CN109805403A - A kind of fluffy extract of saline-alkali land and preparation method thereof - Google Patents
A kind of fluffy extract of saline-alkali land and preparation method thereof Download PDFInfo
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Abstract
A kind of fluffy extract of saline-alkali land and preparation method thereof, it is related to a kind of fluffy extract of saline-alkali land, the fluffy stem and leaf part of saline-alkali land and the fluffy seed part of saline-alkali land are extracted respectively, and it is different from the nutrient content of seed part according to the fluffy stem and leaf part of alkali, the ratio of saline-alkali land fluffy stem-leaf extract and the fluffy seed extract of saline-alkali land is deployed, the health food with special function is made.
Description
[technical field]
The present invention relates to a kind of fluffy extracts of saline-alkali land, more particularly, to a kind of fluffy extract of saline-alkali land and its preparation
Method.
[background technique]
Suaeda salsa is annual herb salification plant, and botany classification is Chenopodiaceae (chenopodiaceae) Suaeda
(suaeda forsk.exscop), is mainly grown on the saline-alkali wasteland at beach, lakeside, desert etc., is a kind of typical saline and alkaline
Ground indicator plant.Alkali is fluffy to have ecological protection and improvement result to soil, is known as " pionner " of alkaline land improvement.Research
It was found that the fluffy fresh and tender cauline leaf of alkali, the fluffy seed of alkali are full of nutrition, rich in fat, protein, crude fibre, minerals, microelement and more
Kind vitamin etc., great Development volue.
The nutritional ingredient of Suaeda salsa:
1, nutrient: the fluffy stem leaf protein matter of alkali, fat, carbohydrate three nutritious elements content are higher.The fluffy kind of alkali
Nutritional ingredient is completely enriched in son and cauline leaf, and seed fat content accounts for the 36.5% of dry matter, is higher than soybean, fresh and tender cauline leaf
Protein content account for the 40% of dry matter.
2, amino acid: measuring 16 kinds of amino acid altogether in Suaeda salsa, wherein there is 8 kinds of essential amino acids, and content compared with
It is high.Essential amino acid content is more superior than soybean, egg and spirulina in its cauline leaf and seed, close to world health group
The complete protein standard knitted.Research confirms that unsaturated fatty acid content is high in Suaeda plant seed, and produces rich in human body
Essential amino acid, linoleic acid, linolenic acid needed for development have expansion blood vessel, enhance human immunity, are depressured, hypoglycemic, prevention and treatment
The effect of cardiovascular disease, can be used for preventing cardiovascular disease, be the elderly, sub-healty adults and the excellent edible health of Healthy People
Oil.
3, microelement and Microbial anticorrosive additive: alkali is fluffy containing there are many essential trace elements of the human body and vitamins abundant.Its
Middle calcium, magnesium, zinc, iron, nickel content are abundant, and calcium, phosphorus, iron and core yellow cellulose content are much higher than vegetables such as spinach, tomato and carrots.
High 10 times of the more general food of alkalinity or so.Vitamin C content is higher than or is equivalent to general vegetables, and vitamin B content is general
5-8 times of vegetables is much higher than spirulina.
4, unsaturated fatty acid: the crude fat content of the fluffy seed of alkali considerably beyond soybean (crude fat content 23%-25%),
Unsaturated fatty acid content is abundant in seed, and the 90% of the total fat of Zhan, wherein the content of essential fatty acid is up to 70% or more,
Linolenic acid accounts for 6.08%, has the linolenic acid content of important health-care efficacy up to 6.08% human body in common seepweed seeds oil, with soybean oil
Quite with wheat malt oil, it is much higher than other common edible oils.Common seepweed seeds oil is rich in microelement Se, and liposoluble vitamin contains
Amount is higher, especially vitamin E, and content is up to 2mg/g, and numerous studies sufficiently show that common seepweed seeds oil has high nutrition to protect
Strong value, is a kind of table oil, can be used as new oil resource and developed.
5, haematochrome: fluffy alkali is natural haematochrome marennin source, and application publication number is the patent of CN102653634A
Document discloses a kind of method for extracting Betacyanins from Suaeda salsa by ultrasonic wave added, which provides one kind
The method that Betacyanins are extracted from Suaeda salsa can extract the fluffy haematochrome of alkali, haematochrome is in food in the Suaeda salsa red autumnal leaves phase
It is the pigment additive of high value in industry, the production of Suaeda salsa natural red colouring matter can fill up this blank in market.Comprehensive
It closes in the processing fluffy product of alkali, produces the fluffy leaf green of alkali using the filtrate of the fluffy juice of alkali, this pigment can be used as the complementary color of condensed food
Agent.
6, conjugated linoleic acid: contain conjugated linoleic acid, the patent document of application publication number CN104710299A in the fluffy seed of alkali
A kind of extracting method of conjugated linoleic acid in the fluffy seed of alkali is disclosed, which is extracted from the fluffy seed of alkali using low boiling point solvent
Common seepweed seeds oil, then the extraction purification conjugated linoleic acid from common seepweed seeds oil；A large amount of scientific research proves that conjugated linoleic acid has anti-
Tumour, anti-oxidant, antiatherosclerosis, norcholesterol, anticancer improve immunity, raising skeleton density, prevention and treatment diabetes etc.
A variety of important physiological functions；And it is solid to reduce animal and body's cholesterol and triglycerides and low-density lipoprotein gallbladder
Alcohol can also reduce animal and body fat, increase muscle.
7, selenium: the fluffy middle Se content of alkali is high, application publication number are as follows: the patent document of CN106578918A discloses a kind of selenium-rich
The fluffy healthy and nutritious noodle of alkali and its production technology, it is 10 times high that patent document research demonstrates the fluffy middle more general food of Se content of alkali
Left and right, and the patent document using high activity Se-enriched yeast two-step fermentation zymotechnique by inorganic selenium be converted into safety and
The better organic selenium of auxotype, improves the organic selenium content in healthy and nutritious noodle, through organic in detection healthy and nutritious noodle
The content of selenium reaches 150~200 μ g/Kg,
Selenium is referred to as " king of anti-cancer " in body trace element by scientist, and scientific circles are the study found that blood selenium level
Height is closely bound up with the generation of cancer, and science confirms: the high anti-oxidation just because of " selenium " acts on, and appropriate supplement can be played and be prevented
Organ aging and lesion delay senescence, and enhancing is immune, resists disease, resist toxic heavy metal, mitigate chemicotherapy side effect,
Cancer-resisting, selenium are the nutrients for uniquely having certain direct relation with virus infection, and selenium-supply is conducive to the variation of blocking virus, adds
The rehabilitation of fast sick body.Selenium is the essential trace elements of the human body.Studies have shown that low selenium or selenium deficiency crowd not only can by appropriate selenium-supply
The generation of enough pre- preventing tumor, hepatopathy etc., and body immunity can be improved, the vitals such as the maintenance heart, liver, lung, stomach are just
Chang Gongneng prevents the generation of senile Cardial or cerebral vascular diseases.
