CN109626903A - Polymer cement waterproof paint and preparation method thereof - Google Patents
Polymer cement waterproof paint and preparation method thereof Download PDFInfo
- Publication number
- CN109626903A CN109626903A CN201811618562.7A CN201811618562A CN109626903A CN 109626903 A CN109626903 A CN 109626903A CN 201811618562 A CN201811618562 A CN 201811618562A CN 109626903 A CN109626903 A CN 109626903A
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- polymer cement
- waterproof paint
- cement waterproof
- titanium dioxide
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Classifications
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B28/00—Compositions of mortars, concrete or artificial stone, containing inorganic binders or the reaction product of an inorganic and an organic binder, e.g. polycarboxylate cements
- C04B28/02—Compositions of mortars, concrete or artificial stone, containing inorganic binders or the reaction product of an inorganic and an organic binder, e.g. polycarboxylate cements containing hydraulic cements other than calcium sulfates
- C04B28/04—Portland cements
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2111/00—Mortars, concrete or artificial stone or mixtures to prepare them, characterised by specific function, property or use
- C04B2111/00474—Uses not provided for elsewhere in C04B2111/00
- C04B2111/00482—Coating or impregnation materials
- C04B2111/00508—Cement paints
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2111/00—Mortars, concrete or artificial stone or mixtures to prepare them, characterised by specific function, property or use
- C04B2111/20—Resistance against chemical, physical or biological attack
- C04B2111/27—Water resistance, i.e. waterproof or water-repellent materials
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2111/00—Mortars, concrete or artificial stone or mixtures to prepare them, characterised by specific function, property or use
- C04B2111/20—Resistance against chemical, physical or biological attack
- C04B2111/28—Fire resistance, i.e. materials resistant to accidental fires or high temperatures
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2111/00—Mortars, concrete or artificial stone or mixtures to prepare them, characterised by specific function, property or use
- C04B2111/50—Flexible or elastic materials
- C04B2111/503—Elastic materials
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2201/00—Mortars, concrete or artificial stone characterised by specific physical values
- C04B2201/50—Mortars, concrete or artificial stone characterised by specific physical values for the mechanical strength
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Ceramic Engineering (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Inorganic Chemistry (AREA)
- Materials Engineering (AREA)
- Structural Engineering (AREA)
- Organic Chemistry (AREA)
- Paints Or Removers (AREA)
- Compositions Of Macromolecular Compounds (AREA)
Abstract
The invention discloses a kind of polymer cement waterproof paints and preparation method thereof.The polymer cement waterproof paint includes liquid material and powder, and the liquid material includes the component of following parts by weight: 10-15 parts of EVA lotion, 10-15 parts of acrylate polymer emulsion, 5040 0.05-0.1 parts of dispersing agent, 0.8-1 parts of ethylene glycol monobutyl ether, methyl silicon resin 0.1-0.3 parts poly-, 0.06-0.12 parts of polyoxypropylene ethylene oxide glycerin ether, 0.2-0.4 parts of anti-aging agent, 0.2-0.4 parts of crosslinking agent, 0.1-0.2 parts of fungicide, 0.1-0.2 parts of dry film mould inhibitor；The powder includes the component of following parts by weight: 8-10 parts of portland cement, 4-6 parts of powdered whiting, 4-6 parts of silica flour, 0.5-1.5 parts of wollastonite, 0.5-0.8 parts of montmorillonite, 0.1-0.2 parts of nano-titanium dioxide, 0.04-0.08 parts of calgon, 0.4-0.6 parts of chlorinated paraffin.The invention has the benefit that the polymer cement-base waterproof coating has good durability.
Description
Technical field
The present invention relates to building coating, in particular to a kind of polymer cement waterproof paint and preparation method thereof.
Background technique
Polymer cement waterproof paint, also known as JS water-repellent paint are with the polymerization such as acrylate, ethane-acetic acid ethyenyl ester
Object lotion and cement are primary raw material, and filler is added and other auxiliary agents are formulated, solid through moisture evaporation and hydrated reaction of cement
It is melted into the double-component aqueous water-repellent paint of film.
