CN109810812A - A kind of safflower amino acid soap and preparation method thereof - Google Patents
A kind of safflower amino acid soap and preparation method thereof Download PDFInfo
- Publication number
- CN109810812A CN109810812A CN201910260719.1A CN201910260719A CN109810812A CN 109810812 A CN109810812 A CN 109810812A CN 201910260719 A CN201910260719 A CN 201910260719A CN 109810812 A CN109810812 A CN 109810812A
- Authority
- CN
- China
- Prior art keywords
- parts
- safflower
- amino acid
- acid soap
- oil
- Prior art date
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- 235000012661 lycopene Nutrition 0.000 description 1
- OAIJSZIZWZSQBC-GYZMGTAESA-N lycopene Chemical compound CC(C)=CCC\C(C)=C\C=C\C(\C)=C\C=C\C(\C)=C\C=C\C=C(/C)\C=C\C=C(/C)\C=C\C=C(/C)CCC=C(C)C OAIJSZIZWZSQBC-GYZMGTAESA-N 0.000 description 1
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- 239000004223 monosodium glutamate Substances 0.000 description 1
- 235000016709 nutrition Nutrition 0.000 description 1
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- Cosmetics (AREA)
- Detergent Compositions (AREA)
Abstract
The present invention relates to a kind of safflower amino acid soaps and preparation method thereof, safflower amino acid soap of the invention, using sodium cocoyl glutamate as substrate, the mixing of various plants extract is added after heating, demoulding obtains the safflower amino acid soap with reparation, moisturizing, beauty, anti-inflammatory and anti-aging function.Safflower, goldleaf and amino acid soap preferably merge, and by the way that the effective component in safflower to be uniformly dissolved among soap base, effectively play the effect of safflower effective component, the effect of greatly improving safflower property, reaction efficiency is high, and the reaction time is short, the dissolution rate of fully reacting, crocin is high；By adding goldleaf, make perfumed soap color stability, anti-oxidant, moisture proof, corrosion-resistant and anti-mildew, long-time service can promote skin metabolism, keep skin smooth fine and smooth, retain youthful vitality；Increase the shelf-life of safflower amino acid soap of the invention.
Description
Technical field
The invention belongs to technical field of daily necessities, and in particular to a kind of safflower amino acid soap and preparation method thereof.
Background technique
Perfumed soap is a kind of our common daily necessities washing products, and B.C. Rome can be traced using perfumed soap earliest by the mankind
Empire；Safflower is a kind of pure natural Chinese herbal medicine, and there are many trophic factors that chapiter includes, and contains a variety of carrotene
Class compound (crocin) is the principle active component in safflower, has the multiple efficacies such as anti-oxidant, antitumor, content
About 10-25%, wherein separating to obtain crocin (crocin) -1, crocin -2, crocin -3, crocin -4, trans-
With cis- safron dimethyl ester, α-or beta carotene, α-bayer acid (α-crocetin), zeaxanthin, lycopene, kind
Safflower hardship glucoside (picrocrocin).Another 0.4%-1.3% containing volatile oil, main (safranal) containing safranal in oil, is kind
Furthermore the decomposition product of safflower hardship glucoside contains Isorhamnetin, Kaempferide and vitamin B1 and Wei Sheng secondly containing eucalyptol, firpene etc.
Plain B2.
Existing safflower soap product, processing method usually add safflower when casting into mold, or will
Safflower is simply adhered to soap body surface, cause the effective component in safflower cannot sufficiently discharge or soap base combine, thus
Effective using effect is not had when in use.
In consideration of it, applying for this patent.
Summary of the invention
In order to solve the above problems existing in the present technology, the present invention provides a kind of safflower amino acid soap and its preparations
Method.Safflower amino acid soap has reparation, moisturizing, beauty, anti-inflammatory and anti-aging function.
It is an object of the present invention to provide a kind of safflower amino acid soaps.
Another object of the present invention is to provide a kind of preparation method of safflower amino acid soap.
The safflower amino acid soap of specific embodiment according to the present invention, the safflower amino acid soap by following raw material and
Pure water preparation, the raw material include: by weight
90-110 parts of sodium cocoyl glutamate；10-20 parts of triethanolamine；20-30 parts of glycerol；15-20 parts of D-sorbite；
15-25 parts of propylene glycol；5-7 parts of ethyl alcohol；5-10 parts of glycine betaine, 2-3 parts of ginseng seed oil；2-3 parts of ginseng root extract；Apricot kernel oil 2-
3 parts；2-3 parts of olive oil；2-3 parts of coconut oil；0.1-0.5 parts and goldleaf 0.006-0.01 parts of safflower；The pure water
For 5-10 parts by weight.
The safflower amino acid soap of specific embodiment according to the present invention, wherein the raw material includes: cocounut oil by weight
100 parts of acyl glutamic acid sodium；10 parts of triethanolamine；20 parts of glycerol；20 parts of D-sorbite；20 parts of propylene glycol；6 parts of ethyl alcohol；Beet
10 parts of alkali, 2 parts of oil of ginseng seed；2 parts of ginseng root extract；2 parts of apricot kernel oil；2 parts of olive oil；2 parts of coconut oil；Safflower
0.16 part and 0.006 part of goldleaf.
The safflower amino acid soap of specific embodiment according to the present invention, wherein the safflower is dry safflower
Pistil stigma, the goldleaf are goldleaf clast, and the partial size of the goldleaf is 0.10-0.15 microns, and purity is not less than 99%.
The safflower amino acid soap of specific embodiment according to the present invention, wherein at least contain in the ginseng root extract
There are 35% parts by weight alkene terpene substances and 4.0% parts by weight general ginsenoside.
