CN109809757A - A kind of preparation and application of the aqueous high molecular material with sandstone style and a construction molding - Google Patents
A kind of preparation and application of the aqueous high molecular material with sandstone style and a construction molding Download PDFInfo
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Abstract
The present invention relates to a kind of preparation and application of aqueous high molecular material with sandstone style and a construction molding.Specifically, the invention discloses a kind of aqueous high molecular material and its preparation method and application, the composition of the aqueous high molecular material is detailed in specification.The present invention makes it have construction molding of architectural style and energy for sandstone by addition sand and additive under the premise of guaranteeing identical aqueous high molecular material property.It not only can solve the high disadvantage of the cumbersome of exterior wall texture style facing, cost in this way, but also the single situation of general low price cement base facing style can be improved, and promoted the development of exterior wall finish, meet the environmental protection policy of national energy conservation and emission reduction.
Description
Technical field
The invention belongs to the field of building materials, more particularly to it is a kind of with sandstone style and construction molding it is aqueous
The preparation and application of high molecular material.
Background technique
With the exploitation in national city and the development of Urbanization Construction, people are increasingly heavier to the exterior wall finish of building
Depending on.On the decoration of exterior wall of some high-grade cells, except materials such as the glazed tiles, mosaic, marble being widely used, there are also true
Mineral varnish, mastic paint and the texture exterior coating such as colorful, these decoration of exterior wall are that building increases beautiful color and magnificent matter
Sense, thus by the favor of people.However, whether marble or lacquer, these exterior wall finish are pasted due to cost height, edge
The factors such as many and diverse, heavy workload, limit its scope of application.It, may be because being negative when ceramic tile is as skyscraper finish coat
, there is brick risk in the problems such as wind pressure, there is certain risk；The construction of the texture exterior coating such as lacquer, mastic paint, colorful
The process is more complicated, and construction system is complicated, including priming paint, middle painting, finishing coat, cover etc., and typically at least need to construct 2-3 ability
Reach texture effect, cost of labor, time cost consumption are larger.
In recent years, China had introduced a kind of novel aqueous high molecular ornament materials from foreign countries, and its advantages are that moulding is rich
Richness, color variation range are wide.It is made of cementitious material, aggregate, polymeric binder, pigment and additive etc., main to use
In construction wall surface and the decoration of ceiling.Its thermodynamic property is close with the decorative mortar in exterior wall heat-preserving system, is more suitable for
Make the exterior facing of exterior wall heat-preserving system.Thickness is only 1-3mm, and light weight avoids tile decorative surface due to the reasons such as negative wind pressure
The drawbacks of falling off, so that external thermal insulation system be made to have more safety in use；It is prepared with organic materials such as coating
Finish coat is compared, it more preferably, is more matched with the outer heat preservation system compatibility for belonging to inorganic material.
In developed country, this aqueous high molecular material has replaced ceramic tile and coating to be widely used in the inner, external wall of building
Decoration.Although due to its excellent performance and meeting currently, it is also very low in the occupation rate of market of China's ornament materials
The development trend of " safe and environment-friendly, energy saving ", with research application further deeply, will certainly in China's modern building,
Decoration of exterior wall opens up a new approach, especially on the exterior facing of exterior wall heat-preserving system.
Summary of the invention
The purpose of the present invention is to provide a kind of aqueous high molecular material with sandstone style and construction molding and
Preparation method and application.
First aspect present invention provides a kind of aqueous high molecular material, and the aqueous high molecular material contains following component
Or it is grouped as by following group:
Cement: 15~35 parts by weight
Coarse sand: 30~50 parts by weight
Fine sand: 10~30 parts by weight
Filler: 10~30 parts by weight
Additive: 0.8~18 parts by weight.
In another preferred example, the additive contains following component or is grouped as by following group:
Rubber powder: 8~15 parts by weight
Hydrophober: 0.1~0.5 parts by weight
Cellulose ether: 0.1~0.5 parts by weight
Starch ether: 0.1~0.5 parts by weight
Toner: 0.5~3 parts by weight.
