CN109603458A - Formaldehyde scavenger and preparation method thereof in a kind of film forming room - Google Patents
Formaldehyde scavenger and preparation method thereof in a kind of film forming room Download PDFInfo
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- CN109603458A CN109603458A CN201811560504.3A CN201811560504A CN109603458A CN 109603458 A CN109603458 A CN 109603458A CN 201811560504 A CN201811560504 A CN 201811560504A CN 109603458 A CN109603458 A CN 109603458A
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- film forming
- formaldehyde scavenger
- formaldehyde
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
- B01D53/34—Chemical or biological purification of waste gases
- B01D53/46—Removing components of defined structure
- B01D53/72—Organic compounds not provided for in groups B01D53/48 - B01D53/70, e.g. hydrocarbons
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
- B01D53/34—Chemical or biological purification of waste gases
- B01D53/74—General processes for purification of waste gases; Apparatus or devices specially adapted therefor
- B01D53/77—Liquid phase processes
- B01D53/78—Liquid phase processes with gas-liquid contact
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D2259/00—Type of treatment
- B01D2259/45—Gas separation or purification devices adapted for specific applications
- B01D2259/4508—Gas separation or purification devices adapted for specific applications for cleaning air in buildings
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- General Chemical & Material Sciences (AREA)
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- Chemical Kinetics & Catalysis (AREA)
- Solid-Sorbent Or Filter-Aiding Compositions (AREA)
- Disinfection, Sterilisation Or Deodorisation Of Air (AREA)
Abstract
The present invention is formaldehyde scavenger and preparation method thereof in a kind of film forming room.It can quickly form one layer of film for uniformly containing efficient aldehyde remover in furniture surface, can the formaldehyde that discharged in furniture be stopped and be disposed completely, and can removed easily after a period of use in film, sprayed again, noresidue is pollution-free.The present invention includes the component of following mass percent: formaldehyde scavenger 1-20%;Hygroscopic agent 0.5-10%;Film forming agent 1-8%;Spreading agent 1-10%;Appropriate pH adjusting agent;Essence 0-0.5%;Deionized water surplus.
Description
Technical field
The present invention relates to a kind of formaldehyde scavengers, and in particular to formaldehyde scavenger and preparation method thereof in a kind of film forming room.
Background technique
Formaldehyde is in the 2nd of China's toxic chemical priority acccess control list, has been determined as by the World Health Organization carcinogenic
With cause deformed material, be generally acknowledged allergen, and one of potential strong mutagen, and be considered and leukaemia is sent out
There is causalities between life.Excessive formaldehyde can generate apparent stimulation to eyes, respiratory tract, human body mucous membrane and skin and make
With;Acute poisoning can lead to shed tears, runny nose, the symptoms such as cough, cause various respiratory tract disease;Chronic inhalation of low concentration can lead to
Unrelenting headache, inability, insomnia etc.;Long-term sucking low dosage can cause chronic respiratory disease, feminine menstrual disorder, neonate
Matter reduction, chromosome abnormality, or even induce nasopharyngeal carcinoma;The mouths such as nervous system, liver of meeting infringer when high concentration.
Indoor formaldehyde is mainly derived from glued board, fine workmanship's template, medium density fibre board (MDF) and the particieboard, wooden core that finishing uses
The artificial boards such as plate.These finishing materials are primarily due to use aldehydes polymer resin binder --- Lauxite, at present
Such plate is in house ornamentation occupation rate of market up to 80% or more, but the adhesive feature is after deliquescing or room temperature meeting when being more than 20 DEG C
Free formaldehyde is decomposited, is the main reason for causing Formaldehyde Pollution of Indoor Air.