The safflower amino acid soap of specific embodiment according to the present invention, wherein the preparation side of the ginseng root extract
Method, comprising the following steps:
S1: ginseng is cleaned, be put in baking room be dried to moisture content be 5-6%, be then cooled to 40 DEG C hereinafter,
It is ground into ginseng powder；
S2: the ginseng powder that step S1 is obtained is immersed in polar organic solvent and extracts 2-3h at a temperature of 60-80 DEG C, is obtained
To extracting solution, extracting solution is boiled off into the polar organic solvent at 60-80 DEG C, obtains mixing leaching liquor；
S3: mixing leaching liquor obtained in step S2 is immersed in non-polar organic solvent, at a temperature of 60-80 DEG C
Circulation extract 3-5h, be cooled to room temperature, filter, gained filtrate is boiled off at 60-80 DEG C the non-polar organic solvent to get
Ginseng root extract.
The safflower amino acid soap of specific embodiment according to the present invention, further, the ginseng powder, the polarity
The weight ratio of organic solvent and the non-polar organic solvent is 1:6:7, and the polar organic solvent is ethyl alcohol, described non-
Polar organic solvent is water.
The preparation method of the safflower amino acid soap of specific embodiment according to the present invention, including following preparation step:
(1) sodium cocoyl glutamate of above-mentioned parts by weight is heated to dissolving while stirring, then by triethanolamine, pure
Water purification, glycerol, D-sorbite, propylene glycol, ethyl alcohol, glycine betaine are added in the dissolved sodium cocoyl glutamate, are stirred
It mixes and is warming up to 80-90 DEG C, form amino acid soap base liquid until completely dissolved；
(2) ginseng seed oil, ginseng root extract, apricot kernel oil, olive oil and coconut oil are added to step (1) and obtained
The amino acid soap base liquid in mixed, 70 DEG C -90 DEG C of heat preservation dissolve and are simultaneously uniformly mixed, and safflower and goldleaf is then added
It keeps the temperature and is uniformly mixed, defoaming cooling forms soap lye；
(3) soap lye that step (2) obtains is injected in mold and is demoulded after cooled and solidified, overlay film is packed to get safflower ammonia
Base acid soap.
The preparation method of the safflower amino acid soap of specific embodiment according to the present invention, wherein in step (1), heating
Speed be 1-2 DEG C/min.The too fast reduction that will cause color change and effective component, the cleaning effect of finished product are bad.
The preparation method of the safflower amino acid soap of specific embodiment according to the present invention, wherein in step (2), be added
Safflower and goldleaf are simultaneously uniformly mixed, and after golden yellow after solution colour entire body and close saturation, natural lemon juice are added and is adjusted to pH
5.5, while defoaming is cooled to 45-65 DEG C of formation soap lye.Safflower and goldleaf is added and is uniformly mixed, is allowed to be uniformly suspended in it
In, form suspension.
The preparation method of the safflower amino acid soap of specific embodiment according to the present invention, wherein cooling in step (3)
The time of solidification is 4 hours or more, and through modifying punching press after demoulding, then overlay film packaging is to get safflower amino acid soap.
Sodium cocoyl glutamate, alias: cocounut oil acyl monosodium glutamate；N- cocoyl-Pidolidone list sodium, classification:
Anionic surfactant；Appearance: colourless to weak yellow liquid；White solid；Safety is high, extremely soft to skin, no
Easily cause allergy and phototoxicity；Foam is appropriate, and washing force is strong, has outstanding adaptability to hard water；It can be quickly by biological institute
It decomposes；Because containing fatty acid, therefore solution, micellelike can be made to obtain required viscosity；Suitable for solid fraction body, liquid body, paste, powder
The commodity of the various forms such as shape；The moisturizing adsorbed while increasing skin of ether sulfate such as (SLES) on the skin can be reduced
Performance；Damaged hair can effectively be repaired；Have the function of in acidic environment sterilization and it is antistatic, to the cardability of hair
Show splendid effect；It can be used for all kinds of creams systems, help emulsification, for increasing the moisture retention and patch skin of product；
Usage: can cooperate with compounding with a variety of surfactants, to reduce system irritation, increase skin moisture-keeping, enhance the comb of hair
Rationality and plentiful degree.Purposes: transparent system or (pearly-lustre) facial cleanser, shampoo, bath oil, soap, detergent, shaving cream, tooth
Cream and industrial products.
D-sorbite, alias sorbierite；It is odorless for white hygroscopic powder or crystalline powder, sheet or particle.It can be used for
Produce ascorbic raw material, nutritive sweetener, wetting agent, chelating agent and stabilizer；As toothpaste, cosmetics, tobacco tune
Humectant etc..
Glycine betaine is a kind of alkaloid, has strong moisture pick-up properties, so often using resistive connection in manufacture craft
Block agent processing.Antitumor, blood pressure lowering, anti-peptic ulcer and gastrointestinal dysfunction treat liver diseases；As feed addictive
Have the function of to provide methyl donor, some methionine can be saved；With adjusting internal osmotic pressure, mitigation stress, promote fatty generation
It thanks and is synthesized with protein, improve the function of lean meat percentage, and the curative effect of anticoccidial drug can be enhanced；It is used as in aquatic animal feed and lures
Eat agent.In the present invention, glycine betaine is used for Osmolyte regulator, and stabilizer can maintain Premeabilisation of cells pressure, and antitumor, blood pressure lowering promotees
Entering fat fat metabolism enhances immunity of organisms.
Safflower, main function are blood, have blood-nourishing, invigorate blood circulation, enrich blood, promoting circulation of blood, regulating blood condition, promote blood circulation and wait function
Energy.In addition, safflower also has activating microcirculation and removing stasis medicinal, removing pattogenic heat from the blood and toxic material from the body, resolving stagnation for tranquilization and other effects, irregular menstruation, menostasis, the postpartum stasis of blood are cured mainly
The gynecological diseases such as hemoperitoneum pain, infertile, to treatment cardiovascular and cerebrovascular disease, adjusting hepatic and renal function, three height of tune, antitumor cancers etc.
Significant in efficacy, safflower can also bring certain effect for beauty and skin care.The present invention plays moisturizing using safflower,
Improve skin cell and anti-aging, activating microcirculation and removing stasis medicinal, adjusts endocrine effect, finished product is to by qi depression to blood stasis endocrine disorder
Caused small pox and color spot effect are very good, are beneficial to speckle removing, acne removing.
