CN109568214A - A kind of passion fruit shell extract preparation method - Google Patents
A kind of passion fruit shell extract preparation method Download PDFInfo
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- CN109568214A CN109568214A CN201910050706.1A CN201910050706A CN109568214A CN 109568214 A CN109568214 A CN 109568214A CN 201910050706 A CN201910050706 A CN 201910050706A CN 109568214 A CN109568214 A CN 109568214A
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- 244000288157 Passiflora edulis Species 0.000 title claims abstract description 80
- 235000000370 Passiflora edulis Nutrition 0.000 title claims abstract description 80
- 239000000284 extract Substances 0.000 title claims abstract description 28
- 238000002360 preparation method Methods 0.000 title claims abstract description 17
- 239000012141 concentrate Substances 0.000 claims abstract description 17
- 239000000843 powder Substances 0.000 claims abstract description 15
- 239000013049 sediment Substances 0.000 claims abstract description 13
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 30
- 239000007788 liquid Substances 0.000 claims description 24
- 239000000706 filtrate Substances 0.000 claims description 19
- KWYUFKZDYYNOTN-UHFFFAOYSA-M Potassium hydroxide Chemical compound [OH-].[K+] KWYUFKZDYYNOTN-UHFFFAOYSA-M 0.000 claims description 12
- 238000000605 extraction Methods 0.000 claims description 11
- 238000010438 heat treatment Methods 0.000 claims description 8
- 238000001914 filtration Methods 0.000 claims description 7
- 238000000874 microwave-assisted extraction Methods 0.000 claims description 7
- 239000000203 mixture Substances 0.000 claims description 7
- 238000000643 oven drying Methods 0.000 claims description 7
- 238000010792 warming Methods 0.000 claims description 6
- 230000001476 alcoholic effect Effects 0.000 claims description 2
- 238000004108 freeze drying Methods 0.000 abstract description 3
- 238000007873 sieving Methods 0.000 abstract 1
- 235000019441 ethanol Nutrition 0.000 description 11
- 238000000034 method Methods 0.000 description 9
- 235000013399 edible fruits Nutrition 0.000 description 7
- 238000011084 recovery Methods 0.000 description 7
- 229930003944 flavone Natural products 0.000 description 5
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- 238000005265 energy consumption Methods 0.000 description 4
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- GVJHHUAWPYXKBD-UHFFFAOYSA-N (±)-α-Tocopherol Chemical compound OC1=C(C)C(C)=C2OC(CCCC(C)CCCC(C)CCCC(C)C)(C)CCC2=C1C GVJHHUAWPYXKBD-UHFFFAOYSA-N 0.000 description 2
- 208000024172 Cardiovascular disease Diseases 0.000 description 2
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- CUXYLFPMQMFGPL-UHFFFAOYSA-N (9Z,11E,13E)-9,11,13-Octadecatrienoic acid Natural products CCCCC=CC=CC=CCCCCCCCC(O)=O CUXYLFPMQMFGPL-UHFFFAOYSA-N 0.000 description 1
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- LQJBNNIYVWPHFW-UHFFFAOYSA-N 20:1omega9c fatty acid Natural products CCCCCCCCCCC=CCCCCCCCC(O)=O LQJBNNIYVWPHFW-UHFFFAOYSA-N 0.000 description 1
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- 206010011224 Cough Diseases 0.000 description 1
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- 206010062717 Increased upper airway secretion Diseases 0.000 description 1
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- ZQPPMHVWECSIRJ-UHFFFAOYSA-N Oleic acid Natural products CCCCCCCCC=CCCCCCCCC(O)=O ZQPPMHVWECSIRJ-UHFFFAOYSA-N 0.000 description 1
- 239000005642 Oleic acid Substances 0.000 description 1
- 239000004952 Polyamide Substances 0.000 description 1
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- CUXYLFPMQMFGPL-SUTYWZMXSA-N all-trans-octadeca-9,11,13-trienoic acid Chemical compound CCCC\C=C\C=C\C=C\CCCCCCCC(O)=O CUXYLFPMQMFGPL-SUTYWZMXSA-N 0.000 description 1
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- 238000009835 boiling Methods 0.000 description 1
- 239000006227 byproduct Substances 0.000 description 1
