CN109528579B - Moisturizing and repairing emulsion spray and preparation method thereof - Google Patents
Moisturizing and repairing emulsion spray and preparation method thereof Download PDFInfo
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Abstract
The invention discloses moisturizing and repairing emulsion spray and a preparation method thereof, belonging to the technical field of cosmetics and comprising the following components in percentage by mass: 2.5 to 7.5 percent of emulsifier, 4 to 14 percent of emollient, 0.25 to 1.35 percent of preservative, 1 to 7 percent of efficacy additive, 0.05 to 0.2 percent of anti-inflammatory agent, 5 to 29 percent of humectant, 0.02 to 0.2 percent of chelating agent, 0.85 to 2.2 percent of thickening agent, 0.19 to 0.42 percent of pH regulator, 0.01 to 0.03 percent of flavoring agent and the balance of deionized water; the efficacy additive is prepared by compounding a mixture of jojoba oil and pomegranate flower extract and tetrahydro-methyl pyrimidine carboxylic acid in a mass ratio of (0.5-4) to (0.5-3). The emulsion spray of the invention has good moisturizing and repairing effects.
Description
Technical Field
The invention belongs to the technical field of cosmetics, and particularly relates to moisturizing and repairing emulsion spray and a preparation method thereof.
Background
With the improvement of living standards, people pay more and more attention to beauty makeup. Cosmetics sold on the market are various in types, such as lipstick, emulsion spray, facial cleanser, sunscreen lotion and the like. However, existing emulsion sprays suffer from several disadvantages: has poor moisturizing and repairing effects.
Therefore, there is a need for an improved emulsion spray in the hope of a better moisturizing and healing effect.
Disclosure of Invention
The invention aims to overcome the defects in the prior art and provides the moisturizing and repairing emulsion spray and the preparation method thereof.
In order to achieve the purpose, the invention adopts the technical scheme that: the moisturizing and repairing emulsion spray comprises the following components in percentage by mass: 2.5-7.5% of emulsifier, 4-14% of emollient, 0.25-1.35% of preservative, 1-7% of efficacy additive, 0.05-0.2% of anti-inflammatory agent, 5-29% of humectant, 0.02-0.2% of chelating agent, 0.85-2.2% of thickening agent, 0.19-0.42% of pH regulator, 0.01-0.03% of flavoring agent and the balance of deionized water; the efficacy additive is prepared by compounding a mixture of jojoba oil and pomegranate flower extract and tetrahydro-methyl pyrimidine carboxylic acid in a mass ratio of (0.5-4) to (0.5-3).
The mixture of the jojoba oil and the pomegranate flower extract can preserve moisture and repair: can repair skin barrier, has strong free radical scavenging ability, improves hydrophilic membrane and cutin, and has effects of keeping moisture and repairing. The tetrahydro-methyl pyrimidine carboxylic acid can enhance skin immunity, accelerate cell repair, repair sunlight damage and save a water locking system, so that the cosmetic has moisturizing and repairing effects. The invention unexpectedly discovers that when the efficacy additive is compounded by the mixture of the jojoba oil and the pomegranate flower extract and the tetrahydro-methyl pyrimidine carboxylic acid, the 2 compositions synergistically increase the repair efficacy of the emulsion spray and can improve the moisturizing efficacy of the emulsion spray.
As an improvement of the technical scheme, the emulsifier is prepared by compounding a mixture of cetearyl olive oil and an olive oil sorbitol ester, a mixture of cetearyl alcohol and cetearyl glucoside and cetearyl alcohol according to the mass ratio of (1-3) to (0.5-1.5).
The hexadecyl-octadecyl olive oil and the olive oil sorbitol ester are obtained by esterifying hexadecyl-octadecyl alcohol, sorbitol and olive oil, and have good skin absorbability and moisture retention. The mixture of cetearyl alcohol and cetearyl glucoside is an O/W nonionic sugar based emulsifier with natural mild properties.
As an improvement of the technical scheme, the emollient is prepared by compounding polydimethylsiloxane, jojoba oil and a mixture of cyclopentasiloxane and cyclohexasiloxane in a mass ratio of (2-4) to (1-5).
The polydimethylsiloxane has the functions of lubricating performance and ultraviolet resistance and has good air permeability. Jojoba oil has soothing effect on allergic skin, and can restore vitality and luster to dry hair and dry wrinkle skin. When the emollient is compounded by dimethyl silicone polymer, jojoba oil, cyclopentasiloxane and cyclohexasiloxane according to the mass ratio of (2-4) to (1-5), the emollient can promote the skin of a human body to absorb emulsion spray, and can improve the moisturizing and repairing effects of the emulsion spray.
As an improvement of the technical scheme, the preservative is prepared by compounding 0.1-0.2%, 0.05-0.15% and 0.1-1% of methyl hydroxybenzoate, ethyl hydroxybenzoate and a mixture of phenoxyethanol and ethylhexylglycerin in percentage by mass in emulsion spraying.