Goldleaf is beneficial to treat the illnesss such as frightened epilepsy, demented, palpitaition and sore, the golden ultrafine particle of activity is used as in the present invention
It uses, by adding goldleaf, on the one hand can not only increase soap body glossiness keeps perfumed soap glittering and translucent, but also super as active gold
Fine particle can also enhance cutaneous permeability, optimize the absorption of nutriment, have after human body use and adjust skin soda acid nourishing flesh
Skin, the injury for preventing ultraviolet light exclude toxin, prevent pigmentogenic effect, and on the other hand, addition goldleaf can make perfumed soap color
Damp stables, anti-oxidant, moisture proof, corrosion-resistant and anti-mildew to improve the shelf-life of perfumed soap, and are planted with other in the present invention
Object extract liquor combines, and becomes and leads the wet factor, and effectively holding skin moisture, long-time service can promote skin metabolism, make skin
Smooth exquisiteness, retains youthful vitality.
Ginseng seed oil, ginseng seed oil of the invention pass through multi-stage separation supercritical CO2It is refined after extraction.Method of refining
Are as follows: it will be from multi-stage separation supercritical CO2Resulting ginseng seed crude oil is extracted, is added in molecular distillation sample jar, molecule is adjusted
Distillation technique parameter, i.e. vacuum degree 2-9Pa, 100-150 DEG C of vapo(u)rizing temperature, knifing rotating speed 100-300rmin-1, charging rate
10-50mL·min-1And 20-50 DEG C of condensation temperature, refining treatment is carried out, after the completion of refining process, opens heavy constituent outlet valve
Door collects resulting ginseng seed oil after refining.Skin can be made to keep moist for a long time with ginseng root extract collective effect, increased
Skin elasticity, bright color enable skin shine beautiful expression.
Apricot kernel oil, rich in the micro of protein, unsaturated fatty acid, vitamin, inorganic salts, dietary fiber and needed by human body
Element has the function of moistening lung, stomach invigorating, regains one's strength of body, and amygdalin is even more natural anti-cancer active matter, also has good
Antioxidative stabilizer.It is added to apricot kernel oil in the present invention and plays the role of moisturizing and anti-aging and flavouring.
Olive oil, be remainder of the olive fruit after all squeezing extraction process using chemolysis at
Obtained from reason.With moisten effect, so being widely used for production cosmetics, such as hair conditioner, shampoo, cream；May be used also
Prevent and treat AIDS virus diffusion.It is that it is utilized to moisten and oxidation resistant effect in the present invention.
Coconut oil plays the role of antibacterial, anti-inflammatory, oxidation resistant in the present invention.
The invention has the benefit that
1, various plants extract etc. is added using sodium cocoyl glutamate as substrate in safflower amino acid soap of the invention
The obtained safflower amino acid soap with reparation, moisturizing, beauty, anti-inflammatory and anti-aging function；Its finished product is as clear as crystal, is in
Golden yellow, good appearance, have certain cleaning skin effect, pH close to human skin, will not do harm to huamn body and according to
Lai Xing；
2, present inventor has found in studying for a long period of time, and safflower, goldleaf and amino acid soap can be merged preferably, leads to
It crosses and is uniformly dissolved in the effective component in safflower among soap base, effectively play the effect of safflower effective component, significantly
Safflower the effect of property is improved, reaction efficiency is high, and the reaction time is short, fully reacting, and the dissolution rate of crocin is high, is surveyed with HPLC
The content for determining crocin, the dissolution rate for measuring crocin after lemon juice is added may be up to 63% or more.Wherein, safflower and
The additive amount of goldleaf and mixed temperature are even more important, and safflower additive amount is few, then active constituent content is lower, safflower addition
The effect of amount mostly can not only improve cost, cause to waste, and will affect goldleaf, the stability of finished product, color and permeability；Gold
Foil content height can then generate the effects of discoloration, reduce the application value of crocin；The too high or too low for temperature of mixing can be made
At dissolution insufficient, the reduction of dissolution rate and effective component and the appearance of finished product.
3, a large amount of vegetable oil and other plant extract be joined in safflower amino acid soap of the invention, passes through cocounut oil
Acyl sodium glutamate and glycine betaine form a large amount of macromolecular network, lock the nutritional ingredient in plant extracts, are allowed to not
Easily flowing, improves the content of effective component to the full extent；
4, by addition goldleaf, on the one hand can not only increase soap body glossiness keeps perfumed soap glittering and translucent, but also as work
Property gold ultrafine particle can also enhance cutaneous permeability, optimize the absorption of nutriment, after human body use have adjust skin soda acid
The injury nourished skin, prevent ultraviolet light excludes toxin, prevents pigmentogenic effect, and on the other hand, addition goldleaf can make
Perfumed soap color stability, anti-oxidant, moisture proof, corrosion-resistant and anti-mildew, to improve the shelf-life of perfumed soap, and in the present invention
Other plant extract liquor combines, and becomes and leads the wet factor, and effectively holding skin moisture, long-time service can promote skin metabolism,
Keep skin smooth fine and smooth, retains youthful vitality；Increase the shelf-life of safflower amino acid soap of the invention.
Detailed description of the invention
Fig. 1 is the amino acid soap according to made of the specific embodiment 3 of invention；
Fig. 2 is the safflower amino acid soap according to made of the comparative example 2 of invention；
Fig. 3 is the amino acid soap according to made of the comparative example 3 of invention；
Fig. 4 is the safflower amino acid soap according to made of the comparative example 4 of invention；
Fig. 5 is the comparison diagram of the safflower amino acid soap according to made of the comparative example 5 of invention and the embodiment of the present invention 3,
In, 1 is safflower amino acid soap made of comparative example 5, and 2 be safflower amino acid soap made of the embodiment of the present invention 3；
Fig. 6 is commercially available safflower amino acid soap.
