherein, water is deionized water；Cheating components are that citric acid and sodium citrate are answered with what the ratio of weight ratio 1:2 mixed
Close object；Infiltration component is sodium secondary alkyl sulfonate；Dispersion and emulgate ingredient are isomerous tridecanol polyoxyethylene ether and alkyl polyoxy second
The compound that alkene ether is mixed with the ratio of weight ratio 9:10；Washing group is divided into lauryl sodium sulfate；Esters group is divided into dehydration mountain
Pears alcohol trioleate (Span-85)；Organic solvent constituent is ethylene glycol monobutyl ether
The embodiment of the present invention 1 additionally provides a kind of preparation method of multi-functional printing and dyeing additive intermediate, specifically include as
Lower step:
(1) according to multi-functional printing and dyeing intermediate as described above, each raw material for standby is weighed；
(2) it first warms the water to 50 DEG C, cheating components is added, then stir 15min to being uniformly mixed；
(3) 65 DEG C are then warming up to, be then added while stirring infiltration component, dispersion and emulgate ingredient, washing component and
Esters component, and 1h is stirred under the conditions of 65 DEG C；
(4) it is eventually adding organic solvent constituent, is stirred evenly, is cooled to 40 DEG C, discharging obtains the multi-functional printing and dyeing and adds
Add agent intermediate.
Embodiment 2
The embodiment of the present invention 2 discloses a kind of multi-functional printing and dyeing additive intermediate, the component including following parts by weight: 30
The water, 2 parts of cheating components, 10 parts of infiltration component, 22 parts of dispersion and emulgate ingredient of part, 20 parts of washing component, 10 parts
Esters component and 6 parts of organic solvent constituent.
Wherein, water is deionized water；Cheating components are sodium citrate；Infiltration component is fast penetrant T；Dispersion and emulsification
Group is divided into the compound that isomerous tridecanol polyoxyethylene ether and alkyl polyoxyethylene ether are mixed with 1:1；Washing group is divided into dodecane
The compound that base benzene sulfonic acid sodium salt and lauryl sodium sulfate are mixed with 1:1；Esters group is divided into sorbitan trioleate
(Span-85)；Organic solvent constituent is butyl cellosolve.
The embodiment of the present invention 2 additionally provides a kind of preparation method of multi-functional printing and dyeing additive intermediate, specifically include as
Lower step:
(1) according to multi-functional printing and dyeing intermediate as described above, each raw material for standby is weighed；
(2) it first warms the water to 40 DEG C, cheating components is added, then stir 30min to being uniformly mixed；
(3) 70 DEG C are then warming up to, be then added while stirring infiltration component, dispersion and emulgate ingredient, washing component and
Esters component, and 1h is stirred under the conditions of 70 DEG C；
(4) it is eventually adding organic solvent constituent, is stirred evenly, is cooled to 40 DEG C, discharging obtains the multi-functional printing and dyeing and adds
Add agent intermediate.
Embodiment 3
The embodiment of the present invention 3 discloses a kind of multi-functional printing and dyeing additive intermediate, the component including following parts by weight: 30
The water, 0.5 part of cheating components, 15 parts of infiltration component, 25 parts of dispersion and emulgate ingredient of part, 20 parts of washing component, 10
The esters component and 9.5 parts of organic solvent constituent of part.
Wherein, water is deionized water；Cheating components are glucose；Infiltration component is sodium secondary alkyl sulfonate and quickly penetrating agent
The compound that T is mixed with 1:2；Dispersion and emulgate ingredient are isomerous tridecanol polyoxyethylene ether and fatty alcohol polyoxyethylene ether with 2:
3 mixed compounds；Washing group is divided into fatty alcohol-ether sodium sulfate；Esters group is divided into anhydrous sorbitol laurate；Organic solvent
Group is divided into ethyl alcohol
The embodiment of the present invention 3 additionally provides a kind of preparation method of multi-functional printing and dyeing additive intermediate, specifically include as
Lower step:
(1) according to multi-functional printing and dyeing intermediate as described above, each raw material for standby is weighed；
(2) it first warms the water to 60 DEG C, cheating components is added, then stir 15min to being uniformly mixed；
(3) 70 DEG C are then warming up to, be then added while stirring infiltration component, dispersion and emulgate ingredient, washing component and
Esters component, and 2h is stirred under the conditions of 70 DEG C；
(4) it is eventually adding organic solvent constituent, is stirred evenly, is cooled to 45 DEG C, discharging obtains the multi-functional printing and dyeing and adds
Add agent intermediate.