The Chinese patent of Publication No. CN106118481A disclose a kind of self-healing polymers cement waterproof paint and its
Preparation method.The water-repellent paint is dual-component coating, and liquid material A is grouped as by the group with heavyweight percentage: polymer emulsion 70-
80%, hydroxyethyl cellulose 0.5-1%, defoaming agent 3-5%, water surplus；Powder material B is grouped as by the group of percentage by weight:
Portland cement 20-35%, high water absorbency polymer 5-15%, silicon dioxide powder 3-10%, dispersing agent 1-3%, water-reducing agent 1-
3%, make the polymer 5-15%, calcium hydroxide 3-5%, quartz sand 10-30%, filler surplus of microcapsule wall material.
But the problem of the deficiency of durability existing for the water-repellent paint, have much room for improvement.
Summary of the invention
The object of the present invention is to provide a kind of polymer cement-base waterproof coatings.The polymer cement-base waterproof coating has
Good durability.
Above-mentioned technical purpose of the invention has the technical scheme that
A kind of polymer cement waterproof paint, including liquid material and powder, the liquid material include the component of following parts by weight:
10-15 parts of EVA lotion
10-15 parts of acrylate polymer emulsion
5040 0.05-0.1 parts of dispersing agent
0.8-1 parts of ethylene glycol monobutyl ether
Poly- methyl silicon resin 0.1-0.3 parts
0.06-0.12 parts of polyoxypropylene ethylene oxide glycerin ether
0.2-0.4 parts of anti-aging agent
0.2-0.4 parts of crosslinking agent
0.1-0.2 parts of fungicide
0.1-0.2 parts of dry film mould inhibitor
The powder includes the component of following parts by weight:
8-10 parts of portland cement
4-6 parts of powdered whiting
4-6 parts of silica flour
0.5-1.5 parts of wollastonite
0.5-0.8 parts of montmorillonite
0.1-0.2 parts of titanium dioxide
0.04-0.08 parts of calgon
0.4-0.6 parts of chlorinated paraffin.
The present invention is further arranged to: the anti-aging agent is 2,2 '-thiobis (4- methyl-6-tert-butylphenol).
The present invention is further arranged to: the crosslinking agent is melamine resin.
The present invention is further arranged to: the fungicide is Acticide HF, and the dry film mould inhibitor is Acticide
EPW。
The present invention is further arranged to: the titanium dioxide is nanoscale.
The present invention is further arranged to: the titanium dioxide is Detitanium-ore-type.
Another goal of the invention of the present invention is to provide a kind of preparation method of polymer cement waterproof paint, including walks as follows
It is rapid:
Step 1: according to parts by weight, weighing 10-15 parts of EVA lotion, 10-15 parts of acrylate polymer emulsion, dispersing agent 5040
0.05-0.1 parts, 0.8-1 parts of ethylene glycol monobutyl ether, methyl silicon resin 0.1-0.3 parts poly-, polyoxypropylene ethylene oxide glycerin ether
0.06-0.12 parts, 0.2-0.4 parts of anti-aging agent, 0.2-0.4 parts of crosslinking agent, 0.1-0.2 parts of fungicide, dry film mould inhibitor 0.1-0.2
Part, 8-10 parts of portland cement, 4-6 parts of powdered whiting, 4-6 parts of silica flour, 0.5-1.5 parts of wollastonite, montmorillonite 0.5-0.8
Part, 0.1-0.2 parts of titanium dioxide, 0.04-0.08 parts of calgon, 0.4-0.6 parts of chlorinated paraffin；
Step 2: EVA lotion and acrylate polymer emulsion are stirred dispersion with 1000-1200rad/min, then plus
Enter dispersing agent 5040, ethylene glycol monobutyl ether, poly- methyl silicon resin, polyoxypropylene ethylene oxide glycerin ether, anti-aging agent, crosslinking agent,
Fungicide and dry film mould inhibitor, obtain liquid material after mixing；
Step 3: by portland cement, powdered whiting, silica flour, wollastonite, montmorillonite, titanium dioxide, calgon and
Chlorinated paraffin is stirred dispersion with 3000-3500rad/min, obtains powder after mixing；
Step 4: liquid material being added in powder, is stirred and is dispersed to without obvious agglomerated particle, stirring with 800-1000rad/min
It is stood after uniformly.