- 150000001720 carbohydrates Chemical class 0.000 description 1
- 235000021466 carotenoid Nutrition 0.000 description 1
- 150000001747 carotenoids Chemical class 0.000 description 1
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- 150000001875 compounds Chemical class 0.000 description 1
- 235000009508 confectionery Nutrition 0.000 description 1
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- 206010012601 diabetes mellitus Diseases 0.000 description 1
- 235000014113 dietary fatty acids Nutrition 0.000 description 1
- 235000013325 dietary fiber Nutrition 0.000 description 1
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- 229930195729 fatty acid Natural products 0.000 description 1
- 150000004665 fatty acids Chemical class 0.000 description 1
- 230000035558 fertility Effects 0.000 description 1
- 239000003337 fertilizer Substances 0.000 description 1
- 239000000835 fiber Substances 0.000 description 1
- 235000013305 food Nutrition 0.000 description 1
- 235000013373 food additive Nutrition 0.000 description 1
- 239000002778 food additive Substances 0.000 description 1
- WIGCFUFOHFEKBI-UHFFFAOYSA-N gamma-tocopherol Natural products CC(C)CCCC(C)CCCC(C)CCCC1CCC2C(C)C(O)C(C)C(C)C2O1 WIGCFUFOHFEKBI-UHFFFAOYSA-N 0.000 description 1
- 230000004054 inflammatory process Effects 0.000 description 1
- 230000000968 intestinal effect Effects 0.000 description 1
- QXJSBBXBKPUZAA-UHFFFAOYSA-N isooleic acid Natural products CCCCCCCC=CCCCCCCCCC(O)=O QXJSBBXBKPUZAA-UHFFFAOYSA-N 0.000 description 1
- 239000010977 jade Substances 0.000 description 1
- 210000003734 kidney Anatomy 0.000 description 1
- 238000002386 leaching Methods 0.000 description 1
- 229960004488 linolenic acid Drugs 0.000 description 1
- KQQKGWQCNNTQJW-UHFFFAOYSA-N linolenic acid Natural products CC=CCCC=CCC=CCCCCCCCC(O)=O KQQKGWQCNNTQJW-UHFFFAOYSA-N 0.000 description 1
- 125000005481 linolenic acid group Chemical group 0.000 description 1
- 239000011344 liquid material Substances 0.000 description 1
- 239000011159 matrix material Substances 0.000 description 1
- 229910052751 metal Inorganic materials 0.000 description 1
- 230000000474 nursing effect Effects 0.000 description 1
- ZQPPMHVWECSIRJ-KTKRTIGZSA-N oleic acid Chemical compound CCCCCCCC\C=C/CCCCCCCC(O)=O ZQPPMHVWECSIRJ-KTKRTIGZSA-N 0.000 description 1
- 235000021313 oleic acid Nutrition 0.000 description 1
- 239000001814 pectin Substances 0.000 description 1
- 229920001277 pectin Polymers 0.000 description 1
- 235000010987 pectin Nutrition 0.000 description 1
- 208000026435 phlegm Diseases 0.000 description 1
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- 229920002647 polyamide Polymers 0.000 description 1
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- 230000002936 tranquilizing effect Effects 0.000 description 1
- 230000001228 trophic effect Effects 0.000 description 1
- 238000002137 ultrasound extraction Methods 0.000 description 1
- 235000021122 unsaturated fatty acids Nutrition 0.000 description 1
- 150000004670 unsaturated fatty acids Chemical class 0.000 description 1
- 235000015112 vegetable and seed oil Nutrition 0.000 description 1
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- 229940046009 vitamin E Drugs 0.000 description 1
- 239000011709 vitamin E Substances 0.000 description 1
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Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L19/00—Products from fruits or vegetables; Preparation or treatment thereof
- A23L19/03—Products from fruits or vegetables; Preparation or treatment thereof consisting of whole pieces or fragments without mashing the original pieces
- A23L19/07—Fruit waste products, e.g. from citrus peel or seeds
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
- A23L33/10—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives
- A23L33/105—Plant extracts, their artificial duplicates or their derivatives
