CN109645194A - 能改善喷雾干燥粘壁的复合果糖粉组合物及喷雾干燥方法 - Google Patents
能改善喷雾干燥粘壁的复合果糖粉组合物及喷雾干燥方法 Download PDFInfo
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- A23G3/36—Sweetmeats, confectionery or marzipan; Processes for the preparation thereof characterised by the composition containing organic or inorganic compounds
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- A23G3/00—Sweetmeats; Confectionery; Marzipan; Coated or filled products
- A23G3/34—Sweetmeats, confectionery or marzipan; Processes for the preparation thereof
- A23G3/36—Sweetmeats, confectionery or marzipan; Processes for the preparation thereof characterised by the composition containing organic or inorganic compounds
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23G—COCOA; COCOA PRODUCTS, e.g. CHOCOLATE; SUBSTITUTES FOR COCOA OR COCOA PRODUCTS; CONFECTIONERY; CHEWING GUM; ICE-CREAM; PREPARATION THEREOF
- A23G3/00—Sweetmeats; Confectionery; Marzipan; Coated or filled products
- A23G3/34—Sweetmeats, confectionery or marzipan; Processes for the preparation thereof
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Abstract
本发明涉及一种能改善喷雾干燥粘壁的复合果糖粉组合物及喷雾干燥方法,属于复合果糖粉喷雾干燥技术领域。所述复合果糖粉组合物是由如下重量份的原料和辅料组成的:原料:F55液态果糖100份,水200份,麦芽糊精20份,蔗糖14份;辅料:微晶纤维素3‑10份,氯化钙3‑8份,二氧化硅5‑15份。优点是:辅料组合物可以增加混悬液的流动性、提高物料的软化点,增强混悬液的雾化效果,通过多种辅料组合使用,发挥各自优势,从不同角度发挥防粘壁作用。可显著提高复合果糖液喷雾干燥粉末得率,改善喷雾干燥过程中的粉料粘壁问题,提高了产品质量和粉末收率,通过对比具体实验结果可知,使用本发明技术,可明显提高粉末平均收率88.6%,具有显著的经济效益。
Description
技术领域
本发明属于复合果糖粉喷雾干燥技术领域,尤其是一种改善复合果糖液喷雾干燥粘壁的方法以及辅料组成物。
背景技术
果糖是葡萄糖的异构体,是人们所熟悉的一种糖,其主要成分和性质接近于天然果汁,具有水果清香;在味感方面,味觉甜度比蔗糖浓,且具有清凉感。可作为上等营养型甜味剂使用,近几十年来,果糖的使用量增长了十几个百分点,在甜味剂使用上占有很大的市场,具有很广阔的应用空间。
液态果糖产品包装麻烦,对包装要求高;采用真空负压灌装是比较理想的,但设备投资大。包装材料昂贵,同时运输也不方便,在运输过程中容易出现漏液、包装物变形等问题。作为功能性食品配料添加到别的产品中往往要受产品状态的影响,颗粒类、粉剂类产品,要添加液体果糖,一般要求对生产工艺进行调整,若添加量少则达不到相应效果。相反,果糖的粉状产品可直接按需求量添加到粉剂、液体、颗粒等产品中,应用十分方便。
复合果糖粉是以液态果糖、麦芽糊精、蔗糖为原料配置成的混悬液,是一种可代替蔗糖应用于食品行业的新型糖粉。