As an improvement of the technical scheme, the humectant is prepared by compounding a sodium pyrrolidone carboxylic acid mixture, glycerol and 1, 3-butanediol in a mass ratio of (3-9) - (1-10), wherein the sodium pyrrolidone carboxylic acid mixture is prepared by compounding deionized water, glycerol, sodium pyrrolidone carboxylic acid, erythritol, a Chondrus crispus extract and xanthan gum.
Sodium pyrrolidone carboxylate (PCA-Na) has relatively strong hygroscopicity and can absorb moisture from air; the sodium pyrrolidone carboxylate mixture provides excellent smooth feeling and moisturizing effect to the cosmetic. When the humectant is compounded by sodium pyrrolidone carboxylate mixture, glycerin and 1, 3-butanediol in a mass ratio of (3-9): (1-10): 1-10), the above 3 compositions can obviously increase the effect of emulsion spraying.
As an improvement of the technical scheme, the thickening agent is prepared by compounding acrylic acid (ester)/behenyl alcohol polyether-25 methacrylate copolymer and xanthan gum according to the mass ratio of (0.8-2) to (0.05-0.2); the chelating agent is disodium ethylene diamine tetraacetate, the pH regulator is sodium hydroxide, the flavoring agent is essence, and the anti-inflammatory agent is 5-uroethyl lactam.
The acrylic acid (ester)/behenyl alcohol polyether-25 methacrylate copolymer has the characteristics of pseudoplastic shear thinning and instant paste recombination, can prepare directional spray to form uniformly dispersed liquid drops, and solves the problem that a material body with consistency in the market cannot be sprayed. 5-uroethyl lactam can promote wound healing, and has antibacterial and anti-inflammatory effects.
As an improvement of the technical scheme, the emulsion spray is composed of the following components in percentage by mass: 2.5-7.5% of emulsifier, 4-14% of emollient, 0.25-1.35% of preservative, 1-7% of efficacy additive, 0.05-0.2% of anti-inflammatory agent, 5-29% of humectant, 0.02-0.2% of chelating agent, 0.85-2.2% of thickening agent, 0.19-0.42% of pH regulator, 0.01-0.03% of flavoring agent and the balance of deionized water; the efficacy additive is prepared by compounding a mixture of jojoba oil and pomegranate flower extracts and tetrahydro-methyl pyrimidine carboxylic acid in a mass ratio of (0.5-4) - (0.5-3), the emulsifier is prepared by compounding a mixture of hexadecadecyl olive oil and olive oil sorbitol ester, a mixture of cetearyl alcohol and cetearyl glucoside and cetearyl alcohol in a mass ratio of (1-3) - (0.5-1.5), the emollient is prepared by compounding polydimethylsiloxane, jojoba oil and a mixture of cyclopentasiloxane and cyclohexasiloxane in a mass ratio of (2-4) - (1-5), the preservative is prepared by compounding a mixture of methylparaben, ethylparaben and a mixture of ethanol and ethylhexyl glycerol in an emulsion spray in a mass percentage of (0.1-0.2%), (0.05-0.15%), (0.1-1%), the humectant is compounded by sodium pyrrolidone carboxylate mixture, glycerin and 1, 3-butanediol in a mass ratio of (3-9) - (1-10), the sodium pyrrolidone carboxylate mixture is compounded by deionized water, glycerin, sodium pyrrolidone carboxylate, erythritol, a carrageen crispatus extract and xanthan gum, the thickener is compounded by acrylic acid (ester)/behenyl alcohol polyether-25 methacrylate copolymer and xanthan gum in a mass ratio of (0.8-2) - (0.05-0.2), the chelating agent is disodium ethylene diamine tetraacetate, the pH regulator is sodium hydroxide, the flavoring agent is essence, and the anti-inflammatory agent is 5-urethyl lactam.
As a further improvement of the technical scheme, the emulsion spray is composed of the following components in percentage by mass: 5% of emulsifier, 9% of emollient, 0.75% of preservative, 3% of efficacy additive, 0.1% of anti-inflammatory agent, 16% of humectant, 0.1% of chelating agent, 1.1% of thickening agent, 0.23% of pH regulator, 0.02% of aromatizer and the balance deionized water.
