CN109692642A - Two-in-one filter device - Google Patents
Two-in-one filter device Download PDFInfo
- Publication number
- CN109692642A CN109692642A CN201910038548.8A CN201910038548A CN109692642A CN 109692642 A CN109692642 A CN 109692642A CN 201910038548 A CN201910038548 A CN 201910038548A CN 109692642 A CN109692642 A CN 109692642A
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- CN
- China
- Prior art keywords
- fixedly connected
- kettle
- wall
- washing
- washing kettle
- Prior art date
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- Pending
Links
- 238000005406 washing Methods 0.000 claims abstract description 57
- 230000007246 mechanism Effects 0.000 claims abstract description 25
- 230000018044 dehydration Effects 0.000 claims abstract description 10
- 238000006297 dehydration reaction Methods 0.000 claims abstract description 10
- 238000010438 heat treatment Methods 0.000 claims abstract description 9
- 239000007788 liquid Substances 0.000 claims abstract description 7
- 238000006243 chemical reaction Methods 0.000 claims description 25
- 239000003381 stabilizer Substances 0.000 claims description 7
- 235000005121 Sorbus torminalis Nutrition 0.000 claims description 3
- 244000152100 Sorbus torminalis Species 0.000 claims description 3
- 239000000565 sealant Substances 0.000 claims description 3
- 230000005611 electricity Effects 0.000 claims description 2
- 238000004519 manufacturing process Methods 0.000 abstract description 13
- 238000000034 method Methods 0.000 abstract description 7
- BEARMXYKACECDH-UHFFFAOYSA-N methylsulfonylmethylbenzene Chemical compound CS(=O)(=O)CC1=CC=CC=C1 BEARMXYKACECDH-UHFFFAOYSA-N 0.000 abstract description 7
- 238000001914 filtration Methods 0.000 abstract description 3
- 238000010924 continuous production Methods 0.000 abstract description 2
- 238000003912 environmental pollution Methods 0.000 abstract description 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 14
- 239000000126 substance Substances 0.000 description 12
- 230000000694 effects Effects 0.000 description 8
- 239000002994 raw material Substances 0.000 description 8
- 239000000463 material Substances 0.000 description 5
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 4
- 238000002425 crystallisation Methods 0.000 description 4
- 230000008025 crystallization Effects 0.000 description 4
- 239000007789 gas Substances 0.000 description 4
- TYCOFFBAZNSQOJ-UHFFFAOYSA-N 2-[4-(3-fluorophenyl)phenyl]propanoic acid Chemical compound C1=CC(C(C(O)=O)C)=CC=C1C1=CC=CC(F)=C1 TYCOFFBAZNSQOJ-UHFFFAOYSA-N 0.000 description 3
- 229950001284 fluprofen Drugs 0.000 description 3
- 238000009434 installation Methods 0.000 description 3
- 239000000047 product Substances 0.000 description 3
- 238000003756 stirring Methods 0.000 description 3
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 description 2
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 2
- RAHZWNYVWXNFOC-UHFFFAOYSA-N Sulphur dioxide Chemical compound O=S=O RAHZWNYVWXNFOC-UHFFFAOYSA-N 0.000 description 2
- 230000003115 biocidal effect Effects 0.000 description 2
- 230000015572 biosynthetic process Effects 0.000 description 2
- 238000010586 diagram Methods 0.000 description 2
- GKCXXDSWWDWUHS-BYPYZUCNSA-N ethyl (2s)-2-amino-3-hydroxypropanoate Chemical compound CCOC(=O)[C@@H](N)CO GKCXXDSWWDWUHS-BYPYZUCNSA-N 0.000 description 2
- 239000003317 industrial substance Substances 0.000 description 2
- VNWKTOKETHGBQD-UHFFFAOYSA-N methane Chemical compound C VNWKTOKETHGBQD-UHFFFAOYSA-N 0.000 description 2
- 238000002156 mixing Methods 0.000 description 2
- 230000001681 protective effect Effects 0.000 description 2
- 239000007787 solid Substances 0.000 description 2
- 238000003786 synthesis reaction Methods 0.000 description 2
- OTVAEFIXJLOWRX-NXEZZACHSA-N thiamphenicol Chemical compound CS(=O)(=O)C1=CC=C([C@@H](O)[C@@H](CO)NC(=O)C(Cl)Cl)C=C1 OTVAEFIXJLOWRX-NXEZZACHSA-N 0.000 description 2
- 229960003053 thiamphenicol Drugs 0.000 description 2
- 241000894006 Bacteria Species 0.000 description 1
- OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 description 1
- ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical compound [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 description 1
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 1
- ISWSIDIOOBJBQZ-UHFFFAOYSA-N Phenol Chemical compound OC1=CC=CC=C1 ISWSIDIOOBJBQZ-UHFFFAOYSA-N 0.000 description 1
- OAICVXFJPJFONN-UHFFFAOYSA-N Phosphorus Chemical compound [P] OAICVXFJPJFONN-UHFFFAOYSA-N 0.000 description 1
- ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 description 1
- 238000003723 Smelting Methods 0.000 description 1
- 229910000831 Steel Inorganic materials 0.000 description 1
- NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical group [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 description 1
- 150000001298 alcohols Chemical class 0.000 description 1
