CN109793689A - A kind of disposable hair film of moisture-keeping nutrient and preparation method thereof - Google Patents
A kind of disposable hair film of moisture-keeping nutrient and preparation method thereof Download PDFInfo
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- CN109793689A CN109793689A CN201910255438.7A CN201910255438A CN109793689A CN 109793689 A CN109793689 A CN 109793689A CN 201910255438 A CN201910255438 A CN 201910255438A CN 109793689 A CN109793689 A CN 109793689A
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Abstract
The invention discloses disposable hair films of a kind of moisture-keeping nutrient and preparation method thereof, the disposable hair film of moisture-keeping nutrient is in terms of mass fraction, including following components: 0.5-5 parts of sodium alginate, 0.1-2 parts of polyvinylpyrrolidone PVP-K30, 0.01-2 parts of collagen, 0.01-2 parts of fibroin, 0.5-3 parts of amino acid humectant, 0.5-3 parts of peg-7 glyceryl cocoate, 0.5-5 parts of ethoxy urea, two 0.1-1 parts of palm acyloxyethyl alkyl dimethyl ammonium chlorides, 0.5-2 parts of olive oil, 0.5-2 parts of camellia oil, 0.5-3 parts of glycerol, 4-20 parts of plant extracts, 50-80 parts of deionized water.Hair film of the invention is free of any chemical noxious additive, and while provide nutrition to hair, also has a stronger replenishing water and preserving moisture performance, the present invention have the characteristics that it is nontoxic, do not stimulate, not allergy, safety and environmental protection, disposable, easy to use.
Description
Technical field
The invention belongs to washing product technical fields, and in particular to a kind of disposable hair film of moisture-keeping nutrient and preparation method thereof.
Background technique
Hair film is a kind of moist hair " treatment wax ", it is the process of deep layer maintenance that it, which seems that women applies late frost,
Containing having plenty of nutriment and moisture in hair film, they can enter in hair through the hair scale piece on hair, help repairing fiber
Tissue helps hair to rejuvenate.
Hair is withered, it is lackluster be that manually pigment has filled up these empty, hairs because cavity , treatment oil occurs in hair
Just seem very full, but these artificial colors can be lost gradually with hair washing, solarization etc., hair restores as usual, Er Qiexian again
Contain a large amount of chemical substance in some hair films, the health for influencing user is used for a long time.
Summary of the invention
To solve the above-mentioned problems, the present invention provides a kind of disposable hair film of moisture-keeping nutrient, Environmental Safety, it is easy to use and
And better performances.
The technical solution of the present invention is as follows: a kind of disposable hair film of moisture-keeping nutrient, in terms of mass fraction, including following components:
0.5-5 parts of sodium alginate, 0.1-2 parts of polyvinylpyrrolidone PVP-K30,0.01-2 parts of collagen, silk egg
0.01-2 parts white, 0.5-3 parts of amino acid humectant, 0.5-3 parts of peg-7 glyceryl cocoate, 0.5-5 parts of ethoxy urea, two
0.1-1 parts of palm acyloxyethyl alkyl dimethyl ammonium chloride, 0.5-2 parts of olive oil, 0.5-2 parts of camellia oil, 0.5-3 parts of glycerol, plant
4-20 parts of extract, 50-80 parts of deionized water.
Preferably, the plant extracts is by 0.5-5 parts of Radix Isatidis, 0.5-2 parts of rosemary, Cape jasmine in terms of mass fraction
Son flower 0.5-2 part, 0.5-5 parts of dark plum, 0.5-3 parts of purple perilla, 0.5-4 parts of folium isatidis, 0.5-3 parts of dandelion extract form.
Preferably, in terms of mass fraction, including following components:
3 parts of sodium alginate, 1 part of polyvinylpyrrolidone PVP-K30,1 part of collagen, 2 parts of fibroin, amino acid
0.5 part of moisturizer, 2.2 parts of peg-7 glyceryl cocoate, 3 parts of ethoxy urea, two palm acyloxyethyl alkyl dimethyl ammonium chlorides
0.8 part, 1 part of olive oil, 0.9 part of camellia oil, 2 parts of glycerol, 18 parts of plant extracts, 75 parts of deionized water.