Specific embodiment
Specific embodiment is given below, explanation that the present invention will be further explained, it is pointed out that: the present invention not office
It is limited to following preferred forms, anyone skilled in the art can all show that other are various forms of under the inspiration of the present invention
Product, however, make any variation in its shape or structure, it is all that there is technical solution identical or similar to the present application,
It is within the scope of the present invention.
In the following embodiments, in 1 parts by weight generation, refers to 1g.
Embodiment 1
A kind of safflower amino acid soap is present embodiments provided, the safflower amino acid soap is by following raw material and pure water
Preparation, the raw material include: by weight
90 parts of sodium cocoyl glutamate；10 parts of triethanolamine；30 parts of glycerol；15 parts of D-sorbite；25 parts of propylene glycol；Second
5 parts of alcohol；10 parts of glycine betaine, 3 parts of oil of ginseng seed；3 parts of ginseng root extract；2 parts of apricot kernel oil；3 parts of olive oil；Coconut oil 2
Part；0.5 part and 0.006 part of goldleaf of safflower；The pure water is 10 parts by weight.
Preparation method, including following preparation step:
(1) sodium cocoyl glutamate of above-mentioned parts by weight is heated to dissolving while stirring, then by triethanolamine, pure
Water purification, glycerol, D-sorbite, propylene glycol, ethyl alcohol, glycine betaine are added in the dissolved sodium cocoyl glutamate, are stirred
It mixes and is warming up to 85 DEG C, form amino acid soap base liquid until completely dissolved；
(2) ginseng seed oil, ginseng root extract, apricot kernel oil, olive oil and coconut oil are added to step (1) and obtained
The amino acid soap base liquid in mixed, keep the temperature 80 DEG C dissolve and be uniformly mixed, then be added safflower and goldleaf heat preservation
It 80 DEG C and is uniformly mixed, defoaming cooling forms soap lye；
(3) soap lye that step (2) obtains is injected in mold and is demoulded after cooled and solidified, overlay film is packed to get safflower ammonia
Base acid soap.
Embodiment 2
A kind of safflower amino acid soap is present embodiments provided, the safflower amino acid soap is by following raw material and pure water
Preparation, the raw material includes: 100 parts of sodium cocoyl glutamate by weight；10 parts of triethanolamine；20 parts of glycerol；Sorbose
20 parts of alcohol；20 parts of propylene glycol；6 parts of ethyl alcohol；10 parts of glycine betaine, 2 parts of oil of ginseng seed；2 parts of ginseng root extract；2 parts of apricot kernel oil；Oil
2 parts of olive fruit oil；2 parts of coconut oil；0.16 part of dry safflower pistil stigma and partial size are 0.12 micron, and purity is not less than
0.006 part of 99% goldleaf clast；Pure water is 8 parts by weight；Wherein, 35% weight is at least contained in the ginseng root extract
Part alkene terpene substances and 4.0% parts by weight general ginsenoside；
The preparation method of ginseng root extract, comprising the following steps:
S1: ginseng is cleaned, and being put in baking room and being dried to moisture content is 5%, is then cooled to 38 DEG C, then powder
It is broken into ginseng powder；
S2: the ginseng powder that step S1 is obtained is immersed in polar organic solvent and extracts 3h at a temperature of 70 DEG C, is mentioned
Liquid is taken, extracting solution is boiled off into the polar organic solvent at 70 DEG C, obtains mixing leaching liquor；
S3: mixing leaching liquor obtained in step S2 is immersed in non-polar organic solvent, is followed at a temperature of 70 DEG C
Ring extracts 4h, is cooled to room temperature, and filters, gained filtrate is boiled off to the non-polar organic solvent at 70 DEG C to get ginseng
Extract；The weight ratio of the ginseng powder, the polar organic solvent and the non-polar organic solvent is 1:6:7,
The polar organic solvent is ethyl alcohol, and the non-polar organic solvent is water.
The preparation method of safflower amino acid soap, including following preparation step:
(1) sodium cocoyl glutamate of above-mentioned parts by weight being heated to dissolving while stirring, the speed of heating is 1 DEG C/
Then triethanolamine, pure water, glycerol, D-sorbite, propylene glycol, ethyl alcohol, glycine betaine are added to dissolved described by min
It in sodium cocoyl glutamate, stirs and is warming up to 90 DEG C, form amino acid soap base liquid until completely dissolved；
(2) ginseng seed oil, ginseng root extract, apricot kernel oil, olive oil and coconut oil are added to step (1) and obtained
The amino acid soap base liquid in mixed, keep the temperature 70 DEG C dissolve and be uniformly mixed, dry safflower gynoecium is then added
Column cap and goldleaf keep the temperature and are uniformly mixed, defoaming cooling, and after golden yellow after solution colour entire body and close saturation, natural lemon is added
PH is adjusted to 5.5 by juice, while defoaming is cooled to 45-65 DEG C, forms soap lye；
(3) through modifying punching press, overlay film after being demoulded after cooled and solidified 4 hours in the soap lye injection mold obtained step (2)
Packaging is to get safflower amino acid soap.