To solve the problems, such as Formaldehyde Pollution of Indoor Air, various formaldehyde scavengers, especially photocatalyst are had studied both at home and abroad and its is answered
Mould assembly aldehyde remover report is especially more.CN201510181982.3 has invented cold catalyst (carrying platinum nanometer rutile titania titanium dioxide) 1-8%;
Nano-silver colloid 0.1-0.5% and amphipathic fibroin albumen 5-15%;Ethylene urea 5-10% compounding can reach except aldehyde at 24 hours
To except aldehyde rate 97.9%;CN201611143931.2 has invented a kind of antistatic low-light light touching type formaldehyde scavenger and its preparation side
Method, by modified aqueous polyurethane emulsion (Acrylate Modified Aqueous Polyurethane multiple emulsion) 35%, water soluble Beta-cyclodextrin 8%, carboxyl
SBR modified latex 9.5%, antistatic agent (ethyoxyl laurel ester amine) 5%, Formaldehyde decomposition enzyme 7%, aqueous hyper-dispersant (aqueous light
Quick polyurethane hyper-dispersant) 6%, nano-stephanoporate silicon dioxide 0.5%, n-butanol 3% and stabilizer (HH972-2) 1% compounded,
It can reach at 1 hour except aldehyde rate > 40%;CN201610571870.3 has invented a kind of photocatalyst type formaldehyde scavenger and its system
Preparation Method, 1-10% nanometer silver paste solution, the photocatalyst (nanometer anatase titania colloidal solution) of 1-15%, 0-5% lauroyl
Base glutamic acid surfactant, 0-5% polyethylene glycol, formaldehyde catching agent (the 2- imidazolidinone, 1,3- diaminourea and two of 1-8%
Methylacetamide), remaining deionized water.But the aldehyde remover of photocatalyst is at high cost, and very strong to light dependence, practical application effect
Fruit is general, and it is more difficult to promote.
Formaldehyde is once evaporate into air, it is more difficult to be captured, even if using most effective formaldehyde scavenger, if contact is not
To formaldehyde, or in the case where concentration of formaldehyde is especially low, except aldehyde performance is all excessively poor, formaldehyde is only removed into ability in source
Reach really except aldehyde.In order to find better formaldehyde adsorbent or agent for capturing, contact formaldehyde scavenger preferably with formaldehyde.
CN02113857 invents a kind of novel methylene oxide scavenging agent with the halide of hydrazides substance and metal, nitrate, sulphite etc.
Substance is as aldehyde remover, and assist infiltration agent, carries out capture elimination mainly for artificial board inside release free formaldehyde, but at
Type furniture surface applies matcoveredn, and addition bleeding agent effect is smaller, it is more difficult to give full play to it except aldehyde performance.
CN201610784900.9 invents a kind of furniture formaldehyde scavenger that percdation surface layer persistently captures and preparation method, using end
Amino dissaving polymer 1-5%, Carboxymethyl chitosan 5-10%, bleeding agent (fatty alcohol polyoxyethylene ether compound) 0.1-
1%, buffer (phosphate buffer, phthalate buffer, citrate buffer solution) 0.1-1%, coalescing agent (propylene glycol
Butyl ether, propylene glycol methyl ether acetate) 0.1-1%, balance deionized water.The patent is mainly removed using Carboxymethyl chitosan
Aldehyde, it is at high cost, except aldehyde efficiency is general.CN201610661461.2 invents a kind of high-efficiency formaldehyde scavenging agent, with trihydroxy methyl ammonia
10-20 parts of methylmethane, 5-15 parts of saleratus, bleeding agent (sulfated castor oil, sodium alkyl sulfonate, sodium alkyl benzene sulfonate, amber
Acid alkyl ester sodium sulfonate, sulfamic acid sodium, fatty alcohol polyoxyethylene ether and alkyl phenol polyoxyethylene ether) 2-5 parts, film forming agent it is (poly-
Ethylene, polyurethane, acrylic resin, acrylate modified butadiene resin) 3-6 parts, 4-6 parts of ammonium hydroxide, extract solution from aloe 5-15
Part is main component, and wherein ammonium hydroxide smell is larger, is not suitable for interior use, extract solution from aloe higher cost, and saleratus is stablized
Property is poor.
The prior art can't be fully solved the problem of Formaldehyde Pollution of Indoor Air, and it is clear to need to develop a kind of good film-forming property, formaldehyde
Except high-efficient and low-cost formaldehyde scavenger.
