CN109744237A - A kind of synergistic composition containing Duraset - Google Patents
A kind of synergistic composition containing Duraset Download PDFInfo
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- CN109744237A CN109744237A CN201711079969.2A CN201711079969A CN109744237A CN 109744237 A CN109744237 A CN 109744237A CN 201711079969 A CN201711079969 A CN 201711079969A CN 109744237 A CN109744237 A CN 109744237A
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- duraset
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
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- Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
- Y02A40/00—Adaptation technologies in agriculture, forestry, livestock or agroalimentary production
- Y02A40/10—Adaptation technologies in agriculture, forestry, livestock or agroalimentary production in agriculture
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Abstract
The present invention relates to a kind of synergistic compositions containing Duraset, effective active composition is active components A and active constituent B, active components A is Duraset, active constituent B is selected from any one following compound: super quick albumen, gibberellic acid, antibacterial peptide, humic acid, adjust naphthenic acid and its salt, Brodifacoum, flumetralim, the present composition increases effective absorption of the crop to fertilizer, supplemental crop disadvantage part is well grown, adjust the balance of crop internal water, to activate the metabolic system of crop, crop cell is promoted to increase, root activity is reinforced, improve crop fruit-setting rate, promote Fruit, prevent shattering, volume increase, Delaying Leaf-Senescence, improve crop lodging tolerance, the drought resisting of certain crops can also be improved, the ability of cold-resistant and disease and insect resistance.
Description
Technical field
The invention belongs to technical field of pesticide, are related to a kind of answering on crops of the synergistic composition containing Duraset
With.
Technical background
Duraset increases fruit-setting rate, enhances the photosynthesis of crop significantly, use by promoting plant to bloom more
The obvious greening of rear blade thickens, becomes larger, and increases absorption and utilization rate to carbon dioxide, increases the substances such as protein, lipid
Accumulation storage, promotes cell division and growth.
Super quick albumen, gibberellic acid, antibacterial peptide, humic acid, tune naphthenic acid and its salt, Brodifacoum, flumetralim are
The common plant growth regulator of pesticide field.
Applicant it is found through experiment that, by the different Duraset of the mechanism of action and super quick albumen, gibberellic acid, antibacterial peptide,
Humic acid adjusts naphthenic acid and its salt, Brodifacoum, flumetralim to be compounded respectively, promotes crop cell to increase, root system is lived
Power is reinforced, improves crop fruit-setting rate, and Delaying Leaf-Senescence improves crop lodging tolerance, can also improve the anti-of certain crops
The ability of drought, cold-resistant and disease and insect resistance, synergistic effect is obvious, and dosage and times for spraying reduction, control cost are low.
Summary of the invention
The purpose of the present invention is to propose to a kind of with synergistic function, the phthalein containing toluene that use cost is low, effect is good
The composition of propylhomoserin.
The present invention is achieved through the following technical solutions:
A kind of synergistic composition containing Duraset, effective active composition are active components A and active constituent B, spy
Sign is: the weight ratio of active components A and active constituent B are 200 ︰, 1~1 ︰ 50, and the active components A is Duraset,
Active constituent B is selected from super quick albumen, gibberellic acid, antibacterial peptide, humic acid, adjusts naphthenic acid and its salt, Brodifacoum, flumetralim
One of kind, active components A and the preferred weight ratio of active constituent B are 100 ︰, 1~1 ︰ 30 in composition;It is wherein highly preferred
Scheme is: the weight ratio of Duraset and super quick albumen or gibberellic acid or Brodifacoum or tune naphthenic acid and its salt is
20 ︰, 1~1 ︰ 5;The weight ratio of Duraset and antibacterial peptide is 80 ︰ 1~1
︰ 1;The weight ratio of Duraset and humic acid or flumetralim is 5 ︰, 1~1 ︰ 20.
Synergistic composition of the present invention containing Duraset can be configured to according to methods well known to those skilled in the art
Dosage form be wettable powder, soluble powder, soluble granule, soluble liquid, water dispersible granules, aqua, granule,
Aqueous emulsion, microemulsion, suspending agent, effervescent tablet, seed coat agent, liniment can also be made.
The synergistic composition containing Duraset, wherein effective active composition content account for total weight 0.1%~
60%, preferably 1%~50%, highly preferred content is 5%~30%.
