CN109828064B - HPLC fingerprint image establishing method for effective part group of periploca forrestii schltr - Google Patents
HPLC fingerprint image establishing method for effective part group of periploca forrestii schltr Download PDFInfo
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- CN109828064B CN109828064B CN201910016854.1A CN201910016854A CN109828064B CN 109828064 B CN109828064 B CN 109828064B CN 201910016854 A CN201910016854 A CN 201910016854A CN 109828064 B CN109828064 B CN 109828064B
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- periploca forrestii
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- periploca
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- 241000753128 Periploca <moth> Species 0.000 title claims abstract description 65
- 238000000034 method Methods 0.000 title claims abstract description 41
- 238000004128 high performance liquid chromatography Methods 0.000 title claims abstract description 34
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- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 37
- NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 claims description 24
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 21
- 238000005303 weighing Methods 0.000 claims description 20
- PZIRUHCJZBGLDY-UHFFFAOYSA-N Caffeoylquinic acid Natural products CC(CCC(=O)C(C)C1C(=O)CC2C3CC(O)C4CC(O)CCC4(C)C3CCC12C)C(=O)O PZIRUHCJZBGLDY-UHFFFAOYSA-N 0.000 claims description 19
- 239000000843 powder Substances 0.000 claims description 19
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- CWVRJTMFETXNAD-KLZCAUPSSA-N Neochlorogenin-saeure Natural products O[C@H]1C[C@@](O)(C[C@@H](OC(=O)C=Cc2ccc(O)c(O)c2)[C@@H]1O)C(=O)O CWVRJTMFETXNAD-KLZCAUPSSA-N 0.000 claims description 17
- CWVRJTMFETXNAD-JUHZACGLSA-N chlorogenic acid Chemical compound O[C@@H]1[C@H](O)C[C@@](O)(C(O)=O)C[C@H]1OC(=O)\C=C\C1=CC=C(O)C(O)=C1 CWVRJTMFETXNAD-JUHZACGLSA-N 0.000 claims description 17
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- 238000001179 sorption measurement Methods 0.000 claims description 16
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- GYFFKZTYYAFCTR-JUHZACGLSA-N 4-O-trans-caffeoylquinic acid Chemical compound O[C@@H]1C[C@](O)(C(O)=O)C[C@@H](O)[C@H]1OC(=O)\C=C\C1=CC=C(O)C(O)=C1 GYFFKZTYYAFCTR-JUHZACGLSA-N 0.000 claims description 13
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- GWTUHAXUUFROTF-UHFFFAOYSA-N pseudochlorogenic acid Natural products C1C(O)C(O)C(O)CC1(C(O)=O)OC(=O)C=CC1=CC=C(O)C(O)=C1 GWTUHAXUUFROTF-UHFFFAOYSA-N 0.000 description 2
- 239000013558 reference substance Substances 0.000 description 2
- CWVRJTMFETXNAD-NXLLHMKUSA-N trans-5-O-caffeoyl-D-quinic acid Chemical compound O[C@H]1[C@H](O)C[C@](O)(C(O)=O)C[C@H]1OC(=O)\C=C\C1=CC=C(O)C(O)=C1 CWVRJTMFETXNAD-NXLLHMKUSA-N 0.000 description 2
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- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
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CN110702813B (en) * | 2019-10-23 | 2022-03-11 | 贵州中医药大学 | Miao medicine caulis et folium periplocae HPLC fingerprint spectrum research and multi-component content determination method |
CN114166954B (en) * | 2021-04-07 | 2023-10-17 | 国药集团同济堂(贵州)制药有限公司 | Preparation method and quality detection method of black bone vine standard decoction |
Citations (1)
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CN107607649A (en) * | 2017-09-17 | 2018-01-19 | 贵阳中医学院 | A kind of detection method of Heiguteng exract |
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Patent Citations (1)
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CN107607649A (en) * | 2017-09-17 | 2018-01-19 | 贵阳中医学院 | A kind of detection method of Heiguteng exract |
Non-Patent Citations (3)
Title |
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HPLC同时测定银黄颗粒中7种有机酸及4种黄酮类成分;杨世艳 等;《中草药》;20130228;第44卷(第3期);摘要,第302页 * |
基于指纹图谱的金银花物质组纯化工艺研究;李守信 等;《中草药》;20150131;第46卷(第1期);摘要,第56-57页 * |
黑骨藤超高效液相色谱特征图谱的研究;赵喜玲 等;《药物分析杂志》;20161231;第36卷(第11期);摘要,第1964-1965页 * |
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Address after: 550025 South Road, University Town, Huaxi District, Guizhou, Guiyang Applicant after: Guizhou University of Traditional Chinese Medicine Address before: 550025 South Road, University Town, Huaxi District, Guizhou, Guiyang Applicant before: Guiyang College of Traditional Chinese Medicine |
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Address after: 550025 No.4, Dongqing Road, Huaxi University Town, Huaxi District, Guiyang City, Guizhou Province Patentee after: Guizhou University of Traditional Chinese Medicine Address before: 550025 Dongqing South Road, Daxuecheng, Huaxi District, Guiyang City, Guizhou Province Patentee before: Guizhou University of Traditional Chinese Medicine |
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Application publication date: 20190531 Assignee: First Affiliated Hospital of Guizhou University of Traditional Chinese Medicine Assignor: Guizhou University of Traditional Chinese Medicine Contract record no.: X2021520000001 Denomination of invention: Establishment of HPLC fingerprint of effective parts of Celastrus angustifolia Granted publication date: 20200811 License type: Common License Record date: 20210305 |
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EC01 | Cancellation of recordation of patent licensing contract | ||
EC01 | Cancellation of recordation of patent licensing contract |
Assignee: First Affiliated Hospital of Guizhou University of Traditional Chinese Medicine Assignor: Guizhou University of Traditional Chinese Medicine Contract record no.: X2021520000001 Date of cancellation: 20221118 |