The reference of embodiment technique for applying:
One, pre-treating technology:
Fabric uses cotton grey cloth, and the multi-functional printing and dyeing additive intermediate that above-described embodiment 1~3 is prepared is configured to
Concentration is 1g/L, and hydrogen peroxide 5mL/L, NaOH 1g/L is then added, according to bath raio: 1:20, is warming up to 95 DEG C of constant temperature stirrings
After 30min, cold water is washed, and dries survey capillary effect, the results are shown in Table 1.
Capillary effect test: the cloth specimen to be measured after refined penetrant treating is cut into through the cloth 2 to 30cm, broadwise 5cm
Block has clip to clamp as heavy burden along broadwise pencil standardized line level marks at from one end 1cm under scribing line.Before measurement,
About 2 liter distilled water are added in the Storage water tank of capillary effect analyzer.Adjust horizontal instrument, adjustment liquid level and rod reading zero point
Alignment.Then increase crossbearer, sample cloth upper end be fixed on crossbearer with clip, and make its lower end pencil cross just with
The alignment of rod reading zero point.Crossbearer is declined together with scale and sample again, until rod reading zero point and horizontal face contact
Until, and open stopwatch immediately and start timing, the height (cm) that liquid rises when recording 30 minutes.As liquid lifting height is irregular
It is uneven, minimum should be read.
Two, it soaps technique:
Fabric: 5% (owf) active black XD-70R dyes cotton of not soaping, the print that above-described embodiment 1~3 is prepared
It is 1g/L that dye additive intermediate, which is configured to concentration, is 1:20 according to bath raio, after being warming up to 95 DEG C or more constant temperature stirring 20min,
Cold water is washed, and dries colour examining fastness, the results are shown in Table 1.
(dry) test of colour fastness to rubbing: referring to GB/T 3920-1997, " textile color stability tests rub resistance color jail
Degree ".
Fastness to soaping test: referring to GB/T 3921-2008 " textile color stability test fastness to soaping ".
Table 1
Blank sample in above-mentioned table 1 refers to the sample for not adding multi-functional printing and dyeing additive intermediate.
It can obviously be learnt by the above results: among the multi-functional printing and dyeing additive that the embodiment of the present invention 1~3 is prepared
Body can significantly improve the capillary effect of fabric, while significantly improve the fastness to soaping and colour fastness to rubbing of fabric, have excellent
Different using effect.
Each embodiment in this specification is described in a progressive manner, the highlights of each of the examples are with other
The difference of embodiment, the same or similar parts in each embodiment may refer to each other.For device disclosed in embodiment
For, since it is corresponded to the methods disclosed in the examples, so being described relatively simple, related place is said referring to method part
It is bright.
The foregoing description of the disclosed embodiments enables those skilled in the art to implement or use the present invention.
Various modifications to these embodiments will be readily apparent to those skilled in the art, as defined herein
General Principle can be realized in other embodiments without departing from the spirit or scope of the present invention.Therefore, of the invention
It is not intended to be limited to the embodiments shown herein, and is to fit to and the principles and novel features disclosed herein phase one
The widest scope of cause.
Claims (9)
1. a kind of multi-functional printing and dyeing additive intermediate, which is characterized in that the component including following parts by weight: 20~40 parts
Water, 0.1~2 part of cheating components, 1~15 part of infiltration component, 5~25 parts of dispersion and emulgate ingredient, 5~20 parts of washing
Component, 10~20 parts of esters component and 5~15 parts of organic solvent constituent.