8, flavone compound: Suaeda salsa contains flavone compound, it is known that naturally occurring plant flavone is shown
Extensive bioactivity, including anti-oxidant, antitumor, antiatherosclerosis, anti-inflammatory etc.；Application publication number are as follows:
The patent document of CN103027962A discloses a kind of Suaeda salsa extracting flavonoids and content assaying method, patent document research
It is higher to demonstrate Suaeda salsa (S.salsa) leaf flavonoids content, and has stronger antioxidant activity, in addition, application publication number
Are as follows: CN104987340A and application publication number are as follows: the patent document of 105017199A individually disclose a kind of fluffy flavone A of alkali and its
Preparation method and purposes and a kind of fluffy flavones of alkali and its preparation method and application, two parts of patent documents, which are studied, to be demonstrated from alkali
A kind of isolated noval chemical compound is extracted in fluffy herb, which has good suppression to lipopolysaccharide-induced Spleen cell proliferation
System activity, IC50 can be used for preparing the drug for the treatment of hypoimmunity disease and mention from the fluffy herb ethyl alcohol of alkali up to 0.39 μM
A kind of noval chemical compound isolated in object is taken, which has to lipopolysaccharide-induced B lymphocyte proliferation and ConA
The T lymphocyte proliferation of induction has significant inhibitory activity, and result of study finds that the fluffy flavones B of alkali is living with good immunosupress
Property；There is the compound of medical value many in flavone compound, these compounds are for preventing and treating cardiovascular and cerebrovascular disease, as can drop
The brittleness of low blood vessel improves the permeability of blood vessel, reduces blood lipid and cholesterol, prevention and treatment senile hypertension, cerebral hemorrhage, coronary heart disease,
Angina pectoris, expansion coronary vasodilator, increase coronary flow.Many flavones ingredients have cough-relieving, eliminating the phlegm, relieving asthma and the work of antibacterial
Property, while there is malicious protect liver, solution liver, antimycotic, treatment acute hepatitis, chronic hepatitis, cirrhosis and free radical resisting and antioxidation.
It was bloomed to the Suaeda liaotungensis kitag phenological period it has been observed that Suaeda liaotungensis kitag seedling-growing time is about mid-April by continuous 2 years
Time is about mid-July, and Grain Ripening is about mid-September.Fluffy emerged from mid-April to mid-July of alkali sees flower, can be considered seedling
Phase, but enter after June, plant gradually lignifying, especially red phenotype plant lignifying occurs relatively early, basal part of stem
Edible value is lost, edible part is only limited at the top of plant therefore May 10 to June 10 is that alkali is fluffy edible best
Picking time.
A large amount of patent and paper literature research demonstrate fluffy middle the be rich in various nutrients of alkali at present, however, alkali
Fluffy to be divided into the fluffy stem and leaf part of alkali and the fluffy seed part of alkali, nutritional ingredient contained by the fluffy stem and leaf part of alkali and the fluffy seed part of alkali is biased to not
Together, wherein the fluffy stem and leaf part of alkali is rich in mineral elements and the vitamin Cs, vitamin such as calcium, iron, phosphorus, zinc, sodium, potassium, iodine, copper, manganese
B1, vitamin B6, vitamin B5, vitamin B12, vitamin B2Equal vitamins, the fluffy seed part of alkali are rich in: Ser (serine), Asp
(aspartic acid), Thr (threonine), Pro (proline), Ala (alanine), Arg (arginine), Val (valine), Met (egg
Propylhomoserin), Ile (isoleucine), Leu (leucine), Trp (tryptophan), Phe (phenylalanine), His (histidine), Lys (rely
Propylhomoserin), Tyr (tyrosine), amino acid and the micro member of conjugated linoleic acid and anticancer such as Glu (glutamic acid) and Gly (glycine)
Element --- selenium, for the difference of nutrient contained by the fluffy stem and leaf part of alkali and the fluffy seed part of alkali, the effect played is also different,
It according to fluffy the developed food of alkali is uniformly processed alkali is fluffy at present, does not distinguish the fluffy stem and leaf part of alkali and the fluffy seed part of alkali
It comes, thus the nutriment contained by the fluffy various pieces of alkali is not given full play of into effect, so that fluffy middle the be rich in battalion of alkali
Feeding element fails to play good curative effect.
[summary of the invention]
In order to overcome the shortcomings in the background art, the present invention discloses a kind of fluffy extract of saline-alkali land and its preparation side
Method extracts the fluffy stem and leaf part of saline-alkali land and the fluffy seed part of saline-alkali land respectively, and according to the fluffy stem and leaf part of alkali and seed part
Nutrient content is different, deploys the ratio of saline-alkali land fluffy stem-leaf extract and the fluffy seed extract of saline-alkali land, and being made has special project
The health food of function.
For achieving the above object, the present invention adopts the following technical scheme:
It is new to acquire the 5-6 month that weight ratio is 1:1 to 2:1 respectively for a kind of fluffy extract of saline-alkali land and preparation method thereof
The fluffy seed of saline-alkali land of the fluffy stem of fresh salt-soda soil saline-alkali land, Ye He 10-11 month seed maturity, by collected fresh salt-soda soil
The fluffy cauline leaf inspissated juice of alkali is obtained after the fluffy cauline leaf process of alkali, the fluffy seed of collected saline-alkali land is obtained after processing is refined saline and alkaline
Ground common seepweed seeds oil, then the fluffy cauline leaf inspissated juice of alkali obtained and common seepweed seeds oil are mixed to get the fluffy extract A of weight reducing type saline-alkali land.
Acquisition weight ratio is the fluffy stem of 5-6 month fresh salt-soda soil saline-alkali land of 1:5 to 2:5, plants the Ye He 10-11 month respectively
The fluffy seed of the saline-alkali land in sub- maturity period will obtain the fluffy cauline leaf inspissated juice of alkali after the collected fresh fluffy cauline leaf process of saline-alkali land,
The fluffy seed of collected saline-alkali land is obtained into salt-soda soil common seepweed seeds oil after processing is refined, then the fluffy cauline leaf of alkali obtained is concentrated
Juice and common seepweed seeds oil are mixed to get the fluffy extract B of nutritive saline-alkali land alkali.
A kind of fluffy extract of saline-alkali land and preparation method thereof acquires the 5-6 month that weight ratio is 1:25 or 2:25 respectively
The fluffy seed of saline-alkali land of the fluffy stem of fresh salt-soda soil saline-alkali land, Ye He 10-11 month seed maturity, will be collected fresh saline and alkaline
The fluffy cauline leaf inspissated juice of alkali is obtained after the fluffy cauline leaf process of ground alkali, and the fluffy seed of collected saline-alkali land is obtained into salt after processing is refined
Alkali ground common seepweed seeds oil, then the fluffy cauline leaf inspissated juice of alkali obtained and common seepweed seeds oil are mixed to get the fluffy extract of curative effect-type saline-alkali land
C。
Fluffy extract of the saline-alkali land and preparation method thereof, by the fluffy stem and leaf part of collected saline-alkali land according to super
Sound wave auxiliary enzymatic treatment obtains the fluffy cauline leaf inspissated juice of saline-alkali land, and the ultrasound wave auxiliary enzyme method handles to obtain saline-alkali land
Fluffy cauline leaf inspissated juice is successively prepared by following step:
Step 1, the fluffy stem of fresh saline-alkali land and blade are acquired, (model: BSA- in guarantor's food peace food purifying machine is put into
S901AS) clean 1 time~3 times, purpose: removal impurity and agriculture are residual, kill bacterium, guarantee that safety edible is used；
Step 2, by after cleaning Jian Peng stem and blade be put into vegetable-chopper (model: FC-306) be cut into every section of 1cm~
2cm；
Step 3, the Jian Peng stem cut and blade are mixed with deionized water 1:0.5~1:2, using colloid mill (model:
JM50) mashing is handled to 30 mesh~50 mesh；
Step 4, continue the slurries in pulverising step 3 extremely using high-accuracy Wet ultrafine grinding equipment (model: QDGX-18)
60 mesh~200 mesh；
Step 5, the smashed material of step 4 is put into ultrasonic wave dynamic countercurrent circulation extracting concentrating equipment (model: JYT-
LN-C), add deionized water by feed liquid mass ratio 1:20~1:50, add 2%~4% (w/w) cellulase, it is added 0.05%~
0.08% vitamin C, enzymolysis time 20min~30min, 30 DEG C~50 DEG C of hydrolysis temperature, ultrasonic power 50w~200w is mentioned
Taking number is 1~2 time, extracting solution vacuum-concentrcted, filtering；
Step 6, the filter residue in step 5 carries out micro-wave vacuum disinfection equipment (model: RWBZ-08S), microwave power
350W~550W, 40 DEG C~60 DEG C of temperature；(being used in the food such as biscuit)
Step 7, the filtered extracting solution of step 5 is subjected to coarse filtration, ultrafiltration by reverse osmosis unit, sterile filling is up to salt
The alkali ground fluffy cauline leaf inspissated juice of alkali；
Step 8, the fluffy cauline leaf inspissated juice concentration analysis of saline-alkali land, the fluffy cauline leaf inspissated juice of saline-alkali land that step 7 is obtained
The refractive index of salt-soda soil common seepweed seeds oil is measured by sonde-type digital display refractometer.