Synergistic composition containing Duraset is for coordinate plant growth, the germination of promotion crop, raising fruit-setting rate, guarantor
Flower, volume increase, purposes resistant to lodging.
Surfactant selected by antibacterial volume increase composition of the invention is known in those skilled in the art: can be with
Selected from one or more of dispersing agent, wetting agent, thickener or defoaming agent.This can also be contained according to different dosage forms, in preparation
Stabilizer well known to the technical staff of field, antifreeze etc..
Comprising following constituent content when composition is made wettable powder: active components A 0.05%~50%, activity at
Divide B 0.05%~50%, dispersing agent 2%~10%, wetting agent 2%~10%, filler surplus.
Comprising following constituent content when composition is made soluble granule: active components A 0.05%~50%, activity at
Point B0.05%~50%, binder 0~8%, colorant 0.1%-2%, dispersing agent 2%~10%, wetting agent 2%~10%,
Filler surplus.
Composition includes following constituent content when soluble powder is made: active components A 0.05%~50%, active constituent
B 0.05%~50%, dispersing agent 2%~8%, wetting agent 1%-7%, stabilizer 0~5%, filler surplus.
Composition includes following constituent content when soluble liquid is made: active components A 0.05%~30%, active constituent
B 0.05%~30%, emulsifier 1%~10%, cosolvent 2%~6%, solvent add to 100%.
Composition includes following constituent content when water dispersible granules are made: active components A 0.05%~50%, activity at
Point B 0.05%~50%, dispersing agent 3%~12%, wetting agent 1%~8%, disintegrating agent 1%~10%, binder 0~8%,
Filler surplus.
Composition includes following constituent content when aqua is made: active components A 0.05%~30%, active constituent B
0.05%~30%, cosolvent 2%~6%, wetting agent 1%-10%, antifreeze 0~8%, deionized water add to 100%.
Wettable powder the key technical indexes of the invention:
Soluble granule the key technical indexes of the invention:
Soluble powder the key technical indexes of the invention:
Soluble liquid the key technical indexes of the invention:
Water dispersible granules the key technical indexes of the invention:
Aqua the key technical indexes of the invention:
The present invention has the advantages that
(1) Duraset and super quick albumen, gibberellic acid, antibacterial peptide, humic acid, adjust naphthenic acid and its salt, to chlorobenzene oxygen second
After sour sodium, flumetralim compounding, there is apparent synergy and lasting effect;(2) to cereal crops, legume crop, fibre crops, sugar
Expect crop, melon crop, fruits crop, dry fruit crop, hobby crop, root crop, oil crops, flower crop,
Medicinal crop, crop, the coordinate plant growth on green manure pasture crop have greater activity;(3) reduce pesticide medication
Amount, reduces residual quantity of the pesticide on crop, alleviates environmental pollution;(4) to safety of human and livestock, Environmental compatibility is good;And
The enhancing of preparation adhesion strength, resistance of rainwater washing against;(5) shift to an earlier date crop germinating time, bud uniformity improves, and quality is improved,
Flower is protected, fruit-setting rate is improved, is resistant to lodging.
Specific embodiment
Below with reference to embodiment to further instruction of the present invention, the percentage in embodiment is weight percentage, but
The present invention is not limited thereto.
Application Example one
Examples 1 to 8 wettable powder
Duraset, active constituent B, dispersing agent, wetting agent, filler are uniformly mixed in mixed cylinder, through air-flow powder
Broken machine remixes uniformly after crushing, and can be prepared by wettable powder product of the present invention, is specifically shown in Table 1.
1 Examples 1 to 8 each component of table and parts by weight
9~16 soluble granule of embodiment
Duraset, active constituent B, binder (can add can be not added), colorant, dispersing agent, wetting agent, filler are existed
It is uniformly mixed in mixed cylinder, is passing through extrusion granulation, drying, and screened soluble granule of the present invention is made produced
Product are specifically shown in Table 2.
2 embodiment of table, 9~16 each component and parts by weight
17~24 soluble powder of embodiment
By Duraset, active constituent B, dispersing agent, wetting agent, stabilizer (can add can be not added), filler in mixed cylinder
In be uniformly mixed, remix after being smashed by air jet mill uniformly, can be prepared by soluble powder product of the present invention, have
Body is shown in Table 3.