In conclusion the invention has the following advantages:
1, EVA lotion has permanent flexibility, good resistance to acid and alkali, ultraviolet-resistant aging, good compatibility, film forming
And cementability.Acrylate polymer emulsion is capable of forming good luster and water-fast film, and bonding securely, is not easy to peel off, in room temperature
Under flexible and elastic, good weatherability, but tensile strength is not high；
2, dispersing agent 5040 is anionic surfactant, has brilliant wetting and dispersing performance.The foaminess of dispersing agent 5040
It is low, the mobility of coating can be improved, the excellent properties with stable slurry viscosity；
3, ethylene glycol monobutyl ether can slowly volatilize after film is formed, and promote the Plastic Flow and flexible deformation of lotion, improve
It coalesces performance.Ethylene glycol monobutyl ether carries out dissolution to lotion to make lotion surface soften, and promotes lotion vulnerable to compressive strain, melts
Synthesize film.The addition of ethylene glycol monobutyl ether can reduce the minimum film formation temperature of lotion；
4, poly- methyl silicon resin has good high temperature resistant, electrical insulation capability, moisture resistance waterproof, fire-retardant, anticorrosion etc. a variety of；
5, polyoxypropylene ethylene oxide glycerin ether is able to suppress foam and generates or eliminate the foam generated, has the foam inhibition time
Long, the features such as effect is good, antifoaming speed is fast, thermal stability is good；
6,2,2 '-thiobis (4- methyl-6-tert-butylphenol) have good result to thermal oxidation resistance, fatigue aging, can destroy
Hydroperoxides have auto-synergistic effect；
7, melamine resin can be improved the crosslinking degree of acrylate polymer emulsion, improve water-repellent paint intensity,
Puncture resistance, surfaces of tacky, water resistance and heat aging, hence it is evident that improve the construction and service performance of composite water-proof paint；
8, Acticide HF be common fungicide, including 5-Chloro-2-methyl-4-isothiazolin-3-one, 2- methyl -4- different
Thiazoline -3- ketone and formaldehyde concentrate.Acticide EPW is common dry film mould inhibitor.Acticide HF and Acticide
EPW all has good antibacterial and mouldproof performance；
9, portland cement is significant to the Effect on Mechanical Properties of water-repellent paint.In molding film, 80% cement is not joined
With aquation, the effect of filler is acted only as, but crucial effect is played in the part of aquation in film.The aluminium that hydrated cementitious generates
Salt generates crosslinked action with the active group in polymer emulsion, to change the shaping speed of water-repellent paint, while making to polymerize
The water resistance of object, weatherability, resistance to acid and alkali etc. have great raising；
10, the addition of powdered whiting, silica flour and wollastonite can adjust the performance and liquid powder ratio of water-repellent paint；
11, montmorillonite can obstruct ultraviolet light, the transmission of hydrone and the warm-up movement of restriction molecule, to greatly improve painting
The mechanical property of film, resistance to ultraviolet, heat-resisting and water resistance；
12, Nano titanium dioxide can not only increase the mechanical property of water-repellent paint, and it is old to improve its uvioresistant
Change and heat ageing ability；
13, calgon is that white powder crystallizes or colourless transparent glass sheet or blocks of solid, soluble easily in water, insoluble in having
Solvent.Calgon hygroscopicity is very strong, and moisture can gradually be absorbed and be in glutinous jelly by being placed in air；
14, the addition of chlorinated paraffin can increase the flexibility and adhesive force of film.
Specific embodiment
Embodiment 1-5 is used to illustrate the component of polymer cement waterproof paint.Embodiment 1-5 polymer cement waterproof paint
Component be shown in Table 1.
Table 1, embodiment 1-5 polymer cement waterproof paint component table
Note: unit " part " refers to parts by weight；Anti-aging agent is 2,2 '-thiobis (4- methyl-6-tert-butylphenol)；Crosslinking agent is trimerization
Cyanamide formaldehyde resin；Fungicide is Acticide HF；Dry film mould inhibitor is Acticide EPW；Titanium dioxide is that nanoscale is sharp
Titanium ore type titanium dioxide.
