CN109925184B - Nanometer thermal massage paste body, plaster and preparation method - Google Patents
Nanometer thermal massage paste body, plaster and preparation method Download PDFInfo
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Abstract
The invention discloses a nanometer thermal massage paste body, a patch, a paste and a preparation method. A nanometer thermal massage paste body has ball beads with diameter of 1-9 mm. A nanometer thermal massage patch comprises a substrate layer, a substrate layer and a protective layer, wherein the substrate layer is a paste body, the substrate layer comprises a non-woven fabric with self-adhesive on one side, an impermeable pearlized film, a rubber or foam leak-proof sealing ring, and the protective layer comprises a silk screen non-woven fabric and release paper. A nanometer thermal massage cream is prepared by cooling paste body, and packaging. The nanometer moxibustion ointment or the nanometer moxibustion patch is suitable for use in physiotherapy departments of hospitals, clinics of traditional Chinese medicine, health preserving halls, massage homes and families, and has large market demands; the raw materials used in the production are commercial products, are easy to purchase, and are suitable for industrial mass production.
Description
Technical Field
The invention relates to the technical field of manufacturing of externally-applied paste and paste products for human bodies, in particular to a nanometer thermal massage paste mud body, a paste and a preparation method thereof.
Background
1. Along with the development of market economy and the gradual improvement of the physical and living standard of people and the health requirement of people, various health care massage is generated, the health care massage refers to stimulation information generated by operating at proper parts of a human body, the nerve and body fluid adjusting function of the human body is influenced by a reflection mode, and the health care massage can not only condition the health of people, but also relax the mood and relieve fatigue of people, thereby achieving the purposes of enhancing health care physique and conditioning and relieving various sub-health symptoms;
And (3) hot compress sticking: also called as heating patches and warming patches, with continuous intensive research on hot compress patches, the hot compress patches are widely used for physical therapy, health care and alleviation of various symptoms. Chinese patent 201410019889.8 is a Chinese medicinal hot compress patch for improving microcirculation and relieving pain, and can generate heat within about 5-10 minutes after the product is unsealed, wherein the temperature of the generated heat is 40-55 ℃ and the duration is 10-15 hours; the Chinese patent 201420684248.X, a self-heating magnetic moxibustion plaster, wherein one of two materials of carbon powder or iron powder is placed in the self-heating bag, when in use, the oxygen-insulating plaster at the bottom of the self-heating bag is uncovered, and the medicine bag is adhered to the bottom and attached to the affected part or acupoint of human body; the traditional Chinese medicine hot compress patch or moxibustion patch adopts iron powder heating bag made of iron powder, active carbon, salt, etc.;
external application paste: chinese patent 201510770850.4A Chinese medicinal hot compress agent and its preparation and application method, the preparation method comprises: grinding the raw materials into powder according to a certain proportion, and wetting with water, wherein the ratio of the powder to the water is 10 (1-2). The using method comprises the following steps: the Chinese medicinal hot compress paste is applied on the skin surface of patient, and hot compressed for 1 half an hour at 45-50deg.C. The traditional Chinese medicine hot compress medicament is a manually controlled hot compress medicament;
1. The existing external paste, traditional Chinese medicine hot compress paste or medicinal moxibustion paste product for human body does not have the defect of synchronous conditioning function with massage at the moxibustion applying position during spreading or applying human body moxibustion therapy, and the external paste, traditional Chinese medicine hot compress paste or medicinal moxibustion paste product for synchronous conditioning of human body by using fingering and palm massage has yet to be developed;
2. the existing traditional Chinese medicine hot compress patch or medicinal moxibustion patch heats an iron powder heating bag made of materials such as iron powder, active carbon, salt and the like, and the iron powder heating bag is not suitable for application of fingering and palm massage patches; the traditional Chinese medicine hot compress medicament with artificial temperature control can not keep comfortable constant temperature for a long time, the use method is inconvenient, the traditional Chinese medicine hot compress medicament is not suitable for the application of massage cream using fingering and palm massage, and new products are to be developed;
therefore, there is a need for a thermal massage paste which can produce comfortable thermal sensation on skin, has long thermal sensation time and promotes blood circulation without using an iron powder heating bag and a hot compress paste without manually controlling the temperature, and then the thermal massage paste is prepared into a patch or paste which can be used for finger or palm massage at moxibustion application positions when the thermal massage paste is spread or applied to a human body for moxibustion.
2. Publication of:
1. ball application material publication:
the application of the stone needle therapy in clinic and household preventive care is increasingly wide, the stone needle therapy is one of external treatment methods of traditional Chinese medicine, and the action part of the stone needle is mainly on the skin by taking the traditional Chinese medicine theory, especially the meridian theory as guidance, so that the meridian leather theory has a more direct guidance effect on the stone needle therapy. The concept and the function of the six percutaneous parts are analyzed, so that the application rule of the theory of the percutaneous parts in the stone needle therapy is explained initially, and the meridian theory is guided to further supplement the stone needle therapy.
The scientific research of national medicine report/2007/3 month/23 day/002 edition of medicine service Chen Shutang negative ions of Chinese awareness network negative ions and health care effects thereof proves that the negative ions in the air have good medical care functions on human bodies. Because it can directly act on promoting metabolism and relieving fatigue, etc.; negative ion powder such as chinese patent: 201210009268.2 ion powder of coral fossil, tourmaline, opal, serpentine, maifanitum, QIBINGSHI, north America stone, yiwangshi, shell, diatomaceous earth, ferric oxide, aluminum oxide, zirconium oxide and zirconium phosphate is prepared, and can be used for health product and cosmetic;
2. adsorption support application material publication:
(1) Attapulgite: the attapulgite clay used in the medicine and the pharmaceutical preparation of Changsha 410013 in China university medical college and applied to China has the advantages of absorption, rheological property and no toxicity to human bodies, and can be used as auxiliary materials.
(2) Rectorite: soil therapy in China, guangdong microelement science, volume 19, phase 1 article number 1006 4476X (2012) 01 0001 20 rectorite, in the medical treatment, is such as the lubricity, thermal stability and high temperature resistance of mica layers, the hydrophilicity, expansibility, colloid, suspension, adsorptivity, cation exchange and the like of montmorillonite. Swelling with water, and can be dissociated into paste. In addition, the composition also contains a plurality of elements beneficial to human bodies, such as Si, ca, mg, na, S, P, fe, zn, se, co, sr, la and the like;
3. Thermal agent publication for thermal substrates: the Chinese known network analyzer 2014 high performance liquid chromatography is used for measuring a thermal sensitizer (also called a thermal sensitizer in Guangzhou market quality supervision and detection institute) in a personal care product, wherein the thermal sensitizer is added to enable the product to generate thermal feeling on skin and enable a human body to feel comfortable, and the common thermal sensitizer comprises gingerol (zingerone) and vanillyl butyl ether (vanilly butyl ether) which are natural thermal sensitizer substitutes and can not burn skin.