In another preferred example, the cement is one or more of aluminate cement, portland cement；And/or
The intensity (MPa) of the cement selects in 32.5,42.5 and 52.5.
In another preferred example, the coarse sand is one or more of general white sand, river sand, quartz sand, and described
The mesh number of coarse sand is between 10-40 mesh.
In another preferred example, the mesh number of the coarse sand is in 10-20.
In another preferred example, the fine sand is one or more of general white sand, river sand, quartz sand, and described
The mesh number of fine sand is between 40-180 mesh.
In another preferred example, the mesh number of the fine sand is in 40-80.
In another preferred example, the filler is selected from one or more of dry powder, silica flour, mica powder.
In another preferred example, the rubber powder is selected from copolymer, the vinyl acetate-versatic acid of ethylene-vinyl acetate
One or more of ethylene copolymer, acrylic copolymer, ethylene-vinyl laurate-vinyl chloride terpolymer；With/
Or
The hydrophober is modified organic silicon class hydrophober；And/or
The cellulose ether is selected from methylcellulose, hydroxyethylmethylcellulose, carboxymethyl cellulose, ethyl cellulose
Element, benzylcellulose, hydroxyethyl cellulose, hydroxypropyl methyl cellulose, cyanethyl cellulose, benzyl cyanethyl cellulose, carboxylic
One or more of methyl hydroxyethylcellulose and benzyl cellulose；And/or
The starch ether is selected from one or more of hydroxyalkyl starch ether, carboxymethyl starch ether, cationic starch ether；
And/or
The toner is inorganic toner and/or organic toner.
In another preferred example, the hydrophober is redispersible alkane silicon substrate hydrophober.
In another preferred example, the inorganic toner is selected from one of iron oxide yellow, iron oxide red, iron oxide black or several
Kind.
In another preferred example, organic toner is selected from one or more of organic red, organic yellow.
Second aspect of the present invention provides a kind of preparation method of aqueous high molecular material described in first aspect present invention, institute
Method is stated comprising steps of under agitation, cement, coarse sand and fine sand, filler and additive are uniformly mixed, to obtain
The aqueous high molecular material.
In another preferred example, the time required for the mixing is 400-800s.
In another preferred example, the time required for the mixing is 600s.
In another preferred example, the cement, the coarse sand and fine sand, the filler and the additive point
Not not as described above.
Third aspect present invention provides a kind of application of aqueous high molecular material described in first aspect present invention, this is sent out
Aqueous high molecular material described in bright first aspect is applied to metope, and specific steps include:
Aqueous high molecular material described in water and first aspect is mixed with weight ratio for the ratio of 1:4.5-4, is sufficiently stirred
It mixes uniformly, carries out criticizing using commonly batch knife scraping, and polished with plastics polishing plate.
In another preferred example, the polishing should carry out immediately after batch scraping.
In another preferred example, machine stirring can be used in described stir, and stirs 3min or more.
It should be understood that above-mentioned each technical characteristic of the invention and having in below (eg embodiment) within the scope of the present invention
It can be combined with each other between each technical characteristic of body description, to form a new or preferred technical solution.As space is limited, exist
This no longer tires out one by one states.
Specific embodiment
The present inventor's in-depth study by long-term, is unexpectedly prepared a kind of aqueous high molecular material.The material
In practical external wall construction in application, can have the texture effect of sandstone, and can a construction molding.Specifically, the present inventor
By adding additive or auxiliary agent (rubber powder, hydrophober, cellulose ether, starch ether and color in cement, coarse sand, fine sand, filler
Powder), a kind of aqueous high molecular material with sandstone style, a material construction molding of energy is prepared, and can obviously change
Kind this complicated drawback of exterior wall texture decoration construction also is compliant with country to be greatly promoted the development of external wall decorative material
The development trend of " energy-saving and environmental protection ".On this basis, inventor completes the present invention.