- 150000001299 aldehydes Chemical class 0.000 description 1
- -1 alkane hydrocarbons Chemical class 0.000 description 1
- 150000001336 alkenes Chemical class 0.000 description 1
- 150000001345 alkine derivatives Chemical class 0.000 description 1
- 229910021529 ammonia Inorganic materials 0.000 description 1
- BFNBIHQBYMNNAN-UHFFFAOYSA-N ammonium sulfate Chemical compound N.N.OS(O)(=O)=O BFNBIHQBYMNNAN-UHFFFAOYSA-N 0.000 description 1
- 229910052921 ammonium sulfate Inorganic materials 0.000 description 1
- 235000011130 ammonium sulphate Nutrition 0.000 description 1
- 150000008064 anhydrides Chemical class 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 239000006227 byproduct Substances 0.000 description 1
- 239000011575 calcium Substances 0.000 description 1
- 229910052791 calcium Inorganic materials 0.000 description 1
- 150000001720 carbohydrates Chemical class 0.000 description 1
- 150000007942 carboxylates Chemical class 0.000 description 1
- 239000003183 carcinogenic agent Substances 0.000 description 1
- 238000005119 centrifugation Methods 0.000 description 1
- DVRDHUBQLOKMHZ-UHFFFAOYSA-N chalcopyrite Chemical compound [S-2].[S-2].[Fe+2].[Cu+2] DVRDHUBQLOKMHZ-UHFFFAOYSA-N 0.000 description 1
- 229910052951 chalcopyrite Inorganic materials 0.000 description 1
- 239000000460 chlorine Substances 0.000 description 1
- 229910052801 chlorine Inorganic materials 0.000 description 1
- 238000004140 cleaning Methods 0.000 description 1
- 239000003245 coal Substances 0.000 description 1
- 238000004939 coking Methods 0.000 description 1
- 229940079593 drug Drugs 0.000 description 1
- 239000003814 drug Substances 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 150000002148 esters Chemical class 0.000 description 1
- 150000002170 ethers Chemical class 0.000 description 1
- 229910052949 galena Inorganic materials 0.000 description 1
- 125000000623 heterocyclic group Chemical group 0.000 description 1
- 229930195733 hydrocarbon Natural products 0.000 description 1
- 229910052500 inorganic mineral Inorganic materials 0.000 description 1
- 229910017053 inorganic salt Inorganic materials 0.000 description 1
- 229910052742 iron Inorganic materials 0.000 description 1
- 150000002576 ketones Chemical class 0.000 description 1
- 239000010410 layer Substances 0.000 description 1
- XCAUINMIESBTBL-UHFFFAOYSA-N lead(ii) sulfide Chemical compound [Pb]=S XCAUINMIESBTBL-UHFFFAOYSA-N 0.000 description 1
- 239000011707 mineral Substances 0.000 description 1
- 239000003345 natural gas Substances 0.000 description 1
- 150000002825 nitriles Chemical class 0.000 description 1
- JRZJOMJEPLMPRA-UHFFFAOYSA-N olefin Natural products CCCCCCCC=C JRZJOMJEPLMPRA-UHFFFAOYSA-N 0.000 description 1
- 150000007524 organic acids Chemical class 0.000 description 1
- 239000012044 organic layer Substances 0.000 description 1
- 239000003208 petroleum Substances 0.000 description 1
- 239000011574 phosphorus Substances 0.000 description 1
- 229910052698 phosphorus Inorganic materials 0.000 description 1
- 239000011591 potassium Substances 0.000 description 1
- 229910052700 potassium Inorganic materials 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 150000004053 quinones Chemical class 0.000 description 1
- 238000007789 sealing Methods 0.000 description 1
- 239000011734 sodium Substances 0.000 description 1
- 229910052708 sodium Inorganic materials 0.000 description 1
- 239000010959 steel Substances 0.000 description 1
- 238000003860 storage Methods 0.000 description 1
- 238000006467 substitution reaction Methods 0.000 description 1
- WGPCGCOKHWGKJJ-UHFFFAOYSA-N sulfanylidenezinc Chemical compound [Zn]=S WGPCGCOKHWGKJJ-UHFFFAOYSA-N 0.000 description 1
- 239000011593 sulfur Substances 0.000 description 1
- 229910052717 sulfur Inorganic materials 0.000 description 1
- 230000001360 synchronised effect Effects 0.000 description 1
- 239000002699 waste material Substances 0.000 description 1
- 229910052984 zinc sulfide Inorganic materials 0.000 description 1
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/18—Stationary reactors having moving elements inside
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D29/00—Filters with filtering elements stationary during filtration, e.g. pressure or suction filters, not covered by groups B01D24/00 - B01D27/00; Filtering elements therefor
- B01D29/01—Filters with filtering elements stationary during filtration, e.g. pressure or suction filters, not covered by groups B01D24/00 - B01D27/00; Filtering elements therefor with flat filtering elements
- B01D29/03—Filters with filtering elements stationary during filtration, e.g. pressure or suction filters, not covered by groups B01D24/00 - B01D27/00; Filtering elements therefor with flat filtering elements self-supporting
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D35/00—Filtering devices having features not specifically covered by groups B01D24/00 - B01D33/00, or for applications not specifically covered by groups B01D24/00 - B01D33/00; Auxiliary devices for filtration; Filter housing constructions