Embodiment 3
A kind of safflower amino acid soap is present embodiments provided, the safflower amino acid soap is by following raw material and pure water
Preparation, the raw material includes: 110 parts of sodium cocoyl glutamate by weight；20 parts of triethanolamine；20 parts of glycerol；Sorbose
20 parts of alcohol；15 parts of propylene glycol；7 parts of ethyl alcohol；5 parts of glycine betaine, 2 parts of oil of ginseng seed；2 parts of ginseng root extract；3 parts of apricot kernel oil；Oil
3 parts of olive fruit oil；2 parts of coconut oil；0.3 part and 0.01 part of goldleaf clast of dry safflower pistil stigma；Pure water is 5 weight
Part；Wherein, 35% parts by weight alkene terpene substances and the 4.0% total soap of parts by weight ginseng are at least contained in the ginseng root extract
Glycosides；
The preparation method of safflower amino acid soap, including following preparation step:
(1) sodium cocoyl glutamate of above-mentioned parts by weight being heated to dissolving while stirring, the speed of heating is 1 DEG C/
Then triethanolamine, pure water, glycerol, D-sorbite, propylene glycol, ethyl alcohol, glycine betaine are added to dissolved described by min
It in sodium cocoyl glutamate, stirs and is warming up to 90 DEG C, form amino acid soap base liquid until completely dissolved；
(2) ginseng seed oil, ginseng root extract, apricot kernel oil, olive oil and coconut oil are added to step (1) and obtained
The amino acid soap base liquid in mixed, keep the temperature 70 DEG C dissolve and be uniformly mixed, dry safflower gynoecium is then added
Column cap and goldleaf keep the temperature 70 DEG C and are uniformly mixed, defoaming cooling, after golden yellow after solution colour entire body and close saturation, are added natural
PH is adjusted to 5.5 by lemon juice, while defoaming is cooled to 45-65 DEG C, forms soap lye；
(3) through modifying punching press, overlay film after being demoulded after cooled and solidified 4 hours in the soap lye injection mold obtained step (2)
Packaging is to get safflower amino acid soap, as shown in Figure 1.
Comparative example 1
This comparative example provides a kind of safflower amino acid soap, and the safflower amino acid soap is by following raw material and pure water
Preparation, the raw material includes: 110 parts of sodium cocoyl glutamate by weight；20 parts of triethanolamine；20 parts of glycerol；Sorbose
20 parts of alcohol；15 parts of propylene glycol；7 parts of ethyl alcohol；5 parts of glycine betaine, 2 parts of oil of ginseng seed；3 parts of apricot kernel oil；3 parts of olive oil；Coconut
2 parts of oil；0.3 part and 0.01 part of goldleaf clast of dry safflower pistil stigma；Pure water is 5 parts by weight；
The preparation method of safflower amino acid soap, including following preparation step:
(1) sodium cocoyl glutamate of above-mentioned parts by weight being heated to dissolving while stirring, the speed of heating is 1 DEG C/
Then triethanolamine, pure water, glycerol, D-sorbite, propylene glycol, ethyl alcohol, glycine betaine are added to dissolved described by min
It in sodium cocoyl glutamate, stirs and is warming up to 90 DEG C, form amino acid soap base liquid until completely dissolved；
(2) ginseng seed oil, apricot kernel oil, olive oil and coconut oil are added to the amino acid that step (1) obtains
It is mixed in soap base liquid, keeps the temperature 70 DEG C and dissolve and be uniformly mixed, dry safflower pistil stigma and goldleaf is then added and protects
70 DEG C of temperature is simultaneously uniformly mixed, defoaming cooling, and after golden yellow after solution colour entire body and close saturation, natural lemon juice is added by pH tune
It is 5.5, while defoaming is cooled to 45-65 DEG C, forms soap lye；
(3) through modifying punching press, overlay film after being demoulded after cooled and solidified 4 hours in the soap lye injection mold obtained step (2)
Packaging is to get safflower amino acid soap.
This comparative example and embodiment 3 only difference is that, without ginseng root extract in raw material；Also do not add in preparation method
Add ginseng root extract.
Comparative example 2
This comparative example provides a kind of safflower amino acid soap, and the safflower amino acid soap is by following raw material and pure water
Preparation, the raw material includes: 110 parts of sodium cocoyl glutamate by weight；20 parts of triethanolamine；20 parts of glycerol；Sorbose
20 parts of alcohol；15 parts of propylene glycol；7 parts of ethyl alcohol；5 parts of glycine betaine, 2 parts of oil of ginseng seed；2 parts of ginseng root extract；3 parts of apricot kernel oil；Oil
3 parts of olive fruit oil；2 parts of coconut oil；1.0 parts and 0.01 part of goldleaf clast of dry safflower pistil stigma；Pure water is 5 weight
Part；Wherein, 35% parts by weight alkene terpene substances and the 4.0% total soap of parts by weight ginseng are at least contained in the ginseng root extract
Glycosides；
The preparation method of safflower amino acid soap, including following preparation step:
(1) sodium cocoyl glutamate of above-mentioned parts by weight being heated to dissolving while stirring, the speed of heating is 1 DEG C/
Then triethanolamine, pure water, glycerol, D-sorbite, propylene glycol, ethyl alcohol, glycine betaine are added to dissolved described by min
It in sodium cocoyl glutamate, stirs and is warming up to 90 DEG C, form amino acid soap base liquid until completely dissolved；
(2) ginseng seed oil, ginseng root extract, apricot kernel oil, olive oil and coconut oil are added to step (1) and obtained
The amino acid soap base liquid in mixed, keep the temperature 70 DEG C dissolve and be uniformly mixed, dry safflower gynoecium is then added
Column cap and goldleaf keep the temperature and are uniformly mixed, defoaming cooling, and after golden yellow after solution colour entire body and close saturation, natural lemon is added
PH is adjusted to 5.5 by juice, while defoaming is cooled to 45-65 DEG C, forms soap lye；
(3) through modifying punching press, overlay film after being demoulded after cooled and solidified 4 hours in the soap lye injection mold obtained step (2)
Packaging is to get safflower amino acid soap.
This comparative example and embodiment 3 only difference is that, be added to excessive safflower, finished product is as shown in Figure 2.