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L5/00—Preparation or treatment of foods or foodstuffs, in general; Food or foodstuffs obtained thereby; Materials therefor
- A23L5/10—General methods of cooking foods, e.g. by roasting or frying
- A23L5/13—General methods of cooking foods, e.g. by roasting or frying using water or steam
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L5/00—Preparation or treatment of foods or foodstuffs, in general; Food or foodstuffs obtained thereby; Materials therefor
- A23L5/30—Physical treatment, e.g. electrical or magnetic means, wave energy or irradiation
- A23L5/34—Physical treatment, e.g. electrical or magnetic means, wave energy or irradiation using microwaves
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/08—Anti-ageing preparations
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/10—General cosmetic use
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- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Nutrition Science (AREA)
- Chemical & Material Sciences (AREA)
- Food Science & Technology (AREA)
- Polymers & Plastics (AREA)
- Public Health (AREA)
- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
- Veterinary Medicine (AREA)
- Botany (AREA)
- Mycology (AREA)
- Dermatology (AREA)
- Microbiology (AREA)
- Birds (AREA)
- Epidemiology (AREA)
- Biotechnology (AREA)
- Gerontology & Geriatric Medicine (AREA)
- Medicines Containing Plant Substances (AREA)
Abstract
It the invention discloses a kind of passion fruit shell extract preparation method, mainly comprises the steps that and strips passion fruit shell, dry, grind sieving；A certain amount of passion fruit shell powder is weighed again, is extracted respectively using two sections of boiling-microwave, and freeze-drying obtains a kind of passion fruit shell extract after finally collecting obtained sediment and concentrate merging.
Description
Technical field
The invention belongs to plant resources extractive technique fields, and in particular to a kind of passion fruit shell extract preparation method.
Background technique
Passion fruit (Passion Flower) is also known as passionflower, passion fruit, and the perennial herbaceous stem in the torrid zone to half woody climber is climbed
Accessory fruit tree originates in Australia and Brazil, subtropical and tropical zones is now distributed widely in, at present in China Guangdong, Guangxi, river
There is cultivation on the ground such as Soviet Union, Anhui, Hunan, Guizhou, Fujian, Yunnan, Hainan, and with fastest developing speed with Guangxi province.Passion fruit fruit juice tool
There is the fragrance of the pleasant of the various fruits such as guava, pineapple, banana, mango, apple, smoked plum.It is reported that passion fruit has
Promote the production of body fluid to quench thirst, eliminate fatigue, refresh oneself sober up, skin-protecting face nursing, weight-reducing defaecation, clearing away the lungheat and moisturizing, preventing phlegm from forming and stopping coughing, enriching yin and nourishing kidney, anti-cancer
A variety of medicines and health protection functions such as anti-ageing, tranquilizing the mind antianxiety, the antibacterial, prevention and cure of cardiovascular disease of antalgic and inflammation relieving, thus also it is known as " fruit
In king ".
In the market, passion fruit is mainly used for making beverage, the leaching of ice fine jade and candy.It is annual with passion fruit in beverage industry
The production of fruit juice can generate a large amount of agricultural and sideline product, wherein 40% is passion fruit residue, 90% is that passion fruit shell and hundred are fragrant in residue
Fruit seed.These byproducts have corresponding functional component and utility value, such as pigment, carbohydrate, more junket classes, dietary fiber, have
Machine acid, fragrance etc. can be used as food additives, and these ingredients have inoxidizability and bacteriostatic activity, can be used for pre- anti-cancer
Disease, cardiovascular disease and diabetes etc..