The present invention also provides the preparation methods of the disposable hair film of above-mentioned moisture-keeping nutrient, comprising the following steps:
(1) dark plum, purple perilla, folium isatidis, dandelion, Radix Isatidis, fan the preparation of the plant extracts: are weighed by mass parts
Repeatedly fragrant, gardenia, and impurity is removed, natural air drying is crushed into powder, and sieving is added deionized water, is cooked by slow fire, is cooled to
Room temperature, centrifuge separation collect supernatant and filter residue respectively, deionized water are added in filter residue, is cooked by slow fire, is cooled to room temperature,
Supernatant is collected in centrifuge separation, merges supernatant twice, and ethyl alcohol is added, and ultrasonic extraction 2~4 hours, filtrate was collected in filtering,
Concentration filtrate obtains the plant extracts；
(2) deionized water is added in dispersion machine, sets mixing speed as 1200~1800r/min, it while stirring will be extra large
Mosanom is added to the water, and is sufficiently stirred and makes it completely dissolved；
(3) polyvinylpyrrolidone PVP-K30 is added thereto while stirring, is sufficiently uniformly dissolved it；
(4) collagen, fibroin, amino acid humectant are added thereto, are stirred to dissolve uniformly；
(5) peg-7 glyceryl cocoate, ethoxy urea, two palm acyloxyethyl alkyl dimethyl ammonium chlorides, olive are sequentially added
Olive oil, camellia oil, glycerol stir to dissolve uniformly；
(6) plant extracts is added, stirs to dissolve and the disposable hair film of the moisture-keeping nutrient uniformly can be obtained.
Preferably, crossing the sieve of 50-100 mesh in the step (1), 10-20 times of gross mass of deionized water, mild fire is added
It decocts 5-6 hours, is cooled to room temperature, be centrifugated with the revolving speed of 1000-1500r/min, collect supernatant and filter residue respectively,
The deionized water of 5-10 times of its quality is added in filter residue, is cooked by slow fire 3-4 hours, is cooled to room temperature, with 1000~1500r/min
Revolving speed centrifuge separation collect supernatant, merge supernatant twice, 75% ethyl alcohol of 10~20 times of weights, ultrasonic extraction 2-4 be added
Hour, filtering, and filtrate is collected, by filtrate through 50-60 DEG C of temperature concentrated by rotary evaporation, obtain plant extracts.
Compared with prior art, the beneficial effects of the present invention are embodied in:
Hair film of the invention be free of any chemical noxious additive, and to hair provide nutrition while, also have compared with
Strong replenishing water and preserving moisture performance, the present invention have the characteristics that it is nontoxic, do not stimulate, not allergy, safety and environmental protection, disposable, easy to use.
Specific embodiment
Embodiment 1
A kind of preparation method of the disposable hair film of moisture-keeping nutrient, comprising the following steps:
(1) preparation of plant extracts: dark plum is weighed by mass parts, purple perilla, folium isatidis, dandelion, Radix Isatidis, fan change
Fragrant, gardenia, and impurity is removed, natural air drying is crushed into powder, and crosses the sieve of 50-100 mesh, and 10-20 times of gross mass of addition is gone
Ionized water is cooked by slow fire 5-6 hours, is cooled to room temperature, and is centrifugated with the revolving speed of 1000-1500r/min, collects supernatant respectively
The deionized water of 5-10 times of its quality is added in liquid and filter residue in filter residue, is cooked by slow fire 3-4 hours, is cooled to room temperature, with 1000
Supernatant is collected in the revolving speed centrifuge separation of~1500r/min, merges supernatant twice, 75% ethyl alcohol of 10~20 times of weights is added,
Ultrasonic extraction 2-4 hours, filtering, and filtrate is collected, by filtrate through 50-60 DEG C of temperature concentrated by rotary evaporation, obtain plant extracts；
(2) deionized water is added in dispersion machine, sets mixing speed as 1200~1800r/min, it while stirring will be extra large
Mosanom is added to the water, and is sufficiently stirred and makes it completely dissolved；
(3) polyvinylpyrrolidone PVP-K30 is added thereto while stirring, is sufficiently uniformly dissolved it；
(4) collagen, fibroin, amino acid humectant are added thereto, are stirred to dissolve uniformly；
(5) peg-7 glyceryl cocoate, ethoxy urea, two palm acyloxyethyl alkyl dimethyl ammonium chlorides, olive are sequentially added
Olive oil, camellia oil, glycerol stir to dissolve uniformly；
(6) plant extracts is added, stirs to dissolve and the disposable hair film of moisture-keeping nutrient uniformly can be obtained.