- B01D35/02—Filters adapted for location in special places, e.g. pipe-lines, pumps, stop-cocks
- B01D35/027—Filters adapted for location in special places, e.g. pipe-lines, pumps, stop-cocks rigidly mounted in or on tanks or reservoirs
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D9/00—Crystallisation
- B01D9/004—Fractional crystallisation; Fractionating or rectifying columns
- B01D9/0045—Washing of crystals, e.g. in wash columns
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D9/00—Crystallisation
- B01D9/0059—General arrangements of crystallisation plant, e.g. flow sheets
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F33/00—Other mixers; Mixing plants; Combinations of mixers
- B01F33/80—Mixing plants; Combinations of mixers
- B01F33/82—Combinations of dissimilar mixers
- B01F33/821—Combinations of dissimilar mixers with consecutive receptacles
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/0053—Details of the reactor
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/0053—Details of the reactor
- B01J19/0066—Stirrers
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/28—Moving reactors, e.g. rotary drums
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J4/00—Feed or outlet devices; Feed or outlet control devices
- B01J4/001—Feed or outlet devices as such, e.g. feeding tubes
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C315/00—Preparation of sulfones; Preparation of sulfoxides
- C07C315/06—Separation; Purification; Stabilisation; Use of additives
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D9/00—Crystallisation
- B01D2009/0086—Processes or apparatus therefor
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Chemistry (AREA)
- Crystallography & Structural Chemistry (AREA)
- Filtration Of Liquid (AREA)
Abstract
The invention discloses two-in-one filter devices, including washing kettle, the lower end of the washing kettle is fixedly connected with the support base of multiple axial spaced sets, the lower end of the washing kettle is equipped with liquid outlet, the interior bottom of the washing kettle is fixedly connected with the support rod of axial spaced set, the upper end of multiple support rods is fixedly connected with fixed plate jointly, the fixed plate is equipped with washing dehydration mechanism, the inner wall of the washing kettle is fixedly connected with that there are two the heating plates that are oppositely arranged, the inner wall of the washing kettle is fixedly connected with temperature inductor, the side wall of the washing kettle is fixedly connected with temperature indicator.Structure of the invention design is reasonable, due to being completely closed the production of filtering, No leakage, it in this way can be to avoid the harm occurred to human body and environment to the industrialized preparing process of methylsulfonyltoluene, without any environmental pollution, and continuous production may be implemented, improve the efficiency of production, in order to be able to be satisfied with the production requirement of enterprise.
Description
Technical field
The present invention relates to the production equipment technology of organic chemical industry more particularly to two-in-one filter devices.
Background technique
There are many industrial chemicals type, have many uses.Chemicals has as many as 500~7,000,000 kinds in the whole world, goes out on the market
Sell circulation more than 100,000 kinds, and it is annual there are also more than 1000 kinds of new chemicals to come out, and wherein have 150~200 kinds of quilts
It is considered carcinogenic substance.Industrial chemicals can be generally divided into Organic Chemicals and Inorganic Chemicals two major classes.Organic chemical industry is former
Material: alkane hydrocarbons and their derivates, olefin and its derivatives, alkynes and derivative, quinones, aldehydes, alcohols, ketone, phenol can be divided into
Class, ethers, anhydride, esters, organic acid, carboxylate, carbohydrate, heterocyclic, nitrile, halogenated class, amine acyl class, other kinds
Class；Inorganic Chemicals: the primary raw material of inorganic chemical product is the minerals commonly used in chemical industry such as sulfur-bearing, sodium, phosphorus, potassium, calcium (see inorganic salt worker
Industry) and coal, petroleum, natural gas and empty gas and water etc..In addition, the by-product and waste and inorganic chemical industry of many industrial departments
Raw material, such as: the coke-stove gas of coking production process in steel and iron industry, ammonia contained therein can be recycled with sulfuric acid and is made
Ammonium sulfate, chalcopyrite, galena, zincblende smelting exhaust gas in sulfur dioxide can be used to produce sulfuric acid etc.
