CN109748591A - A kind of liquid ceramics mud degumming agent and preparation method thereof - Google Patents
A kind of liquid ceramics mud degumming agent and preparation method thereof Download PDFInfo
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- CN109748591A CN109748591A CN201910248933.5A CN201910248933A CN109748591A CN 109748591 A CN109748591 A CN 109748591A CN 201910248933 A CN201910248933 A CN 201910248933A CN 109748591 A CN109748591 A CN 109748591A
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- degumming agent
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- ceramics mud
- calgon
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Abstract
The invention discloses a kind of liquid ceramics mud degumming agent, which includes the raw material composition of following weight percents: 48%-50% liquid alkaline: 13%, water: and 5%, calgon: 5%, Sodium Polyacrylate: 5%, 50Be waterglass: 72%；The present invention is to utilize liquid alkaline, water, calgon, Sodium Polyacrylate, waterglass reacts liquid ceramics mud degumming agent obtained after mixing according to a certain percentage, accelerate being sufficiently mixed for mud and degumming agent, mud dispergation difficulty is effectively reduced, improve the dispergation performance to mud, it is ensured that mud has good and stable quality.
Description
Technical field
The present invention relates to technical field of ceramic production, in particular to a kind of liquid ceramics mud degumming agent.
Background technique
Ceramic mud is a complicated solid-liquid dispersing system, and dispersion left floating tiny solid particle, mud in the liquid phase
Solid particle in slurry includes silicate and aluminium mineral material, each type oxide and non-oxidized substance, in dispersion, due to weight
Power and electrostatic force can cause to reunite and settle, reunite in order to prevent and settle to the effect of dispersed phase, keep the stability of slurry,
Make to keep optimal electrostatic repulsion between particle and particle to be highly important.The mechanism of action of degumming agent is exactly to pass through raising system
Particle zeta potential in system guarantees repulsion appropriate between particle, so that system be made to reach dynamic equilibrium, mud stabilization is kept not send out
It is raw to reunite and settle.
But existing ceramic mud degumming agent, predominantly silicate, phosphate product, dispergation performance is lower, generation
Mud is poor quality and unstable.
Summary of the invention
The purpose of the present invention is to provide a kind of liquid ceramics mud degumming agents and preparation method thereof, to solve above-mentioned background
The problem of being proposed in technology.
To achieve the above object, the present invention provides following scheme:
A kind of liquid ceramics mud degumming agent, the liquid ceramics mud degumming agent include the raw material composition of following weight percents:
48%-50% liquid alkaline: 13%, water: 5%, calgon: 5%, Sodium Polyacrylate: 5%, 50Be waterglass: 72%.
As a further solution of the present invention: the liquid ceramics mud degumming agent includes the raw material group of following weight percents
At: 49%-50% liquid alkaline: 13%, water: 5%, calgon: 5%, Sodium Polyacrylate: 5%, 50Be waterglass: 72%.
As further scheme of the invention: the liquid ceramics mud degumming agent includes the raw material of following weight percents
Composition: 49% liquid alkaline: 13%, water: 5%, calgon: 5%, Sodium Polyacrylate: 5%, 50Be waterglass: 72%.
It is a further object of the present invention to provide the preparation methods of main body, include the following steps:
1) by liquid alkaline, water, calgon, Sodium Polyacrylate, 50Be waterglass proportionally put into blender be stirred it is mixed
Reaction is closed, solidliquid mixture is made；
2) it is passed through vapor into the built-in coil pipe of the blender equipped with the made solidliquid mixture of step 1), and passes through heat transfer pair
The made solidliquid mixture of step 1) carries out continuous heating and stirs, when temperature rises 80 DEG C, in the made mixture of step 1)
Calgon and Sodium Polyacrylate sufficiently dissolve, and form mixed liquor；
3) mixed liquor made from step 2 is injected to stand in cooling bay and is cooled to 20 DEG C, obtain liquid ceramics mud degumming agent；
4) product inspection, check the weight, pack, being put in storage.
As further embodiment of the invention, the built-in coil pipe of the step 1) blender is uniformly equidistantly mounted on described
The inner wall of step 1) blender, and the outer wall of built-in coil pipe is coated with anti-corrosion heat-conductive coating.