Fluffy extract of the saline-alkali land and preparation method thereof, by the fluffy seed of collected saline-alkali land according to overcritical two
Carbonoxide extraction produces salt-soda soil common seepweed seeds oil, the supercritical carbon dioxide extraction method produce salt-soda soil common seepweed seeds oil according to
It is secondary to be prepared by following step:
Step 1, the fluffy seed of saline-alkali land is acquired, impurity elimination is screened, is sent into cleaning screen after the fluffy seed metering of saline-alkali land and is screened,
Remove soil, rubble, seed shell and dust；Through magnetic separator except de-iron is miscellaneous, stone remover removes rubble, clod, and impurity content is small after screening
In 0.1%；
Step 2, the fluffy seed of saline-alkali land is put into vacuum oven, uniformly spreads out, is dried in vacuo, vacuum drying temperature
Degree is 40-60 DEG C, vacuum degree 10Pa-200Pa, vacuum drying time 3h-6h；
Step 3, the fluffy seed of saline-alkali land is crushed after vacuum drying with pulverizer, is crushed to mesh number as 60 mesh to 150
Mesh；
Step 4, the fluffy powder of seeds of saline-alkali land being subjected to supercritical carbon dioxide extracting, separate mode is the second-order separation, one
Grade separating still pressure is 8-10MPa, and the second-order separation kettle pressure is 5-8MPa, and level-one separating still temperature is regulated to 55 DEG C, two fractions
35 DEG C are regulated to from kettle temperature degree, extraction time 2.5h-4.5h；
Step 5, the isolate in level-one separating still and the second-order separation kettle is collected, evaporates isolate using spiral evaporator
In ethyl alcohol, then under the conditions of 40 DEG C in a vacuum drying oven further removal ethyl alcohol；
Step 6, the isolate in level-one separating still and the second-order separation kettle is after step 5 removes ethyl alcohol, in level-one separating still
Isolate directly as the isolate in the second-order separation kettle is centrifuged with centrifuge, centrifugal rotational speed 30r/min-50r/
Min, centrifugation time 20min take upper layer oil reservoir, are incorporated in the salt-soda soil common seepweed seeds oil in level-one separating still after collection, mixing
Salt-soda soil common seepweed seeds oil after uniformly to be prepared.
Step 7, the fluffy seed oil concentration analysis of saline-alkali land passes through sonde-type number to the salt-soda soil common seepweed seeds oil that step 6 obtains
The refractive index of aobvious refractometer measurement salt-soda soil common seepweed seeds oil.
Fluffy extract of the saline-alkali land and preparation method thereof, the fluffy cauline leaf inspissated juice of saline-alkali land and saline-alkali land is fluffy
The fluffy extract A of weight reducing type saline-alkali land that seed oil is mixed to get measures the fluffy extract of saline-alkali land by sonde-type digital display refractometer
Refractive index be 1.6236.
Fluffy extract of the saline-alkali land and preparation method thereof, the fluffy cauline leaf inspissated juice of saline-alkali land and saline-alkali land is fluffy
The fluffy extract B of nutritive saline-alkali land alkali that seed oil is mixed to get measures the fluffy extract of saline-alkali land by sonde-type digital display refractometer
Refractive index be 1.5237.
Fluffy extract of the saline-alkali land and preparation method thereof, the fluffy cauline leaf inspissated juice of saline-alkali land and saline-alkali land is fluffy
The fluffy extract C of curative effect-type saline-alkali land that seed oil is mixed to get measures the fluffy extract of saline-alkali land by sonde-type digital display refractometer
Refractive index be 1.4942.
Fluffy extract of the saline-alkali land and preparation method thereof, ultrasound wave auxiliary enzyme method handle to obtain the fluffy stem of saline-alkali land
Reverse osmosis unit system configuration described in the step 7 of leaf inspissated juice are as follows: pretreatment system, smart filtration system, corollary system；Pre- place
Reason system is made of mechanical filter, adsorption filter, cartridge filter；Smart filtration system is by hollow-fibre ultrafiltration device group
At；Corollary system is made of water purification pot, electrical control system, and mechanical filter filtering can remove body refuse and fiber in extracting solution
Deng, after through adsorption filter filtering can remove oil removal, however the impurity such as algae can be removed through mechanical filter filtering.
Fluffy extract of the saline-alkali land and preparation method thereof, ultrasound wave auxiliary enzyme method handle to obtain the fluffy stem of saline-alkali land
Ultrafiltration described in the step 7 of leaf inspissated juice is hollow-fibre membrane ultrafiltration to remove the microorganisms such as bacterium in extracting solution, mould, it is described in
Empty fiber membrane diameter be 0.01 μm~0.001 μm, feed rate be 900L/h~1500L/h, pressure 0.045Mpa~
0.18Mpa, feed concentration be the 200 μ g/L of μ g/L~400, ultrafiltration time 100min~400min, backwash cycle 10min~
40min, backwash time 20min~120min, upper operation 10min~40min, upper backwash 20s~120s, lower operation 10min~
40min, lower backwash 20s~120s.
Due to the adoption of the technical scheme as described above, the invention has the following beneficial effects:
The present invention lays particular stress on difference according to nutritional ingredient and content different in the fluffy cauline leaf of saline-alkali land and the fluffy seed of saline-alkali land,
In order to play effect possessed by the nutritional ingredient contained by the fluffy cauline leaf of saline-alkali land and the fluffy seed of saline-alkali land to greatest extent, lead to
It crosses ultrasound wave auxiliary enzyme method and the fluffy cauline leaf process of 5-6 month saline-alkali land is obtained into the fluffy cauline leaf inspissated juice of saline-alkali land, by overcritical
CO2Extraction handles the fluffy seed of 10-11 month saline-alkali land to obtain salt-soda soil common seepweed seeds oil, and then the saline-alkali land that processing is obtained
Fluffy cauline leaf inspissated juice and salt-soda soil common seepweed seeds oil difference mix in proportion according to final curative effect to be achieved, reach special special
It controls, with strong points, the direct purpose of effect, specific mixed proportion and curative effect achieved are as follows:
Acquisition weight ratio is the fluffy stem of 5-6 month fresh salt-soda soil saline-alkali land of 1:1 to 2:1, plants the Ye He 10-11 month respectively
The fluffy cauline leaf inspissated juice of saline-alkali land obtained and salt-soda soil common seepweed seeds oil are simultaneously mixed to get by the fluffy seed of the saline-alkali land in sub- maturity period
The fluffy extract A of weight reducing type saline-alkali land, rich in the fluffy haematochrome of vitamin, alkali being rich in the fluffy cauline leaf of a large amount of saline-alkali land
Equal nutrients, and contain a small amount of salt-soda soil common seepweed seeds oil, the haematochrome in the fluffy cauline leaf of saline-alkali land is natural pigment, the color
Element is researched and analysed as water-soluble anthocyanidin, security performance with higher, and has anti-mutation, anti-oxidant, drop
The healthcare functions such as blood pressure, protection liver, antioxidant activity is analysis shows alkali is fluffy to O-2Free radical has stronger scavenging effect, often
Haematochrome in the edible fluffy cauline leaf of saline-alkali land is conducive to remove oxygen radical excessive in vivo, to be good for one's health and grow
Longevity, the fluffy extract A of weight reducing type saline-alkali land can supplement needed by human body mineral element and vitamin, and low oil, low fat play benefit
Longevity beauty treatment, the effect for moulding of reducing weight；
Acquisition weight ratio is the fluffy stem of 5-6 month fresh salt-soda soil saline-alkali land of 1:25 to 2:25, the Ye He 10-11 month respectively
The fluffy seed of the saline-alkali land of seed maturity simultaneously mixes the fluffy cauline leaf inspissated juice of saline-alkali land obtained and salt-soda soil common seepweed seeds oil
The fluffy extract C of curative effect-type saline-alkali land arrived, rich in be rich in the fluffy seed of a large amount of saline-alkali land conjugated linoleic acid, selenium and
The nutrients such as flavone compound, conjugated linoleic acid have antitumor, anti-oxidant, antiatherosclerosis, norcholesterol, resist
Cancer improves immunity, improves a variety of important physiological functions such as skeleton density, prevention and treatment diabetes；Known naturally occurring plant flavone
It shows extensive bioactivity, including anti-oxidant, antitumor, antiatherosclerosis, anti-inflammatory, can be used for preventing and treating heart and brain blood
Pipe disease improves the permeability of blood vessel, reduces blood lipid and cholesterol, prevent and treat senile hypertension, brain as can reducing the brittleness of blood vessel
Hemorrhage, coronary heart diseases and angina pectoris, expansion coronary vasodilator, increase coronary flow；The selenium energy with " king of anticancer " title being rich in
Enough cancer-resistings prevent cardiovascular and cerebrovascular disease, anti-curing oncoma, promote sugared part metabolism, reduce blood glucose and glucose in urine, improve patient of diabetes
The symptom of person；The fluffy extract C of curative effect-type saline-alkali land has powerful efficient functional, plays the role of health-care physiotherapeutic；
Acquisition weight ratio is the fluffy stem of 5-6 month fresh salt-soda soil saline-alkali land of 1:5 to 2:5, plants the Ye He 10-11 month respectively
The fluffy cauline leaf inspissated juice of saline-alkali land obtained and salt-soda soil common seepweed seeds oil are simultaneously mixed to get by the fluffy seed of the saline-alkali land in sub- maturity period
The fluffy extract B of weight reducing type saline-alkali land, wherein the fluffy cauline leaf inspissated juice of saline-alkali land and salt-soda soil common seepweed seeds oil ratio are suitable,
Weighing apparatus nutrition supplements the daily essential nutrient element of human body comprehensively, suitable for people of all ages.