Wherein, Organic Chemicals is the primary raw material for producing D-4-methylsulfonylphserine serine ethyl ester to methylsulfonyltoluene, and
D-4-methylsulfonylphserine serine ethyl ester is the primary raw material for producing Thiamphenicol, Fluprofen again.Fluprofen and Thiamphenicol are countries
Two kind new medicines and state key encourage the product of development.Fluprofen is the broad spectrum activity that company, the U.S. shilling develops
Veterinary antibiotic is widely used in and kills various " gram " yin and yang attribute bacterium, is currently one of antibiotic best in the world, is chlorine
The replacement of mycin.
Currently, the existing process units to methylsulfonyltoluene is usually all using intermittent reaction equipment, in production
Can not persistently be produced and processed in the process, it is lower so as to cause the production efficiency to methylsulfonyltoluene, simultaneously cannot be automatic
Change is produced, and causes the large labor intensity of staff, and to the production of methylsulfonyltoluene for environment pollution also compared with
Greatly, so that the production requirement of enterprise cannot be satisfied with.
Summary of the invention
The purpose of the present invention is to solve disadvantages existing in the prior art, and the two-in-one filter device proposed,
It, in this way can be to avoid hair to the industrialized preparing process of methylsulfonyltoluene due to being completely closed the production of filtering, No leakage
The raw harm to human body and environment, without any environmental pollution, and may be implemented continuous production, improves the efficiency of production, so as to
In can satisfy the production requirement in enterprise.
To achieve the goals above, present invention employs following technical solutions:
Two-in-one filter device, including washing kettle, the lower end of the washing kettle are fixedly connected with multiple axial spaced sets
Support base, the lower end of the washing kettle is equipped with liquid outlet, and the interior bottom of the washing kettle, which is fixedly connected with, axial equidistantly to be set
The support rod set, the upper end of multiple support rods are fixedly connected with fixed plate jointly, and the fixed plate is equipped with washing dehydration
Mechanism, the inner wall of the washing kettle are fixedly connected there are two the heating plate being oppositely arranged, and the inner wall of the washing kettle is fixedly connected
There is temperature inductor, the side wall of the washing kettle is fixedly connected with temperature indicator, the temperature inductor and temperature indicator
Electrical connection, the inner wall of the washing kettle are fixedly connected with annulus, and the lower end of the annulus is equipped with circular groove, and the annulus passes through two
Fixed mechanism is fixedly connected with the screen pack being arranged in circular groove, and the upper end of the washing kettle is fixedly connected between multiple axial directions etc.
Stabilizer blade away from setting, the lower end of multiple stabilizer blades are fixedly connected with reaction kettle jointly, and the upper end of the washing kettle is connected with
Adapter tube, the other end of the connecting tube are connected to the lower end of reaction kettle, and the valve of control switch is equipped in the connecting tube, described
The upper end of reaction kettle is fixedly connected with 7 shape plates, and the upper end of the 7 shape plate is fixedly connected with first motor, sets in the reaction kettle
There is rabbling mechanism, the output shaft end of the first motor runs through the upper end of 7 shape plates and connect with rabbling mechanism, first electricity
The output shaft of machine and 7 shape plates are rotatablely connected.
Preferably, the lower end of multiple support bases is provided with anti-skid chequer.
Preferably, the washing dehydration mechanism includes the second motor for being fixedly connected on fixed plate lower end, the fixed plate
Lower end be fixedly connected with the shield for protecting the second motor, second motor is located at the inside of shield, described solid
The upper end of fixed board is rotatably connected to cylinder, and the output shaft end of second motor runs through the lower end of fixed plate and is fixedly connected on
The lower end of cylinder, the output shaft and fixed plate of second motor are rotatablely connected, and the inner wall of the cylinder is embedded to be equipped with filtering
Net, the inner wall of the cylinder are fixedly connected with multiple agitating plates.
Preferably, the inner wall of the washing kettle is fixedly connected with deflector, and the deflector is located at lower section and the cylinder of annulus
Between the top of body.
Preferably, the fixed mechanism includes the cylindrical cavity being arranged in annulus, and the inner wall of the cylindrical cavity slidably connects cunning
Plate, the side wall of the slide plate are fixedly connected with bolt, and one end of the bolt is run through the inner wall of cylindrical cavity and extended in circular groove, institute
It states bolt to be slidably connected with annulus, the side wall of the screen pack is equipped with the jack matched with bolt, the lower end of the slide plate
It is fixedly connected with pull rod, the lower end of the pull rod runs through the interior bottom of cylindrical cavity and extends to outside, and the pull rod and annulus slide
Connection, the cylindrical cavity is interior to be equipped with spring, and the both ends of the spring are respectively fixedly connected on the side wall of slide plate and the inner wall of cylindrical cavity.