In conjunction with table 1, the preparation method of polymer cement waterproof paint described further below.
A kind of preparation method of polymer cement waterproof paint, includes the following steps:
Step 1: according to parts by weight, weigh EVA lotion, acrylate polymer emulsion, dispersing agent 5040, ethylene glycol monobutyl ether,
Poly- methyl silicon resin, polyoxypropylene ethylene oxide glycerin ether, anti-aging agent, crosslinking agent, fungicide, dry film mould inhibitor, silicate cement
Mud, powdered whiting, silica flour, wollastonite, montmorillonite, titanium dioxide, calgon, chlorinated paraffin；
Step 2: EVA lotion and acrylate polymer emulsion are stirred dispersion with 1000-1200rad/min, then plus
Enter dispersing agent 5040, ethylene glycol monobutyl ether, poly- methyl silicon resin, polyoxypropylene ethylene oxide glycerin ether, anti-aging agent, crosslinking agent,
Fungicide and dry film mould inhibitor, obtain liquid material after mixing；
Step 3: by portland cement, powdered whiting, silica flour, wollastonite, montmorillonite, titanium dioxide, calgon and
Chlorinated paraffin is stirred dispersion with 3000-3500rad/min, obtains powder after mixing；
Step 4: liquid material being added in powder, is stirred and is dispersed to without obvious agglomerated particle, stirring with 800-1000rad/min
It is stood after uniformly.
The preparation method parameter list of table 2, polymer cement waterproof paint
Comparative example 1
Select the embodiment 1 as a comparison case 1 of the Chinese patent of Publication No. CN106118481A.
Durability test
Embodiment 1-5 and comparative example 1 are tried referring to GB/T 18244-2000 " architectural waterproof material aging testing method "
It tests.
Hot air aging is carried out below and the test number of days of artificial climate accelerated ageing is 49 days.
1 durability test record sheet of table 3, embodiment 1-5 and comparative example
Note: stretching strength retentivity and elongation at break conservation rate are bigger, show that durability is higher.
As known from Table 3, compared to comparative example 1, the present invention has excellent durability.
The present embodiment is only explanation of the invention, is not limitation of the present invention, and those skilled in the art exist
It can according to need the modification that not creative contribution is made to the present embodiment after reading this specification, but as long as in the present invention
Scope of the claims in all by the protection of Patent Law.
Claims (7)
1. a kind of polymer cement waterproof paint, it is characterized in that: including liquid material and powder, the liquid material includes following parts by weight
Component:
10-15 parts of EVA lotion
10-15 parts of acrylate polymer emulsion
5040 0.05-0.1 parts of dispersing agent
0.8-1 parts of ethylene glycol monobutyl ether
Poly- methyl silicon resin 0.1-0.3 parts
0.06-0.12 parts of polyoxypropylene ethylene oxide glycerin ether
0.2-0.4 parts of anti-aging agent
0.2-0.4 parts of crosslinking agent
0.1-0.2 parts of fungicide
0.1-0.2 parts of dry film mould inhibitor
The powder includes the component of following parts by weight:
8-10 parts of portland cement
4-6 parts of powdered whiting
4-6 parts of silica flour
0.5-1.5 parts of wollastonite
0.5-0.8 parts of montmorillonite
0.1-0.2 parts of titanium dioxide
0.04-0.08 parts of calgon
0.4-0.6 parts of chlorinated paraffin.
2. polymer cement waterproof paint according to claim 1, it is characterized in that: the anti-aging agent is 2,2 '-thiobis
(4- methyl-6-tert-butylphenol).
3. polymer cement waterproof paint according to claim 1, it is characterized in that: the crosslinking agent is melamino-formaldehyde
Resin.
4. polymer cement waterproof paint according to claim 1, it is characterized in that: the fungicide is Acticide HF,
The dry film mould inhibitor is Acticide EPW.
5. polymer cement waterproof paint according to claim 1, it is characterized in that: the titanium dioxide is nanoscale.
6. polymer cement waterproof paint according to claim 1, it is characterized in that: the titanium dioxide is Detitanium-ore-type.