2. the multi-functional printing and dyeing additive intermediate of one kind according to claim 1, which is characterized in that the water include go from
Sub- water.
3. the multi-functional printing and dyeing additive intermediate of one kind according to claim 1, which is characterized in that the cheating components packet
Include one of citric acid, sodium citrate or sodium gluconate or a variety of mixtures.
4. the multi-functional printing and dyeing additive intermediate of one kind according to claim 1, which is characterized in that the infiltration component packet
Include one of sodium secondary alkyl sulfonate, fast penetrant T or alkyl glycosides or a variety of mixtures.
5. the multi-functional printing and dyeing additive intermediate of one kind according to claim 1, which is characterized in that the dispersion and emulsification
Component includes isomerous tridecanol polyoxyethylene ether, fatty alcohol polyoxyethylene ether, isomerous tridecanol polyoxyethylene ether, tallow amine polyoxy
One of vinethene, fatty acid methyl ester ethoxylate or alkyl polyoxyethylene ether or a variety of mixtures.
6. the multi-functional printing and dyeing additive intermediate of one kind according to claim 1, which is characterized in that the washing group subpackage
Include fatty alcohol-ether sodium sulfate, fatty acid methyl ester ethoxylate sulfonate, neopelex or lauryl sodium sulfate
One of or a variety of mixtures.
7. the multi-functional printing and dyeing additive intermediate of one kind according to claim 1, which is characterized in that the esters group subpackage
Include glycerin polyoxyethylene ether trioleate, Ergol, sorbitan trioleate, anhydrous sorbitol laurate or one
One of diglycol ethylene benzoic ether or a variety of mixtures.
8. the multi-functional printing and dyeing additive intermediate of one kind according to claim 1, which is characterized in that the organic solvent group
Divide includes one of ethyl alcohol, isopropanol, ethylene glycol monobutyl ether or butyl cellosolve or a variety of mixtures.
9. a kind of preparation method of multi-functional printing and dyeing additive intermediate, which is characterized in that specifically comprise the following steps:
(1) multi-functional printing and dyeing intermediate described in any one according to claim 1~8, weighs each raw material for standby；
(2) it first warms the water to 40~60 DEG C, cheating components is added, then stir 15-30min to being uniformly mixed；
(3) it is then warming up to 60-70 DEG C, infiltration component, dispersion and emulgate ingredient, washing component and ester are then added while stirring
Class component, and 1-2h is stirred under the conditions of 60~70 DEG C；
(4) it is eventually adding organic solvent constituent, is stirred evenly, is cooled to 40~50 DEG C, discharging obtains the multi-functional printing and dyeing and adds
Add agent intermediate.
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN110284285A (en) * | 2019-07-04 | 2019-09-27 | 常州安达环保科技有限公司 | A kind of non-aqueous dyeing method of dacron |
| CN111733022A (en) * | 2020-07-21 | 2020-10-02 | 何结平 | Cleaning agent for printing and dyeing soaping and preparation method thereof |
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| CN105369613A (en) * | 2014-08-27 | 2016-03-02 | 浙江安诺其助剂有限公司 | Application of polyester fabric treating agent |
| CN105369612A (en) * | 2014-08-27 | 2016-03-02 | 浙江安诺其助剂有限公司 | Polyester fabric treating agent |
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| CN103952905A (en) * | 2014-05-13 | 2014-07-30 | 浙江丝科院轻纺材料有限公司 | One-bath multifunctional treating agent and preparation method thereof |
| CN105369613A (en) * | 2014-08-27 | 2016-03-02 | 浙江安诺其助剂有限公司 | Application of polyester fabric treating agent |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN110284285A (en) * | 2019-07-04 | 2019-09-27 | 常州安达环保科技有限公司 | A kind of non-aqueous dyeing method of dacron |
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