Summary of the invention
In view of this, the present invention provides formaldehyde scavenger and preparation method thereof in a kind of film forming room.It can be in furniture surface
One layer of film for uniformly containing efficient aldehyde remover is quickly formed, can the formaldehyde that discharged in furniture be stopped and be disposed completely,
And can be removed easily after a period of use in film, it sprays again, noresidue is pollution-free.
In order to solve the problems existing in the prior art, the technical scheme is that formaldehyde scavenger in a kind of film forming room,
It is characterized in that: the component comprising following mass percent:
Formaldehyde scavenger 1-20%;
Hygroscopic agent 0.5-10%;
Film forming agent 1-8%;
Spreading agent 1-10%;
It is 5-7.0 that pH adjusting agent, which adjusts pH value,
Essence 0-0.5%
Deionized water surplus.
The formaldehyde scavenger is selected from sodium pyrosulfite, sodium sulfite, hydrazide kind compound.
The hygroscopic agent is one of glycerol, propylene glycol, polyethylene glycol, sorbierite or a variety of.
The film forming agent is polysaccharide polymer, polyvinyl alcohol, polyurethane, styrene/acrylic acid co-polymer, propylene
Acid/maleic acid and containing the one or more of sulfonated styrene polymer.
The spreading agent is polyether modified siloxane, and structural formula is (CH3)3SiO(CH3SiRO)m(CH3SiOCH3)nSi(CH3)3Wherein R represents (CH2)3O(EO)a(PO)bH), a+b=3-10, m+n=4-20.
The pH adjusting agent is citric acid, and product pH is made to be maintained at 5-7 range.
The preparation method of formaldehyde scavenger in a kind of film forming room, which is characterized in that the preparation method is real according to the following steps
It applies:
Step 1: it stocks up by the component of following mass percent:
Formaldehyde scavenger 1-20%;
Hygroscopic agent 0.5-10%;
Film forming agent 1-8%;
Spreading agent 1-10%;
It is 5-7.0 that pH adjusting agent, which adjusts pH value,
Essence 0-0.5%
Deionized water surplus.
Step 2: deionized water being added into batch tank, is then added formaldehyde scavenger, and stirring is to being completely dissolved;
Step 3: being added portionwise film forming agent and spreading agent under stiring, stirs uniform and stable to system;
Step 4: being added hygroscopic agent and pH adjusting agent, and stirring is to being completely dissolved;
Step 5: being added essence under stiring, stirs 20-30min;
Step 6: sampling Detection, finished product packing.
Compared with prior art, advantages of the present invention is as follows:
1, the present invention has good film forming, is compounded, can be quickly formed in furniture surface with spreading agent using film forming agent
Even transparent film, is covered on furniture surface, and formaldehyde in furniture is completely enclosed in film, formaldehyde is avoided to evaporate into air, will
It is eliminated in source, most effective and rapid.
2, the formaldehyde scavenger that uses of the present invention, fast with formaldehyde reaction speed, raw material is easy to get low in cost, free from extraneous odour, raw
The features such as production. art is simple, and preparation is convenient, is easy to produce in batches, and product cost is ideal may be used on removing for plate and furniture
Aldehyde.
Specific embodiment
In order to make the objectives, technical solutions, and advantages of the present invention clearer, with reference to embodiments, to the present invention
It is further elaborated.It should be appreciated that the specific embodiments described herein are merely illustrative of the present invention, it is not used to
Limit the present invention.
Embodiment one:
Formaldehyde scavenger includes the component of following mass percent in a kind of film forming room:
Formaldehyde scavenger 1%;
Hygroscopic agent 0.5%;
Film forming agent 1%;
Spreading agent 1%;
It is 5-7.0 that pH adjusting agent, which adjusts pH value,
Deionized water surplus.
The formaldehyde scavenger is selected from sodium pyrosulfite.
Hygroscopic agent is glycerol, propylene glycol.
The film forming agent is polysaccharide polymer, polyvinyl alcohol.