The present invention utilizes ultrasonic wave auxiliary, aqueous enzymatic extraction and ultrafiltration technology, three for the fluffy stem and leaf part of saline-alkali land
Joint greatly remains the water-soluble functional components of the fluffy stem and leaf part of alkali, and aqueous enzymatic method combination ultrasonic wave physical process utilizes
The properties such as very big acceleration, strong cavitation effect, high vibration that it is generated are reduced and are asked when extracting, and avoid temperature change pair
The activity change of effective component.The method simple production process, consuming time are few, reduce production work intensity, have with product
It is high to imitate ingredient, reduces the advantages that temperature changes bring adverse effect；The present invention is for the fluffy seed part over-extraction of saline-alkali land with facing
Boundary CO2There are extraction extraction efficiency height, no solvent residue toxicity, active skull cap components and heat-sensitive ingredients to be not easy to be decomposed
It destroys, the natural feature of extract can be kept to the maximum extent, it can be achieved that the advantages of Selective Separation.
[Detailed description of the invention]
Fig. 1 is the overall structure diagram of sonde-type digital display refractometer.
Fig. 2 is that sonde-type digital display refractometer optical signal issues side schematic diagram of internal structure.
Fig. 3 is sonde-type digital display refractometer optical signal receiving side schematic diagram of internal structure.
Fig. 4 is sonde-type digital display refractometer probe schematic diagram of internal structure.
Fig. 5 is the schematic diagram of the section structure when sonde-type digital display refractometer probe is connect with optical fiber interface.
Fig. 6 is sonde-type digital display refractometer electrical block diagram.
In figure: 1. hosts；2. display screen；3. on & off switch；4. tuning up key；5. locking key；6. optical fiber interface；7. probe；
8. optical fiber；9. fibre-optical splice；10. signal processing circuit board；11. laser light source control circuit board；12. laser light source A；13. swashing
Radiant B；14. laser light source C；15. reflecting mirror A；16. battery；17. light intensity sensor；18. reflecting mirror B；19. prism A；20.
Trimming groove；21. probing shell；22. prism B；23. reflecting mirror C；24. naked fibre hole A；25. naked fibre hole B；26. optical fiber A；27.
Optical fiber B；28. tapered lens.
[specific embodiment]
The present invention can be explained in more detail by the following examples, the open purpose of the present invention is intended to protect the present invention
All changes and improvements in range, the invention is not limited to the following examples；
It is new to acquire the 5-6 month that weight ratio is 1:1 to 2:1 respectively for a kind of fluffy extract of saline-alkali land and preparation method thereof
The fluffy seed of saline-alkali land of the fluffy stem of fresh salt-soda soil saline-alkali land, Ye He 10-11 month seed maturity, by collected fresh salt-soda soil
The fluffy cauline leaf inspissated juice of alkali is obtained after the fluffy cauline leaf process of alkali, the fluffy seed of collected saline-alkali land is obtained after processing is refined saline and alkaline
Ground common seepweed seeds oil, then the fluffy cauline leaf inspissated juice of alkali obtained and common seepweed seeds oil are mixed to get the fluffy extract A of weight reducing type saline-alkali land.
It is new to acquire the 5-6 month that weight ratio is 1:5 to 2:5 respectively for a kind of fluffy extract of saline-alkali land and preparation method thereof
The fluffy seed of saline-alkali land of the fluffy stem of fresh salt-soda soil saline-alkali land, Ye He 10-11 month seed maturity, by collected fresh salt-soda soil
The fluffy cauline leaf inspissated juice of alkali is obtained after the fluffy cauline leaf process of alkali, the fluffy seed of collected saline-alkali land is obtained after processing is refined saline and alkaline
Ground common seepweed seeds oil, then the fluffy cauline leaf inspissated juice of alkali obtained and common seepweed seeds oil are mixed to get the fluffy extract B of nutritive saline-alkali land alkali.
A kind of fluffy extract of saline-alkali land and preparation method thereof acquires the 5-6 month that weight ratio is 1:25 or 2:25 respectively
The fluffy seed of saline-alkali land of the fluffy stem of fresh salt-soda soil saline-alkali land, Ye He 10-11 month seed maturity, will be collected fresh saline and alkaline
The fluffy cauline leaf inspissated juice of alkali is obtained after the fluffy cauline leaf process of ground alkali, and the fluffy seed of collected saline-alkali land is obtained into salt after processing is refined
Alkali ground common seepweed seeds oil, then the fluffy cauline leaf inspissated juice of alkali obtained and common seepweed seeds oil are mixed to get the fluffy extract of curative effect-type saline-alkali land
C。
Fluffy extract of the saline-alkali land and preparation method thereof, by the fluffy stem and leaf part of collected saline-alkali land according to super
Sound wave auxiliary enzymatic treatment obtains the fluffy cauline leaf inspissated juice of saline-alkali land, and the ultrasound wave auxiliary enzyme method handles to obtain saline-alkali land
Fluffy cauline leaf inspissated juice is successively prepared by following step:
Step 1, the fluffy stem of fresh saline-alkali land and blade are acquired, (model: BSA- in guarantor's food peace food purifying machine is put into
S901AS) clean 1 time~3 times, purpose: removal impurity and agriculture are residual, kill bacterium, guarantee that safety edible is used；
Step 2, by after cleaning Jian Peng stem and blade be put into vegetable-chopper (model: FC-306) be cut into every section of 1cm~
2cm；
Step 3, the Jian Peng stem cut and blade are mixed with deionized water 1:0.5~1:2, using colloid mill (model:
JM50) mashing is handled to 30 mesh~50 mesh；
Step 4, continue the slurries in pulverising step 3 extremely using high-accuracy Wet ultrafine grinding equipment (model: QDGX-18)
60 mesh~200 mesh；
Step 5, the smashed material of step 4 is put into ultrasonic wave dynamic countercurrent circulation extracting concentrating equipment (model: JYT-
LN-C), add deionized water by feed liquid mass ratio 1:20~1:50, add 2%~4% (w/w) cellulase, it is added 0.05%~
0.08% vitamin C, enzymolysis time 20min~30min, 30 DEG C~50 DEG C of hydrolysis temperature, ultrasonic power 50w~200w is mentioned
Taking number is 1~2 time, extracting solution vacuum-concentrcted, filtering；
Step 6, the filter residue in step 5 carries out micro-wave vacuum disinfection equipment (model: RWBZ-08S), microwave power
350W~550W, 40 DEG C~60 DEG C of temperature；(being used in the food such as biscuit)；
Step 7, the filtered extracting solution of step 5 is subjected to coarse filtration, ultrafiltration by reverse osmosis unit, sterile filling is up to salt
The alkali ground fluffy cauline leaf inspissated juice of alkali；
Step 8, the fluffy cauline leaf inspissated juice concentration analysis of saline-alkali land, the fluffy cauline leaf inspissated juice of saline-alkali land that step 7 is obtained
The refractive index of the fluffy seed cauline leaf inspissated juice of saline-alkali land is measured by sonde-type digital display refractometer.