3 embodiment of table, 17~24 each component and parts by weight
25~32 soluble liquid of embodiment
Emulsifier, cosolvent are uniformly mixed by high speed shear, Duraset, active constituent B is added, in ball mill
Middle ball milling 2~3 hours makes diameter of particle all at 5 μm hereinafter, surplus is supplied with solvent, can be prepared by it is of the present invention can
Dissolubility liquor product, is specifically shown in Table 4.
4 embodiment of table, 25~32 each component and parts by weight
33~40 water dispersible granules of embodiment
Duraset, active constituent B, dispersing agent, wetting agent, disintegrating agent, filler etc. are obtained through air-flow crushing together
The partial size needed adds other auxiliary agents such as binder (can add can be not added), obtains granulation materials.Item is quantified into feeding fluidisation
In bed granulating drier after granulation and drying, it can be prepared by water dispersible granules product of the present invention, be specifically shown in Table 5.
5 embodiment of table, 33~40 each component and content
41~48 aqua of embodiment
Together by Duraset, active constituent B, wetting agent, antifreeze (can add can be not added), solvent, deionized water etc.
Mixing is made the aqua product of the present composition, is specifically shown in Table 6.
6 embodiment of table, 41~48 each component and parts by weight
By quick albumen super in table 1-6, gibberellic acid, antibacterial peptide, humic acid, adjust naphthenic acid and its salt, flumetralim, to chlorobenzene oxygen second
Sour sodium exchanges, and novel formulation can be made.
The experiment of two indoor toxicity test of Application Example
One, for studying object: tomato adjusts growth
Test medicine is provided by Shaanxi Meibang Pesticide Co., Ltd..
Experimental design: Duraset and super quick albumen raw medicine and the two different ratio mixture are determined by preliminary experiment
Effective inhibition concentration range.
7 Duraset of table compounds the adjusting growth to tomato with super quick albumen
As shown in Table 7, Duraset and super quick albumen proportion have good promotion to make tomato in 1 50~80 ︰ 1 of ︰
With.Growth promotion rate is maximum when wherein Duraset and super quick protein by weight ratio are 3:1, and can promote plant growth and
Crop quality is improved, therefore, there is good application and popularization value.
Two, for studying object: wheat adjusts growth
Test medicine is provided by Shaanxi Meibang Pesticide Co., Ltd..
It is for trying object with wheat, the method for combining jointing initial stage cauline leaf spraying using wheat seed soaking measures two kinds of medicaments
And its different ratio is to the adjustment effect of wheat growth, it is wet by soil is tested with 250 × 300mm plastic tub alms bowl using pot-culture method
Degree is adjusted to being quantitatively filled at the 2/3 of basin alms bowl after 65%, is selected the uniform wheat seed of full seed, is tested according to seed soaking
Design concentration carries out seed soaking, soil surface is uniformly placed in after drying, then mulching soil thickness 2.0-3.0cm, sows
Amount is 10/basin.After planting wheat is placed in temperature, illumination and the controllable artificial climate room of humidity, it is quantitative as needed
Watering.After wheat tillering, adjustment artificial climate room temperature is 3 ± 1 DEG C and carries out artificial vernalization treatment 20d, then will be after vernalization
Wheat be transferred in the wet controllable glasshouse of warm light that (20 DEG C~30 DEG C of temperature, humidity is 60%~75%, and Light To Dark Ratio is
14:10), growing to jointing initial stage according to the cauline leaf spraying treatment concentration of experimental design carries out spraying treatment, at Duraset
Reason concentration is 4mg/L, and humic acid concentration for the treatment of is 4mg/L.With reference to plant growth regulator indoor biometrics experiment criterion (NY/T
2061.1-2011, NY/T 2061.2-2011) and Colby method.It tests and shares medicine 2 times, at the beginning of wheat seed soaking and plant jointing
Phase cauline leaf spraying treatment.Spray value is 450L/hm2.Using absolute value investigation method.40 days investigation plant heights and root after wheat emergence
It is long, 20 days investigation Plant Height in Wheat after cauline leaf spraying treatment.Inhibited with the theoretical plant height that Gowing method calculates each processing hybrid combining
Rate E0 (E0=X+Y-X*Y/100), then compared with actual measurement plant height inhibiting rate (E), both evaluations are mixed to peanut growth tune
The synergy of section.X is effective constituents A dosage in formula when being P plant height inhibiting rate, root long growth rate;Y is effective component B use
Experimental result, is now reported as follows by plant height inhibiting rate, root long growth rate when amount is Q:
8 Duraset of table compounds the toxicity test analysis of results table that growth is adjusted to wheat with humic acid
As shown in Table 8, after Duraset and humic acid are used in mixed way, can activated plant metabolic system and keep plant raw
Long quickening vigor enhancing, promotes plant cell to increase, and breaking dormancy prevents fruit drop, improves product quality, improves yield,
The disease-resistant, pest-resistant of crop, drought resisting, cold-resistant, ability resistant to lodging, Duraset and humic acid are improved in 1 50~60 ︰ 1 of ︰,
There is preferable adjustment effect to wheat root long and plant height, especially when Duraset and humic acid weight ratio are 1:1, synergy is made
With the most obvious, and stalk can be promoted strong, laid a good foundation for wheat increase yield.
