CN109585120A - Permanent magnet magnetization method based on magnetic seal transcription technology - Google Patents

Permanent magnet magnetization method based on magnetic seal transcription technology Download PDF

Info

Publication number
CN109585120A
CN109585120A CN201811325924.3A CN201811325924A CN109585120A CN 109585120 A CN109585120 A CN 109585120A CN 201811325924 A CN201811325924 A CN 201811325924A CN 109585120 A CN109585120 A CN 109585120A
Authority
CN
China
Prior art keywords
magnetic
thin film
permanent
magnetic seal
permanent magnet
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
CN201811325924.3A
Other languages
Chinese (zh)
Other versions
CN109585120B (en
Inventor
支钞
崔伟斌
唐彬
王月
屈明山
李严军
李寅鑫
王支荣
刘显学
余丙军
袁涛
曾德群
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Institute of Electronic Engineering of CAEP
Original Assignee
Institute of Electronic Engineering of CAEP
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Institute of Electronic Engineering of CAEP filed Critical Institute of Electronic Engineering of CAEP
Priority to CN201811325924.3A priority Critical patent/CN109585120B/en
Publication of CN109585120A publication Critical patent/CN109585120A/en
Application granted granted Critical
Publication of CN109585120B publication Critical patent/CN109585120B/en
Expired - Fee Related legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Classifications

    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01FMAGNETS; INDUCTANCES; TRANSFORMERS; SELECTION OF MATERIALS FOR THEIR MAGNETIC PROPERTIES
    • H01F13/00Apparatus or processes for magnetising or demagnetising
    • H01F13/003Methods and devices for magnetising permanent magnets

Landscapes

  • Engineering & Computer Science (AREA)
  • Power Engineering (AREA)
  • Thin Magnetic Films (AREA)
  • Recording Or Reproducing By Magnetic Means (AREA)
  • Hard Magnetic Materials (AREA)
  • Manufacturing Of Magnetic Record Carriers (AREA)

Abstract

The invention discloses the permanent magnet magnetization method based on magnetic seal transcription technology, step includes: 1) to prepare magnetic seal and body to be marked, and the Curie temperature of the permanent magnetic thin film of the magnetic seal is higher than the Curie temperature of the permanent magnetic thin film of body to be marked;2) lower surface of the magnetic seal prepared is bonded with the upper surface of body to be marked, is then heated, then gradually annealed, thus by the magnetic transcription of magnetic seal to wait mark on body.Compared to conventional method, the present invention can easily realize magnetic history, and be suitable for any substrate, expand the scope of application significantly.