喷雾干燥是近百年发展起来并得到广泛应用的一种新型高效干燥工艺,它是采用雾化器将原料液分散为雾滴,并用热空气干燥雾滴而获得产品的一种干燥方法。但在喷雾干燥过程中,由于原材料性质原因容易出现粉料粘壁的现象,尤其是糖分多的液态果糖、麦芽糊精、蔗糖混合的混悬液。
现有技术中有报道用可溶性淀粉和糊精或轻质氧化镁的方式解决高糖分物料喷雾干燥粘壁的问题,但可溶性淀粉、糊精或轻质氧化镁的组合,仍不能改善液态果糖喷雾干燥的粘壁问题。
发明内容
本发明提供一种能改善喷雾干燥粘壁的复合果糖粉组合物及喷雾干燥方法,以解决复合果糖液喷雾干燥粉末得率低,和喷雾干燥过程中粉料粘壁的问题。
本发明采取的技术方案是,所述复合果糖粉组合物是由如下重量份的原料和辅料组成的:
原料:F55液态果糖100份,水200份,麦芽糊精20份,蔗糖14份;
辅料:微晶纤维素3-10份,氯化钙3-8份,二氧化硅5-15份。
本发明所述辅料:微晶纤维素5-8份,氯化钙4-5.5份,二氧化硅6-10份。
本发明所述辅料:微晶纤维素8-10份,氯化钙6-8份,二氧化硅12-15份。
一种能改善喷雾干燥粘壁的复合果糖粉组合物的喷雾干燥方法,包括下列步骤:
(1)配置复合果糖液:
取F55液态果糖100份,加水200份,搅匀后加麦芽糊精20份,待继续搅匀后加入蔗糖14份,搅拌均匀,配置成混悬液备用;
(2)喷雾干燥:
向步骤(1)配置好的混悬液中加入微晶纤维素3-10份,氯化钙3-8份,二氧化硅5-15份,搅拌均匀后进行喷雾干燥,进风温度120℃、雾化压力0.75bar、进液体积流量4ml/min、气体流量40m3/h,制得复合果糖粉。
本发明的优点是:辅料组合物可以增加混悬液的流动性、提高物料的软化点,增强混悬液的雾化效果,通过多种辅料组合使用,发挥各自优势,从不同角度发挥防粘壁作用。可显著提高复合果糖液喷雾干燥粉末得率,改善喷雾干燥过程中的粉料粘壁问题,提高了产品质量和粉末收率,通过对比具体实验结果可知,使用本发明技术,可明显提高粉末平均收率88.6%,具有显著的经济效益。
具体实施方式
实施例1
(1)配置复合果糖液:
取F55液态果糖100份,加水200份,搅匀后加麦芽糊精20份,待继续搅匀后加入蔗糖14份,搅拌均匀,配置成混悬液备用;
(2)喷雾干燥:
向步骤(1)配置好的混悬液中加入微晶纤维素3份,氯化钙3份,二氧化硅5份,搅拌均匀后进行喷雾干燥,进风温度120℃、雾化压力0.75bar、进液体积流量4ml/min、气体流量40m3/h,制得复合果糖粉。
实施例2
(1)配置复合果糖液:
取F55液态果糖100份,加水200份,搅匀后加麦芽糊精20份,待继续搅匀后加入蔗糖14份,搅拌均匀,配置成混悬液备用;
(2)喷雾干燥:
向步骤(1)配置好的混悬液中加入微晶纤维素6.5份,氯化钙5.5份,二氧化硅10份,搅拌均匀后进行喷雾干燥,进风温度120℃、雾化压力0.75bar、进液体积流量4ml/min、气体流量40m3/h,制得复合果糖粉。
实施例3
(1)配置复合果糖液:
取F55液态果糖100份,加水200份,搅匀后加麦芽糊精20份,待继续搅匀后加入蔗糖14份,搅拌均匀,配置成混悬液备用;
(2)喷雾干燥:
向步骤(1)配置好的混悬液中加入微晶纤维素10份,氯化钙8份,二氧化硅15份,搅拌均匀后进行喷雾干燥,进风温度120℃、雾化压力0.75bar、进液体积流量4ml/min、气体流量40m3/h,制得复合果糖粉。
实施例4
(1)配置复合果糖液:
取F55液态果糖100份,加水200份,搅匀后加麦芽糊精20份,待继续搅匀后加入蔗糖14份,搅拌均匀,配置成混悬液备用;
(2)喷雾干燥:
向步骤(1)配置好的混悬液中加入微晶纤维素5份,氯化钙4份,二氧化硅6份,搅拌均匀后进行喷雾干燥,进风温度120℃、雾化压力0.75bar、进液体积流量4ml/min、气体流量40m3/h,制得复合果糖粉。
实施例5
(1)配置复合果糖液:
取F55液态果糖100份,加水200份,搅匀后加麦芽糊精20份,待继续搅匀后加入蔗糖14份,搅拌均匀,配置成混悬液备用;
(2)喷雾干燥:
向步骤(1)配置好的混悬液中加入微晶纤维素6.5份,氯化钙4.8份,二氧化硅8份,搅拌均匀后进行喷雾干燥,进风温度120℃、雾化压力0.75bar、进液体积流量4ml/min、气体流量40m3/h,制得复合果糖粉。
实施例6
(1)配置复合果糖液:
取F55液态果糖100份,加水200份,搅匀后加麦芽糊精20份,待继续搅匀后加入蔗糖14份,搅拌均匀,配置成混悬液备用;
(2)喷雾干燥:
向步骤(1)配置好的混悬液中加入微晶纤维素8份,氯化钙5.5份,二氧化硅10份,搅拌均匀后进行喷雾干燥,进风温度120℃、雾化压力0.75bar、进液体积流量4ml/min、气体流量40m3/h,制得复合果糖粉。
实施例7
(1)配置复合果糖液:
取F55液态果糖100份,加水200份,搅匀后加麦芽糊精20份,待继续搅匀后加入蔗糖14份,搅拌均匀,配置成混悬液备用;
(2)喷雾干燥:
向步骤(1)配置好的混悬液中加入微晶纤维素8份,氯化钙6份,二氧化硅12份,搅拌均匀后进行喷雾干燥,进风温度120℃、雾化压力0.75bar、进液体积流量4ml/min、气体流量40m3/h,制得复合果糖粉。
实施例8
(1)配置复合果糖液:
取F55液态果糖100份,加水200份,搅匀后加麦芽糊精20份,待继续搅匀后加入蔗糖14份,搅拌均匀,配置成混悬液备用;
(2)喷雾干燥:
向步骤(1)配置好的混悬液中加入微晶纤维素9份,氯化钙7份,二氧化硅13.5份,搅拌均匀后进行喷雾干燥,进风温度120℃、雾化压力0.75bar、进液体积流量4ml/min、气体流量40m3/h,制得复合果糖粉。
下边通过实验来进一步说明本发明的效果。
实验所用原料:F55液态果糖(中粮生化能源公主岭有限公司)、麦芽糊精(中粮生化能源公主岭有限公司)、蔗糖(福临门);
实验所用辅料:微晶纤维素、氯化钙、二氧化硅;
实验所用设备:B-290型喷雾干燥仪(瑞士BUCHI公司),IKA搅拌器,分析天平。
实验方法:
1、对照品1、2,不加辅料,进行二批次复合果糖液喷雾干燥实验,计算粉末收率;
取F55液态果糖100份,加水200份,搅匀后加麦芽糊精20份,待继续搅匀后加入蔗糖14份,搅拌均匀,配置成混悬液备用;
搅拌均匀后喷雾干燥,喷雾干燥工艺条件,进风温度120℃、雾化压力0.75bar、进液体积流量4ml/min、气体流量40m3/h;
2、选取本发明实施例1、2、3,计算粉末收率。
实验结果如下表:
由上述结果可知,通过添加辅料,可显著提高复合果糖液喷雾干燥粉末收率,同时改善了喷雾干燥过程中的粉料粘壁问题。
Claims (6)
1.一种能改善喷雾干燥粘壁的复合果糖粉组合物,所述复合果糖粉组合物是由如下重量份的原料和辅料组成的:
原料:F55液态果糖100份,水200份,麦芽糊精20份,蔗糖14份;
其特征在于:
辅料:微晶纤维素3-10份,氯化钙3-8份,二氧化硅5-15份。
2.根据权利要求1所述的一种能改善喷雾干燥粘壁的复合果糖粉组合物,其特征在于:
辅料:微晶纤维素5-8份,氯化钙4-5.5份,二氧化硅6-10份。
3.根据权利要求1所述的一种能改善喷雾干燥粘壁的复合果糖粉组合物,其特征在于:
辅料:微晶纤维素8-10份,氯化钙6-8份,二氧化硅12-15份。
4.一种能改善喷雾干燥粘壁的复合果糖粉组合物的喷雾干燥方法,其特征在于包括下列步骤:
(1)配置复合果糖液:
取F55液态果糖100份,加水200份,搅匀后加麦芽糊精20份,待继续搅匀后加入蔗糖14份,搅拌均匀,配置成混悬液备用;
(2)喷雾干燥:
向步骤(1)配置好的混悬液中加入微晶纤维素3-10份,氯化钙3-8份,二氧化硅5-15份,搅拌均匀后进行喷雾干燥,进风温度120℃、雾化压力0.75bar、进液体积流量4ml/min、气体流量40m3/h,制得复合果糖粉。
5.根据权利要求4所述的一种能改善喷雾干燥粘壁的复合果糖粉组合物的喷雾干燥方法,其特征在于:步骤(2)中加入微晶纤维素5-8份,氯化钙4-5.5份,二氧化硅6-10份。
6.根据权利要求4所述的一种能改善喷雾干燥粘壁的复合果糖粉组合物的喷雾干燥方法,其特征在于:步骤(2)中加入微晶纤维素8-10份,氯化钙6-8份,二氧化硅12-15份。
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US5102682A (en) * | 1991-01-31 | 1992-04-07 | Kraft General Foods, Inc. | Sucrose and fructose-containing food mix and process |
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