Fluffy extract of the saline-alkali land and preparation method thereof, by the fluffy seed of collected saline-alkali land according to overcritical two
Carbonoxide extraction produces salt-soda soil common seepweed seeds oil, the supercritical carbon dioxide extraction method produce salt-soda soil common seepweed seeds oil according to
It is secondary to be prepared by following step:
Step 1, the fluffy seed of saline-alkali land is acquired, impurity elimination is screened, is sent into cleaning screen after the fluffy seed metering of saline-alkali land and is screened,
Remove soil, rubble, seed shell and dust；Through magnetic separator except de-iron is miscellaneous, stone remover removes rubble, clod, and impurity content is small after screening
In 0.1%；
Step 2, the fluffy seed of saline-alkali land is put into vacuum oven, uniformly spreads out, is dried in vacuo, vacuum drying temperature
Degree is 40-60 DEG C, vacuum degree 10Pa-200Pa, vacuum drying time 3h-6h；
Step 3, the fluffy seed of saline-alkali land is crushed after vacuum drying with pulverizer, is crushed to mesh number as 60 mesh to 150
Mesh；
Step 4, the fluffy powder of seeds of saline-alkali land being subjected to supercritical carbon dioxide extracting, separate mode is the second-order separation, one
Grade separating still pressure is 8-10MPa, and the second-order separation kettle pressure is 5-8MPa, and level-one separating still temperature is regulated to 55 DEG C, two fractions
35 DEG C are regulated to from kettle temperature degree, extraction time 2.5h-4.5h；
Step 5, the isolate in level-one separating still and the second-order separation kettle is collected, evaporates isolate using spiral evaporator
In ethyl alcohol, then under the conditions of 40 DEG C in a vacuum drying oven further removal ethyl alcohol；
Step 6, the isolate in level-one separating still and the second-order separation kettle is after step 5 removes ethyl alcohol, in level-one separating still
Isolate directly as the isolate in the second-order separation kettle is centrifuged with centrifuge, centrifugal rotational speed 30r/min-50r/
Min, centrifugation time 20min take upper layer oil reservoir, are incorporated in the salt-soda soil common seepweed seeds oil in level-one separating still after collection, mixing
Salt-soda soil common seepweed seeds oil after uniformly to be prepared；
Step 7, the fluffy seed oil concentration analysis of saline-alkali land passes through sonde-type number to the salt-soda soil common seepweed seeds oil that step 6 obtains
The refractive index of aobvious refractometer measurement salt-soda soil common seepweed seeds oil.
Fluffy extract of the saline-alkali land and preparation method thereof, the fluffy cauline leaf inspissated juice of saline-alkali land and saline-alkali land is fluffy
The fluffy extract A of weight reducing type saline-alkali land that seed oil is mixed to get measures the fluffy extract of saline-alkali land by sonde-type digital display refractometer
Refractive index be 1.6236.
Fluffy extract of the saline-alkali land and preparation method thereof, the fluffy cauline leaf inspissated juice of saline-alkali land and saline-alkali land is fluffy
The fluffy extract B of nutritive saline-alkali land alkali that seed oil is mixed to get measures the fluffy extract of saline-alkali land by sonde-type digital display refractometer
Refractive index be 1.5237.
Fluffy extract of the saline-alkali land and preparation method thereof, the fluffy cauline leaf inspissated juice of saline-alkali land and saline-alkali land is fluffy
The fluffy extract C of curative effect-type saline-alkali land that seed oil is mixed to get measures the fluffy extract of saline-alkali land by sonde-type digital display refractometer
Refractive index be 1.4942.
Fluffy extract of the saline-alkali land and preparation method thereof, ultrasound wave auxiliary enzyme method handle to obtain the fluffy stem of saline-alkali land
Reverse osmosis unit system configuration described in the step 7 of leaf inspissated juice are as follows: pretreatment system, smart filtration system, corollary system.Pre- place
Reason system is made of mechanical filter, adsorption filter, cartridge filter；Smart filtration system is by hollow-fibre ultrafiltration device group
At；Corollary system is made of water purification pot, electrical control system, and mechanical filter filtering can remove body refuse and fiber in extracting solution
Deng, after through adsorption filter filtering can remove oil removal, however the impurity such as algae can be removed through mechanical filter filtering.
Fluffy extract of the saline-alkali land and preparation method thereof, ultrasound wave auxiliary enzyme method handle to obtain the fluffy stem of saline-alkali land
Ultrafiltration described in the step 7 of leaf inspissated juice is hollow-fibre membrane ultrafiltration to remove the microorganisms such as bacterium in extracting solution, mould, it is described in
Empty fiber membrane diameter be 0.01 μm~0.001 μm, feed rate be 900L/h~1500L/h, pressure 0.045Mpa~
0.18Mpa, feed concentration be the 200 μ g/L of μ g/L~400, ultrafiltration time 100min~400min, backwash cycle 10min~
40min, backwash time 20min~120min, upper operation 10min~40min, upper backwash 20s~120s, lower operation 10min~
40min, lower backwash 20s~120s.
Wherein, the fluffy cauline leaf inspissated juice of measurement saline-alkali land, salt-soda soil common seepweed seeds oil and the fluffy three kinds of extracts of saline-alkali land
Refractive index used in sonde-type digital display refractometer are as follows:
A kind of sonde-type digital display refractometer in conjunction with described in Figure of description 1-6, including host 1 and probe 7, in host 1
Part is upper layer and lower layer, and 1 inside upper layer of host is that optical signal issues side, and 1 inside lower layer of host is optical signal receiving side, described
It includes signal processing circuit board 10 and laser light source control circuit board 11,10 He of signal processing circuit board that optical signal, which issues side,
It is electrically connected between laser light source control circuit board 11, is equipped with tapered lens 28 in 1 inside upper layer optical fiber interface of host, 6 exit,
Reflecting mirror A15, the reflecting mirror A15 and level side are equipped at the 1 inside upper layer upper right corner of end hosts of tapered lens 28
Be 45 ° to angle, at the 1 inside upper layer lower right corner of the opposite side reflecting mirror A15 host be equipped with laser light source A12, laser light source B13,
Laser light source C14, angle is 4 ° between the laser light source A12 and laser light source B13, the laser light source B13 and swash
Angle is 4 ° between radiant C14, the laser light source A12, laser light source B13, in laser light source C14 laser diode rule
Lattice are respectively ML101J25 Mitsubishi 650nm 100mw, the Europe Si Lang 450nm 80mw and PL520A, the Europe PL450B Si Lang 520nm
120mw；The optical signal receiving side includes battery 16 and prism A19, and the battery 16 is detachable rechargeable battery, for letter
Number processing circuit plate 10, laser light source control circuit board 11, light intensity sensor 17 are powered, in 1 inside lower layer optical fiber interface 6 of host
Exit is equipped with prism A19, is equipped with trimming groove 20 in the side of prism A19, right in the 1 inside lower layer of diagonal host of prism A19
Reflecting mirror B18 is equipped at inferior horn, the angle of the reflecting mirror B18 and vertical direction is 29 °, the host 1 on the opposite reflecting mirror B18
Internal lower layer's lower right-hand corner is equipped with light intensity sensor 17, and the light intensity sensor 17 is electrically connected with signal processing circuit board 10；?