The spreading agent is polyether modified siloxane, and structural formula is (CH3)3SiO(CH3SiRO)m(CH3SiOCH3)nSi(CH3)3Wherein R represents (CH2)3O(EO)a(PO)bH), a+b=3-10, m+n=4-20.
The pH adjusting agent is citric acid, and product pH is made to be maintained at 5 ranges.
The preparation method is implemented according to the following steps:
Step 1: it stocks up by the component of following mass percent:
Formaldehyde scavenger 1%;
Hygroscopic agent 0.5%;
Film forming agent 1%;
Spreading agent 1%;
It is 5-7.0 that pH adjusting agent, which adjusts pH value,
Deionized water surplus.
Step 2: deionized water being added into batch tank, is then added formaldehyde scavenger, and stirring is to being completely dissolved;
Step 3: being added portionwise film forming agent and spreading agent under stiring, stirs uniform and stable to system;
Step 4: being added hygroscopic agent and pH adjusting agent, and stirring is to being completely dissolved;
Step 5: sampling Detection, finished product packing.
Embodiment two:
Formaldehyde scavenger includes the component of following mass percent in a kind of film forming room:
Formaldehyde scavenger 20%;
Hygroscopic agent 10%;
Film forming agent 8%;
Spreading agent 10%;
It is 5-7.0 that pH adjusting agent, which adjusts pH value,
Essence 0.5%
Deionized water surplus.
The formaldehyde scavenger sodium sulfite, hydrazide kind compound.
Hygroscopic agent is polyethylene glycol, sorbierite.
The film forming agent is polyurethane, styrene/acrylic acid co-polymer, acrylic acid/maleic acid and contains sulphur
Change the one or more of styrene polymer.
The spreading agent is polyether modified siloxane, and structural formula is (CH3)3SiO(CH3SiRO)m(CH3SiOCH3)nSi(CH3)3Wherein R represents (CH2)3O(EO)a(PO)bH), a+b=3-10, m+n=4-20.
The pH adjusting agent is citric acid, and product pH is made to be maintained at 7 ranges.
The preparation method is implemented according to the following steps:
Step 1: it stocks up by the component of following mass percent:
Formaldehyde scavenger 20%;
Hygroscopic agent 10%;
Film forming agent 8%;
Spreading agent 10%;
It is 5-7.0 that pH adjusting agent, which adjusts pH value,
Essence 0.5%
Deionized water surplus
Step 2: deionized water being added into batch tank, is then added formaldehyde scavenger, and stirring is to being completely dissolved;
Step 3: being added portionwise film forming agent and spreading agent under stiring, stirs uniform and stable to system;
Step 4: being added hygroscopic agent and pH adjusting agent, and stirring is to being completely dissolved;
Step 5: being added essence under stiring, stirs 20-30min;
Step 6: sampling Detection, finished product packing.
Embodiment three:
Formaldehyde scavenger includes the component of following mass percent in a kind of film forming room:
Formaldehyde scavenger 15%;
Hygroscopic agent 8%;
Film forming agent 6%;
Spreading agent 7%;
It is 6 that pH adjusting agent, which adjusts pH value,
Essence 0.3%
Deionized water surplus.
The formaldehyde scavenger is selected from sodium pyrosulfite, sodium sulfite, hydrazide kind compound.
Hygroscopic agent is one of glycerol, propylene glycol, polyethylene glycol, sorbierite or a variety of.
The film forming agent is polysaccharide polymer, polyvinyl alcohol, polyurethane, styrene/acrylic acid co-polymer, propylene
Acid/maleic acid and containing the one or more of sulfonated styrene polymer.
The spreading agent is polyether modified siloxane, and structural formula is (CH3)3SiO(CH3SiRO)m(CH3SiOCH3)nSi(CH3)3Wherein R represents (CH2)3O(EO)a(PO)bH), a+b=3-10, m+n=4-20.
The pH adjusting agent is citric acid, and product pH is made to be maintained at 5-7 range.