Comparative example 3
This comparative example provides a kind of safflower amino acid soap, and the safflower amino acid soap is by following raw material and pure water
Preparation, the raw material includes: 110 parts of sodium cocoyl glutamate by weight；20 parts of triethanolamine；20 parts of glycerol；Sorbose
20 parts of alcohol；15 parts of propylene glycol；7 parts of ethyl alcohol；5 parts of glycine betaine, 2 parts of oil of ginseng seed；2 parts of ginseng root extract；3 parts of apricot kernel oil；Oil
3 parts of olive fruit oil；2 parts of coconut oil；0.01 part of goldleaf clast；Pure water is 5 parts by weight；Wherein, in the ginseng root extract
At least contain 35% parts by weight alkene terpene substances and 4.0% parts by weight general ginsenoside；
The preparation method of safflower amino acid soap, including following preparation step:
(1) sodium cocoyl glutamate of above-mentioned parts by weight being heated to dissolving while stirring, the speed of heating is 1 DEG C/
Then triethanolamine, pure water, glycerol, D-sorbite, propylene glycol, ethyl alcohol, glycine betaine are added to dissolved described by min
It in sodium cocoyl glutamate, stirs and is warming up to 90 DEG C, form amino acid soap base liquid until completely dissolved；
(2) ginseng seed oil, ginseng root extract, apricot kernel oil, olive oil and coconut oil are added to step (1) and obtained
The amino acid soap base liquid in mixed, keep the temperature 70 DEG C and dissolve and be uniformly mixed, goldleaf is then added keeps the temperature and 70 DEG C and mix
It closes uniformly, defoaming cooling, after golden yellow after solution colour entire body and close saturation, natural lemon juice is added by pH and is adjusted to 5.5, simultaneously
Defoaming is cooled to 45-65 DEG C, forms soap lye；
(3) through modifying punching press, overlay film after being demoulded after cooled and solidified 4 hours in the soap lye injection mold obtained step (2)
Packaging is to get amino acid soap.
This comparative example and embodiment 3 only difference is that, safflower is not contained in raw material, is not added in preparation method yet
Safflower, finished product are as shown in Figure 3.
Comparative example 4
This comparative example provides a kind of safflower amino acid soap, and the safflower amino acid soap is by following raw material and pure water
Preparation, the raw material includes: 110 parts of sodium cocoyl glutamate by weight；20 parts of triethanolamine；20 parts of glycerol；Sorbose
20 parts of alcohol；15 parts of propylene glycol；7 parts of ethyl alcohol；5 parts of glycine betaine, 2 parts of oil of ginseng seed；2 parts of ginseng root extract；3 parts of apricot kernel oil；Oil
3 parts of olive fruit oil；2 parts of coconut oil and dry 0.3 part of safflower pistil stigma；Pure water is 5 parts by weight；Wherein, the people
Join and at least contains 35% parts by weight alkene terpene substances and 4.0% parts by weight general ginsenoside in root extract；
The preparation method of safflower amino acid soap, including following preparation step:
(1) sodium cocoyl glutamate of above-mentioned parts by weight being heated to dissolving while stirring, the speed of heating is 1 DEG C/
Then triethanolamine, pure water, glycerol, D-sorbite, propylene glycol, ethyl alcohol, glycine betaine are added to dissolved described by min
It in sodium cocoyl glutamate, stirs and is warming up to 90 DEG C, form amino acid soap base liquid until completely dissolved；
(2) ginseng seed oil, ginseng root extract, apricot kernel oil, olive oil and coconut oil are added to step (1) and obtained
The amino acid soap base liquid in mixed, keep the temperature 70 DEG C dissolve and be uniformly mixed, dry safflower gynoecium is then added
Column cap keeps the temperature 70 DEG C and is uniformly mixed, defoaming cooling, and after golden yellow after solution colour entire body and close saturation, natural lemon juice is added
PH is adjusted to 5.5, while defoaming is cooled to 45-65 DEG C, forms soap lye；
(3) through modifying punching press, overlay film after being demoulded after cooled and solidified 4 hours in the soap lye injection mold obtained step (2)
Packaging is to get safflower amino acid soap.
This comparative example and embodiment 3 only difference is that, without containing in goldleaf clast and preparation method in the raw material
Goldleaf clast is not added, and finished product is as shown in Figure 4 yet.
Comparative example 5
This comparative example provides a kind of safflower amino acid soap, and the safflower amino acid soap is by following raw material and pure water
Preparation, the raw material includes: 110 parts of sodium cocoyl glutamate by weight；20 parts of triethanolamine；20 parts of glycerol；Sorbose
20 parts of alcohol；15 parts of propylene glycol；7 parts of ethyl alcohol；5 parts of glycine betaine, 2 parts of oil of ginseng seed；2 parts of ginseng root extract；3 parts of apricot kernel oil；Oil
3 parts of olive fruit oil；2 parts of coconut oil；0.3 part and 0.01 part of goldleaf clast of dry safflower pistil stigma；Pure water is 5 weight
Part；Wherein, 35% parts by weight alkene terpene substances and the 4.0% total soap of parts by weight ginseng are at least contained in the ginseng root extract
Glycosides；
The preparation method of safflower amino acid soap, including following preparation step:
(1) sodium cocoyl glutamate of above-mentioned parts by weight being heated to dissolving while stirring, the speed of heating is 1 DEG C/
Then triethanolamine, pure water, glycerol, D-sorbite, propylene glycol, ethyl alcohol, glycine betaine are added to dissolved described by min
It in sodium cocoyl glutamate, stirs and is warming up to 90 DEG C, form amino acid soap base liquid until completely dissolved；
(2) ginseng seed oil, ginseng root extract, apricot kernel oil, olive oil and coconut oil are added to step (1) and obtained
The amino acid soap base liquid in mixed, keep the temperature 70 DEG C and dissolve and be uniformly mixed, then cool to 50 DEG C, be then added dry
Dry safflower pistil stigma and goldleaf keep the temperature 50 DEG C and are uniformly mixed, defoaming cooling, golden yellow and close to solution colour entire body
After saturation, natural lemon juice is added by pH and is adjusted to 5.5, while defoaming is cooled to 45-65 DEG C, forms soap lye；
(3) through modifying punching press, overlay film after being demoulded after cooled and solidified 4 hours in the soap lye injection mold obtained step (2)
The safflower ammonia that packaging obtains to get safflower amino acid soap, the safflower amino acid soap and embodiment 3 of the formation of this comparative example 5
Base acid soap is compared as shown in Figure 5.