As further scheme of the invention, the mixeding liquid temperature formed in the step 2 is 80 DEG C -85 DEG C.
As further scheme of the invention, inside is in sealing state when blender is stirred.
Compared with prior art, the beneficial effects of the present invention are: the present invention is to utilize liquid alkaline, water, calgon, poly- third
Olefin(e) acid sodium, waterglass react liquid ceramics mud degumming agent obtained, accelerate mud and dispergation after mixing according to a certain percentage
Agent is sufficiently mixed, and mud dispergation difficulty is effectively reduced, and improves the dispergation performance to mud, it is ensured that mud have it is good and
Stable quality.
Specific embodiment
Below in conjunction with specific embodiment, the technical scheme of the present invention will be explained in further detail.
Embodiment 1
A kind of liquid ceramics mud degumming agent, the liquid ceramics mud degumming agent include the raw material composition of following weight percents:
48% liquid alkaline: 13%, water: 5%, calgon: 5%, Sodium Polyacrylate: 5%, 50Be waterglass: 72%.
1) by liquid alkaline, water, calgon, Sodium Polyacrylate, 50Be waterglass proportionally puts into blender, and starting is stirred
The machine of mixing is stirred hybrid reaction, and solidliquid mixture is made；
2) it is passed through vapor into the built-in coil pipe of the blender equipped with the made solidliquid mixture of step 1), vapor is in built-in disk
Heat is discharged in pipe, and the made solidliquid mixture of step 1) is transferred heat to by way of heat transfer, while passing through stirring
Machine carries out uniform stirring, by smearing anti-corrosion heat-conductive coating in built-in coil pipe outer wall, enhances the thermal conductivity of built-in coil pipe, simultaneously
The corrosion that coil pipe built in blender is subject to is alleviated, and blender remains high-seal during the work time, avoids raw material
In moisture heated be evaporated to the external world, it is ensured that the ratio of water keeps stablizing in raw material, when stirring built-in temperature and rising 80 DEG C, step
Calgon and Sodium Polyacrylate in rapid 1) made mixture sufficiently dissolve, and form mixed liquor；
3) blender stops stirring, is simultaneously stopped into built-in coil pipe and inputs vapor, and opening blender will be made from step 2
It is stood in mixed liquor injection cooling bay and is cooled to 20 DEG C, obtain liquid ceramics mud degumming agent；
4) product inspection, check the weight, pack, being put in storage.
Embodiment 2
A kind of liquid ceramics mud degumming agent, the liquid ceramics mud degumming agent include the raw material composition of following weight percents:
49% liquid alkaline: 13%, water: 5%, calgon: 5%, Sodium Polyacrylate: 5%, 50Be waterglass: 72%.
1) by liquid alkaline, water, calgon, Sodium Polyacrylate, 50Be waterglass proportionally puts into blender and stirred
Hybrid reaction is mixed, solidliquid mixture is made；
2) it is passed through vapor into the built-in coil pipe of the blender equipped with the made solidliquid mixture of step 1), vapor is in built-in disk
Heat is discharged in pipe, and the made solidliquid mixture of step 1) is transferred heat to by way of heat transfer, while passing through stirring
Machine carries out uniform stirring, by smearing anti-corrosion heat-conductive coating in built-in coil pipe outer wall, enhances the thermal conductivity of built-in coil pipe, simultaneously
The corrosion that coil pipe built in blender is subject to is alleviated, and blender remains high-seal during the work time, avoids raw material
In moisture heated be evaporated to the external world, it is ensured that the ratio of water keeps stablizing in raw material, when stirring built-in temperature and rising 80 DEG C, step
Calgon and Sodium Polyacrylate in rapid 1) made mixture sufficiently dissolve, and form mixed liquor；
3) blender stops stirring, is simultaneously stopped into built-in coil pipe and inputs vapor, and opening blender will be made from step 2
It is stood in mixed liquor injection cooling bay and is cooled to 20 DEG C, obtain liquid ceramics mud degumming agent；
4) product inspection, check the weight, pack, being put in storage.