4. Ultrasonic Chinese medicinal extract disclosure: for example, chinese patent application No. 201210260414.9 is a novel mud therapy product for external application and heating of human body and application thereof; the preparation method comprises the steps of conditioning and relieving difficult joint pain symptoms such as cervical spondylosis, scapulohumeral periarthritis, lumbar disc herniation, rheumatism, wind-damp type arthritis, hyperosteogeny and the like, and extracting and concentrating the traditional Chinese medicine raw materials by ultrasonic to obtain extract;
5. essential oil antioxidant and antibacterial disclosure:
(1) Chinese knowledge net bloo paper classification No.: s482.2, the synergistic effect of various antibacterial components of the lavender essential oil in researching the oxidation resistance and antibacterial activity of the lavender essential oil in the university of stone river endows the essential oil with stronger antibacterial effect, and the lavender essential oil has good oxidation resistance as the common antioxidants;
(2) Chinese learning net (journal), social science II; engineering science and technology I, light industry, handindustry; antibacterial action of shallow-analysis tea polyphenols at 2012.36 and antioxidation function of Changchun university of life sciences of Changchun university of medical university of Changchun university of life sciences were: the primary purpose of this document is to elucidate the bacteriostatic and antioxidant functions of tea polyphenols in combination with recent decade of research clues on tea polyphenols. The main content comprises: the physicochemical properties of tea polyphenols are briefly described; the bacteriostasis and antioxidation functions of tea polyphenol are described.
Disclosure of Invention
In order to overcome the defects of the prior art, the invention provides a nanometer thermal massage paste body, and then the paste body is prepared into a patch or a paste which can be used for massaging finger and palm at a moxibustion position when the paste body is spread or applied to a human body for moxibustion therapy and a preparation method.
The invention adopts the following technical scheme:
1. a nanometer thermal massage paste body has ball beads with diameter of 1-9 mm.
A nanometer thermal massage patch comprises a substrate layer, a substrate layer and a protective layer, wherein the substrate layer is a paste body, the substrate layer comprises a non-woven fabric with self-adhesive on one side, an impermeable pearlized film, rubber or foam leak-proof sealing ring, and the protective layer comprises a silk screen non-woven fabric and release paper;
The non-woven fabric with the self-adhesive on one side is adhered with an anti-seepage pearlescent film, the part of the non-woven fabric with the self-adhesive on the other side, which is positioned outside the anti-seepage pearlescent film, is an adhesive area, rubber or foam anti-leakage sealing rings are adhered on the anti-seepage pearlescent film, a matrix layer is arranged in the rubber or foam anti-leakage sealing rings, and the height of the matrix layer is the same as that of the rubber or foam anti-leakage sealing rings;
the matrix layer is coated with silk screen non-woven fabric, the silk screen non-woven fabric is adhered to the rubber or foam leak-proof sealing ring, and the release paper is adhered to a self-adhesive area reserved on the non-woven fabric with self-adhesive on one side.
A nanometer thermal massage cream is prepared by cooling and packaging paste body with 1-9mm diameter ball beads.
2. The preparation method of the invention comprises the following steps:
1. the balls with the diameter of 1-9mm are preferably nano ceramic balls or nano plastic balls:
A. the preparation method of the nano ceramic ball comprises the following steps:
grinding: grinding stone needle powder, anion powder, far infrared powder, germanite powder, tourmaline powder and magnetite powder respectively by using a grinder until the powder particle size is less than 100 nanometers;
and (3) batching: taking one or more of 35-75 parts of stone needle powder, 10-60 parts of negative ion powder, 10-60 parts of far infrared powder, 10-60 parts of germanite powder, 10-60 parts of tourmaline powder and 10-60 parts of magnetite powder by weight, and then adding 18-28% of silicon dioxide by the total mass of the ingredients by weight;
Sintering: sintering into nano ceramic balls with the diameter of 1-9mm by using a ceramic sintering furnace and a ceramic sintering process;
B. the preparation method of the nano plastic ball bead comprises the following steps:
grinding: grinding stone needle powder, anion powder, far infrared powder, germanite powder, tourmaline powder and magnetite powder respectively by using a grinder until the powder particle size is less than 100 nanometers;
and (3) batching: taking ground nanoscale powder, adding one or more of 30-65 parts by weight of stone needle powder, 10-60 parts by weight of negative ion powder, 10-60 parts by weight of far infrared powder, 10-60 parts by weight of germanite powder, 10-60 parts by weight of tourmaline powder and 10-60 parts by weight of magnetite powder, and adding 25-30% by weight of polyvinyl chloride (pvc) or polypropylene (pp) or high-density polyethylene (HDPE) and 3-5% by weight of triethyl citrate or epoxidized soybean oil;
and (3) forming: plasticizing and fusing the ingredients, and making plastic balls into nano plastic balls with the diameter of 1-9mm by a plastic ball forming machine;
2. preparation of adsorption carrier:
grinding: grinding attapulgite and rectorite respectively by using a grinder until the particle size of the attapulgite and rectorite is less than 100 nanometers;
and (3) batching: taking ground attapulgite and rectorite nanoscale powder, and stirring and mixing;
and (3) sterilization: the mixed nano-scale powder is sterilized by an ionizing radiation sterilization method at the sterilization temperature of 50-90 ℃ for 40-60 minutes to obtain the adsorption carrier of the nano-scale powder of rectorite and attapulgite for standby;
3. The heat sensitive matrix is one or two of gingerol and vanillyl butyl ether;
4. chinese herbal medicine extract: an ultrasonic traditional Chinese medicine extract obtained by adopting an ultrasonic traditional Chinese medicine extraction method is an external treatment prescription permitted by the traditional national medicine standard;
5. auxiliary materials: an adsorption carrier; the moisturizing solvent is one of glycerol, propylene glycol, sorbitol and medical vaseline; the antioxidant antibacterial matrix is one or more of lavender essential oil, tea polyphenol essential oil, ginger essential oil, peppermint essential oil and clove essential oil; the preservative is one or more of methylparaben, benzoic acid and sorbic acid; the transdermal absorption matrix is azone;
6. preparing a paste body:
and (3) sterilization: sterilizing the ball with ionizing radiation at 50-60deg.C for 40-60 min;
the ingredients comprise, by weight, 10-30 parts of ball, 10-20 parts of Chinese herbal medicine extract, 1-5 parts of heat sensitive matrix and auxiliary materials: 30-60 parts of adsorption carrier, 45-75 parts of moisturizing solvent, 5-12 parts of antioxidant and antibacterial matrix, 0.1-0.5 part of preservative and 0.1-0.5 part of transdermal absorption matrix;
mixing: heating a full-automatic stirring type hot-melt pot, adding a moisturizing solvent in auxiliary materials into the pot, cooling to 50-60 ℃ after heating to 80-85 ℃, adding a Chinese herbal medicine extract, a heat sensitive matrix, an antioxidant antibacterial matrix, a preservative and a transdermal absorption matrix, stirring uniformly, adding an adsorption carrier, setting the stirring rotation speed to be 150 r/min, stirring and mixing for 30 min, adding beads, setting the stirring rotation speed to be 50 r/min, stirring and mixing for 25 min, cooling to 35-45 ℃ to obtain a paste body, and placing the paste body into a heat preservation feed barrel for heat preservation;
7. Base layer: the non-woven fabric with the self-adhesive on one side is adhered with an anti-seepage pearlescent film in the middle, the part of the non-woven fabric with the self-adhesive on one side, which is positioned outside the anti-seepage pearlescent film, is an adhesive area, and rubber or foam anti-leakage sealing rings are adhered on the anti-seepage pearlescent film for later use;
8. a matrix layer: spreading the paste body in the rubber or foam leakage-proof sealing ring of the base layer by adopting a spreading process to form a matrix layer, wherein the height of the matrix layer is the same as that of the leakage-proof sealing ring;
9. and (3) a protective layer: and coating the periphery of the matrix layer and the rubber or foam anti-seepage sealing ring with the silk-screen non-woven fabric, and then bonding the release paper and the non-drying adhesive area of the basal layer.