Description

Permanent magnet magnetization method based on magnetic seal transcription technology
Technical field
The present invention relates to the magnetization technology fields of membranaceous permanent magnet, and in particular to the permanent magnetism based on magnetic seal transcription technology Body Magnitizing method.
Background technique
Actuator miniaturization and it is integrated be realize current technological development trend and industry needs, for make it is small-sized Change high-performance micromagnetism actuator, needs to make the permanent magnet of miniaturization.However, the assembly to small magnet, the operations such as magnetization are multiple It is miscellaneous.To solve this problem, Fujiwara et al. has used the method for laser thermally assisted magnetic to realize a kind of thin-film permanent magnet Microsize region magnetizes (bibliography: Fujiwara, et al, " Micromagnetization patterning of Sputtered NdFeB/Ta multilayered films utilizing laser assisted heating ", Sensors and Actuators A:Physical, Vol. 220, pp. 298-304,2014.), as shown in Figure 1, should Technology is formed substantially according to following steps: 1, being formed a film, magnetize (PM film deposition and pulse Magnetization);2, apply external magnetic field (Application of external DC magnetic field);3, swash Light heats (Laser heating);4, region magnetic pole overturning (Partial magnetization reversal);5, laser is swept It retouches and completes film micro area magnetization (micro magnetization).The technology can the heating easy to accomplish to permanent magnetic thin film magnetize, But in order to realize the local heating to permanent magnetic thin film, it is necessary to using the good quartz base plate of thermal insulation, to other thermal insulations Substrate such as Si, metal of difference etc. is not applicable, therefore has limited to the scope of application of the technology significantly.
Summary of the invention
It is an object of the invention in view of the above-mentioned problems, providing the permanent magnet magnetization side based on magnetic seal transcription technology Method, this Magnitizing method is easy to operate, and the requirement to substrate without thermal insulation.
To achieve the above object, the present invention is special using the permanent magnet magnetization method as follows based on magnetic seal transcription technology Sign is that steps are as follows:
1) magnetic seal and body to be marked are prepared;
The body to be marked includes underlying substrate and permanent magnetic thin film, and the permanent magnetic thin film of body to be marked selects Fe-B rare-earth permanent magnet (NdFeB).Because the underlying substrate deposited to NdFeB permanent magnet does not have the requirement of thermal insulation, made in deposition Cheng Zhong need to only meet and bear process environments, such as film deposition temperature, baking oven heating temperature.Further, the magnetic print The Curie temperature of the permanent magnetic thin film of chapter is higher than the Curie temperature of the permanent magnetic thin film of body to be marked.
The magnetic seal includes the permanent magnetic thin film of top substrate layer and carrying magnetic pattern.The permanent magnetic thin film of carrying magnetic pattern is selected Be shirt cobalt rare-earth permanent magnet (SmCo);The top substrate layer substrate excellent using thermal insulation, such as quartz base plate etc..So, SmCo permanent magnet need to be deposited in the excellent top substrate layer of thermal insulation, be made by conventional laser thermally assisted magnetic technology, Required magnetic pattern is written in magnetic seal.
2) lower surface of the magnetic seal prepared is bonded with the upper surface of body to be marked, i.e. the lower surface of SmCo film It is bonded with the upper surface of NdFeB film, is then heated, heating temperature rises to the Curie temperature of NdFeB, then gradually moves back Fire, thus by the magnetic pattern transcription of magnetic seal to wait mark on body.
In step 2, the heating requirements are as follows: heating temperature is greater than the Curie temperature of NdFeB, and heating temperature is less than The Curie temperature of SmCo.
In step 2, the process gradually annealed and requirement are as the hot magnetization process of body to be marked.
In the heating process of step 2, when the temperature wait mark body reaches Curie temperature, itself does not both have magnetic Property, and coercive force also becomes zero.And the Curie temperature of magnetic seal has not yet been reached at this time, still have magnetism, can for magnetization to It marks body and external magnetic field is provided.Under external magnetic field effect, the direction of magnetization of body to be marked can be along this magnetic direction.With Temperature gradually cools down, and is finally completed magnetization.
Beneficial effects of the present invention are as follows:
Magnetization method of the invention is easy to operate, is suitable for any substrate;This method can be magnetized with mass, it is only necessary to prepare one Magnetic seal is covered, then then can be recycled, realizes magnetizing for multiple batches of print body.
Detailed description of the invention
Fig. 1 is the step schematic diagram of the laser thermally assisted magnetic technology of background technique.
Fig. 2-4 is the realization step schematic diagram of magnetic seal transcription of the present invention.
Specific embodiment
Below by specific embodiment and cooperate attached drawing, the present invention is described in detail.
Based on the permanent magnet magnetization method of magnetic seal transcription technology, magnetization step is as follows:
1) magnetic seal and body to be marked are prepared;The body to be marked includes underlying substrate and permanent magnetic thin film, and the magnetic seal includes The permanent magnetic thin film of top substrate layer and carrying magnetic pattern.
In the present embodiment, the Curie temperature of the permanent magnetic thin film as magnetic seal carrying magnetic pattern needs to be higher than body to be marked The Curie temperature of permanent magnetic thin film.In the present embodiment, the material that the permanent magnetic thin film of magnetic seal is selected is shirt cobalt rare-earth permanent magnet (SmCo), the material that the permanent magnetic thin film of body to be marked is selected is Fe-B rare-earth permanent magnet (NdFeB).
As in Figure 2-4, in the present embodiment: by using the mode of thermally assisted magnetic shown in FIG. 1 by required magnetic Property pattern be written in magnetic seal, the substrate for needing to select thermal insulation excellent, thus magnetic seal top substrate layer using quartz Substrate;And the substrate that NdFeB permanent magnet is deposited does not have the requirement of thermal insulation, is only subjected to process environments, such as film Depositing temperature, baking oven heating temperature etc., therefore the underlying substrate of body to be marked can use any substrate.
In the present embodiment, the laser thermally assisted magnetic technology of magnetic seal is made, with reference to describing in background technique bibliography Specific step and parameter index.
2) lower surface of the magnetic seal prepared is bonded with the upper surface of body to be marked, i.e. the lower surface of SmCo film It is bonded with the upper surface of NdFeB film, is subsequently placed in oven and is heated, then gradually annealing (i.e. with furnace, that is, cold), thus By the magnetic transcription of magnetic seal to wait mark on body.
In the present embodiment, the requirement of oven heat are as follows: the Curie temperature of the temperature > NdFeB of heating, and the temperature heated The Curie temperature of < SmCo.
The principle process that the present invention realizes is as follows:
The magnetic seal prepared is bonded up and down with body to be marked, is then heated.During heating, when body to be marked When temperature reaches Curie temperature, itself both do not have magnetism, and coercive force also becomes zero.And at this point, magnetic print has not yet been reached The Curie temperature of chapter material still has magnetism, can provide external magnetic field to magnetize body to be marked.Under this magnetic fields, to The direction of magnetization for marking body can be along this magnetic direction.As temperature gradually cools down, it is finally completed magnetization.