It tests group Shanghai Co., Ltd through spectrum Buddhist nun to detect the finished product of the embodiment of the present invention 3, testing result is such as
Shown in table 1:
The finished product detection result of 1 embodiment 3 of table
1-3 of the embodiment of the present invention and comparative example 1-5 finished product is taken to be detected respectively, wherein the detection method of crocin
Are as follows: take in 1-3 of the embodiment of the present invention and comparative example 1-4 finished product respectively without visible safranine chapiter etc. quality stripping and slicing, use
The content of HPCL measurement crocin.Comparing result is as shown in table 2:
Table 2 detects comparing result
Above-mentioned test proves, adds goldleaf, and on the one hand can not only increase soap body glossiness keeps perfumed soap glittering and translucent, but also
Cutaneous permeability can also be enhanced as active golden ultrafine particle, optimize the absorption of nutriment, there is adjuster after human body use
The injury that skin soda acid nourishes skin, prevents ultraviolet light excludes toxin, prevents pigmentogenic effect, on the other hand, adds goldleaf
Can make perfumed soap color stability, anti-oxidant, moisture proof, corrosion-resistant and anti-mildew, to improve the shelf-life of perfumed soap, and with this hair
Other plant extract liquor in bright combines, and becomes and leads the wet factor, and effectively holding skin moisture, long-time service can promote skin newly old
Metabolism keeps skin smooth fine and smooth, retains youthful vitality；Increase the shelf-life of safflower amino acid soap of the invention.
The additive amount and mixed temperature of safflower and goldleaf are even more important, and 0.14g safflower is added in 100g finished product and is
Good, safflower additive amount is few, then active constituent content is lower, safron loss by dissolution, and filigree color is thin out；Safflower adds
The effect of dosage mostly can not only improve cost, cause to waste, and will affect goldleaf, the stability of finished product, color and permeability,
Influence the beauty of finished product；The effects of goldleaf content height can then generate discoloration, fade, reduces the application value of crocin；Mixing
It is too high or too low for temperature will cause dissolve insufficient, the reduction of dissolution rate and effective component and the appearance of finished product.This reality
It applies the equal block shape of finished product all in example and comparative example to complete, surface is smooth.
Safflower amino acid soap of the invention is added various plants extract etc. and obtains using sodium cocoyl glutamate as substrate
The safflower amino acid soap with reparation, moisturizing, beauty, anti-inflammatory and anti-aging function arrived.
Safflower amino acid soap of the invention is used for 100 voluntary users, with above-described embodiment 1-3 and comparative example
Safflower amino acid soap made from 1-5 or amino acid soap are sample, make the daily bathing of user primary, after 25 days, 50 days, 75 days
The results are shown in Table 3 for the number of the skin quality improvement situation of observation user, the improvement of record skin quality and skin lubrication:
3 skin quality investigation result of table
| Group | Efficiently individual quantity after 25 days | Efficiently individual quantity after 50 days | Efficiently individual quantity after 75 days |
| Embodiment 1 | 36 | 65 | 86 |
| Embodiment 2 | 45 | 63 | 75 |
| Embodiment 3 | 53 | 73 | 91 |
| Comparative example 1 | 50 | 60 | 71 |
| Comparative example 2 | 55 | 59 | 83 |
| Comparative example 3 | 38 | 45 | 60 |
| Comparative example 4 | 42 | 61 | 76 |
| Comparative example 5 | 40 | 63 | 72 |
Safflower amino acid soap made from 1-3 of the embodiment of the present invention is applied to DPPH radicals scavenging effect expedition
Testing procedure: sample solution 1.5mL and DPPH solution 1.5mL are added in tool plug test tube, is protected from light after shaking up
30min measures absorbance (AS) at 517nm wavelength, while measuring 1.5mL0.1mmol/L DPPH solution and 1.5mL ethyl alcohol
The absorbance (AC) and 1.5mL sample solution of mixed liquor and the absorbance (AB) of 1.5mL alcohol mixeding liquid, calculation formula:
Safflower amino acid soap made from 1-3 of the embodiment of the present invention has the effect for removing DPPH free radical, and embodiment 1 is made
The safflower amino acid soap obtained is 39.7% to the clearance rate of two kinds of free radicals, safflower amino acid soap pair made from embodiment 2
The clearance rate of two kinds of free radicals is close to 45.5%, clearance rate of the safflower amino acid soap made from embodiment 3 to two kinds of free radicals
It is 59.3%, close to 60%；Safflower amino acid soap made from comparative example 1 is 21.1% to the clearance rate of two kinds of free radicals, right
Safflower amino acid soap made from ratio 2 is 23.5% to the clearance rate of two kinds of free radicals, safflower amino made from comparative example 3
Sour soap is 11.3% to the clearance rates of two kinds of free radicals, and safflower amino acid soap made from comparative example 4 is clear to two kinds of free radicals
Except rate is 32.9%, safflower amino acid soap made from comparative example 5 is 17.7% to the clearance rate of two kinds of free radicals, illustrates this hair
Bright product has preferable effect at anti-oxidant aspect.
In short, comparative example 1 is not added with ginseng root extract, inoxidizability is not so good, and comparative example 2 is added to excessive
Safflower, although crocin content is higher, finished product dirt-removing power is poor, and the experience effect of user is not very good；It is right
Ratio 3 is not added with safflower, and crocin content is lower, and the effect for improving skin quality is bad；Comparative example 4 is not added with goldleaf, improves
The effect of skin quality is bad；Temperature when the mixing safflower of comparative example 5 and goldleaf is lower, causes crocin dissolution rate low.
Existing safflower soap product, as shown in fig. 6, its processing method is usually to add hiding into mold when casting
Safflower, or safflower is simply adhered to soap body surface causes the effective component in safflower that cannot sufficiently discharge or soap base
In conjunction with to not have effective using effect when in use.Safflower amino acid soap of the invention, is by the effective of safflower
Ingredient is uniformly dissolved into soap base, and the another goldleaf and other plant extracts etc. of being added play any a part in finished product can
To identical reparation, moisturizing, beauty, anti-inflammatory and anti-aging function.