Nanometer heat sensation massage cream: placing the paste body obtained in the step 6 into a storage barrel, and naturally cooling to normal temperature for later use; the packaging container is a double-layer dark-color wide-mouth bottle or barrel, and is sterilized by an ionizing radiation sterilization method, wherein the sterilization temperature is 50-60 ℃ and the sterilization time is 30-50 minutes; filling into sterilized bottle or barrel, and sealing.
The invention has the advantages that (the nanometer thermal massage paste is abbreviated as nanometer moxibustion paste ):
1. the nanometer moxibustion paste or the nanometer moxibustion paste prepared from the paste body is respectively spread or stuck on the fatigue parts of the shoulders, the neck, the waist and the back of a human body, so that the paste is comfortable for people, meanwhile, the balls in the nanometer moxibustion paste or the nanometer moxibustion paste are pressed by gentle fingering or palm method, the penetration force of the ball pressing moxibustion part is strong, the fatigue and the mood of the people are relieved, and the defect that the moxibustion part is not synchronous with massage in the moxibustion treatment of the traditional external paste, the traditional Chinese medicine hot compress paste or the medical moxibustion paste product is solved;
2. The paste body of the heat-sensitive matrix, the nano moxibustion paste or the nano moxibustion paste prepared from the paste body generate heat feeling on human skin during moxibustion therapy, the heat feeling time is long, the heat feeling is comfortable, and the defect that an iron powder heating bag is not suitable for massaging by using fingering and palm, and the traditional Chinese medicine hot compress paste with artificial temperature control cannot keep comfortable constant temperature for a long time, so that the use method is inconvenient, and the iron powder heating bag is not suitable for massaging by using fingering and palm is solved; when the nanometer moxibustion patch is used, after the moxibustion application part is cleaned, the release paper on the moxibustion patch is uncovered, and the moxibustion therapy can be performed by applying the moxibustion patch to a human body; when the nanometer moxibustion ointment is used, after cleaning the moxibustion part, the nanometer moxibustion ointment is spread on the moxibustion part of human body, and covered with a plastic film for 30-40 min;
3. the nanometer moxibustion ointment or the nanometer moxibustion patch is suitable for use in physiotherapy departments of hospitals, clinics of traditional Chinese medicine, health preserving halls, massage homes and families, and has large market demands; the raw materials used in the production are commercial products, are easy to purchase, and are suitable for industrial mass production.
FIG. 1 is a front view of a structure of a nano thermal massage patch of the present invention;
FIG. 2 is a bottom view of FIG. 1;
fig. 3 is a schematic diagram of the structure of the nano thermal massage paste body and paste according to the invention.
The invention is further described below with reference to the drawings.
Example 1 as shown in fig. 3, a nano thermal massage paste body 4 is provided, and the paste body 4 is provided with ball beads 8 with diameters of 1-9 mm.
Is prepared from spherical beads 8 with the diameter of 1-9mm, a thermal sensitive matrix, chinese herbal medicine extracts and auxiliary materials, and the preparation method comprises the following steps:
1. the balls with the diameter of 1-9mm are preferably nano ceramic balls or nano plastic balls:
A. the preparation method of the nano ceramic ball comprises the following steps:
grinding: grinding stone needle powder, anion powder, far infrared powder, germanite powder, tourmaline powder and magnetite powder respectively by using a grinder until the powder particle size is less than 100 nanometers;
and (3) batching: taking ground nanoscale powder, and adding 18% silicon dioxide by weight of the ingredients according to one of 35 parts of stone needle powder, 10 parts of negative ion powder, 10 parts of far infrared powder, 10 parts of germanite powder, 60 parts of tourmaline powder and 60 parts of magnetite powder;
sintering: sintering into nano ceramic balls with the diameter of 1-9mm by using a ceramic sintering furnace and a ceramic sintering process;
B. the preparation method of the nano plastic ball bead comprises the following steps:
grinding: grinding stone needle powder, anion powder, far infrared powder, germanite powder, tourmaline powder and magnetite powder respectively by using a grinder until the powder particle size is less than 100 nanometers;
And (3) batching: taking ground nanoscale powder, and adding 25% polyvinyl chloride and 3% triethyl citrate by weight of the ingredients according to the weight parts of one of 30 parts of stone needle powder, 10 parts of negative ion powder, 10 parts of far infrared powder, 10 parts of germanite powder, 60 parts of tourmaline powder and 60 parts of magnetite powder;
and (3) forming: plasticizing and fusing the ingredients, and making plastic balls into nano plastic balls with the diameter of 1-9mm by a plastic ball forming machine;
2. preparation of adsorption carrier:
grinding: grinding attapulgite and rectorite respectively by using a grinder until the particle size of the attapulgite and rectorite is less than 100 nanometers;
and (3) batching: taking ground attapulgite and rectorite nanoscale powder, and stirring and mixing;
and (3) sterilization: the mixed nano-scale powder is sterilized by an ionizing radiation sterilization method, the sterilization temperature is 50 ℃ and the time is 40 minutes, and the adsorption carrier of the nano-scale powder of rectorite and attapulgite is obtained for standby;
3. the heat sensitive matrix is gingerol;
4. chinese herbal medicine extract: an ultrasonic traditional Chinese medicine extract obtained by adopting an ultrasonic traditional Chinese medicine extraction method is an external treatment prescription permitted by the traditional national medicine standard;
5. auxiliary materials: an adsorption carrier; the moisturizing solvent is glycerol; the antioxidant antibacterial matrix is one of lavender essential oil, tea polyphenol essential oil, ginger essential oil, peppermint essential oil and clove essential oil; the preservative is one of methylparaben, benzoic acid and sorbic acid; the transdermal absorption matrix is azone;
6. Preparing a paste body:
and (3) sterilization: sterilizing the ball with ionizing radiation at 50deg.C for 60 min;
the ingredients comprise, by weight, 10 parts of ball, 10 parts of Chinese herbal medicine extract, 1 part of heat sensitive matrix and auxiliary materials: 30 parts of adsorption carrier, 45 parts of moisturizing solvent, 5 parts of antioxidant and antibacterial matrix, 0.1 part of preservative and 0.1 part of transdermal absorption matrix;
mixing: the method comprises the steps of using a full-automatic stirring type hot-melt pot, firstly adding a moisturizing solvent into the pot, heating to 80 ℃, cooling to 50 ℃, then adding a Chinese herbal medicine extract, a thermo-sensitive matrix, an antioxidant antibacterial matrix, a preservative and a transdermal absorption matrix, stirring uniformly, then adding an adsorption carrier, setting the stirring rotation speed to be 150 r/min, stirring and mixing for 30 minutes, adding ball beads, setting the stirring rotation speed to be 50 r/min, stirring and mixing for 25 minutes, cooling to 35 ℃ to obtain a paste body, and placing the paste body into a heat-preservation feed barrel for heat preservation for later use.