In above-mentioned preparation process, in terms of mass fraction, the proportion of each component are as follows:
3 parts of sodium alginate, 1 part of polyvinylpyrrolidone PVP-K30,1 part of collagen, 2 parts of fibroin, amino acid
0.5 part of moisturizer, 2.2 parts of peg-7 glyceryl cocoate, 3 parts of ethoxy urea, two palm acyloxyethyl alkyl dimethyl ammonium chlorides
0.8 part, 1 part of olive oil, 0.9 part of camellia oil, 2 parts of glycerol, 18 parts of plant extracts, 75 parts of deionized water.
In terms of mass fraction, the plant extracts is by 3 parts of Radix Isatidis, 1 part of rosemary, 1 part of gardenia, 4 parts of dark plum, purple
Soviet Union 2 parts, 4 parts of folium isatidis, 2 parts of dandelion extract composition.
In use, taking appropriate product in the centre of the palm, it sufficiently is applied to healthy hair middle and back (dry and wet hair) after rubbing, is not necessarily to
It rinses.
Embodiment 2
The present embodiment the difference from embodiment 1 is that, the proportion of each component is not identical, preparation method and 1 phase of embodiment
Together.In the present embodiment in terms of mass fraction, the proportion of each component are as follows:
0.5 part of sodium alginate, 2 parts of polyvinylpyrrolidone PVP-K30,0.01 part of collagen, 2 parts of fibroin, ammonia
0.5 part of base acid moisturizer, 3 parts of peg-7 glyceryl cocoate, 0.5 part of ethoxy urea, two palm acyloxyethyl dimethylammonium chlorides
1 part of ammonium, 0.5 part of olive oil, 2 parts of camellia oil, 0.5 part of glycerol, 20 parts of plant extracts, 50 parts of deionized water.
In terms of mass fraction, the plant extracts is by 3 parts of butter fruit, 0.5 part of Radix Isatidis, 2 parts of rosemary, gardenia
0.5 part, 5 parts of dark plum, 0.5 part of purple perilla, 4 parts of folium isatidis, 0.5 part of dandelion extract composition.
Embodiment 3
The present embodiment the difference from embodiment 1 is that, the proportion of each component is not identical, preparation method and 1 phase of embodiment
Together.In the present embodiment in terms of mass fraction, the proportion of each component are as follows:
5 parts of sodium alginate, 0.1 part of polyvinylpyrrolidone PVP-K30,2 parts of collagen, 0.01 part of fibroin, ammonia
3 parts of base acid moisturizer, 0.5 part of peg-7 glyceryl cocoate, 5 parts of ethoxy urea, two palm acyloxyethyl alkyl dimethyl ammonium chlorides
0.1 part, 2 parts of olive oil, 0.5 part of camellia oil, 3 parts of glycerol, 4 parts of plant extracts, 80 parts of deionized water.
In terms of mass fraction, the plant extracts is by 0.5 part of butter fruit, 5 parts of Radix Isatidis, 0.5 part of rosemary, gardenia
2 parts, 0.5 part of dark plum, 3 parts of purple perilla, 0.5 part of folium isatidis, 3 parts of dandelion extract composition.
1, safety evaluatio
Referring to " cosmetics safety technical specification " (2015 editions) to the health of disposable hair film obtained, chemistry, sense organ, physics and chemistry
Index is tested, and experimental result see the table below.
Through examining, the hygienic chemistry of the disposable hair film of the embodiment of the present invention 1~3, microorganism, toxicologic index meet
The requirement of " cosmetics safety technical specification " (2015 editions).
The disposable hair film inspection result that 1 embodiment of the present invention of table is prepared
2, storage stability is tested
Stability test is carried out again after product obtained is placed for 24 hours.
It to accurately measure the stability of product, need to store for a long time, but also can have difference because of the Different Results in storage area
It is different, for laboratory research, by long-term storage, experiment process must be delayed, therefore survey using the method for strengthening natural conditions
The stability of fixed output quota product.