The one side wall of host 1 is equipped with optical fiber interface 6, and fibre-optical splice 9 is connected with optical fiber interface 6, the fibre-optical splice 9 and probe
It is connected between 7 by optical fiber 8, includes optical fiber A26 and optical fiber B27 in optical fiber 8, be internally provided in probe 7 naked
Fine hole A24 and naked fibre hole B25 is equipped with probing shell 21 outside probe 7, is equipped with prism B22 in 7 head sides of popping one's head in, described
Prism B22 be made of the glass of ZF7 material, pop one's head in the 7 head other sides be equipped with reflecting mirror C23, on the upper surface of host 1
It is respectively equipped with display screen 2, display screen 2 is 12846 Liquid Crystal Modules, and on & off switch 3 tunes up key 4, tunes up key 4 and uses before measuring
In correction, reduce error, locking key 5, locking key 5 is read for lock-screen.
Wherein, 4 ° of angles, laser light source B13 and laser light source C14 are set between laser light source A12 and laser light source B13
Between setting 4 ° of angles be it is a branch of in order to merge into three beams of laser, according to the specific size of the present apparatus and requirement setting folder
Angle is 4 °；It is in order to enable reflected light back is to designated position, 29 ° of folders that the angle that reflecting mirror B18 and vertical direction is arranged, which is 29,
Angle is calculated according to this refractometer overall dimensions；Signal processing circuit board 10 and laser light source control circuit board 11 are used for
The calculating of reading.
In the folding of the fluffy cauline leaf inspissated juice of measurement saline-alkali land, salt-soda soil common seepweed seeds oil and the fluffy three kinds of extracts of saline-alkali land
When penetrating rate, after the probe 7 of sonde-type digital display refractometer is put into testing liquid, press on sonde-type digital display refractometer host
After on & off switch 3 is switched on, signal processing circuit board 10 and laser light source control circuit board 11 are powered and start to work, laser light source control
Circuit board 11 drives laser light source A12, laser light source B13, laser light source C14 work, by laser light source A12, laser light source
B13, laser light source C14 issue laser, directive reflecting mirror A15, and laser directive tapered lens 28 after reflecting mirror A15 reflection swashs
Light through tapered lens 28 enter optical fiber A26, through optical fiber 8 transmission after by optical fiber A26 the other end project, laser into
Enter naked fibre hole A24, enters back into prism B22, for laser from directive testing liquid after prism B22 injection, laser a part can be to be measured
Reflection liquid, a part can inject testing liquid, and the laser directive reflecting mirror C23 reflected by testing liquid, laser is through reflecting mirror
Enter naked fibre hole B25 after C23 reflection, enter back into optical fiber B27, laser is by the another of optical fiber B27 after the transmission of optical fiber 8
One end is projected, laser directive reflecting mirror B18, laser directive light intensity sensor after reflecting mirror B18 reflects after prism A19 refraction
17, light intensity sensor 17 sends data to signal processing circuit board 10 after detecting luminous intensity, and signal processing circuit board 10 calculates
And return luminous intensity is measured, the refractive index of prepare liquid is obtained by calculating intensity value, finally shows measurement result in display screen 2,
Its circuit structure connection figure is as shown in Figure 6.
Refractive index is one of important physical constant of substance, and refractive index is closely related with solution concentration, and many pure materials are all
With certain refractive index, refractive index will change if wherein containing impurity, deviation occur, impurity is more, and deviation is got over
Greatly.Therefore, by the measurement of refractive index, the purity of substance can be measured.Sonde-type digital display refractometer is the total reflection according to light
The instrument of principle design, it can quantitatively be analyzed using the index of refraction of the measuring method measurement unknown materials for body critical angle of being all-trans
Ingredient in the fluffy cauline leaf inspissated juice of saline-alkali land, salt-soda soil common seepweed seeds oil and the fluffy three kinds of extracts of saline-alkali land, test solution
Purity, whether the auxiliary allotment fluffy three kinds of extracts of saline-alkali land reach required CONCENTRATION STATE, and table 1 is to be rolled over by sonde-type digital display
The refractive index situation of the light instrument experiment measurement fluffy three kinds of extracts of saline-alkali land:
The refractive index of the fluffy three kinds of extracts of 1 saline-alkali land of table
By the folding that saline-alkali land five measurement results of fluffy three kinds of extracts can be seen that with the fluffy extract A of saline-alkali land
Penetrating rate average value is 1.6236, and the refractive index average value of the fluffy extract B of saline-alkali land is 1.5237, the fluffy extract C of saline-alkali land
Refractive index average value be 1.4942, by measure the fluffy three kinds of extracts of saline-alkali land refractive index, can with inspection institute with
Whether the concentration of the fluffy three kinds of extracts of saline-alkali land complies with standard, to guarantee that the fluffy three kinds of extracts of the saline-alkali land matched are dense
Spend it is constant, and then guarantee the fluffy three kinds of extracts of saline-alkali land be rich in different proportion nutrition composition.
It is micro- by half for nutritional ingredient composition and content situation in the fluffy stem and leaf part of saline-alkali land and the fluffy seed of saline-alkali land
Measure Kjeldahl nitrogen determination crude protein content；Using determination of crude oil by Soxhlet extraction；Using gravimetry crude fibre
Content；Moisture content is measured using atmosphere pressure desiccation；Carbohydrate content is measured using anthrone colorimetry；Using high temperature ashing
Method measures content of ashes；Amino acid content is measured using Hitachi 835-50 type high-speed amino acid analyzer；Using fluorescence spectrophotometer light
Degree method measures tryptophan composition and content；Using atomic absorption spectroscopy determination mineral element, wherein selenium element fluorescence
Spectrophotometry measurement；Every nutritional ingredient and content are shown in Table 2-4, every battalion in the fluffy cauline leaf of saline-alkali land in the fluffy seed of saline-alkali land
It forms point and content is shown in Table 5-7:
Main nutrient composition content in 2 salt-soda soil common seepweed seeds oil of table
3 salt-soda soil common seepweed seeds oil Mineral Element Contents (μ g/g) of table
The composition and content (mg/g) of amino acid in 4 salt-soda soil common seepweed seeds oil of table
Note: band * person is essential amino acid.
The fluffy stem leaf extract nutrient content of 5 saline-alkali land of table
The fluffy stem leaf extract Mineral Concentrations of 6 saline-alkali land of table
The fluffy stem leaf extract amino acid content of 7 saline-alkali land of table
Note: band * person is essential amino acid.
Pass through nutritional ingredient composition and content situation in the fluffy stem leaf extract of measurement saline-alkali land and salt-soda soil common seepweed seeds oil
It can be seen that
The comparison of table 2 and table 5 can be seen that crude protein, crude fat content in the common seepweed seeds oil of salt-soda soil: 18.75% and
23.46%, much higher than crude protein, crude fat content in the fluffy stem leaf extract of saline-alkali land: 3.020% and 1.380%, and salt
Alkali in common seepweed seeds oil crude fat content account for 23.46%, be higher than soybean (crude fat content 18.80%), be good plant
Oil sources can be used as good protein sources, vitamin in the fluffy stem leaf extract of saline-alkali land since its crude protein content is also higher
Content is higher, in addition, the chemotrophy ingredient of salt-soda soil common seepweed seeds oil and the fluffy stem leaf extract of saline-alkali land is complete and enriches.