Example 2A nanometer thermal massage paste body 4, the paste body 4 is provided with a ball 8 with a diameter of 1-9 mm.
Is prepared from spherical beads 8 with the diameter of 1-9mm, a thermal sensitive matrix, chinese herbal medicine extracts and auxiliary materials, and the preparation method comprises the following steps:
1. the balls with the diameter of 1-9mm are preferably nano ceramic balls or nano plastic balls:
A. The preparation method of the nano ceramic ball comprises the following steps:
grinding: grinding stone needle powder, anion powder, far infrared powder, germanite powder, tourmaline powder and magnetite powder respectively by using a grinder until the powder particle size is less than 100 nanometers;
and (3) batching: taking two of 75 parts of stone needle powder, 60 parts of negative ion powder, 60 parts of far infrared powder, 60 parts of germanite powder, 10 parts of tourmaline powder and 10 parts of magnetite powder by weight, and then adding 28% of silicon dioxide by the total mass of the ingredients by weight;
sintering: sintering into nano ceramic balls with the diameter of 1-9mm by using a ceramic sintering furnace and a ceramic sintering process;
B. the preparation method of the nano plastic ball bead comprises the following steps:
grinding: grinding stone needle powder, anion powder, far infrared powder, germanite powder, tourmaline powder and magnetite powder respectively by using a grinder until the powder particle size is less than 100 nanometers;
and (3) batching: taking two of 65 parts by weight of stone needle powder, 60 parts by weight of negative ion powder, 60 parts by weight of far infrared powder, 60 parts by weight of germanite powder, 10 parts by weight of tourmaline powder and 10 parts by weight of magnetite powder, and then adding polypropylene accounting for 30% of the total mass of the ingredients and 5% of epoxidized soybean oil;
And (3) forming: plasticizing and fusing the ingredients, and making plastic balls into nano plastic balls with the diameter of 1-9mm by a plastic ball forming machine;
2. preparation of adsorption carrier:
grinding: grinding attapulgite and rectorite respectively by using a grinder until the particle size of the attapulgite and rectorite is less than 100 nanometers;
and (3) batching: taking ground attapulgite and rectorite nanoscale powder, and stirring and mixing;
and (3) sterilization: the mixed nano-scale powder is sterilized by an ionizing radiation sterilization method, the sterilization temperature is 90 ℃ and the time is 60 minutes, and the adsorption carrier of the nano-scale powder of rectorite and attapulgite is obtained for standby;
3. the thermal substrate is vanillyl butyl ether;
4. chinese herbal medicine extract: an ultrasonic traditional Chinese medicine extract obtained by adopting an ultrasonic traditional Chinese medicine extraction method is an external treatment prescription permitted by the traditional national medicine standard;
5. auxiliary materials: an adsorption carrier; the moisturizing solvent is propylene glycol; the antioxidant and antibacterial matrix is two of lavender essential oil, tea polyphenol essential oil, ginger essential oil, peppermint essential oil and clove essential oil; the preservative is two of methylparaben, benzoic acid and sorbic acid; the transdermal absorption matrix is azone;
6. preparing a paste body:
and (3) sterilization: sterilizing the ball with ionizing radiation at 60deg.C for 40 min;
The ingredients comprise, by weight, 30 parts of ball, 20 parts of Chinese herbal medicine extract, 5 parts of heat sensitive matrix and auxiliary materials: 60 parts of adsorption carrier, 75 parts of moisturizing solvent, 12 parts of antioxidant and antibacterial matrix, 0.5 part of preservative and 0.5 part of transdermal absorption matrix;
mixing: the method comprises the steps of using a full-automatic stirring type hot-melt pot, firstly adding a moisturizing solvent into the pot, heating to 85 ℃, cooling to 60 ℃, then adding a Chinese herbal medicine extract, a thermo-sensitive matrix, an antioxidant antibacterial matrix, a preservative and a transdermal absorption matrix, stirring uniformly, then adding an adsorption carrier, setting the stirring rotation speed to be 150 r/min, stirring and mixing for 30 minutes, adding ball beads, setting the stirring rotation speed to be 50 r/min, stirring and mixing for 25 minutes, cooling to 45 ℃ to obtain a paste body, and placing the paste body into a heat-preservation feed barrel for heat preservation for later use.
Example 3A nanometer thermal massage paste body 4, the paste body 4 is provided with a ball 8 with a diameter of 1-9 mm.
Is prepared from spherical beads 8 with the diameter of 1-9mm, a thermal sensitive matrix, chinese herbal medicine extracts and auxiliary materials, and the preparation method comprises the following steps:
1. the balls with the diameter of 1-9mm are preferably nano ceramic balls or nano plastic balls:
A. the preparation method of the nano ceramic ball comprises the following steps:
grinding: grinding stone needle powder, anion powder, far infrared powder, germanite powder, tourmaline powder and magnetite powder respectively by using a grinder until the powder particle size is less than 100 nanometers;
And (3) batching: taking three of the ground nano-scale powder, namely 55 parts of stone needle powder, 35 parts of negative ion powder, 35 parts of far infrared powder, 35 parts of germanite powder, 35 parts of tourmaline powder and 35 parts of magnetite powder, and then adding 23% of silicon dioxide by weight of the total mass of the ingredients;
sintering: sintering into nano ceramic balls with the diameter of 1-9mm by using a ceramic sintering furnace and a ceramic sintering process;
B. the preparation method of the nano plastic ball bead comprises the following steps:
grinding: grinding stone needle powder, anion powder, far infrared powder, germanite powder, tourmaline powder and magnetite powder respectively by using a grinder until the powder particle size is less than 100 nanometers;
and (3) batching: taking three of 55 parts by weight of stone needle powder, 35 parts by weight of anion powder, 35 parts by weight of far infrared powder, 35 parts by weight of germanite powder, 35 parts by weight of tourmaline powder and 35 parts by weight of magnetite powder, and then adding 28% by weight of high-density polyethylene and 4% by weight of triethyl citrate in the total mass of the ingredients;
and (3) forming: plasticizing and fusing the ingredients, and making plastic balls into nano plastic balls with the diameter of 1-9mm by a plastic ball forming machine;
2. preparation of adsorption carrier:
grinding: grinding attapulgite and rectorite respectively by using a grinder until the particle size of the attapulgite and rectorite is less than 100 nanometers;
And (3) batching: taking ground attapulgite and rectorite nanoscale powder, and stirring and mixing;
and (3) sterilization: the mixed nano-scale powder is sterilized by an ionizing radiation sterilization method, the sterilization temperature is 60 ℃ and the time is 50 minutes, and the adsorption carrier of the nano-scale powder of rectorite and attapulgite is obtained for standby;
3. the thermal substrate is vanillyl butyl ether;
4. chinese herbal medicine extract: an ultrasonic traditional Chinese medicine extract obtained by adopting an ultrasonic traditional Chinese medicine extraction method is an external treatment prescription permitted by the traditional national medicine standard;
5. auxiliary materials: an adsorption carrier; the moisturizing solvent is sorbitol; the antioxidant and antibacterial matrix is three of lavender essential oil, tea polyphenol essential oil, ginger essential oil, peppermint essential oil and clove essential oil; the preservative is methylparaben, benzoic acid and sorbic acid; the transdermal absorption matrix is azone;
6. preparing a paste body:
and (3) sterilization: sterilizing the ball with ionizing radiation at 55deg.C for 50 min;
the ingredients comprise, by weight, 20 parts of ball, 15 parts of Chinese herbal medicine extract, 3 parts of heat sensitive matrix and auxiliary materials: 45 parts of adsorption carrier, 60 parts of moisturizing solvent, 8 parts of antioxidant and antibacterial matrix, 0.3 part of preservative and 0.3 part of transdermal absorption matrix;
Mixing: using a full-automatic stirring type hot-melt pot, firstly adding a moisturizing solvent into the pot, heating to 82 ℃, cooling to 55 ℃, then adding a Chinese herbal medicine extract, a thermo-sensitive matrix, an antioxidant antibacterial matrix, a preservative and a transdermal absorption matrix, stirring uniformly, then adding an adsorption carrier, setting the stirring rotation speed to be 150 r/min, stirring and mixing for 30 minutes, adding ball beads, setting the stirring rotation speed to be 50 r/min, stirring and mixing for 25 minutes, cooling to 40 ℃ to obtain a paste body, and placing the paste body into a heat-preservation feed barrel for heat preservation;
example 4A nanometer thermal massage paste body 4, the paste body 4 is provided with a ball 8 with a diameter of 1-9 mm.