The root and leaf of passion fruit have antianxiety, calm, diuresis, analgesia, the biological effects such as antibiotic property.Leaf and kind
Seed extract contains carotenoid, more junket and vitamin E, has antioxidant activity effect.Contain 55% in passion fruit fruit
Pericarp, 34% fruit juice and 11% fruit seed.Passion fruit seed unsaturated fatty acid rich in, cellulose, fertility age, class are recklessly
Radish element, metallic element etc., insoluble fibre therein can promote function of intestinal canal as a kind of new functional components.Hundred is fragrant
Fruit seed oil content is up to 26%, and wherein fatty acid main component is linolenic acid, linoleic acid, oleic acid, eleostearic acid etc..Passion fruit shell
In rich in there is the medicinal ingredients such as pectin, alkaloid, flavones, polysaccharide, polyphenols, wherein tannin and flavones ingredient content
It is higher.
Microwave abstracting is certain organic components and the matrix made in solid or semisolid substance using the effect of electromagnetic field
It efficiently separates, and is able to maintain a kind of separation method of the script compound state of analysis object.Microwave refers to frequency 300,000,000
The conspicuous electromagnetic wave to 300 gigahertzs.Microwave abstracting mainly has few reagent dosage, energy saving, the small, homogeneous heating of pollution and thermal effect
Rate is higher, process is easily controllable, processing batch is larger, and extraction efficiency is high, time saving, selectivity is preferable.Based on the above advantage, microwave
Extraction is often known as " green extraction process ".
CN201711253854.0 discloses a kind of preparation method with flavones in functional passion fruit shell, tool
Body is to choose the rotten passion fruit shell of fresh nothing, cleans, dries under 70~80 DEG C of 12~16h of oven drying or sunlight, crushes
Machine smashes it through 40 meshes, obtains passion fruit shell powder；Passion fruit shell powder and the ethyl alcohol of 40~70% volume fractions are pressed into liquid
Material is mixed than 30~60mL/g ratio, and mixture is put into ultrasonic extraction instrument after 1~2h of stirring, ultrasonic power is arranged
200~400w handles 30~60min of time, 40~60 DEG C of Extracting temperature, extracting solution is filtered, filtrate vacuum at 50 DEG C is dense
It is reduced to the 1/5 of original volume；Concentrate is crossed into polyamide column, be first eluted to distilled water it is colourless, then with 60~80% ethanol elutions 6
~8 times of column volumes collect eluent；Merge the eluent collected and be concentrated in vacuo to the 1/5 of original volume at 50 DEG C, by concentrate
At -30 DEG C to -10 DEG C freeze-drying 12~for 24 hours, after crushing 4 DEG C preservation；The preparation method recovery rate is high, at low cost, energy consumption
Low, environmental protection, by purifying, purity improves the flavones of preparation, and has good inoxidizability
CN201810180398.X the invention discloses a kind of passion fruit shell extract and preparation method thereof, the method includes
Following steps: by passion fruit shell clean be placed in extractor, be added solvent and be heated to the temperature in extractor be 40~
80 DEG C, cohobation 3~8 hours；Then solution and the filtering in extractor are collected, filtered fluid is obtained；Filtered fluid is concentrated into
The 10~30% of filtered fluid volume, obtain concentrate；Then concentrate is subjected to vacuum spray drying, obtains the extraction of passion fruit shell
Object.The method of the present invention can save passion fruit fragrance from damage to greatest extent, and the passion fruit shell extract of production can directly take orally,
Beverage can be brewed into take, or be supplied to food processing enterprises and used as flavouring or trophic function raw material.
Foregoing invention is primarily present that reagent dosage is big, the time is longer, energy consumption is higher, extract component is single, effective ingredient amount
The disadvantages of few.
Summary of the invention
The object of the present invention is to provide a kind of passion fruit shell extract preparation method, preparation method recovery rate height, cost
Low, the features such as time is short, low energy consumption, environmental protection, a variety of objects such as flavones, polyphenol, polysaccharide and alkaloid are contained in the extract of preparation
Matter, can be used as health care product or cosmetic material uses, and have preferable bioactivity, inoxidizability, moisturizing water-retaining property and skin-friendly
Preferably easily absorb.