Preferably, the first motor is equipped with protective shell.
Preferably, the rabbling mechanism includes through two agitating shafts that reaction kettle upper end is arranged in, two stirrings
Axis is rotatablely connected with reaction kettle, is equidistantly fixedly connected with multiple paddles on two agitating shafts, is stirred described in two
The upper end for mixing axis has been respectively fixedly connected with driving wheel and driven wheel, and the driving wheel is rotatablely connected driven wheel by belt, described
The output shaft end of first motor is fixedly connected on the upper end of driving wheel.
Preferably, the connecting tube is sealed processing by sealant with washing kettle and reaction kettle junction.
Beneficial effects of the present invention:
It 1, can by first motor since driving wheel is rotatablely connected with driven wheel by belt by setting rabbling mechanism
To realize that two agitating shafts synchronize rotation, so that the paddle on two agitating shafts be made to be rotated, in order to be able to fill
That divides is mixed raw material；
2, by setting fixed mechanism, bolt can be pulled out in jack manually by pull rod, realized to screen pack
Disassembly can push slide plate to be resetted, so that bolt be made to be inserted into jack in order to be cleaned using the elastic force effect of spring
The installation of screen pack is fixed in interior realization；
3, by setting washing dehydration mechanism, barrel body rotation is driven by the second motor, it can be right using agitating plate rotation
Warm water is stirred, and is adequately washed to organic liquor, generates centrifugation using barrel body rotation so as to take off to crystallization
Water process.
Detailed description of the invention
Fig. 1 is the structural schematic diagram of two-in-one filter device proposed by the present invention；
Fig. 2 is the partial enlarged view in Fig. 1 of the present invention at A；
Fig. 3 is the partial enlarged view in Fig. 1 of the present invention at B；
Fig. 4 is the positive structure diagram of two-in-one filter device proposed by the present invention.
In figure: 17 shape plates, 2 first motors, 3 reaction kettles, 4 agitating shafts, 5 paddles, 6 stabilizer blades, 7 valves, 8 washing kettles, 9 are led
Flowing plate, 10 heating plates, 11 support bases, 12 liquid outlets, 13 support rods, 14 shields, 15 second motors, 16 fixed plates, 17 cylinders,
It is 18 filter screens, 19 agitating plates, 20 temperature inductors, 21 temperature indicators, 22 connecting tubes, 23 driving wheels, 24 belts, 25 driven
Wheel, 26 springs, 27 slide plates, 28 pull rods, 29 cylindrical cavities, 30 bolts, 31 jacks, 32 screen packs, 33 annulus.
Specific embodiment
Following will be combined with the drawings in the embodiments of the present invention, and technical solution in the embodiment of the present invention carries out clear, complete
Site preparation description, it is clear that described embodiments are only a part of the embodiments of the present invention, instead of all the embodiments.
Referring to Fig.1-4, two-in-one filter device, including washing kettle 8, the lower end of washing kettle 8 are fixedly connected with multiple axial directions etc.
The support base 11 (preferably four) of spacing setting, the lower end of multiple support bases 11 is provided with anti-skid chequer, plays anti-skidding
Effect, the lower end of washing kettle 8 are equipped with liquid outlet 12, are equipped with control switch in liquid storage mouth 12, control the discharge of water, washing kettle 8
Interior bottom is fixedly connected with the support rod 13 of axial spaced set, and the upper end of multiple support rods 13 is fixedly connected with fixation jointly
Plate 16, fixed plate 16 are equipped with washing dehydration mechanism, and the inner wall of washing kettle 8 is fixedly connected with that there are two the heating plates that are oppositely arranged
10, heating plate 10 is the 7 shape plate of arc matched with 8 inner wall of washing kettle, and for the heating of water, the inner wall of washing kettle 8 is fixedly connected
There is temperature inductor 20, the side wall of washing kettle 8 is fixedly connected with temperature indicator 21, temperature inductor 20 and temperature indicator 21
Electrical connection, can observe the temperature of water in washing kettle 8, the inner wall of washing kettle 8 is fixedly connected with annulus 33, and the lower end of annulus 33 is set
There is circular groove, annulus 33 is fixedly connected with the screen pack 32 being arranged in circular groove by two fixed mechanisms, and the inner wall of washing kettle 8 is solid
Surely it is connected with deflector 9, deflector 9 is cone, plays the role of water conservancy diversion, deflector 9 is located at lower section and the cylinder of annulus 33
Between 17 top, the upper end of washing kettle 8 is fixedly connected with the stabilizer blade 6 of multiple axial spaced sets, the lower end of multiple stabilizer blades 6
It is fixedly connected with reaction kettle 3 jointly, the upper end of washing kettle 8 is connected with connecting tube 22, and the other end of connecting tube 22 is connected to reaction
The lower end of kettle 3, connecting tube 22 are sealed processing by sealant with washing kettle 8 and 3 junction of reaction kettle, play sealing
Effect avoids gas from leaking, and the valve 7 of control switch is equipped in connecting tube 22, the upper end of reaction kettle 3 is fixedly connected with 7 shape plates
The upper end of 1,7 shape plate 1 is fixedly connected with first motor 2, and first motor 2 is equipped with protective shell, for protecting first motor 2, instead
It answers and is equipped with rabbling mechanism in kettle 3, the output shaft end of first motor 2 runs through the upper end of 7 shape plates 1 and connect with rabbling mechanism, the
The output shaft of one motor 2 and 7 shape plates 1 are rotatablely connected.