Is prepared from spherical beads 8 with the diameter of 1-9mm, a thermal sensitive matrix, chinese herbal medicine extracts and auxiliary materials, and the preparation method comprises the following steps:
1. the balls with the diameter of 1-9mm are preferably nano ceramic balls or nano plastic balls:
A. the preparation method of the nano ceramic ball comprises the following steps:
grinding: grinding stone needle powder, anion powder, far infrared powder, germanite powder, tourmaline powder and magnetite powder respectively by using a grinder until the powder particle size is less than 100 nanometers;
and (3) batching: taking four of 65 parts by weight of stone needle powder, 40 parts by weight of negative ion powder, 40 parts by weight of far infrared powder, 40 parts by weight of germanite powder, 50 parts by weight of tourmaline powder and 50 parts by weight of magnetite powder, and then adding 27% of silicon dioxide by the total mass of the ingredients;
Sintering: sintering into nano ceramic balls with the diameter of 1-9mm by using a ceramic sintering furnace and a ceramic sintering process;
B. the preparation method of the nano plastic ball bead comprises the following steps:
grinding: grinding stone needle powder, anion powder, far infrared powder, germanite powder, tourmaline powder and magnetite powder respectively by using a grinder until the powder particle size is less than 100 nanometers;
and (3) batching: taking four of 65 parts by weight of stone needle powder, 40 parts by weight of anion powder, 40 parts by weight of far infrared powder, 40 parts by weight of germanite powder, 50 parts by weight of tourmaline powder and 50 parts by weight of magnetite powder, and then adding polyvinyl chloride accounting for 28% of the total mass of the ingredients and triethyl citrate accounting for 3% of the total mass of the ingredients;
and (3) forming: plasticizing and fusing the ingredients, and making plastic balls into nano plastic balls with the diameter of 1-9mm by a plastic ball forming machine;
2. preparation of adsorption carrier:
grinding: grinding attapulgite and rectorite respectively by using a grinder until the particle size of the attapulgite and rectorite is less than 100 nanometers;
and (3) batching: taking ground attapulgite and rectorite nanoscale powder, and stirring and mixing;
and (3) sterilization: the mixed nano-scale powder is sterilized by an ionizing radiation sterilization method, the sterilization temperature is 55 ℃ and the time is 55 minutes, and the adsorption carrier of the nano-scale powder of rectorite and attapulgite is obtained for standby;
3. The heat sensitive matrix is gingerol;
4. chinese herbal medicine extract: an ultrasonic traditional Chinese medicine extract obtained by adopting an ultrasonic traditional Chinese medicine extraction method is an external treatment prescription permitted by the traditional national medicine standard;
5. auxiliary materials: an adsorption carrier; the moisturizing solvent is medical vaseline; the antioxidant and antibacterial matrix is four of lavender essential oil, tea polyphenol essential oil, ginger essential oil, peppermint essential oil and butyl essential oil; the preservative is methylparaben, benzoic acid and sorbic acid; the transdermal absorption matrix is azone;
6. preparing a paste body:
and (3) sterilization: sterilizing the ball with ionizing radiation at 55deg.C for 60 min;
the ingredients comprise, by weight, 25 parts of ball, 16 parts of Chinese herbal medicine extract, 2 parts of heat sensitive matrix and auxiliary materials: 40 parts of adsorption carrier, 60 parts of moisturizing solvent, 9 parts of antioxidant and antibacterial matrix, 0.4 part of preservative and 0.4 part of transdermal absorption matrix;
mixing: using a full-automatic stirring type hot-melt pot, firstly adding a moisturizing solvent into the pot, heating to 82 ℃, cooling to 59 ℃, then adding a Chinese herbal medicine extract, a thermo-sensitive matrix, an antioxidant antibacterial matrix, a preservative and a transdermal absorption matrix, stirring uniformly, then adding an adsorption carrier, setting the stirring rotation speed to be 150 r/min, stirring and mixing for 30 minutes, adding ball beads, setting the stirring rotation speed to be 50 r/min, stirring and mixing for 25 minutes, cooling to 41 ℃ to obtain a paste body, and placing the paste body into a heat-preservation feed barrel for heat preservation;
Example 5A nanometer thermal massage paste body 4, the paste body 4 is provided with ball beads 8 with the diameter of 1-9 mm.