For realize foregoing invention purpose, the technical solution adopted by the present invention is as follows:
A kind of passion fruit shell extract preparation method, comprising the following steps:
(1) fresh passion fruit shell is stripped, the part that removal rots, goes bad cleans up；
(2) by passion fruit shell in 55~65 DEG C of oven dryings 18~for 24 hours, until moisture < 5%；
(3) 20~40 meshes are smashed it through through pulverizer, obtains passion fruit shell powder；
(4) a certain amount of above-mentioned steps 3 will be weighed) in passion fruit shell powder, be added solid-to-liquid ratio 1:5~10 1mol/L hydroxide
Potassium solution is warming up to 60~80 DEG C and keeps the temperature 0.5~1.5h again in rotary digester, then stops heating and is cooled to room temperature；
(5) by above-mentioned steps 4) mixture in digester pours out 95% second that liquid liquor ratio 1:3~5 are added after filtering in filtrate
Alcoholic solution, 20~40 min of water-bath at 40~60 DEG C of temperature are centrifuged 5~15min under 3000~5000r/min after taking-up, receive
Collect obtained sediment 1；
(6) by above-mentioned steps 4) passion fruit shell much filtrate in 80~90% ethanol solutions of its solid-to-liquid ratio 1:15~20 are added, adopt
With being heated to 70~80 DEG C of 5~10 min of extraction under 300W microwave power；
(7) by above-mentioned steps 6) filtrate after Microwave Extraction all merges, 0.5~1.0h is stood at 40~50 DEG C of temperature
Afterwards, it is concentrated in vacuo to the 1/5~1/10 of original volume at 50~65 DEG C, obtains concentrate 2.
(8) obtained sediment 1 will be collected and 20~45h is lyophilized at -20 DEG C~-5 DEG C after the merging of concentrate 2, i.e.,
Obtain a kind of passion fruit shell extract.
The beneficial effect of the present invention compared with the existing technology is:
(1) present invention extracts passion fruit shell using two sections of boiling-microwave method respectively, substantially increase in passion fruit shell effectively at
The recovery rate divided；
(2) bioactivity of effective component is greatly saved by freeze-drying；
(3) this method step is simple, and solvent usage can also be re-used less by distillation, can greatly reduce production cost；
(4) boiling and microwave heating are uniformly in boiling-microwave method and the thermal efficiency is higher, the time is short, low energy consumption, process is easy to control
System, extraction efficiency are high；
(5) present invention is raw material using passion fruit shell, is turned waste into wealth, and added value is improved, and the residue extracted can also make fertilizer
Material or feed are used for agricultural production.
Specific embodiment
The present invention is described in further details below by example, these examples are only used to illustrate the present invention, and unlimited
The scope of the present invention processed.
Embodiment 1
A kind of passion fruit shell extract preparation method, comprising the following steps:
(1) fresh passion fruit shell is stripped, the part that removal rots, goes bad cleans up；
(2) by passion fruit shell 55 DEG C of oven dryings for 24 hours, until moisture < 5%；
(3) 20 meshes are smashed it through through pulverizer, obtains passion fruit shell powder；
(4) a certain amount of above-mentioned steps 3 will be weighed) in passion fruit shell powder, be added solid-to-liquid ratio 1:5 1mol/L potassium hydroxide it is molten
Liquid is warming up to 80 DEG C and keeps the temperature 0.5h again in rotary digester, then stops heating and is cooled to room temperature；
(5) by above-mentioned steps 4) mixture in digester pour out be added in filtrate after filtering liquid liquor ratio 1:3 95% ethyl alcohol it is molten
Liquid, 20 min of water-bath, is centrifuged 15min under 3000r/min after taking-up at 40 DEG C of temperature, the sediment 1 collected；
(6) by above-mentioned steps 4) passion fruit shell much filtrate in 80% ethanol solution of its solid-to-liquid ratio 1:15 is added, it is micro- using 300W
70 DEG C of 5 min of extraction are heated under wave power；
(7) by above-mentioned steps 6) filtrate after Microwave Extraction all merges, after standing 0.5h at 40 DEG C of temperature, at 50 DEG C
Under be concentrated in vacuo to the 1/5 of original volume, obtain concentrate 2.