Product is put in centrifuge, centrifuge speed is adjusted, how long observation product is layered in centrifuge transfer, root
According to formula (1) can approximate calculation product storage time, the storage stability of product is judged with this.
T1Sedimentation time of-liquid the pearl under gravity field action, h.
T2Sedimentation time of-liquid the pearl under effect of centrifugal force, h.
R-centrifuge radius.
G-acceleration of gravity, g=9.8m/s2。
Due to limited time, the storage stability of this disposable hair film is determined using natural conditions method is strengthened.
The disposable hair film obtained prepared by implementing 1,2,3 respectively is placed in the centrifuge that radius is 10cm, with 3600r/min
Revolving speed rotating centrifugal, centrifugation 25.6h, 26.1h, 26.8h after there is water-oil separating phenomenon.It is store according to above-mentioned formula approximate calculation
The time is deposited, the storage stability of disposable hair film is judged with this.
It is to be respectively by strengthening the period of storage that natural conditions method is analyzed to obtain the disposable hair film of above-described embodiment 1,2,3
4.2 years, 4.3 years, 4.4 years, more than 4 years.
3, effect performance
120 testers are selected to use, 120 testers are equally divided into 3 groups of test groups, and every group 40,3 groups of tests
Group uses the hair film of Examples 1 to 3 respectively, every tester two days using primary, be used continuously 8 times, tester according to
Use feeling is given a mark, and every group is averaged to obtain test result, and test result is shown in Table 1.Dry carding (1~5 point) is done
Send out feel (1~5 point), moisture retention (1~5 point), glossiness (1~5 point), repairing effect (1~5 point), score value more high effect more
Good, test result is shown in Table 2.
The evaluation of 2 using effect of table
Resulting disposable hair film will be prepared to press for the disposable hair film brand of situation of selling well of colouring and perming repairing hair quality on the market with domestic
It is compared according to above-mentioned double-blind comparative approach.Through each property for comparing the disposable hair film that the embodiment of the present invention 1~3 is prepared
Energy index is superior to famous brand name hot-sale products in the market.
In addition, also sending barber shop and social crowd to be applicable in prepared disposable hair film, target user is cured hundred people, satisfaction
Up to 96% or more, to hair severity index, there is preferable repairing effect, and disposable, it is convenient and efficient.
Claims (5)
1. a kind of disposable hair film of moisture-keeping nutrient, which is characterized in that in terms of mass fraction, including following components:
0.5-5 parts of sodium alginate, 0.1-2 parts of polyvinylpyrrolidone PVP-K30,0.01-2 parts of collagen, fibroin
0.01-2 parts, 0.5-3 parts of amino acid humectant, 0.5-3 parts of peg-7 glyceryl cocoate, 0.5-5 parts of ethoxy urea, two palm fibres
0.1-1 parts of palmitic acid acyloxyethyl alkyl dimethyl ammonium chloride, 0.5-2 parts of olive oil, 0.5-2 parts of camellia oil, 0.5-3 parts of glycerol, plant mention
Take 4-20 parts of object, 50-80 parts of deionized water.
2. the disposable hair film of moisture-keeping nutrient as described in claim 1, which is characterized in that in terms of mass fraction, the plant extract
Object is by 0.5-5 parts of Radix Isatidis, 0.5-2 parts of rosemary, 0.5-2 parts of gardenia, 0.5-5 parts of dark plum, 0.5-3 parts of purple perilla, folium isatidis
0.5-4 parts, 0.5-3 parts of dandelion of extract composition.
3. the disposable hair film of moisture-keeping nutrient as claimed in claim 2, which is characterized in that in terms of mass fraction, including following components:
3 parts of sodium alginate, 1 part of polyvinylpyrrolidone PVP-K30,1 part of collagen, 2 parts of fibroin, amino acid moisturizing
0.5 part of agent, 2.2 parts of peg-7 glyceryl cocoate, 3 parts of ethoxy urea, two 0.8 part of palm acyloxyethyl alkyl dimethyl ammonium chlorides,
1 part of olive oil, 0.9 part of camellia oil, 2 parts of glycerol, 18 parts of plant extracts, 75 parts of deionized water.