Is prepared from spherical beads 8 with the diameter of 1-9mm, a thermal sensitive matrix, chinese herbal medicine extracts and auxiliary materials, and the preparation method comprises the following steps:
1. the balls with the diameter of 1-9mm are preferably nano ceramic balls or nano plastic balls:
A. the preparation method of the nano ceramic ball comprises the following steps:
grinding: grinding stone needle powder, anion powder, far infrared powder, germanite powder, tourmaline powder and magnetite powder respectively by using a grinder until the powder particle size is less than 100 nanometers;
and (3) batching: taking five of the ground nano-scale powder according to the parts by weight, namely 70 parts of stone needle powder, 55 parts of negative ion powder, 55 parts of far infrared powder, 55 parts of germanite powder, 50 parts of tourmaline powder and 50 parts of magnetite powder, and then adding 20% of silicon dioxide by the total mass of the ingredients;
sintering: sintering into nano ceramic balls with the diameter of 1-9mm by using a ceramic sintering furnace and a ceramic sintering process;
B. the preparation method of the nano plastic ball bead comprises the following steps:
grinding: grinding stone needle powder, anion powder, far infrared powder, germanite powder, tourmaline powder and magnetite powder respectively by using a grinder until the powder particle size is less than 100 nanometers;
And (3) batching: taking five of ground nanoscale powder, namely 60 parts of stone needle powder, 55 parts of negative ion powder, 55 parts of far infrared powder, 45 parts of germanite powder, 45 parts of tourmaline powder and 50 parts of magnetite powder, and then adding polypropylene accounting for 30% of the total mass of the ingredients and epoxidized soybean oil accounting for 3% of the total mass of the ingredients;
and (3) forming: plasticizing and fusing the ingredients, and making plastic balls into nano plastic balls with the diameter of 1-9mm by a plastic ball forming machine;
2. preparation of adsorption carrier:
grinding: grinding attapulgite and rectorite respectively by using a grinder until the particle size of the attapulgite and rectorite is less than 100 nanometers;
and (3) batching: taking ground attapulgite and rectorite nanoscale powder, and stirring and mixing;
and (3) sterilization: the mixed nano-scale powder is sterilized by an ionizing radiation sterilization method, the sterilization temperature is 70 ℃ and the time is 50 minutes, and the adsorption carrier of the nano-scale powder of rectorite and attapulgite is obtained for standby;
3. the heat sensitive matrix uses gingerol and vanillyl butyl ether;
4. chinese herbal medicine extract: an ultrasonic traditional Chinese medicine extract obtained by adopting an ultrasonic traditional Chinese medicine extraction method is an external treatment prescription permitted by the traditional national medicine standard;
5. auxiliary materials: an adsorption carrier; the moisturizing solvent is medical vaseline; the antioxidant antibacterial matrix is lavender essential oil, tea polyphenol essential oil, ginger essential oil, peppermint essential oil and clove essential oil; the preservative is methylparaben and benzoic acid; the transdermal absorption matrix is azone;
6. Preparing a paste body:
and (3) sterilization: sterilizing the ball with ionizing radiation at 50deg.C for 60 min;
the ingredients comprise, by weight, 25 parts of ball, 15 parts of Chinese herbal medicine extract, 3 parts of heat sensitive matrix and auxiliary materials: 35 parts of adsorption carrier, 65 parts of moisturizing solvent, 7 parts of antioxidant and antibacterial matrix, 0.2 part of preservative and 0.2 part of transdermal absorption matrix;
mixing: using a full-automatic stirring type hot-melt pot, firstly adding a moisturizing solvent into the pot, heating to 80 ℃, cooling to 50 ℃, then adding a Chinese herbal medicine extract, a thermo-sensitive matrix, an antioxidant antibacterial matrix, a preservative and a transdermal absorption matrix, stirring uniformly, then adding an adsorption carrier, setting the stirring rotation speed to be 150 r/min, stirring and mixing for 30 minutes, adding ball beads, setting the stirring rotation speed to be 50 r/min, stirring and mixing for 25 minutes, cooling to 35 ℃ to obtain a paste body, and placing the paste body into a heat-preservation feed barrel for heat preservation;
example 6A nanometer thermal massage paste body 4, the paste body 4 is provided with ball beads 8 with the diameter of 1-9 mm.
Is prepared from spherical beads 8 with the diameter of 1-9mm, a thermal sensitive matrix, chinese herbal medicine extracts and auxiliary materials, and the preparation method comprises the following steps:
1. the balls with the diameter of 1-9mm are preferably nano ceramic balls or nano plastic balls:
A. The preparation method of the nano ceramic ball comprises the following steps:
grinding: grinding stone needle powder, anion powder, far infrared powder, germanite powder, tourmaline powder and magnetite powder respectively by using a grinder until the powder particle size is less than 100 nanometers;
and (3) batching: taking the ground nano-scale powder, and adding 21% silicon dioxide of the total mass of the ingredients in parts by weight, wherein the weight is 40 parts of stone needle powder, 50 parts of negative ion powder, 30 parts of far infrared powder, 20 parts of germanite powder, 15 parts of tourmaline powder and 30 parts of magnetite powder;
sintering: sintering into nano ceramic balls with the diameter of 1-9mm by using a ceramic sintering furnace and a ceramic sintering process;
B. the preparation method of the nano plastic ball bead comprises the following steps:
grinding: grinding stone needle powder, anion powder, far infrared powder, germanite powder, tourmaline powder and magnetite powder respectively by using a grinder until the powder particle size is less than 100 nanometers;
and (3) batching: taking 45 parts of stone needle powder, 28 parts of anion powder, 35 parts of far infrared powder, 35 parts of germanite powder, 50 parts of tourmaline powder and 50 parts of magnetite powder in parts by weight, and then adding 26% of high-density polyethylene and 3% of triethyl citrate by weight of the total mass of the ingredients;
and (3) forming: plasticizing and fusing the ingredients, and making plastic balls into nano plastic balls with the diameter of 1-9mm by a plastic ball forming machine;
2. Preparation of adsorption carrier:
grinding: grinding attapulgite and rectorite respectively by using a grinder until the particle size of the attapulgite and rectorite is less than 100 nanometers;
and (3) batching: taking ground attapulgite and rectorite nanoscale powder, and stirring and mixing;
and (3) sterilization: the mixed nano-scale powder is sterilized by an ionizing radiation sterilization method, the sterilization temperature is 80 ℃ and the time is 50 minutes, and the adsorption carrier of the nano-scale powder of rectorite and attapulgite is obtained for standby;
3. the heat sensitive matrix is gingerol and vanillyl butyl ether;
4. chinese herbal medicine extract: an ultrasonic traditional Chinese medicine extract obtained by adopting an ultrasonic traditional Chinese medicine extraction method is an external treatment prescription permitted by the traditional national medicine standard;
5. auxiliary materials: an adsorption carrier; the moisturizing solvent is medical vaseline; the antioxidant antibacterial matrix is lavender essential oil, tea polyphenol essential oil and ginger essential oil; the preservative is methylparaben; the transdermal absorption matrix is azone;
6. preparing a paste body:
and (3) sterilization: sterilizing the ball with ionizing radiation at 60deg.C for 45 min;
the ingredients comprise, by weight, 18 parts of ball, 16 parts of Chinese herbal medicine extract, 4 parts of heat sensitive matrix and auxiliary materials: 55 parts of adsorption carrier, 65 parts of moisturizing solvent, 11 parts of antioxidant and antibacterial matrix, 0.2 part of preservative and 0.2 part of transdermal absorption matrix;
Mixing: using a full-automatic stirring type hot-melt pot, firstly adding a moisturizing solvent into the pot, heating to 85 ℃, cooling to 60 ℃, then adding a Chinese herbal medicine extract, a thermo-sensitive matrix, an antioxidant antibacterial matrix, a preservative and a transdermal absorption matrix, stirring uniformly, then adding an adsorption carrier, setting the stirring rotation speed to be 150 r/min, stirring and mixing for 30 minutes, adding ball beads, setting the stirring rotation speed to be 50 r/min, stirring and mixing for 25 minutes, cooling to 45 ℃ to obtain a paste body, and placing the paste body into a heat-preservation feed barrel for heat preservation;
embodiment 7 as shown in fig. 1 and 2, the nanometer thermal massage patch consists of a substrate layer, a substrate layer and a protective layer, wherein the substrate layer is a paste body 4, the substrate layer consists of a non-woven fabric 1 with a self-adhesive on one side, an impermeable pearlescent film 2 and a rubber or foam leakage-proof sealing ring 3, and the protective layer consists of a silk screen non-woven fabric 5 and release paper 6;
the anti-seepage pearlescent film 2 is adhered to the middle of the non-woven fabric 1 with the self-adhesive on one side, the non-woven fabric 1 with the self-adhesive on one side is provided with the self-adhesive area 7 at the outer part of the anti-seepage pearlescent film 2, the anti-seepage pearlescent film 2 is adhered with the rubber or foam anti-leakage sealing ring 3, the matrix layer is arranged in the rubber or foam anti-leakage sealing ring 3, and the height of the matrix layer is the same as that of the rubber or foam anti-leakage sealing ring 3;
The matrix layer is coated by a silk screen non-woven fabric 5, the silk screen non-woven fabric 5 is adhered to the rubber or foam leakage-proof sealing ring 3, and the release paper 6 is adhered to the non-drying adhesive area 7 on the non-woven fabric 1 with the non-drying adhesive on one side.