The preparation method is implemented according to the following steps:
Step 1: it stocks up by the component of following mass percent:
Formaldehyde scavenger 15%;
Hygroscopic agent 8%;
Film forming agent 6%;
Spreading agent 7%;
It is 6 that pH adjusting agent, which adjusts pH value,
Essence 0.3%
Deionized water surplus.
Step 2: deionized water being added into batch tank, is then added formaldehyde scavenger, and stirring is to being completely dissolved;
Step 3: being added portionwise film forming agent and spreading agent under stiring, stirs uniform and stable to system;
Step 4: being added hygroscopic agent and pH adjusting agent, and stirring is to being completely dissolved;
Step 5: being added essence under stiring, stirs 20-30min;
Step 6: sampling Detection, finished product packing.
The contents of the present invention are not limited to cited by embodiment, and those of ordinary skill in the art are by reading description of the invention
And to any equivalent replacement that technical solution of the present invention is taken, all are covered by the claims of the invention.
Claims (7)
1. formaldehyde scavenger in a kind of film forming room, it is characterised in that: the component comprising following mass percent:
Formaldehyde scavenger 1-20%;
Hygroscopic agent 0.5-10%;
Film forming agent 1-8%;
Spreading agent 1-10%;
It is 5-7.0 that pH adjusting agent, which adjusts pH value,
Essence 0-0.5%
Deionized water surplus.
2. formaldehyde scavenger in a kind of film forming room according to claim 1, it is characterised in that: the formaldehyde scavenger choosing
From sodium pyrosulfite, sodium sulfite, hydrazide kind compound.
3. formaldehyde scavenger in a kind of film forming room according to claim 1 or 2, it is characterised in that: the hygroscopic agent is
One of glycerol, propylene glycol, polyethylene glycol, sorbierite are a variety of.
4. formaldehyde scavenger in a kind of film forming room according to claim 3, it is characterised in that: the film forming agent is polysaccharide
Quasi polymer, polyvinyl alcohol, polyurethane, styrene/acrylic acid co-polymer, acrylic acid/maleic acid and benzene containing sulfonation
It is polyvinyl one or more.
5. formaldehyde scavenger in a kind of film forming room according to claim 4, it is characterised in that: the spreading agent is polyethers
Modified siloxane, structural formula are (CH3)3SiO(CH3SiRO)m(CH3SiOCH3)nSi(CH3)3Wherein R represents (CH2)3O(EO)a
(PO)bH), a+b=3-10, m+n=4-20.
6. formaldehyde scavenger in a kind of film forming room according to claim 6, it is characterised in that: the pH adjusting agent is lemon
Lemon acid, makes product pH be maintained at 5-7 range.
7. the preparation method of formaldehyde scavenger in a kind of film forming room as described in claim 1, which is characterized in that the preparation side
Method is implemented according to the following steps:
Step 1: it stocks up by the component of following mass percent:
Formaldehyde scavenger 1-20%;
Hygroscopic agent 0.5-10%;
Film forming agent 1-8%;
Spreading agent 1-10%;
It is 5-7.0 that pH adjusting agent, which adjusts pH value,
Essence 0-0.5%
Deionized water surplus;
Step 2: deionized water being added into batch tank, is then added formaldehyde scavenger, and stirring is to being completely dissolved;
Step 3: being added portionwise film forming agent and spreading agent under stiring, stirs uniform and stable to system;
Step 4: being added hygroscopic agent and pH adjusting agent, and stirring is to being completely dissolved;
Step 5: being added essence under stiring, stirs 20-30min;
Step 6: sampling Detection, finished product packing.