Three, for studying object: rice adjusts growth
Test medicine is provided by Shaanxi Meibang Pesticide Co., Ltd..
Experimental design: having for Duraset and gibberellic acid raw medicine and the two different ratio mixture is determined by preliminary experiment
Imitate inhibition concentration range.
Duraset is compounded with gibberellic acid to rice germination synergy effect analysis table
As shown in Table 7, Duraset and gibberellic acid, which are matched, has good promotion to rice germination in 1 50~1 ︰ 60 of ︰
Effect.It evaluates its synergy with Gowing method after the two is mixed to find out, as the processing E-E that weight ratio is 1:10Value is maximum, effect
Fruit is carried out.
Four, for studying object: cucumber adjusts growth
Test medicine is provided by Shaanxi Meibang Pesticide Co., Ltd..
Experimental design: having for Duraset and antibacterial peptide raw medicine and the two different ratio mixture is determined by preliminary experiment
Imitate inhibition concentration range.Bear fruit to cucumber, increase production toxicity test.
Co-toxicity coefficient CTC is calculated according to Sun Yunpei equation.CTC < 80 is antagonism, and 80≤CTC≤120 are phase
Add effect, CTC > 120 is synergistic effect, and calculation formula is following, and (using Duraset as standard agent, toxicity index is
100):
Theoretical toxicity index (TTI)=Duraset TI × P of MDurasetTI × P of+antibacterial peptideAntibacterial peptide
In formula: M is the mixture of different ratio
PAntibacterial peptideFor antibacterial peptide shared ratio in the composition
PDurasetFor Duraset shared ratio in the composition
10 Duraset of table compounds the toxicity test analysis of results table that growth is adjusted to cucumber with antibacterial peptide
As shown in Table 10, Duraset and antibacterial peptide, which are matched, adjusts growth and yield to cucumber in 1 10~200 ︰ 1 of ︰
Co-toxicity coefficient be all larger than 120, both illustrate that mixture shows synergistic effect in 1 ︰, 10~200 ︰, 1 range, when toluene phthalein
For the proportion of propylhomoserin and antibacterial peptide in 1 5~100 ︰ 1 of ︰, synergistic effect is more prominent, especially when Duraset and antibacterial peptide
Synergy ratio is maximum when weight ratio is 60:1, and synergistic effect is the most obvious.
Three effect experiment part of Application Example
Test medicine is researched and developed by Shaanxi Meibang Pesticide Co., Ltd., is provided, 20% Duraset wettable of comparison medicament
Pulvis (autogamy), 10% super quick albumen wettable powder (autogamy), 4% gibberellic acid aqua (autogamy), 2% antibacterial peptide wettable powder
Agent (autogamy), 2% humic acid aqua (autogamy).
One, Duraset and fractions of active ingredient B and its pharmacodynamic test adjusted to peanut growth is compounded
This experiment is arranged in Shaanxi Province Pucheng County, and by the way of pouring, with full blossom latter stage, medicament is poured onto Roots of Peanut
Portion, 20 days measurement peanut plant heights before medicine and after medicine, application is primary altogether, measures peanut yield after maturation.Test result is as follows:
11 Duraset of table is compounded with fractions of active ingredient B adjusts growth test to peanut
As can be seen from Table 11, peanut growth can be effectively facilitated after Duraset is compounded with fractions of active ingredient B, to flower
Raw safety does not occur phytotoxicity, all has good facilitation to peanut plant height and yield.