Specifically, washing dehydration mechanism includes the second motor 15 for being fixedly connected on 16 lower end of fixed plate, fixed plate 16
Lower end is fixedly connected with the shield 14 for protecting the second motor 15, play the role of protect the second motor 15, have compared with
Waterproof well, heat-resisting performance, the second motor 15 are located at the inside of shield 14, and the upper end of fixed plate 16 is rotatably connected to cylinder
17, the output shaft end of the second motor 15 runs through the lower end of fixed plate 16 and is fixedly connected on the lower end of cylinder 17, the second motor
15 output shaft and fixed plate 16 is rotatablely connected, and the inner wall of cylinder 17 is embedded to be equipped with filter screen 18, is turned at a high speed using cylinder 17
Movable property gives birth to centrifugal force, can carry out centrifugal dehydration to crystallization, in order to make it quickly dry completion processing, cylinder 17
Inner wall is fixedly connected with multiple agitating plates 19, can play the effect of stirring, to warm water in order to adequately be washed.
Specifically, fixed mechanism includes the cylindrical cavity 29 being arranged in annulus 33, and the inner wall of cylindrical cavity 29 slidably connects slide plate
27, the side wall of slide plate 27 is fixedly connected with bolt 30, and one end of bolt 30 is run through the inner wall of cylindrical cavity 29 and extended in circular groove, inserts
Pin 30 is slidably connected with annulus 33, and the side wall of screen pack 32 is equipped with the jack 31 matched with bolt 30, right for bolt 30
The installation of screen pack 32 is fixed, and the lower end of slide plate 27 is fixedly connected with pull rod 28, for bolt 30 to be pulled out jack 31 manually
It is interior, realize the effect of disassembly, the lower end of pull rod 28 runs through the interior bottom of cylindrical cavity 29 and extends to outside, and pull rod 28 and annulus 33 are sliding
Dynamic connection, cylindrical cavity 29 is interior to be equipped with spring 26, and the both ends of spring 26 are respectively fixedly connected in the side wall and cylindrical cavity 29 of slide plate 27
On wall, slide plate 26 can be pushed to be resetted using the elastic force effect of spring 26, be realized in order to which bolt 30 is inserted into jack 30
It is fixed.
Specifically, rabbling mechanism include through being arranged in two agitating shafts 4 of 3 upper end of reaction kettle, two agitating shafts 4 with
Reaction kettle 3 is rotatablely connected, and is equidistantly fixedly connected with multiple paddles 5, the upper end of two agitating shafts 4 on two agitating shafts 4
It is respectively fixedly connected with driving wheel 23 and driven wheel 25, driving wheel 23 is rotatablely connected driven wheel 25, first motor 2 by belt 24
Output shaft end be fixedly connected on the upper end of driving wheel 23, such structure may be implemented two agitating shafts 4 and synchronize to turn
It is dynamic, so that the paddle on two agitating shafts 4 be made to be rotated, in order to be able to adequately raw material be mixed.