Aqueous high molecular material
The present invention provides a kind of aqueous high molecular material, the high molecular material contains following component or by following component
It constitutes:
Cement: 15~35 parts by weight
Coarse sand: 30~50 parts by weight
Fine sand: 10~30 parts by weight
Filler: 10~30 parts by weight
Additive: 8~18 parts by weight.
In another preferred example, cement is 17~30 parts by weight, preferably, 20~30 parts by weight.
In another preferred example, coarse sand is 35~45 parts by weight, preferably, 40~45 parts by weight.
In another preferred example, fine sand is 15~25 parts by weight, preferably, 20~25 parts by weight.
In another preferred example, filler is 15~25 parts by weight, preferably, 20~25 parts by weight.
In another preferred example, additive is 10~18 parts by weight, preferably, 10~15 parts by weight.
The cement is one or more of aluminate cement, portland cement, intensity (MPa) 32.5,
It is selected in 42.5 and 52.5.
The coarse sand is one or more of general white sand, river sand, quartz sand, and white in appearance is granular, and free from admixture is built
Build intensity height, stable chemical performance.Mesh number selects between 10-40 mesh.
The fine sand is one or more of general white sand, river sand, quartz sand, and appearance is in powdery, graininess, no dirt
Dye, free from admixture, stable chemical performance, sphericity are preferable.Mesh number selects between 40-180 mesh.
The filler is the inert solid material of filling in the material, is generally not involved in reaction, has certain covering to make
With.The filler, selected from one or more of solid materials such as dry powder, silica flour, mica powder.
Additive used in the present invention also contains rubber powder, hydrophober, cellulose ether, starch ether, toner, specific volume
It is as follows:
Rubber powder: 8~15 parts by weight (preferably, 10~15 parts by weight；More preferably, 10~12 parts by weight)
Hydrophober: 0.1~0.5 parts by weight (preferably, 0.1~0.4 parts by weight；More preferably, 0.2~0.4 parts by weight)
Cellulose ether: 0.1~0.5 parts by weight (preferably, 0.1~0.4 parts by weight；More preferably, 0.2~0.4 parts by weight)
Starch ether: 0.1~0.5 parts by weight (preferably, 0.1~0.4 parts by weight；More preferably, 0.2~0.4 parts by weight)
Toner: 0.5~3 parts by weight (preferably, 0.5~2.5 parts by weight；More preferably, 1~2 parts by weight).
The rubber powder is redispersable latex powder, this powder after contact with water can quickly redisperse at lotion,
Since redispersable latex powder has high cementitiousness and unique performance, such as water-resistance, application property and thermal insulation etc..Described
Copolymer of the rubber powder selected from ethylene-vinyl acetate, vinyl acetate-versatic acid ethylene copolymer, one in acrylic copolymer
Kind is several.
The hydrophober, actually a kind of auxiliary agent with hydrophobic effect have antiacid alkali, ageing-resistant, anti-carbon
The functions such as change, the accumulation of salt in the surface soil, moisture-proof, mould proof.Currently, common hydrophober is modified organic silicon class hydrophober, its hydrophobic mechanism is
Using chemical affinity stronger between organo-silicon compound and inorganic silicate material, effectively to change silicate material
Surface characteristic makes up to hydrophobic effect.It has the characteristics that stability it is good, it is at low cost, apply simple process.
The cellulose ether is a kind of high-molecular compound made of cellulose with ether structure, can be dissolved in
Water, dilute alkaline soln and organic solvent, and there is certain thermoplasticity and water-retaining property.In construction, there is construction feel well
With very strong slip resistance.The cellulose ether is mainly selected from methylcellulose, hydroxyethylmethylcellulose, carboxymethyl cellulose
Element, ethyl cellulose, benzylcellulose, hydroxyethyl cellulose, hydroxypropyl methyl cellulose, cyanethyl cellulose, benzyl cyanide second
One or more of base cellulose, carboxymethyl hydroxyethyl cellulose and benzyl cellulose etc..