Embodiment 3
A kind of liquid ceramics mud degumming agent, the liquid ceramics mud degumming agent include the raw material composition of following weight percents:
49% liquid alkaline: 13%, water: 5%, calgon: 5%, Sodium Polyacrylate: 5%, 50Be waterglass: 72%.
1) by liquid alkaline, water, calgon, Sodium Polyacrylate, 50Be waterglass proportionally puts into blender and stirred
Hybrid reaction is mixed, solidliquid mixture is made；
2) it is passed through vapor into the built-in coil pipe of the blender equipped with the made solidliquid mixture of step 1), vapor is in built-in disk
Heat is discharged in pipe, and the made solidliquid mixture of step 1) is transferred heat to by way of heat transfer, while passing through stirring
Machine carries out uniform stirring, by smearing anti-corrosion heat-conductive coating in built-in coil pipe outer wall, enhances the thermal conductivity of built-in coil pipe, simultaneously
The corrosion that coil pipe built in blender is subject to is alleviated, and blender remains high-seal during the work time, avoids raw material
In moisture heated be evaporated to the external world, it is ensured that the ratio of water keeps stablizing in raw material, when stirring built-in temperature and rising 80 DEG C, step
Calgon and Sodium Polyacrylate in rapid 1) made mixture sufficiently dissolve, and form mixed liquor；
3) blender stops stirring, is simultaneously stopped into built-in coil pipe and inputs vapor, and opening blender will be made from step 2
It is stood in mixed liquor injection cooling bay and is cooled to 20 DEG C, obtain liquid ceramics mud degumming agent；
4) product inspection, check the weight, pack, being put in storage.
Using effect test
This investigation is continuously tried out 1 year by 50 enterprises, investigates the effect of the liquid ceramics mud degumming agent various aspects.Assessment item
Mesh standards of grading are as follows: excellent 5 points, good 4 points, general 3 points, poor 2 points, excessively poor 1 point.Wherein commercial product is conventional ceramic dispergation
Agent；
| Test item | Embodiment 1 | Embodiment 2 | Embodiment 3 | Commercial product |
| Concentration of hydraulic mixture | 4.8 | 4.9 | 4.7 | 4.1 |
| Mud moisture content | 4.9 | 4.6 | 5 | 3.5 |
| Mobility | 4.9 | 5 | 4.9 | 3.8 |
| Suspension | 4.9 | 4.9 | 4.8 | 4.2 |
The present invention is using liquid alkaline, water, calgon, Sodium Polyacrylate, and waterglass reacts system after mixing according to a certain percentage
Liquid ceramics mud degumming agent, accelerate being sufficiently mixed for mud and degumming agent, mud dispergation difficulty be effectively reduced, improve
To the dispergation performance of mud, it is ensured that mud has good and stable quality.
Better embodiment of the invention is explained in detail above, but present invention is not limited to the embodiments described above,
Within the knowledge of one of ordinary skill in the art, it can also make without departing from the purpose of the present invention
Various change.
Claims (7)
1. a kind of liquid ceramics mud degumming agent, which is characterized in that the liquid ceramics mud degumming agent includes following weight percent
The raw material of ratio forms: 48%-50% liquid alkaline: 13%, water: and 5%, calgon: 5%, Sodium Polyacrylate: 5%, 50Be waterglass:
72%。
2. liquid ceramics mud degumming agent according to claim 1, which is characterized in that the liquid ceramics mud degumming agent packet
The raw material for including following weight percents forms: 49%-50% liquid alkaline: 13%, water: and 5%, calgon: 5%, Sodium Polyacrylate: 5%,
50Be waterglass: 72%.
3. liquid ceramics mud degumming agent according to claim 1, which is characterized in that the liquid ceramics mud degumming agent packet
The raw material for including following weight percents forms: 49% liquid alkaline: 13%, water: and 5%, calgon: 5%, Sodium Polyacrylate: 5%, 50Be
Waterglass: 72%.