In the present invention, when work, the raw material of a variety of synthetic reactions is put into reaction kettle 3, first motor is then started
2, the output shaft rotation of first motor 2 drives driving wheel 23 to rotate, since driving wheel 23 is rotated with driven wheel 25 by belt 24
Connection, so as to which so that two agitating shafts 4 synchronize rotation, two synchronous rotations of agitating shaft 4 rotate paddle 5,
So as to be stirred to plurality of raw materials, it can be adequately stirred mixing, then control temperature in the kettle 70~80
DEG C, 0.2~1MPa of pressure in kettle after synthesis to be processed, opens valve 7, flows into the material after synthesis by connecting tube 22 and washes
It washs in kettle 8, when material is fallen, material is filtered by screen pack 32, so that the organic layer on material upper layer be separated
Out, the organic liquor after then separating falls into the bottom in cylinder 17 by deflector 9, then opens the switch of heating plate 10,
It is heated by heating plate 10 and is promoted the temperature of water in washing kettle 8 to 60 DEG C of warm water below, pass through temperature indicator 21
The temperature change of 8 water temperature inside of washing kettle can be observed in outside, in order to preferably control water temperature, then starts the
Two motors 15, the second motor 15 output shaft rotation drive cylinder 17 rotate, cylinder 17 rotation by agitating plate 19 to warm water into
Row stirring, adequately washs progress to organic liquor so as to realize, then organic liquor reaction is opened out after crystallization at crystallization
The switch of liquid mouth 12, so as to which the warm water of washing kettle 8 to be discharged, since the second motor 15 continues to rotate, so as to knot
Crystalline substance carries out centrifugal dehydration, and the drying allowed to as soon as possible is got off, finally obtained to methylsulfonyltoluene product, can carried out with serialization
Production；When needing to dismantle screen pack 32, slide plate 27 is pulled to be displaced outwardly by pull rod 28, slide plate 27 is displaced outwardly
It skids off bolt 30 in jack 31, so as to carry out disassembly, cleaning to it, when seated, screen pack 32 is placed on circular groove
Interior, then releasing lever 28, push slide plate 27 to reset, so that bolt 30 is inserted into jack 31 using the elastic force effect of spring 26
The installation of screen pack 32 is fixed in realization, is used in order to filter.
More than, it is merely preferred embodiments of the present invention, but scope of protection of the present invention is not limited thereto, it is any
Those familiar with the art in the technical scope disclosed by the present invention, according to the technique and scheme of the present invention and its invents
Design is subject to equivalent substitution or change, should be covered by the protection scope of the present invention.
Claims (8)
1. two-in-one filter device, including washing kettle (8), which is characterized in that the lower end of the washing kettle (8) is fixedly connected multiple
The lower end of the support base (11) of axial spaced set, the washing kettle (8) is equipped with liquid outlet (12), the washing kettle (8)
Interior bottom is fixedly connected with the support rod (13) of axial spaced set, and the upper end of multiple support rods (13) is jointly fixed to be connected
It is connected to fixed plate (16), the fixed plate (16) is equipped with washing dehydration mechanism, and the inner wall of the washing kettle (8) is fixedly connected with
Two heating plates (10) being oppositely arranged, the inner wall of the washing kettle (8) are fixedly connected with temperature inductor (20), the washing
The side wall of kettle (8) is fixedly connected with temperature indicator (21), and the temperature inductor (20) is electrically connected with temperature indicator (21),
The inner wall of the washing kettle (8) is fixedly connected with annulus (33), and the lower end of the annulus (33) is equipped with circular groove, the annulus (33)
It is fixedly connected the screen pack being arranged in circular groove (32) by two fixed mechanisms, the upper end of the washing kettle (8) is fixed to be connected
It is connected to the stabilizer blade (6) of multiple axial spaced sets, the lower end of multiple stabilizer blades (6) is fixedly connected with reaction kettle (3) jointly,
The upper end of the washing kettle (8) is connected with connecting tube (22), and the other end of the connecting tube (22) is connected under reaction kettle (3)
End, the interior valve (7) for being equipped with control switch of the connecting tube (22), the upper end of the reaction kettle (3) is fixedly connected with 7 shape plates
(1), the upper end of the 7 shape plate (1) is fixedly connected with first motor (2), and rabbling mechanism is equipped in the reaction kettle (3), described
The output shaft end of first motor (2) through 7 shape plates (1) upper end and connect with rabbling mechanism, the first motor (2) it is defeated
Shaft and 7 shape plates (1) are rotatablely connected.
2. two-in-one filter device according to claim 1, which is characterized in that the lower end of multiple support bases (11) is set
It is equipped with anti-skid chequer.
3. two-in-one filter device according to claim 1, which is characterized in that the washing dehydration mechanism includes fixed connects
The second motor (15) in fixed plate (16) lower end is connect, the lower end of the fixed plate (16) is fixedly connected with for protecting the second electricity
The shield (14) of machine (15), second motor (15) are located at the inside of shield (14), the upper end of the fixed plate (16)
It is rotatably connected to cylinder (17), the output shaft end of second motor (15) runs through the lower end of fixed plate (16) and is fixedly connected
In the lower end of cylinder (17), the output shaft of second motor (15) and fixed plate (16) are rotatablely connected, the cylinder (17)
Inner wall is embedded to be equipped with filter screen (18), and the inner wall of the cylinder (17) is fixedly connected with multiple agitating plates (19).
4. two-in-one filter device according to claim 3, which is characterized in that the inner wall of the washing kettle (8) is fixed to be connected
It is connected to deflector (9), the deflector (9) is located between the lower section of annulus (33) and the top of cylinder (17).