The starch ether refers to that etherification starch, etherification starch refer to hydroxyl and reactive substance in starch molecule
React the starch substituent group ether generated.Since the etherification of starch improves viscosity stability, and ether under strongly alkaline conditions
Key is less likely to occur to hydrolyze, and therefore, etherification starch is applied in many industrial circles.The starch ether is selected from hydroxyalkyl
One or more of starch ether, carboxymethyl starch ether, cationic starch ether etc..
The toner is a kind of powdered rubber for colouring, in the media such as water, grease, resin, organic solvent not
Dissolution, but can equably disperse in these media and medium can be made to colour, and there is certain covering power.The color
Powder is selected from inorganic toner (such as iron oxide yellow, iron oxide red, iron oxide black) and organic toner (such as organic red, organic yellow)
One or more of.
The preparation method of aqueous high molecular material
Aqueous high molecular material of the invention can be made by the following method, and described method includes following steps: stir
Under the conditions of, by cement, coarse sand and fine sand, filler and additive, it is uniformly mixed (such as after stirring 600s), is obtained described aqueous
High molecular material.
Cement, the coarse sand and the fine sand, the filler, the additive (rubber powder, hydrophober, fiber
Plain ether, starch ether, toner) as described above.
The application of aqueous high molecular material
Aqueous high molecular material of the invention can be used for exterior wall, such as: a certain amount of water is weighed, according to water and material of the present invention
Expect that weight ratio is the ratio of 1:4.5-4, add aqueous high molecular material of the present invention, machine stirs 3min or more, sufficiently
It stirs evenly, carries out criticizing using commonly batch knife scraping, and polished with plastics polishing plate.
Polishing should carry out immediately, and large-area construction coordinative construction, a people crowd must scrape in double harness, another person's polishing.
Pay attention to receiving and be scraped, mortar thickness is the diameter of maximum sand grains, and thickness is excessive to will affect grinding effect.
Main advantages of the present invention include:
Aqueous high molecular material of the invention provides a kind of sandstone decoration effect similar with mastic paint for outer surface of wall
Fruit greatly reduces exterior wall texture under the premise of guaranteeing the exterior walls performances such as corresponding compression strength, flexural strength, water absorption
The construction technology of ornament materials shortens construction period, saves cost of labor.
This aqueous high molecular material prepared material and can reach colourful design, for the modern times by different
Building decorating inner and external walls open up a new way, and meet the development trend requirement of " safety and environmental protection, energy conservation ".
Present invention will be further explained below with reference to specific examples.It should be understood that these embodiments are merely to illustrate the present invention
Rather than it limits the scope of the invention.In the following examples, the experimental methods for specific conditions are not specified, usually according to conventional strip
Part or according to the normal condition proposed by manufacturer.Unless otherwise stated, otherwise percentage and number are calculated by weight.
Unless otherwise defined, it anticipates known to all professional and scientific terms as used herein and one skilled in the art
Justice is identical.In addition, any method similar to or equal to what is recorded and material can be applied to the method for the present invention.Wen Zhong
The preferred implement methods and materials are for illustrative purposes only.
The preparation of the aqueous high molecular material of Examples 1 to 5 different colours
Different raw materials is accurately weighed according to the proportion by weight in table 1, is opened stirring, is sequentially added the raw material in table 1,
After stirring 600s, side is uniformly mixed.Then the water of addition 17~22% stirs evenly, and constructs.
The mass parts of each component in 1 Examples 1 to 5 of table
In table " -- " indicate without.
The aluminate cement that cement used in Examples 1 to 5 is 32.5.
Coarse sand used in Examples 1 to 5 is 10-20 mesh quartz sand.
Fine sand used in Examples 1 to 5 is 40-80 mesh quartz sand.
Filler used in Examples 1 to 5 is dry powder, and main component is powdered whiting, and content is more than or equal to
98%, white in appearance, oil absorption is in 12-16ml/100g, and pH value between 8-10, stablize by performance.