Claims (9)

1. the permanent magnet magnetization method based on magnetic seal transcription technology, it is characterised in that steps are as follows:
1) magnetic seal and body to be marked are prepared;Wherein, the Curie temperature of the permanent magnetic thin film of the magnetic seal is higher than body to be marked The Curie temperature of permanent magnetic thin film;
2) the magnetic seal prepared is bonded with body to be marked, i.e. the lower surface of the permanent magnetic thin film of magnetic seal and body to be marked The upper surface of permanent magnetic thin film be bonded, then heated, heating temperature rises to the Curie of the permanent magnetic thin film of body to be marked Temperature, then gradually anneal, thus by the permanent magnetic thin film of the magnetic pattern transcription on the permanent magnetic thin film of magnetic seal to body to be marked.
2. the permanent magnet magnetization method according to claim 1 based on magnetic seal transcription technology, it is characterised in that: the magnetic Seal includes the permanent magnetic thin film of top substrate layer and the carrying magnetic pattern positioned at lower layer.
3. the permanent magnet magnetization method according to claim 2 based on magnetic seal transcription technology, it is characterised in that: the band The permanent magnetic thin film of magnetic pattern uses shirt cobalt rare-earth permanent magnet.
4. the permanent magnet magnetization method according to claim 2 or 3 based on magnetic seal transcription technology, it is characterised in that: institute Top substrate layer is stated using quartz base plate.
5. the permanent magnet magnetization method according to claim 4 based on magnetic seal transcription technology, it is characterised in that: the magnetic Seal is made of laser thermally assisted magnetic technology, required magnetic pattern is written in the permanent magnetic thin film of magnetic seal.
6. the permanent magnet magnetization method according to claim 1 based on magnetic seal transcription technology, it is characterised in that: it is described to Marking body includes underlying substrate and the permanent magnetic thin film positioned at upper layer.
7. the permanent magnet magnetization method according to claim 6 based on magnetic seal transcription technology, it is characterised in that: it is described to The permanent magnetic thin film for marking body selects Fe-B rare-earth permanent magnet.
8. the permanent magnet magnetization method according to claim 6 or 7 based on magnetic seal transcription technology, it is characterised in that: institute Underlying substrate is stated using any substrate.
9. the permanent magnet magnetization method according to claim 1 based on magnetic seal transcription technology, it is characterised in that: step 2 In, the heating temperature is greater than the Curie temperature of NdFeB, and heating temperature is less than the Curie temperature of SmCo.
CN201811325924.3A 2018-11-08 2018-11-08 Permanent magnet magnetizing method based on magnetic seal transfer technology Expired - Fee Related CN109585120B (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201811325924.3A CN109585120B (en) 2018-11-08 2018-11-08 Permanent magnet magnetizing method based on magnetic seal transfer technology

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201811325924.3A CN109585120B (en) 2018-11-08 2018-11-08 Permanent magnet magnetizing method based on magnetic seal transfer technology

Publications (2)

Publication Number Publication Date
CN109585120A true CN109585120A (en) 2019-04-05
CN109585120B CN109585120B (en) 2021-02-26

Family

ID=65921834

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201811325924.3A Expired - Fee Related CN109585120B (en) 2018-11-08 2018-11-08 Permanent magnet magnetizing method based on magnetic seal transfer technology

Country Status (1)

Country Link
CN (1) CN109585120B (en)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN114141470A (en) * 2021-11-29 2022-03-04 中国工程物理研究院电子工程研究所 Micro-area magnetizing device and method based on MEMS (micro-electromechanical systems) micro-coil

Citations (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH0669034A (en) * 1992-08-17 1994-03-11 Daido Steel Co Ltd Magnetizing coil for rodlike multipolar magnet and magnetizing device thereof
CN1755387A (en) * 2004-09-28 2006-04-05 雅马哈株式会社 Magnetic sensor using giant magnetoresistive elements and method for manufacturing the same
CN1969210A (en) * 2004-02-12 2007-05-23 帕诺拉马实验室有限公司 Structured waveguide including holding bounding region
CN101202145A (en) * 2007-10-30 2008-06-18 电子科技大学 Transverse exchange-coupled magnetic information storage medium material and preparation method thereof
CN102804291A (en) * 2009-06-02 2012-11-28 相关磁学研究有限公司 A field emission system and method
WO2016053379A1 (en) * 2014-09-29 2016-04-07 Apple Inc. Method for magnetizing multiple zones in a monolithic piece of magnetic material
US20160180874A1 (en) * 2014-12-22 2016-06-23 Ming Chi University Of Technology Hard magnetic alloy thin film used in high density perpendicular magnetic recording medium
CN105925937A (en) * 2016-06-26 2016-09-07 彭晓领 Preparation method of orientation magnetic films
CN108028128A (en) * 2015-09-21 2018-05-11 高通股份有限公司 Programmable magnet orientation in magnetic array