The comparison of table 3 and table 6 can be seen that salt-soda soil common seepweed seeds oil Mineral Elements potassium and the content of sodium is the abundantest,
This is related with the saline-alkali environment that it grows, close with human health in salt-soda soil common seepweed seeds oil and the fluffy stem leaf extract of saline-alkali land
It is higher to cut the constituent contents such as relevant iron, calcium, zinc, copper, manganese, it is seen then that the fluffy seed of saline-alkali land and the fluffy cauline leaf of saline-alkali land are one
The good mineral matter nutritional source of kind, in addition, also containing selenium in the fluffy seed of saline-alkali land, selenium is referred to as the micro member of human body by scientist
" king of anti-cancer " in element, therefore, the fluffy seed of exploitation saline-alkali land and using the selenium contained by the fluffy seed of saline-alkali land can for the mankind with
Carry out high value medical health care.
The comparison of table 4 and table 7, which can be seen that in salt-soda soil common seepweed seeds oil and the fluffy stem leaf extract of saline-alkali land, contains 18
Middle amino acid, rich content, it is necessary to which amino acid composition is complete, and wherein it is total to account for amino acid for the fluffy seed essential amino acids content of saline-alkali land
The 36.44% of amount is higher than FAO mode (36.00%), while the ratio between the fluffy seed essential amino acid of saline-alkali land and nonessential amino acid
It (E/N) is 0.573, also above FAO mode (0.56), it is seen then that the fluffy seed albumen of alkali belongs to quality plant albumen；The fluffy stem of saline-alkali land
It is 35.5% that essential amino acids content, which accounts for total amino acid content, in leaf, the reference model (36%) proposed close to FAO, it is necessary to amino acid
Ratio with nonessential amino acid is 55.1%, the reference model (0.56) proposed close to FAO；In addition, the research discovery fluffy seed of alkali
The common seepweed seeds oil obtained after processing is refined has the physicochemical property of general edible oil, and it is next to can be used as a kind of new edible oil
Exploitation, it is rich in unsaturated fatty acid in addition, and especially linoleic acid content is higher than many plants, it can be seen that, the fluffy seed of alkali is a kind of
Vegetable oil new resources containing high linoleic acid have important nutrition health-care functions and biggish Development volue, richness in common seepweed seeds oil
Containing unsaturated fatty acid, total unsaturated fatty acid content is up to 90.65%, and wherein linoleic acid content accounts for 68.74%, is current institute
It was found that one of the higher oil sources of linoleic acid content, physical and chemical index also substantially conforms to edible oil standard, is a kind of ideal protect
Strong edible oil and the good material for preparing conjugated linoleic acid.
By above-mentioned analysis it is found that the nutrition being rich in by salt-soda soil common seepweed seeds oil and the fluffy stem leaf extract of saline-alkali land
Ingredient be biased to it is different, the present invention by the way that the fluffy seed of saline-alkali land and the fluffy cauline leaf of saline-alkali land are deployed in proportion, can by alkali it is fluffy in
The nutritional ingredient effect being rich in maximizes, and plays the fluffy edible value of saline-alkali land to greatest extent.
In order to better illustrate the present invention the advantages of, the fluffy extract of three kinds of saline-alkali lands and diet provided through the invention
Control the effect of respectively reaching three kinds of saline-alkali lands fluffy extract: prolonging life and nursing face, weight reducing moulding；Health-care physiotherapeutic, anticancer hypoglycemic；
Supplement, balanced nutritious purpose comprehensively, it should be noted that three kinds of fluffy extracts of saline-alkali land of the invention can be taken when taking
With taking, a people can be not limited to one kind, be such as directed to obese patient, the fluffy extract of curative effect-type saline-alkali land can also be taken, wherein treating
The conjugated linoleic acid being rich in the fluffy extract of acting type saline-alkali land effectively can help obese patient to lose weight, and the present invention is given below
Typical case:
Case 1
Mr. Li, male, height 168cm, weight 83kg with the method kept on a diet and take a variety of slimming medicines, imitate
Fruit is bad, takes the fluffy extract of weight reducing type saline-alkali land of the present invention and the fluffy extract of curative effect-type saline-alkali land, arranges in pairs or groups sooner or later, respectively
10ml once a day takes 2 months, and weight reduces to 70kg by original 83kg.
Case 2
Mrs Huang, female, 47 years old, the colour of skin was dark yellow, and with menopause symptom, it is saline and alkaline to take weight reducing type of the present invention for sleep insufficiency
The fluffy extract of ground alkali and the fluffy extract of nutritive saline-alkali land alkali are arranged in pairs or groups sooner or later, each 10ml, once a day, after taking 3 months, face
Portion's complexion is ruddy, spirit and QI cleaning, spiritual cephalopodium.
Case 3
Mr. Liu, male 54 years old, suffer from diabetes for many years.Chronic oral treatment diabetes medicament: melbine, and according to doctor
It is raw to enjoin dietary restriction.From in April, 2017, the daily fluffy extract C 10ml of curative effect-type saline-alkali land bfore meals, one day three
It is secondary, adhere to a course for the treatment of (one month), blood glucose level is normal.
Case 4
Mrs Xu, female, 66 years old, diabetic, 13 years sugared ages, eye-blurred.Daily curative effect-type salt-soda soil bfore meals
The fluffy extract C 10ml of alkali, three times per day, a course for the treatment of is got off (one month), Hypoglycemic symptoms and other side effects does not occur,
Blood glucose level is normal, and eyesight is clear before relatively taking, and Management For Complications Retinopathy is improved, and somatosensory is increasingly
It is good.
Part not in the detailed description of the invention is the prior art.
Claims (10)
1. a kind of fluffy extract of saline-alkali land and preparation method thereof, it is characterized in that: the 5-6 that acquisition weight ratio is 1:1 to 2:1 respectively
Month the fluffy stem of fresh salt-soda soil saline-alkali land, Ye He 10-11 month seed maturity the fluffy seed of saline-alkali land, will be collected fresh
The fluffy cauline leaf inspissated juice of alkali is obtained after the fluffy cauline leaf process of saline-alkali land, by the fluffy seed of collected saline-alkali land after processing is refined
To salt-soda soil common seepweed seeds oil, then the fluffy cauline leaf inspissated juice of alkali obtained is mixed to get with common seepweed seeds oil to weight reducing type saline-alkali land is fluffy to be mentioned
Take object A.
2. a kind of fluffy extract of saline-alkali land and preparation method thereof, it is characterized in that: the 5-6 that acquisition weight ratio is 1:5 to 2:5 respectively
Month the fluffy stem of fresh salt-soda soil saline-alkali land, Ye He 10-11 month seed maturity the fluffy seed of saline-alkali land, will be collected fresh
The fluffy cauline leaf inspissated juice of alkali is obtained after the fluffy cauline leaf process of saline-alkali land, by the fluffy seed of collected saline-alkali land after processing is refined
To salt-soda soil common seepweed seeds oil, then the fluffy cauline leaf inspissated juice of alkali obtained is mixed to get with common seepweed seeds oil to nutritive saline-alkali land alkali is fluffy to be mentioned
Take object B.
3. a kind of fluffy extract of saline-alkali land and preparation method thereof, it is characterized in that: acquisition weight ratio is 1:25's or 2:25 respectively
5-6 month the fluffy stem of fresh salt-soda soil saline-alkali land, Ye He 10-11 month seed maturity the fluffy seed of saline-alkali land, will be collected
The fluffy cauline leaf inspissated juice of alkali is obtained after the fresh fluffy cauline leaf process of saline-alkali land, and the fluffy seed of collected saline-alkali land is refined by processing
After obtain salt-soda soil common seepweed seeds oil, then the fluffy cauline leaf inspissated juice of alkali obtained and common seepweed seeds oil are mixed to get curative effect-type saline-alkali land
Fluffy extract C.