Rubber powder used in Examples 1 to 5 is that one kind is made of ethylene-vinyl laurate-vinyl chloride terpolymer
Redispersable latex powder, meet water after can disperse again.When being used in mixed way with inorganic base material, which can assign aqueous height
The stronger caking property of molecular material, flexural strength, deformability and wearability, and be easy to construct.
Hydrophober used in Examples 1 to 5 is redispersible alkane silicon substrate hydrophober, especially suitable as special additive
Conjunction uses outdoors and in wet environment, has splendid hydrophobicity, can greatly reduce the water absorption rate of finished product, strong to bending resistance
Degree, compression strength and wearability slightly have improvement result.
Cellulose ether used in Examples 1 to 5 is the modified hydroxypropyl methyl cellulose of grafting Compositional type, is had excellent
Application property, the sufficient open hour, thermal stability is good, very strong slip resistance.
Starch ether used in Examples 1 to 5 is hydroxypropyl starch ether.It is by starch and propylene oxide or epoxychloropropane
Reaction obtains under alkaline condition.Hydroxypropyl has good hydrophily, can provide starch ether splendid water retention property.Hydroxypropyl
It for nonionic, is influenced small, can be used under the conditions of wider soda acid pH, and replace the stability of ehter bond by electrolyte
Height, substituent group all will not fall off in the chemical reaction processes such as hydrolysis, oxidation, crosslinking.Excellent anti-sag and construction can be provided
Property.When being used in compounding with above-mentioned cellulose ether, synergistic effect can be generated, the water retention property of the aqueous high molecular material is reinforced.
Other than assigning the certain viscosity of the aqueous high molecular material, moreover it is possible to which the characteristic for smooth non-stick knife of constructing is provided.
Toner used in Examples 1 to 5 is inorganic toner, is selected from iron oxide yellow, iron oxide red, iron oxide black.
The test result of Examples 1 to 5 can be seen that under the Different adding amount of toner, can prepare different colours
Aqueous high molecular material can a construction molding after being diluted with water and constructing according to construction technology.
Comparative example 1
With embodiment 1, difference is that 12 parts by weight rubber powders are changed to 12 parts by weight fine sands.
Comparative example 2
With embodiment 1, difference is: 0.3 parts by weight hydrophober is changed to 0.3 parts by weight fine sand.
The mass parts of 2 embodiment 1 of table and comparative example 1,2 each components
In table " -- " indicate without.
Experimental example
According to JC/T 1024-2007 wall facing mortar professional standard to the resulting high molecular material of Examples 1 to 5
The full performance such as operable time, initial dry cracking resistance, water absorption, intensity, alkali burnout resistance, stain resistance, weatherability is surveyed
Examination, the results are shown in Table 2.
3 wall facing mortar professional standard of table
From table 3 it can be seen that the operable time of aqueous high molecular material made from Examples 1 to 5, initial stage dry cracking resistance
The full performance such as property, water absorption, intensity, alkali burnout resistance, stain resistance, weatherability, is to meet JC/T 1024-2007 wall facing
Mortar professional standard.
Comparative experiments example
The same experimental example of method, difference are the material of the material alternative embodiment 1-5 using comparative example 1 and comparative example 2.
4 wall facing mortar professional standard of table
From table 4, it can be seen that the operable time of aqueous high molecular material made from comparative example 1,2, initial stage dry cracking resistance
Property, the full performance such as water absorption, intensity, alkali burnout resistance, stain resistance, weatherability, be not meet JC/T 1024-2007 wall decorations
Facing sand starches professional standard.Reason is that rubber powder used in Examples 1 to 5 is a kind of redispersable latex powder, can after chance water
Disperse again.When being used in mixed way with inorganic base material, it is strong which can assign the stronger caking property of aqueous high molecular material, anti-folding
Degree etc., when not adding rubber powder in comparative example 1, product only relies on aluminate cement and later strength requirement is not achieved.Comparison
In example 2, hydrophober is not added, changes the surface tension of product, is had to its water absorption and alkali burnout resistance, stain resistance very big negative
Face is rung.