Claims (10)
1. a kind of safflower amino acid soap, which is characterized in that the safflower amino acid soap is prepared by following raw material and pure water,
The raw material includes: by weight
90-110 parts of sodium cocoyl glutamate；10-20 parts of triethanolamine；20-30 parts of glycerol；15-20 parts of D-sorbite；The third two
15-25 parts of alcohol；5-7 parts of ethyl alcohol；5-10 parts of glycine betaine, 2-3 parts of ginseng seed oil；2-3 parts of ginseng root extract；2-3 parts of apricot kernel oil；
2-3 parts of olive oil；2-3 parts of coconut oil；0.1-0.5 parts and goldleaf 0.006-0.01 parts of safflower；The pure water is 5-
10 parts by weight.
2. safflower amino acid soap according to claim 1, which is characterized in that the raw material includes: cocounut oil by weight
100 parts of acyl glutamic acid sodium；10 parts of triethanolamine；20 parts of glycerol；20 parts of D-sorbite；20 parts of propylene glycol；6 parts of ethyl alcohol；Beet
10 parts of alkali, 2 parts of oil of ginseng seed；2 parts of ginseng root extract；2 parts of apricot kernel oil；2 parts of olive oil；2 parts of coconut oil；Safflower
0.16 part and 0.006 part of goldleaf.
3. safflower amino acid soap according to claim 1, which is characterized in that the safflower is that dry safflower is female
Stamen column cap, the goldleaf are goldleaf clast, and the partial size of the goldleaf is 0.10-0.15 microns, and purity is not less than 99%.
4. safflower amino acid soap according to claim 1, which is characterized in that at least contain in the ginseng root extract
35% parts by weight alkene terpene substances and 4.0% parts by weight general ginsenoside.
5. safflower amino acid soap according to claim 1, which is characterized in that the preparation side of the ginseng root extract
Method, comprising the following steps:
S1: ginseng is cleaned, and being put in baking room and being dried to moisture content is 5-6%, is then cooled to 40 DEG C hereinafter, crushing
At ginseng powder；
S2: the ginseng powder that step S1 is obtained is immersed in polar organic solvent and extracts 2-3h at a temperature of 60-80 DEG C, is mentioned
Liquid is taken, extracting solution is boiled off into the polar organic solvent at 60-80 DEG C, obtains mixing leaching liquor；
S3: mixing leaching liquor obtained in step S2 is immersed in non-polar organic solvent, is recycled at a temperature of 60-80 DEG C
3-5h is extracted, is cooled to room temperature, filters, gained filtrate is boiled off to the non-polar organic solvent at 60-80 DEG C to get ginseng
Root extract.
6. safflower amino acid soap according to claim 5, which is characterized in that the ginseng powder, the polarity are organic
The weight ratio of solvent and the non-polar organic solvent is 1:6:7, and the polar organic solvent is ethyl alcohol, the nonpolarity
Organic solvent is water.
7. a kind of method for preparing the safflower amino acid soap as described in any one of claim 1-6, which is characterized in that including such as
Lower preparation step:
(1) sodium cocoyl glutamate of above-mentioned parts by weight is heated to dissolving while stirring, then by triethanolamine, pure
Water, glycerol, D-sorbite, propylene glycol, ethyl alcohol, glycine betaine are added in the dissolved sodium cocoyl glutamate, stirring
And it is warming up to 80-90 DEG C, amino acid soap base liquid is formed until completely dissolved；
(2) ginseng seed oil, ginseng root extract, apricot kernel oil, olive oil and coconut oil are added to the institute that step (1) obtains
It states and is mixed in amino acid soap base liquid, 70 DEG C -90 DEG C of heat preservation dissolve and are uniformly mixed, and safflower and goldleaf heat preservation is then added
And be uniformly mixed, defoaming cooling forms soap lye；
(3) soap lye that step (2) obtains is injected in mold and is demoulded after cooled and solidified, overlay film is packed to get safflower amino acid
Soap.
8. the preparation method of safflower amino acid soap according to claim 7, which is characterized in that described to add in step (1)
The speed of heat is 1-2 DEG C/min.
9. the preparation method of safflower amino acid soap according to claim 7, which is characterized in that in step (2), hiding is added
Safflower and goldleaf are simultaneously uniformly mixed, and after golden yellow after solution colour entire body and close saturation, natural lemon juice are added and is adjusted to pH
5.5, while defoaming is cooled to 45-65 DEG C of formation soap lye.
10. the preparation method of safflower amino acid soap according to claim 7, which is characterized in that cooling in step (3)
The time of solidification is 4 hours or more, and through modifying punching press after demoulding, then overlay film packaging is to get safflower amino acid soap.
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110484376A (en) * | 2019-09-12 | 2019-11-22 | 贵州沐木皙颜生物科技有限公司 | A kind of white tea amino acid nanometer transparent soap and its processing method |
| CN109810812B (en) * | 2019-04-02 | 2021-04-06 | 刘伟剑 | Saffron crocus amino acid soap and preparation method thereof |
| CN112812902A (en) * | 2021-02-01 | 2021-05-18 | 湖南医药学院 | Acne-removing and freckle-removing medicated soap and preparation method thereof |
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| CN109810812B (en) * | 2019-04-02 | 2021-04-06 | 刘伟剑 | Saffron crocus amino acid soap and preparation method thereof |
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| CN109810812B (en) * | 2019-04-02 | 2021-04-06 | 刘伟剑 | Saffron crocus amino acid soap and preparation method thereof |
| CN110484376A (en) * | 2019-09-12 | 2019-11-22 | 贵州沐木皙颜生物科技有限公司 | A kind of white tea amino acid nanometer transparent soap and its processing method |
| CN112812902A (en) * | 2021-02-01 | 2021-05-18 | 湖南医药学院 | Acne-removing and freckle-removing medicated soap and preparation method thereof |
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