4. the preparation method of the disposable hair film of moisture-keeping nutrient as described in claims 1 to 3 is any, which is characterized in that including following
Step:
(1) preparation of the plant extracts: dark plum is weighed by mass parts, purple perilla, folium isatidis, dandelion, Radix Isatidis, fan change
Fragrant, gardenia, and impurity is removed, natural air drying is crushed into powder, and sieving is added deionized water, is cooked by slow fire, is cooled to room
Temperature, centrifuge separation collect supernatant and filter residue respectively, deionized water are added in filter residue, is cooked by slow fire, is cooled to room temperature, from
The heart separates and collects supernatant, merges supernatant twice, and ethyl alcohol is added, and ultrasonic extraction 2~4 hours, filtrate was collected in filtering, dense
Contracting filtrate obtains the plant extracts；
(2) deionized water is added in dispersion machine, sets mixing speed as 1200~1800r/min, while stirring by alginic acid
Sodium is added to the water, and is sufficiently stirred and makes it completely dissolved；
(3) polyvinylpyrrolidone PVP-K30 is added thereto while stirring, is sufficiently uniformly dissolved it；
(4) collagen, fibroin, amino acid humectant are added thereto, are stirred to dissolve uniformly；
(5) peg-7 glyceryl cocoate, ethoxy urea, two palm acyloxyethyl alkyl dimethyl ammonium chlorides, olive are sequentially added
Oil, camellia oil, glycerol stir to dissolve uniformly；
(6) plant extracts is added, stirs to dissolve and the disposable hair film of the moisture-keeping nutrient uniformly can be obtained.
5. the preparation method of the disposable hair film of moisture-keeping nutrient as claimed in claim 4, which is characterized in that mistake in the step (1)
The sieve of 50-100 mesh is added 10-20 times of gross mass of deionized water, is cooked by slow fire 5-6 hours, is cooled to room temperature, with 1000-
The revolving speed of 1500r/min is centrifugated, and collects supernatant and filter residue respectively, the deionization of 5-10 times of its quality is added in filter residue
Water is cooked by slow fire 3-4 hours, is cooled to room temperature, and collects supernatant with the revolving speed centrifuge separation of 1000~1500r/min, merges
Supernatant twice is added 75% ethyl alcohol of 10~20 times of weights, ultrasonic extraction 2-4 hours, filters, and collect filtrate, filtrate is passed through
50-60 DEG C of temperature concentrated by rotary evaporation, obtains plant extracts.
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| CN201910255438.7A CN109793689A (en) | 2019-04-01 | 2019-04-01 | A kind of disposable hair film of moisture-keeping nutrient and preparation method thereof |
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| CN201910255438.7A CN109793689A (en) | 2019-04-01 | 2019-04-01 | A kind of disposable hair film of moisture-keeping nutrient and preparation method thereof |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN114288210A (en) * | 2021-12-31 | 2022-04-08 | 广州市芊彩化妆品有限公司 | Wash-free hair conditioner containing cationic hyaluronic acid and preparation method thereof |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH01175924A (en) * | 1987-12-28 | 1989-07-12 | Hoou Kk | Hair treatment agent |
| CN106562914A (en) * | 2016-11-03 | 2017-04-19 | 林振慧 | Hair conditioner |
| CN108451890A (en) * | 2018-06-21 | 2018-08-28 | 佛山市三水区嘉华化学研究院（普通合伙） | A kind of deep layer repairs moisturizing hair film and preparation method thereof |
-
2019
- 2019-04-01 CN CN201910255438.7A patent/CN109793689A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH01175924A (en) * | 1987-12-28 | 1989-07-12 | Hoou Kk | Hair treatment agent |
| CN106562914A (en) * | 2016-11-03 | 2017-04-19 | 林振慧 | Hair conditioner |
| CN108451890A (en) * | 2018-06-21 | 2018-08-28 | 佛山市三水区嘉华化学研究院（普通合伙） | A kind of deep layer repairs moisturizing hair film and preparation method thereof |
Non-Patent Citations (1)
| Title |
|---|
| 黄攀丽等: "海藻酸钠的提取与功能化改性研究进展", 《林产化学与工业》 * |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN114288210A (en) * | 2021-12-31 | 2022-04-08 | 广州市芊彩化妆品有限公司 | Wash-free hair conditioner containing cationic hyaluronic acid and preparation method thereof |
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