(8) by above-mentioned steps 5) and above-mentioned steps 7) collect obtained sediment 1 and concentrate 2 merge after at -20 DEG C
20h is lyophilized to get a kind of passion fruit shell extract is arrived.
Passion fruit shell extract recovery rate is 10.5% in the present embodiment.
Embodiment 2
A kind of passion fruit shell extract preparation method, comprising the following steps:
(1) fresh passion fruit shell is stripped, the part that removal rots, goes bad cleans up；
(2) by passion fruit shell in 65 DEG C of oven drying 18h, until moisture < 5%；
(3) 40 meshes are smashed it through through pulverizer, obtains passion fruit shell powder；
(4) a certain amount of above-mentioned steps 3 will be weighed) in passion fruit shell powder, be added solid-to-liquid ratio 1:10 1mol/L potassium hydroxide
Solution is warming up to 80 DEG C and keeps the temperature 1.5h again in rotary digester, then stops heating and is cooled to room temperature；
(5) by above-mentioned steps 4) mixture in digester pour out be added in filtrate after filtering liquid liquor ratio 1:5 95% ethyl alcohol it is molten
Liquid, 20 min of water-bath under temperature 60 C, is centrifuged 5min under 5000r/min after taking-up, the sediment 1 collected；
(6) by above-mentioned steps 4) passion fruit shell much filtrate in 90% ethanol solution of its solid-to-liquid ratio 1:20 is added, using 300W
80 DEG C of 5 min of extraction are heated under microwave power；
(7) by above-mentioned steps 6) filtrate after Microwave Extraction all merges, after standing 1.0h under temperature 50 C, at 65 DEG C
Under be concentrated in vacuo to the 1/10 of original volume, obtain concentrate 2.
(8) by above-mentioned steps 5) and above-mentioned steps 7) collect obtained sediment 1 and freeze at -5 DEG C after the merging of concentrate 2
45h is done to get a kind of passion fruit shell extract is arrived.
Passion fruit shell extract recovery rate is 12.1% in the present embodiment.
Embodiment 3
A kind of passion fruit shell extract preparation method, comprising the following steps:
(1) fresh passion fruit shell is stripped, the part that removal rots, goes bad cleans up；
(2) by passion fruit shell in 60 DEG C of oven drying 20h, until moisture < 5%；
(3) 30 meshes are smashed it through through pulverizer, obtains passion fruit shell powder；
(4) a certain amount of above-mentioned steps 3 will be weighed) in passion fruit shell powder, be added solid-to-liquid ratio 1:8 1mol/L potassium hydroxide it is molten
Liquid is warming up to 70 DEG C and keeps the temperature 1.0h again in rotary digester, then stops heating and is cooled to room temperature；
(5) by above-mentioned steps 4) mixture in digester pour out be added in filtrate after filtering liquid liquor ratio 1:4 95% ethyl alcohol it is molten
Liquid, 30 min of water-bath under temperature 50 C, is centrifuged 10min under 4000r/min after taking-up, the sediment 1 collected；
(6) by above-mentioned steps 4) passion fruit shell much filtrate in 85% ethanol solution of its solid-to-liquid ratio 1:20 is added, it is micro- using 300W
75 DEG C of 8 min of extraction are heated under wave power；
(7) by above-mentioned steps 6) filtrate after Microwave Extraction all merges, after standing 0.5h under temperature 45 C, at 55 DEG C
Under be concentrated in vacuo to the 1/8 of original volume, obtain concentrate 2.
(8) by above-mentioned steps 5) and above-mentioned steps 7) collect obtained sediment 1 and concentrate 2 merge after at -15 DEG C
30h is lyophilized to get a kind of passion fruit shell extract is arrived.
Passion fruit shell extract recovery rate is 10.3% in the present embodiment.