7. a kind of preparation method of polymer cement waterproof paint, it is characterized in that: including the following steps:
Step 1: according to parts by weight, weighing 10-15 parts of EVA lotion, 10-15 parts of acrylate polymer emulsion, dispersing agent 5040
0.05-0.1 parts, 0.8-1 parts of ethylene glycol monobutyl ether, methyl silicon resin 0.1-0.3 parts poly-, polyoxypropylene ethylene oxide glycerin ether
0.06-0.12 parts, 0.2-0.4 parts of anti-aging agent, 0.2-0.4 parts of crosslinking agent, 0.1-0.2 parts of fungicide, dry film mould inhibitor 0.1-0.2
Part, 8-10 parts of portland cement, 4-6 parts of powdered whiting, 4-6 parts of silica flour, 0.5-1.5 parts of wollastonite, montmorillonite 0.5-0.8
Part, 0.1-0.2 parts of titanium dioxide, 0.04-0.08 parts of calgon, 0.4-0.6 parts of chlorinated paraffin；
Step 2: EVA lotion and acrylate polymer emulsion are stirred dispersion with 1000-1200rad/min, then plus
Enter dispersing agent 5040, ethylene glycol monobutyl ether, poly- methyl silicon resin, polyoxypropylene ethylene oxide glycerin ether, anti-aging agent, crosslinking agent,
Fungicide and dry film mould inhibitor, obtain liquid material after mixing；
Step 3: by portland cement, powdered whiting, silica flour, wollastonite, montmorillonite, titanium dioxide, calgon and
Chlorinated paraffin is stirred dispersion with 3000-3500rad/min, obtains powder after mixing；
Step 4: liquid material being added in powder, is stirred and is dispersed to without obvious agglomerated particle, stirring with 800-1000rad/min
It is stood after uniformly.
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| CN201811618562.7A CN109626903A (en) | 2018-12-27 | 2018-12-27 | Polymer cement waterproof paint and preparation method thereof |
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Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110145039A (en) * | 2019-06-20 | 2019-08-20 | 北京中核北研科技发展股份有限公司 | A kind of acrylate copolymer polyester blank in-place forming macromolecule coiled material and construction method |
| CN110591479A (en) * | 2019-09-05 | 2019-12-20 | 四川东方雨虹建筑材料有限公司 | Anti-freezing acid-resistant polymer cement waterproof coating and preparation method thereof |
| CN111057243A (en) * | 2019-12-27 | 2020-04-24 | 芜湖东方雨虹建筑材料有限公司 | Organic silicon resin, polymer cement waterproof coating and preparation method thereof |
| CN112011274A (en) * | 2020-09-03 | 2020-12-01 | 四川童燊防水工程有限公司 | Organic waterproof emulsion coating and preparation method thereof |
| CN116179009A (en) * | 2022-12-28 | 2023-05-30 | 北京东方雨虹防水技术股份有限公司 | Paraffin oil modifier and preparation method thereof, waterproof coating containing paraffin oil modifier and preparation method of waterproof coating |
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Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110145039A (en) * | 2019-06-20 | 2019-08-20 | 北京中核北研科技发展股份有限公司 | A kind of acrylate copolymer polyester blank in-place forming macromolecule coiled material and construction method |
| CN110591479A (en) * | 2019-09-05 | 2019-12-20 | 四川东方雨虹建筑材料有限公司 | Anti-freezing acid-resistant polymer cement waterproof coating and preparation method thereof |
| CN110591479B (en) * | 2019-09-05 | 2022-02-22 | 四川东方雨虹建筑材料有限公司 | Anti-freezing acid-resistant polymer cement waterproof coating and preparation method thereof |
| CN111057243A (en) * | 2019-12-27 | 2020-04-24 | 芜湖东方雨虹建筑材料有限公司 | Organic silicon resin, polymer cement waterproof coating and preparation method thereof |
| CN112011274A (en) * | 2020-09-03 | 2020-12-01 | 四川童燊防水工程有限公司 | Organic waterproof emulsion coating and preparation method thereof |
| CN116179009A (en) * | 2022-12-28 | 2023-05-30 | 北京东方雨虹防水技术股份有限公司 | Paraffin oil modifier and preparation method thereof, waterproof coating containing paraffin oil modifier and preparation method of waterproof coating |
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Application publication date: 20190416 |