Two, it Duraset and fractions of active ingredient B and its compounds and adjusts wheat growth Experiment on Function
This test arrangement is sprayed using seeding in nursery bed nursery with rice shoot four leaf stage on October 15 the 1st time in Shaanxi Province Pucheng County
Mist transplanted crop field by seedbed sequence October 31, and November 18 the 2nd time is spraying, after 2 months the 3rd time it is spraying, 10-20 days after medicine
Investigation carries out yield investigation to rape safety, height of seedling, planting percent after harvest time, test result is as follows:
12 Duraset of table is compounded with fractions of active ingredient B adjusts growth test to rape
As can be seen from Table 12, growth of rape can be effectively facilitated after Duraset is compounded with fractions of active ingredient B, to oil
Dish safety, can promote rice shoot root system to increase, and prevent high seedling, promote strong sprout, improve grain weight, increase yield.
Three, it Duraset and fractions of active ingredient B and its compounds and adjusts paddy growth Experiment on Function
This test arrangement is in Shaanxi Province's Hanzhong City, in one heart stage of one leaf of rice, carries out spraying treatment, mu water consumption to rice
It is 30kg/ mus.In investigation the early period plant height, mature spike number, mass of 1000 kernel, per mu yield, rate of growth of receiving.Test result is as follows:
13 Duraset of table is compounded with fractions of active ingredient B adjusts paddy growth Experiment on Function
As can be seen from Table 13, paddy growth can be effectively facilitated after Duraset is compounded with fractions of active ingredient B, to water
Rice volume increase is also obviously promoted effect, has preferable safety.
Four, it Duraset and fractions of active ingredient B and its compounds and adjusts cotton growth Experiment on Function
This test arrangement is in Shaanxi Province Weinan City Pucheng County, and the application of Yu Mianhua flowering stage is primary, and interval is applied for the 2nd time after 10 days
Medicine has seen whether after medicine to investigate plant height, single plant fruit branch number after phytotoxicity, last are administered 40 days, at bell number, yield for 15 days.Per acre
Water consumption 40kg, test result are as follows:
14 Duraset of table is compounded with fractions of active ingredient B adjusts cotton growth Experiment on Function
As can be seen from Table 14, Duraset and fractions of active ingredient B have fine promotion to cotton growth and yield
Effect, and to cotton safety, no phytotoxicity.
Claims (5)
1. a kind of synergistic composition containing Duraset, effective active composition is active components A and active constituent B, feature
Be: the weight ratio of active components A and active constituent B are 200 ︰, 1 ~ 1 ︰ 50, and the active components A is Duraset, living
Property ingredient B selected from super quick albumen, gibberellic acid, antibacterial peptide, humic acid, adjust naphthenic acid and its salt, Brodifacoum, in flumetralim
One kind.
2. the synergistic composition according to claim 1 containing Duraset, it is characterised in that: active constituent in composition
The weight ratio of A and active constituent B is 100 ︰, 1 ~ 1 ︰ 30.
3. the synergistic composition according to claim 2 containing Duraset, it is characterised in that:
Duraset and super quick albumen or gibberellic acid or Brodifacoum or adjust the weight ratio of naphthenic acid and its salt be 20 ︰ 1 ~
1 ︰ 5;
The weight ratio of Duraset and antibacterial peptide is 80 ︰, 1 ~ 1 ︰ 1;
The weight ratio of Duraset and humic acid or flumetralim is 5 ︰, 1 ~ 1 ︰ 20.
4. the synergistic composition according to any one of claim 1 to 3 containing Duraset, it is characterised in that: combination
Wettable powder, soluble powder, soluble granule, soluble liquid, water dispersible granules, aqua, granule is made in object.
5. the synergistic composition according to claim 4 containing Duraset is for coordinate plant growth, promotion crop hair
Bud improves fruit-setting rate, protects flower, volume increase, purposes resistant to lodging.
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Citations (1)
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CN106857514A (en) * | 2017-01-11 | 2017-06-20 | 陕西上格之路生物科学有限公司 | A kind of composition of the amino acid of peptide containing benzene and flumetralim |
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CN106857514A (en) * | 2017-01-11 | 2017-06-20 | 陕西上格之路生物科学有限公司 | A kind of composition of the amino acid of peptide containing benzene and flumetralim |
Non-Patent Citations (2)
Title |
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帖汉: "植物调节剂", 《宁夏农林科技》 * |
无: "新型植物生长调节剂――宝赢 ", 《西北园艺(果树)》 * |
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