4. fluffy extract of saline-alkali land according to claim 1-3 and preparation method thereof, it is characterized in that: will acquisition
To the fluffy stem and leaf part of saline-alkali land handle to obtain the fluffy cauline leaf inspissated juice of saline-alkali land according to ultrasound wave auxiliary enzyme method, described is super
Sound wave auxiliary enzymatic treatment obtains the fluffy cauline leaf inspissated juice of saline-alkali land and is successively prepared by following step:
Step 1, the fluffy stem of fresh saline-alkali land and blade are acquired, (model: BSA- in guarantor's food peace food purifying machine is put into
S901AS) clean 1 time~3 times, purpose: removal impurity and agriculture are residual, kill bacterium, guarantee that safety edible is used；
Step 2, by after cleaning Jian Peng stem and blade be put into vegetable-chopper (model: FC-306) and be cut into every section of cm of 1 cm~2；
Step 3, the Jian Peng stem cut and blade are mixed with deionized water 1:0.5~1:2, using colloid mill (model:
JM50) mashing is handled to 30 mesh~50 mesh；
Step 4, continue the slurries in pulverising step 3 to 60 mesh using high-accuracy Wet ultrafine grinding equipment (model: QDGX-18)
~200 mesh；
Step 5, the smashed material of step 4 is put into ultrasonic wave dynamic countercurrent circulation extracting concentrating equipment (model: JYT-LN-
C), add deionized water by feed liquid mass ratio 1:20~1:50, add 2%~4%(w/w) cellulase, it is added 0.05%~0.08%
Vitamin C, the enzymolysis time min of 20 min~30, are extracted by 30 DEG C~50 DEG C of hydrolysis temperature, the ultrasonic power w of 50 w~200
Number is 1~2 time, extracting solution vacuum-concentrcted, filtering；
Step 6, the filter residue in step 5 carries out micro-wave vacuum disinfection equipment (model: RWBZ-08S), 350 W of microwave power
~550 W, 40 DEG C~60 DEG C of temperature；(being used in the food such as biscuit)
Step 7, the filtered extracting solution of step 5 is subjected to coarse filtration, ultrafiltration by reverse osmosis unit, sterile filling is up to salt-soda soil
The fluffy cauline leaf inspissated juice of alkali；
Step 8, the fluffy cauline leaf inspissated juice concentration analysis of saline-alkali land, the fluffy cauline leaf inspissated juice of saline-alkali land obtained to step 7 pass through
The refractive index of sonde-type digital display refractometer measurement salt-soda soil common seepweed seeds oil.
5. fluffy extract of saline-alkali land according to claim 1-3 and preparation method thereof, it is characterized in that: will acquisition
To the fluffy seed of saline-alkali land produce salt-soda soil common seepweed seeds oil, the overcritical titanium dioxide according to supercritical carbon dioxide extraction method
Carbon extraction is produced salt-soda soil common seepweed seeds oil and is successively prepared by following step:
Step 1, the fluffy seed of saline-alkali land is acquired, impurity elimination is screened, is sent into cleaning screen after the fluffy seed metering of saline-alkali land and is screened, removed
Soil, rubble, seed shell and dust；Through magnetic separator except de-iron is miscellaneous, stone remover removes rubble, clod, and impurity content is less than after screening
0.1%；
Step 2, the fluffy seed of saline-alkali land is put into vacuum oven, uniformly spreads out, is dried in vacuo, vacuum drying temperature is
40-60 DEG C, vacuum degree 10Pa-200Pa, vacuum drying time 3h-6h；
Step 3, the fluffy seed of saline-alkali land is crushed with pulverizer after vacuum drying, being crushed to mesh number is 60 mesh to 150 mesh；
Step 4, the fluffy powder of seeds of saline-alkali land is subjected to supercritical carbon dioxide extracting, separate mode is the second-order separation, a fraction
It is 8-10MPa from kettle pressure, the second-order separation kettle pressure is 5-8MPa, and level-one separating still temperature is regulated to 55 DEG C, the second-order separation kettle
Temperature is regulated to 35 DEG C, extraction time 2.5h-4.5h；
Step 5, the isolate in level-one separating still and the second-order separation kettle is collected, is evaporated in isolate using spiral evaporator
Then ethyl alcohol further removes ethyl alcohol in a vacuum drying oven under the conditions of 40 DEG C；
Step 6, point of the isolate in level-one separating still and the second-order separation kettle after step 5 removes ethyl alcohol, in level-one separating still
From object directly as, the isolate in the second-order separation kettle is centrifuged with centrifuge, centrifugal rotational speed be 30r/min -50r/min,
Centrifugation time is 20min, takes upper layer oil reservoir, is incorporated in the salt-soda soil common seepweed seeds oil in level-one separating still after collection, is uniformly mixed
Salt-soda soil common seepweed seeds oil to be prepared afterwards；Step 7, the fluffy seed oil concentration analysis of saline-alkali land, the salt-soda soil that step 6 is obtained
Common seepweed seeds oil measures the refractive index of salt-soda soil common seepweed seeds oil by sonde-type digital display refractometer.
6. fluffy extract of saline-alkali land according to claim 1 and preparation method thereof, it is characterized in that: by the fluffy stem of saline-alkali land
The fluffy extract A of weight reducing type saline-alkali land that leaf inspissated juice and salt-soda soil common seepweed seeds oil are mixed to get passes through sonde-type digital display refractometer
The refractive index for measuring the fluffy extract of saline-alkali land is 1.6236.
7. fluffy extract of saline-alkali land according to claim 2 and preparation method thereof, it is characterized in that: by the fluffy stem of saline-alkali land
The fluffy extract B of nutritive saline-alkali land alkali that leaf inspissated juice and salt-soda soil common seepweed seeds oil are mixed to get passes through sonde-type digital display refractometer
The refractive index for measuring the fluffy extract of saline-alkali land is 1.5237.
8. fluffy extract of saline-alkali land according to claim 1 and preparation method thereof, it is characterized in that: by the fluffy stem of saline-alkali land
The fluffy extract C of curative effect-type saline-alkali land that leaf inspissated juice and salt-soda soil common seepweed seeds oil are mixed to get passes through sonde-type digital display refractometer
The refractive index for measuring the fluffy extract of saline-alkali land is 1.4942.
9. fluffy extract of saline-alkali land according to claim 4 and preparation method thereof, it is characterized in that: ultrasound wave auxiliary enzyme method
Processing obtains reverse osmosis unit system configuration described in the step 7 of the fluffy cauline leaf inspissated juice of saline-alkali land are as follows: pretreatment system, smart mistake
Filter system, corollary system；Pretreatment system is made of mechanical filter, adsorption filter, cartridge filter；Smart filtration system by
Hollow-fibre ultrafiltration device composition；Corollary system is made of water purification pot, electrical control system, and mechanical filter filtering can go to mention
Take body refuse and the fiber etc. in liquid, after through adsorption filter filtering can remove oil removal, however filtered through mechanical filter
The impurity such as algae can be removed.
10. fluffy extract of saline-alkali land according to claim 4 and preparation method thereof, it is characterized in that: ultrasound wave auxiliary enzyme
Method handles to obtain ultrafiltration described in the step 7 of the fluffy cauline leaf inspissated juice of saline-alkali land to be that hollow-fibre membrane ultrafiltration is thin in extracting solution to remove
The microorganisms such as bacterium, mould, the hollow-fibre membrane diameter are 0.01 μm~0.001 μm, and feed rate is 900 L/h~1500
L/h, the pressure Mpa of 0.045 Mpa~0.18, feed concentration are the 200 μ g/L of μ g/L~400,100 min~400 of ultrafiltration time
Min, the backwash cycle min of 10 min~40, backwash time 20 min~120 min are upper operation 10 min~40 min, upper anti-
Wash the s of 20 s~120, lower operation 10 min~40 min, lower backwash 20 s~120 s.
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