All references mentioned in the present invention is incorporated herein by reference, independent just as each document
It is incorporated as with reference to such.In addition, it should also be understood that, after reading the above teachings of the present invention, those skilled in the art can
To make various changes or modifications to the present invention, such equivalent forms equally fall within model defined by the application the appended claims
It encloses.
Claims (10)
1. a kind of aqueous high molecular material, which is characterized in that the aqueous high molecular material contains following component or by such as the following group
It is grouped as:
Cement: 15~35 parts by weight
Coarse sand: 30~50 parts by weight
Fine sand: 10~30 parts by weight
Filler: 10~30 parts by weight
Additive: 0.8~18 parts by weight.
2. aqueous high molecular material as described in claim 1, which is characterized in that the additive contains following component or by such as
The following group is grouped as:
Rubber powder: 8~15 parts by weight
Hydrophober: 0.1~0.5 parts by weight
Cellulose ether: 0.1~0.5 parts by weight
Starch ether: 0.1~0.5 parts by weight
Toner: 0.5~3 parts by weight.
3. aqueous high molecular material as described in claim 1, which is characterized in that the cement is aluminate cement, silicic acid
One or more of salt cement；And/or the intensity (MPa) of the cement selects in 32.5,42.5 and 52.5.
4. aqueous high molecular material as described in claim 1, which is characterized in that the coarse sand is general white sand, river sand, quartz
One or more of sand, and the mesh number of the coarse sand is between 10-40 mesh.
5. aqueous high molecular material as described in claim 1, which is characterized in that the fine sand is general white sand, river sand, quartz
One or more of sand, and the mesh number of the fine sand is between 40-180 mesh.
6. aqueous high molecular material as described in claim 1, which is characterized in that the filler be selected from dry powder, silica flour,
One or more of mica powder.
7. aqueous high molecular material as claimed in claim 2, which is characterized in that
Copolymer, vinyl acetate-versatic acid ethylene copolymer, the acrylic acid that the rubber powder is selected from ethylene-vinyl acetate are total
One or more of polymers, ethylene-vinyl laurate-vinyl chloride terpolymer；And/or
The hydrophober is modified organic silicon class hydrophober；And/or
The cellulose ether is selected from methylcellulose, hydroxyethylmethylcellulose, carboxymethyl cellulose, ethyl cellulose, benzyl
Base cellulose, hydroxyethyl cellulose, hydroxypropyl methyl cellulose, cyanethyl cellulose, benzyl cyanethyl cellulose, carboxymethyl hydroxyl
One or more of ethyl cellulose and benzyl cellulose；And/or
The starch ether is selected from one or more of hydroxyalkyl starch ether, carboxymethyl starch ether, cationic starch ether；With/
Or
The toner is inorganic toner and/or organic toner.
8. the preparation method of aqueous high molecular material described in a kind of claim 1, which is characterized in that the method includes the steps:
Under agitation, cement, coarse sand and fine sand, filler and additive are uniformly mixed, to obtain described in claim 1
Aqueous high molecular material.
9. preparation method as claimed in claim 8, which is characterized in that the time required for the mixing is 400-800s.
10. the application of aqueous high molecular material described in a kind of claim 1, which is characterized in that by aqueous height described in claim 1
Molecular material is applied to metope, and specific steps include:
Water and aqueous high molecular material described in claim 1 are mixed with weight ratio for the ratio of 1:4.5-4, are sufficiently stirred
It is even, it carries out criticizing using commonly batch knife scraping, and polished with plastics polishing plate.
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| CN111171620A (en) * | 2019-11-19 | 2020-05-19 | 立邦涂料(四川)有限公司 | Foam-inhibiting putty with defoaming function and preparation method thereof |
| CN113930081A (en) * | 2021-11-30 | 2022-01-14 | 鲁东大学 | Preparation method of hypha-filled composite building block for building |
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Application publication date: 20190528 |