The preparation method comprises the following steps:
1. base layer: the non-woven fabric 1 with the self-adhesive on one side is adhered with the anti-seepage pearlescent film 2, the part of the non-woven fabric 1 with the self-adhesive on one side, which is positioned outside the anti-seepage pearlescent film 2, is an adhesive area 7, and rubber or foam anti-leakage sealing rings 3 are adhered on the anti-seepage pearlescent film 2 for later use;
2. a matrix layer: spreading the paste body in the rubber or foam leakage-proof sealing ring 3 of the base layer by adopting a spreading process to form a matrix layer 4, wherein the height of the matrix layer 4 is the same as that of the leakage-proof sealing ring 3;
3. and (3) a protective layer: and coating the periphery of the matrix layer 4 and the rubber or foam anti-seepage sealing ring 3 with the silk-screen non-woven fabric 5, and then bonding the release paper 6 and the non-drying adhesive area 7 of the basal layer.
Example 8 As shown in fig. 3, a nano thermal massage cream is obtained by cooling and filling a paste body 4, wherein the paste body 4 is provided with spherical beads 8 with the diameter of 1-9 mm.
The preparation method comprises the following steps:
placing the paste body obtained in the examples 1-6 into a storage vat, naturally cooling to normal temperature for later use; the packaging container is a double-layer dark-color wide-mouth bottle or barrel, and is sterilized by an ionizing radiation sterilization method, wherein the sterilization temperature is 50-60 ℃ and the sterilization time is 30-50 minutes; filling into sterilized bottle or barrel, and sealing.
The nanometer moxibustion plaster and the nanometer moxibustion paste are continuously observed for 9 months. The results show that the nanometer moxibustion plaster and the nanometer moxibustion plaster are respectively applied to the fatigue parts of the shoulders, the neck, the waist and the back of a human body for heat moxibustion treatment, so that the human body is comfortable, meanwhile, the plaster is rubbed by a gentle fingering method or a palm method, and the balls in the plaster are stuck, and the penetration force of the ball massage moxibustion part is strong, so that the human body is relieved from fatigue and has a comfortable mood;
the experience population is as follows:
men and women experience 1400 cases in total, with an average age of 43.5 years, a maximum age of 55 years, and a minimum age of 25 years;
the device comprises: the health care massage bed is used uniformly; temperature: a chamber at 18-20deg.C;
the moxibustion health care massage method comprises the following steps: experimenters learn the text data or audio-visual data provided by the inventor and provided with the map, and know fingering, palm feeling and notes of the health care massage of the nanometer moxibustion plaster and the nanometer moxibustion paste, including fingering and palm feeling of one hand or two hands of the health care massage; the fingering includes finger pressure and finger softness; the palm method comprises palm softness, palm rubbing and palm beating; the fingering and palming methods of one hand or two hands are simple and easy to learn and operate; the moxibustion massage person and the experimenter are mutually changed into the moxibustion massage person and the experimenter, and the moxibustion massage experience is carried out.
The experience group and the control group have the same method;
the grouping is as follows:
the experience group 1, the moxibustion massage people and 100 people of the experience people respectively, wherein the experience people use nanometer moxibustion patches, each person is twice in 12 days, each time is 30-40 minutes, and 3 continuous days, the nanometer moxibustion patches are respectively applied to fatigue parts of shoulders, necks, waists and backs of the experience people for moxibustion therapy, and the moxibustion massage people help to rub and press the ball beads in the nanometer moxibustion patches by gentle fingering or palm method, and the ball beads rub and press the moxibustion parts; after the experience is completed, the moxibustion massage person and the experienter exchange role operations;
the experience group 2, the moxibustion massage people and 100 people of the experience people respectively, wherein the experience people use the nanometer moxibustion paste, each person is twice in 12 days, each time lasts for 30-40 minutes, the nanometer moxibustion paste is respectively applied to fatigue parts of shoulders, necks, waists and backs of the experience people for moxibustion treatment for 3 continuous days, a plastic film is covered, the moxibustion massage people help to rub the ball under the plastic film by gentle fingering or palm method, and the ball rubs and presses the moxibustion part; after the experience is completed, the moxibustion massage person and the experienter exchange role operations;
the experience group 3 and the experience person use the nanometer moxibustion plaster for 200 persons, each person is twice in 12 days, each time lasts for 30-40 minutes, and the nanometer moxibustion plaster is respectively applied to fatigue parts of shoulders, necks, waists and backs of the experience person for moxibustion therapy, and a massage doctor in physiotherapy department is helped to press the ball in the nanometer moxibustion plaster by gentle fingering or palm method, and the ball is pressed on the moxibustion part;
The experience group 4 and the experimenters use the nanometer moxibustion paste 200, each time is carried out twice in 12 days, each time lasts for 30-40 minutes, and the nanometer moxibustion paste is respectively spread on fatigue parts of shoulders, necks, waists and backs of the experimenters to apply moxibustion treatment, and a plastic film is covered, so that a massage engineer in physiotherapy department is helped to rub the beads below the plastic film by gentle fingering or palm method, and the beads are pressed on the moxibustion part;
the control group 5 and the experimenters use the traditional Chinese medicine hot compress for 200 persons, each person is twice in 12 days, each time lasts for 30-40 minutes, the adhesive plaster at the bottom of the iron powder bag of the traditional Chinese medicine hot compress is uncovered when in use, and the medicine bag is pasted on the fatigue parts of the shoulders, the neck, the waist and the back of the experimenters to apply moxibustion therapy;
the control group 6 and experimenters use the existing self-heating magnetic medicinal moxibustion plaster for 200 persons, each person is twice in 12 days, 30-40 minutes each time, and 3 days continuously, the adhesive plaster at the bottom of the iron powder bag of the self-heating magnetic medicinal moxibustion plaster is uncovered when in use, and the medicinal bag is pasted on fatigue parts of shoulders, necks, waists and backs of the experimenters to apply moxibustion therapy;
the control group 7 and the experimenters use the traditional Chinese medicine hot compress paste 200 persons, each person is twice in 12 days, each time lasts for 30-40 minutes, and the traditional Chinese medicine hot compress paste is coated on the skin surface of the fatigue parts of the shoulders, the neck, the waist and the back of the experimenters during use, and the hot compress control temperature is within 45-50 ℃;
None of the above groups were statistically significantly different, and each group was comparable to the balance prior to use.