5. two-in-one filter device according to claim 1, which is characterized in that the fixed mechanism includes being arranged in annulus
(33) inner wall of the cylindrical cavity (29) in, the cylindrical cavity (29) slidably connects slide plate (27), and the side wall of the slide plate (27) is fixed
It is connected with bolt (30), one end of the bolt (30) is run through the inner wall of cylindrical cavity (29) and extended in circular groove, the bolt
(30) it being slidably connected with annulus (33), the side wall of the screen pack (32) is equipped with the jack (31) matched with bolt (30),
The lower end of the slide plate (27) is fixedly connected with pull rod (28), and the interior bottom of cylindrical cavity (29) is run through simultaneously in the lower end of the pull rod (28)
Outside is extended to, the pull rod (28) is slidably connected with annulus (33), is equipped with spring (26) in the cylindrical cavity (29), the spring
(26) both ends are respectively fixedly connected on the side wall of slide plate (27) and the inner wall of cylindrical cavity (29).
6. two-in-one filter device according to claim 1, which is characterized in that the first motor (2) is equipped with protection
Shell.
7. two-in-one filter device according to claim 1, which is characterized in that the rabbling mechanism includes existing through setting
Two agitating shafts (4) of reaction kettle (3) upper end, two agitating shafts (4) are rotatablely connected with reaction kettle (3), described in two
It is equidistantly fixedly connected on agitating shaft (4) multiple paddles (5), the upper end of two agitating shafts (4) is fixed respectively to be connected
It is connected to driving wheel (23) and driven wheel (25), the driving wheel (23) is described by belt (24) rotation connection driven wheel (25)
The output shaft end of first motor (2) is fixedly connected on the upper end of driving wheel (23).
8. two-in-one filter device according to claim 1, which is characterized in that the connecting tube (22) and washing kettle (8)
Processing is sealed by sealant with reaction kettle (3) junction.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201910038548.8A CN109692642A (en) | 2019-01-16 | 2019-01-16 | Two-in-one filter device |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201910038548.8A CN109692642A (en) | 2019-01-16 | 2019-01-16 | Two-in-one filter device |
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| CN109692642A true CN109692642A (en) | 2019-04-30 |
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| Application Number | Title | Priority Date | Filing Date |
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| CN201910038548.8A Pending CN109692642A (en) | 2019-01-16 | 2019-01-16 | Two-in-one filter device |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN110354786A (en) * | 2019-07-31 | 2019-10-22 | 北京鼎翰科技有限公司 | A kind of water treatment agent process units with organic exhaust gas detection function |
| CN111013493A (en) * | 2019-12-28 | 2020-04-17 | 萧县新秀新材料有限公司 | Pipeline reaction system and method for preparing light stabilizer |
| CN111939643A (en) * | 2020-09-21 | 2020-11-17 | 河南弘康环保科技有限公司 | Ultra-clean production system for automobile urea solution |
| CN114534300A (en) * | 2022-02-14 | 2022-05-27 | 安徽晨翔瑞达机械有限公司 | Multifunctional crystallizing tank |
| CN114733227A (en) * | 2022-04-20 | 2022-07-12 | 河南精康制药有限公司 | Device and method for recycling troxerutin crystallization mother liquor |
| CN115301178A (en) * | 2022-09-09 | 2022-11-08 | 新疆农业科学院农业质量标准与检测技术研究所 | Preparation facilities of chrysanthemum ester class magnetic molecular imprinting material |
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| CN110354786A (en) * | 2019-07-31 | 2019-10-22 | 北京鼎翰科技有限公司 | A kind of water treatment agent process units with organic exhaust gas detection function |
| CN111013493A (en) * | 2019-12-28 | 2020-04-17 | 萧县新秀新材料有限公司 | Pipeline reaction system and method for preparing light stabilizer |
| CN111939643A (en) * | 2020-09-21 | 2020-11-17 | 河南弘康环保科技有限公司 | Ultra-clean production system for automobile urea solution |
| CN114534300A (en) * | 2022-02-14 | 2022-05-27 | 安徽晨翔瑞达机械有限公司 | Multifunctional crystallizing tank |
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| CN114733227A (en) * | 2022-04-20 | 2022-07-12 | 河南精康制药有限公司 | Device and method for recycling troxerutin crystallization mother liquor |
| CN114733227B (en) * | 2022-04-20 | 2024-03-12 | 河南精康制药有限公司 | Recycling device and method for troxerutin crystallization mother liquor |
| CN115301178A (en) * | 2022-09-09 | 2022-11-08 | 新疆农业科学院农业质量标准与检测技术研究所 | Preparation facilities of chrysanthemum ester class magnetic molecular imprinting material |
| CN115301178B (en) * | 2022-09-09 | 2024-02-06 | 新疆农业科学院农业质量标准与检测技术研究所 | Preparation facilities of pyrethroid magnetism molecularly imprinted material |
| CN115888614A (en) * | 2023-01-09 | 2023-04-04 | 利安隆（天津）制药有限公司 | Vitamin K2 crude dissolves separation purification integrative production module |
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Application publication date: 20190430 |