4. a kind of preparation method of liquid ceramics mud degumming agent a method according to any one of claims 1-3, which is characterized in that including
Following steps:
1) by liquid alkaline, water, calgon, Sodium Polyacrylate, 50Be waterglass proportionally put into blender be stirred it is mixed
Reaction is closed, solidliquid mixture is made；
2) it is passed through vapor into the built-in coil pipe of the blender equipped with the made solidliquid mixture of step 1), and passes through heat transfer pair
The made solidliquid mixture of step 1) carries out continuous heating and stirs, when temperature rises 80 DEG C, in the made mixture of step 1)
Calgon and Sodium Polyacrylate sufficiently dissolve, and form mixed liquor；
3) mixed liquor made from step 2 is injected to stand in cooling bay and is cooled to 20 DEG C, obtain liquid ceramics mud degumming agent；
4) product inspection, check the weight, pack, being put in storage.
5. the preparation method of liquid ceramics mud degumming agent according to claim 4, which is characterized in that the step 1) is stirred
The built-in coil pipe for mixing machine is uniformly equidistantly mounted on the inner wall of the step 1) blender, and the outer wall of built-in coil pipe is coated with anti-corrosion and leads
Hot coating.
6. the preparation method of liquid ceramics mud degumming agent according to claim 4, which is characterized in that in the step 2
The mixeding liquid temperature of formation is 80 DEG C -85 DEG C.
7. the preparation method of liquid ceramics mud degumming agent according to claim 4, which is characterized in that blender is stirred
Inside is in sealing state when mixing.
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Cited By (6)
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|---|---|---|---|---|
| CN110713388A (en) * | 2019-09-17 | 2020-01-21 | 江西省欧陶科技有限公司 | Ceramic slurry debonder capable of reducing thixotropy of ceramic tile slurry and preparation method thereof |
| CN110746194A (en) * | 2019-11-12 | 2020-02-04 | 太原逸峰源科技有限公司 | Ceramic water reducing agent and preparation method thereof |
| CN111393143A (en) * | 2020-03-31 | 2020-07-10 | 中科院广州化学有限公司 | Desulfurization wastewater debonder and preparation method and application thereof |
| CN111454066A (en) * | 2020-03-20 | 2020-07-28 | 肇庆市欧陶新型材料有限公司 | Polyamine epoxy adduct-containing polymetaphosphonate ceramic water-quality adaptive dispergator |
| CN115073187A (en) * | 2022-07-01 | 2022-09-20 | 江西雄瓷科技有限公司 | Preparation method of compound liquid debonder |
| CN116789456A (en) * | 2023-07-10 | 2023-09-22 | 佛山市奥林万达新型建材有限公司 | Ceramic dispergator and preparation method thereof |
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Cited By (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110713388A (en) * | 2019-09-17 | 2020-01-21 | 江西省欧陶科技有限公司 | Ceramic slurry debonder capable of reducing thixotropy of ceramic tile slurry and preparation method thereof |
| CN110746194A (en) * | 2019-11-12 | 2020-02-04 | 太原逸峰源科技有限公司 | Ceramic water reducing agent and preparation method thereof |
| CN111454066A (en) * | 2020-03-20 | 2020-07-28 | 肇庆市欧陶新型材料有限公司 | Polyamine epoxy adduct-containing polymetaphosphonate ceramic water-quality adaptive dispergator |
| CN111454066B (en) * | 2020-03-20 | 2022-02-11 | 肇庆市欧陶新型材料有限公司 | Polyamine epoxy adduct-containing polymetaphosphonate ceramic water-quality adaptive dispergator |
| CN111393143A (en) * | 2020-03-31 | 2020-07-10 | 中科院广州化学有限公司 | Desulfurization wastewater debonder and preparation method and application thereof |
| CN111393143B (en) * | 2020-03-31 | 2022-04-05 | 中科院广州化学有限公司 | Desulfurization wastewater debonder and preparation method and application thereof |
| CN115073187A (en) * | 2022-07-01 | 2022-09-20 | 江西雄瓷科技有限公司 | Preparation method of compound liquid debonder |
| CN116789456A (en) * | 2023-07-10 | 2023-09-22 | 佛山市奥林万达新型建材有限公司 | Ceramic dispergator and preparation method thereof |
| CN116789456B (en) * | 2023-07-10 | 2024-04-19 | 佛山市奥林万达新型建材有限公司 | Ceramic dispergator and preparation method thereof |
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Application publication date: 20190514 |