Embodiment 4
A kind of passion fruit shell extract preparation method, comprising the following steps:
(1) fresh passion fruit shell is stripped, the part that removal rots, goes bad cleans up；
(2) by passion fruit shell in 60 DEG C of oven drying 20h, until moisture < 5%；
(3) 20 meshes are smashed it through through pulverizer, obtains passion fruit shell powder；
(4) a certain amount of above-mentioned steps 3 will be weighed) in passion fruit shell powder, be added solid-to-liquid ratio 1:7 1mol/L potassium hydroxide it is molten
Liquid is warming up to 70 DEG C and keeps the temperature 0.5h again in rotary digester, then stops heating and is cooled to room temperature；
(5) by above-mentioned steps 4) mixture in digester pours out 95% ethyl alcohol that liquid liquor ratio 1:5 is added after filtering in filtrate
Solution, the water-bath 20min under temperature 45 C, is centrifuged 10min under 4000r/min after taking-up, the sediment 1 collected；
(6) by above-mentioned steps 4) passion fruit shell much filtrate in 90% ethanol solution of its solid-to-liquid ratio 1:15 is added, it is micro- using 300W
75 DEG C of extraction 6min are heated under wave power；
(7) by above-mentioned steps 6) filtrate after Microwave Extraction all merges, after standing 0.8h under temperature 45 C, at 56 DEG C
Under be concentrated in vacuo to the 1/7 of original volume, obtain concentrate 2.
(8) by above-mentioned steps 5) and above-mentioned steps 7) collect obtained sediment 1 and concentrate 2 merge after at -10 DEG C
40h is lyophilized to get a kind of passion fruit shell extract is arrived.
Passion fruit shell extract recovery rate is 11.5% in the present embodiment.
Claims (1)
1. a kind of passion fruit shell extract preparation method, which comprises the following steps:
(1) fresh passion fruit shell is stripped, the part that removal rots, goes bad cleans up；
(2) by passion fruit shell in 55~65 DEG C of oven dryings 18~for 24 hours, until moisture < 5%；
(3) 20~40 meshes are smashed it through through pulverizer, obtains passion fruit shell powder；
(4) a certain amount of above-mentioned steps 3 will be weighed) in passion fruit shell powder, be added solid-to-liquid ratio 1:5~10 1mol/L hydroxide
Potassium solution is warming up to 60~80 DEG C and keeps the temperature 0.5~1.5h again in rotary digester, then stops heating and is cooled to room temperature；
(5) by above-mentioned steps 4) mixture in digester pours out 95% second that liquid liquor ratio 1:3~5 are added after filtering in filtrate
Alcoholic solution, 20~40 min of water-bath at 40~60 DEG C of temperature are centrifuged 5~15min under 3000~5000r/min after taking-up, receive
Collect obtained sediment 1；
(6) by above-mentioned steps 4) passion fruit shell much filtrate in 80~90% ethanol solutions of its solid-to-liquid ratio 1:15~20 are added, adopt
With being heated to 70~80 DEG C of 5~10 min of extraction under 300W microwave power；
(7) by above-mentioned steps 6) filtrate after Microwave Extraction all merges, 0.5~1.0h is stood at 40~50 DEG C of temperature
Afterwards, it is concentrated in vacuo to the 1/5~1/10 of original volume at 50~65 DEG C, obtains concentrate 2；
(8) will collect obtained sediment 1 and concentrate 2 merge after 20~45h is lyophilized at -20 DEG C~-5 DEG C to get to one
Kind passion fruit shell extract.
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN113180146A (en) * | 2021-04-30 | 2021-07-30 | 武汉轻工大学 | Preparation method of passion fruit shell extracting solution and livestock and poultry breeding method |
| CN114391650A (en) * | 2022-02-09 | 2022-04-26 | 麦迪尔(厦门)生物科技有限公司 | Durian shell full-utilization method, durian shell powder prepared by using durian shell full-utilization method and application of durian shell powder |
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| CN113180146A (en) * | 2021-04-30 | 2021-07-30 | 武汉轻工大学 | Preparation method of passion fruit shell extracting solution and livestock and poultry breeding method |
| CN114391650A (en) * | 2022-02-09 | 2022-04-26 | 麦迪尔(厦门)生物科技有限公司 | Durian shell full-utilization method, durian shell powder prepared by using durian shell full-utilization method and application of durian shell powder |
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