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Cited By (11)
Publication number | Priority date | Publication date | Assignee | Title |
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CN110403541A (en) * | 2019-06-28 | 2019-11-05 | 浙江维度环保科技有限公司 | A kind for the treatment of air indoor taste removal construction technology |
CN110449026A (en) * | 2019-08-13 | 2019-11-15 | 杭州易贝环保科技有限公司 | A kind of environment-friendly highly efficient photocatalyst formaldehyde scavenger and preparation method thereof |
CN110922829A (en) * | 2019-12-02 | 2020-03-27 | 怀化学院 | Formaldehyde scavenger and preparation method thereof, artificial board and preparation method of artificial board |
CN111589296A (en) * | 2020-06-09 | 2020-08-28 | 云深(福建)环保科技有限公司 | Indoor formaldehyde scavenger and preparation method thereof |
CN112876991A (en) * | 2021-02-05 | 2021-06-01 | 北京市理化分析测试中心 | Odor sealing agent with formaldehyde removing function and preparation method thereof |
CN112915779A (en) * | 2021-01-12 | 2021-06-08 | 港华(广州)生物科技有限公司 | Photocatalyst formaldehyde removal freshener and preparation method thereof |
CN113058420A (en) * | 2021-03-16 | 2021-07-02 | 河北福赛生物科技发展有限公司 | Biological enzyme formaldehyde scavenger with film covering and sealing performance and preparation method thereof |
CN113385011A (en) * | 2021-06-16 | 2021-09-14 | 杭州华好生物科技有限公司 | Smell removing agent |
CN115418863A (en) * | 2022-10-13 | 2022-12-02 | 佛山市顺德区阿波罗环保器材有限公司 | Composite material for humidity adjustment, preparation method thereof and humidity adjustment equipment |
CN116173714A (en) * | 2023-03-30 | 2023-05-30 | 上海腾灵建设集团有限公司 | Film-forming air treatment agent and preparation method thereof |
CN115418863B (en) * | 2022-10-13 | 2024-05-24 | 佛山市顺德区阿波罗环保器材有限公司 | Composite material for humidity adjustment, preparation method thereof and humidity adjustment equipment |
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CN104629548A (en) * | 2015-02-05 | 2015-05-20 | 洛阳理工学院 | Internal wall paint with air purification function and preparation method thereof |
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CN101045847A (en) * | 2006-03-31 | 2007-10-03 | 中国科学院过程工程研究所 | Adhesive and paint for absorbing formol |
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Cited By (11)
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CN110403541A (en) * | 2019-06-28 | 2019-11-05 | 浙江维度环保科技有限公司 | A kind for the treatment of air indoor taste removal construction technology |
CN110449026A (en) * | 2019-08-13 | 2019-11-15 | 杭州易贝环保科技有限公司 | A kind of environment-friendly highly efficient photocatalyst formaldehyde scavenger and preparation method thereof |
CN110922829A (en) * | 2019-12-02 | 2020-03-27 | 怀化学院 | Formaldehyde scavenger and preparation method thereof, artificial board and preparation method of artificial board |
CN111589296A (en) * | 2020-06-09 | 2020-08-28 | 云深(福建)环保科技有限公司 | Indoor formaldehyde scavenger and preparation method thereof |
CN112915779A (en) * | 2021-01-12 | 2021-06-08 | 港华(广州)生物科技有限公司 | Photocatalyst formaldehyde removal freshener and preparation method thereof |
CN112876991A (en) * | 2021-02-05 | 2021-06-01 | 北京市理化分析测试中心 | Odor sealing agent with formaldehyde removing function and preparation method thereof |
CN113058420A (en) * | 2021-03-16 | 2021-07-02 | 河北福赛生物科技发展有限公司 | Biological enzyme formaldehyde scavenger with film covering and sealing performance and preparation method thereof |
CN113385011A (en) * | 2021-06-16 | 2021-09-14 | 杭州华好生物科技有限公司 | Smell removing agent |
CN115418863A (en) * | 2022-10-13 | 2022-12-02 | 佛山市顺德区阿波罗环保器材有限公司 | Composite material for humidity adjustment, preparation method thereof and humidity adjustment equipment |
CN115418863B (en) * | 2022-10-13 | 2024-05-24 | 佛山市顺德区阿波罗环保器材有限公司 | Composite material for humidity adjustment, preparation method thereof and humidity adjustment equipment |
CN116173714A (en) * | 2023-03-30 | 2023-05-30 | 上海腾灵建设集团有限公司 | Film-forming air treatment agent and preparation method thereof |
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