Patent Citations (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH0669034A (en) * 1992-08-17 1994-03-11 Daido Steel Co Ltd Magnetizing coil for rodlike multipolar magnet and magnetizing device thereof
CN1969210A (en) * 2004-02-12 2007-05-23 帕诺拉马实验室有限公司 Structured waveguide including holding bounding region
CN1755387A (en) * 2004-09-28 2006-04-05 雅马哈株式会社 Magnetic sensor using giant magnetoresistive elements and method for manufacturing the same
CN101202145A (en) * 2007-10-30 2008-06-18 电子科技大学 Transverse exchange-coupled magnetic information storage medium material and preparation method thereof
CN102804291A (en) * 2009-06-02 2012-11-28 相关磁学研究有限公司 A field emission system and method
WO2016053379A1 (en) * 2014-09-29 2016-04-07 Apple Inc. Method for magnetizing multiple zones in a monolithic piece of magnetic material
US20160180874A1 (en) * 2014-12-22 2016-06-23 Ming Chi University Of Technology Hard magnetic alloy thin film used in high density perpendicular magnetic recording medium
CN108028128A (en) * 2015-09-21 2018-05-11 高通股份有限公司 Programmable magnet orientation in magnetic array
CN105925937A (en) * 2016-06-26 2016-09-07 彭晓领 Preparation method of orientation magnetic films

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
RYOGEN FUJIWARA等: ""Micromagnetization patterning of sputtered NdFeB/Ta multilayered films utilizing laser assisted heating"", 《 SENSORS AND ACTUATORS》 *

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN114141470A (en) * 2021-11-29 2022-03-04 中国工程物理研究院电子工程研究所 Micro-area magnetizing device and method based on MEMS (micro-electromechanical systems) micro-coil

Also Published As

Publication number Publication date
CN109585120B (en) 2021-02-26

Similar Documents

Publication Publication Date Title
Chin Permanent magnet films for applications in microelectromechanical systems
Li et al. Most frequently asked questions about the coercivity of Nd-Fe-B permanent magnets
JP3099066B1 (en) Manufacturing method of thin film structure
CN109585120A (en) Permanent magnet magnetization method based on magnetic seal transcription technology
Guan et al. Magnetic composite electroplating for depositing micromagnets
Keller et al. Batch fabrication of 50 μm-thick anisotropic Nd–Fe–B micro-magnets
Hrabec et al. Magnetization reversal in composition-controlled Gd1–xCox ferrimagnetic films close to compensation composition
Wang et al. Thickness and substrate effects on the perpendicular magnetic properties of ultra-thin TbFeCo films
Capraro et al. Barium ferrite thick films for microwave applications
Annadurai et al. Stress analysis, structure and magnetic properties of sputter deposited Ni–Mn–Ga ferromagnetic shape memory thin films
Zare et al. Deposition of magnetoelectric hexaferrite thin films on substrates of silicon
Wang et al. Thermal degradation behavior of amorphous GdFeCo alloy films with perpendicular anisotropy
Liu et al. Coercivity enhancement of sputtered (La, Nd, Dy)-Fe–Co–B multilayers by inserting Ta space layers
Wang et al. A simple method for tuning perpendicular magnetic properties of ultra-thin TbFeCo films
CN108682733B (en) A method of enhancing unusual Nernst effect
Ghasemi The role of annealing temperature on the structural and magnetic consequences of Ta/PrFeB/Ta thin films processed by rapid thermal annealing
Han et al. Microlinear Halbach array of thick-film Nd–Fe–B magnets utilizing local laser irradiation and a direction-changeable external magnetic field
Lileev et al. Properties of hard magnetic Nd–Fe–B films versus different sputtering conditions
JPH1074020A (en) Magnetic recording medium and its production as well as magnetic printer making use of the same
CN105390265B (en) Method for improving performance of rare-earth-iron-boron permanent magnet material
EP1887568B1 (en) Heat assisted magnetic recording medium and method for fabricating the same
CN104064350B (en) A kind of preparation method of the thin magnetic film with positive magnetic anisotropy temperature coefficient
CN104404347A (en) Method for preparing gradient magnetostriction material in situ
CN104810146A (en) Rapid annealing method of ferrite substrate permanent magnetic thin film
Zheng et al. Properties of NdFeB film grown on silicon substrate by PLD under external magnetic field

Legal Events

Date Code Title Description
PB01 Publication
PB01 Publication
SE01 Entry into force of request for substantive examination
SE01 Entry into force of request for substantive examination
GR01 Patent grant
GR01 Patent grant
CF01 Termination of patent right due to non-payment of annual fee
CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20210226

Termination date: 20211108