Results: the symptoms of the experience group control group changed, as shown in table 1,
TABLE 1 fatigue relief, mood comfort comparison experiment data
The method is effective: relieving fatigue, and improving mood, or eliminating fatigue symptoms;
invalidation: relieving fatigue and having no effect of happy mood.
Claims (3)
1. A nanometer thermal massage paste body is characterized in that: is prepared from spherical beads (8) with the diameter of 1-9mm, a thermal medium, chinese herbal medicine extracts and auxiliary materials, and the preparation method comprises the following steps:
1. the spherical beads (8) with the diameter of 1-9mm are nano ceramic spherical beads or nano plastic spherical beads:
A. preparing nano ceramic balls:
grinding: grinding stone needle powder, anion powder, far infrared powder, germanite powder, tourmaline powder and magnetite powder respectively by using a grinder until the powder particle size is less than 100 nanometers;
and (3) batching: taking one or more of 35-75 parts of stone needle powder, 10-60 parts of negative ion powder, 10-60 parts of far infrared powder, 10-60 parts of germanite powder, 10-60 parts of tourmaline powder and 10-60 parts of magnetite powder by weight, and then adding 18-28% of silicon dioxide by the total mass of the ingredients by weight;
Sintering: sintering into nano ceramic balls with the diameter of 1-9mm by using a ceramic sintering furnace and a ceramic sintering process;
B. preparing nano plastic ball beads:
grinding: grinding stone needle powder, anion powder, far infrared powder, germanite powder, tourmaline powder and magnetite powder respectively by using a grinder until the powder particle size is less than 100 nanometers;
and (3) batching: taking one or more of 30-65 parts of stone needle powder, 10-60 parts of anion powder, 10-60 parts of far infrared powder, 10-60 parts of germanite powder, 10-60 parts of tourmaline powder and 10-60 parts of magnetite powder by weight, and then adding 25-30% of polyvinyl chloride or polypropylene or high-density polyethylene and 3-5% of triethyl citrate or epoxidized soybean oil by weight of the total mass of the ingredients;
and (3) forming: plasticizing and fusing the ingredients, and making plastic balls into nano plastic balls with the diameter of 1-9mm by a plastic ball forming machine;
2. preparation of adsorption carrier:
grinding: grinding attapulgite and rectorite respectively by using a grinder until the particle size of the attapulgite and rectorite is less than 100 nanometers;
and (3) batching: taking ground attapulgite and rectorite nanoscale powder, and stirring and mixing;
and (3) sterilization: the mixed nano-scale powder is sterilized by an ionizing radiation sterilization method at the sterilization temperature of 50-90 ℃ for 40-60 minutes to obtain the adsorption carrier of the nano-scale powder of rectorite and attapulgite for standby;
3. The heat sensitive matrix is one or two of gingerol and vanillyl butyl ether;
4. chinese herbal medicine extract: an ultrasonic traditional Chinese medicine extract obtained by adopting an ultrasonic traditional Chinese medicine extraction method is an external treatment prescription permitted by the traditional national medicine standard;
5. auxiliary materials: an adsorption carrier; the moisturizing solvent is one of glycerol, propylene glycol, sorbitol and medical vaseline; the antioxidant antibacterial matrix is one or more of lavender essential oil, tea polyphenol essential oil, ginger essential oil, peppermint essential oil and clove essential oil; the preservative is one or more of methylparaben, benzoic acid and sorbic acid; the transdermal absorption matrix is azone;
6. preparing a paste body:
and (3) sterilization: sterilizing the ball with ionizing radiation at 50-60deg.C for 40-60 min;
the ingredients comprise, by weight, 10-30 parts of ball, 10-20 parts of Chinese herbal medicine extract, 1-5 parts of heat sensitive matrix and auxiliary materials: 30-60 parts of adsorption carrier, 45-75 parts of moisturizing solvent, 5-12 parts of antioxidant and antibacterial matrix, 0.1-0.5 part of preservative and 0.1-0.5 part of transdermal absorption matrix;
mixing: the method comprises the steps of using a full-automatic stirring type hot-melt pot, firstly adding a moisturizing solvent into the pot, heating to 80-85 ℃, cooling to 50-60 ℃, then adding a Chinese herbal medicine extract, a heat sensitive matrix, an antioxidant antibacterial matrix, a preservative and a transdermal absorption matrix, stirring uniformly, then adding an adsorption carrier, setting the stirring rotation speed to be 150 r/min, stirring and mixing for 30 min, adding ball beads, setting the stirring rotation speed to be 50 r/min, stirring and mixing for 25 min, cooling to 35-45 ℃ to obtain a paste body, and placing the paste body into a heat-preserving feed barrel for heat preservation for later use.
2. A nanometer thermal massage patch is characterized in that: the paste body prepared by adopting the method of claim 1 consists of a substrate layer, a substrate layer and a protective layer, wherein the substrate layer is a paste body (4), the substrate layer consists of non-woven fabric (1) with self-adhesive on one surface, an impermeable pearlescent film (2) and a rubber or foam leakage-proof sealing ring (3), and the protective layer consists of silk screen non-woven fabric (5) and release paper (6);
the anti-seepage pearlescent film (2) is adhered to the middle of the non-woven fabric (1) with the self-adhesive on one side, the part of the non-woven fabric (1) with the self-adhesive on one side, which is positioned outside the anti-seepage pearlescent film (2), is a self-adhesive area (7), rubber or foam anti-seepage sealing rings (3) are adhered to the anti-seepage pearlescent film (2), a matrix layer is arranged in the rubber or foam anti-seepage sealing rings (3), and the height of the matrix layer is the same as that of the rubber or foam anti-seepage sealing rings (3);
the matrix layer is coated by a silk-screen non-woven fabric (5), the silk-screen non-woven fabric (5) is adhered to the rubber or foam leakage-proof sealing ring (3), and the release paper (6) is adhered to the non-drying adhesive area (7) on the non-woven fabric (1) with the non-drying adhesive on one side.
3. A nanometer thermal massage cream is characterized in that: the paste body prepared by adopting the method in claim 1 is obtained by cooling and filling the paste body (4), and the paste body (4) is provided with spherical beads (8) with the diameter of 1-9 mm.
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| CN114099415A (en) * | 2021-10-22 | 2022-03-01 | 同芙集团(中国)股份有限公司 | Soothing cream and preparation method thereof |
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