As a further improvement of the technical scheme, the efficacy additive is prepared by compounding a mixture of jojoba oil and pomegranate flower extract in a mass ratio of 2:1 and tetrahydro-methyl pyrimidine carboxylic acid; the emulsifier is prepared by compounding a mixture of hexadecyl-octadecyl olive oil and an olive oil sorbitol ester, a mixture of cetearyl alcohol and cetearyl glucoside and cetearyl alcohol in a mass ratio of 2:2: 1; the emollient is compounded by polydimethylsiloxane, jojoba oil and a mixture of cyclopentasiloxane and cyclohexasiloxane in a mass ratio of 3:3: 3; the preservative is prepared by compounding 0.15 percent, 0.1 percent and 0.5 percent of methyl hydroxybenzoate, ethylparaben and a mixture of phenoxyethanol and ethylhexyl glycerol in emulsion spray by mass percentage; the humectant is prepared by compounding a sodium pyrrolidone carboxylic acid mixture, glycerol and 1, 3-butanediol in a mass ratio of 6:5:5, wherein the sodium pyrrolidone carboxylic acid mixture is prepared by compounding deionized water, glycerol, sodium pyrrolidone carboxylic acid, erythritol, a Chondrus crispus extract and xanthan gum; the thickening agent is prepared by compounding acrylic acid (ester)/behenyl alcohol polyether-25 methacrylate copolymer and xanthan gum according to the mass ratio of 1: 0.1.
In addition, the invention also provides a preparation method of the emulsion spray, which comprises the following steps:
s1) preparing phase a starting material comprising: mixtures of cetearyl olive oil and olive oil sorbitol esters, mixtures of cetearyl alcohol and cetearyl glucoside, cetearyl alcohol, dimethicone, jojoba oil, mixtures of cyclopentasiloxane and cyclohexasiloxane, mixtures of methylparaben, ethylparaben, jojoba seed oil and pomegranate flower extract; uniformly mixing the raw materials of the phase A, and heating to 80-85 ℃ to obtain a phase A;
s2) preparing a raw material of a phase B, wherein the raw material of the phase B comprises the following components: deionized water, glycerol, 1, 3-butanediol, ethylene diamine tetraacetic acid disodium salt, 5-urethyllactam, a mixture of pyrrolidone carboxylic acid sodium salt, tetrahydro-methylpyrimidine carboxylic acid and xanthan gum; uniformly mixing the raw materials of the phase B, and heating to 80-85 ℃ to obtain a phase B;
s3) adding the phase A into the phase B, and homogenizing for 2-5 min; homogenizing, adding acrylic acid (ester)/behenyl alcohol polyether-25 methacrylate copolymer, stirring and mixing to obtain phase C;
s4) adding sodium hydroxide into the phase C, and uniformly stirring; and (3) cooling to 40-45 ℃, adding the mixture of phenoxyethanol and ethylhexyl glycerin and the essence, and uniformly stirring.
The invention has the beneficial effects that: the invention provides a moisturizing and repairing emulsion spray and a preparation method thereof, wherein the emulsion spray comprises the components of an emulsifier, an emollient, a preservative, an efficacy additive, an anti-inflammatory agent, a humectant, a chelating agent, a thickening agent, a pH regulator, an aromatizer and deionized water; the emulsion spray of the invention has the following advantages:
1) when the efficacy additive is compounded by a mixture of jojoba oil and pomegranate flower extract and tetrahydro-methyl pyrimidine carboxylic acid, the 2 compositions synergistically increase the repair efficacy of emulsion spray and can improve the moisturizing efficacy of the emulsion spray;
2) when the humectant is compounded by sodium pyrrolidone carboxylate mixture, glycerin and 1, 3-butanediol in a mass ratio of (3-9) to (1-10), the 3 compositions can obviously increase the effect of emulsion spraying;
3) when the emollient is compounded by polydimethylsiloxane, jojoba oil, cyclopentasiloxane and cyclohexasiloxane according to the mass ratio of (2-4) to (1-5), the emollient can promote human skin to absorb emulsion spray, and can improve the moisturizing and repairing effects of the emulsion spray;
4) when the thickening agent is compounded by acrylic acid (ester)/behenyl polyether-25 methacrylate copolymer and xanthan gum according to the mass ratio of (0.8-2) to (0.05-0.2), directional spray can be prepared to form uniformly dispersed liquid drops, and the phenomenon that a material body with consistency in the market cannot be sprayed is solved.
Detailed Description
To better illustrate the objects, aspects and advantages of the present invention, the present invention will be further described with reference to specific examples.
It should be noted that in the present specification, "mixture of cetostearyl olive oil and olive oil sorbitol ester, mixture of cetearyl alcohol and cetearyl glucoside, cetearyl alcohol complex" means a mixture of 3 components, 3 components are a mixture of cetostearyl olive oil and olive oil sorbitol ester, a mixture of cetearyl alcohol and cetearyl glucoside, cetearyl alcohol; the 'compound of polydimethylsiloxane, jojoba oil and a mixture of cyclopentasiloxane and cyclohexasiloxane' means that the compound is formed by mixing 3 components, wherein the 3 components are a mixture of polydimethylsiloxane, jojoba oil, cyclopentasiloxane and cyclohexasiloxane; the 'compounded mixture of methyl hydroxybenzoate, ethylparaben, phenoxyethanol and ethylhexylglycerin' means that the mixture is formed by mixing 3 components, wherein the 3 components are the mixture of methyl hydroxybenzoate, ethylparaben, phenoxyethanol and ethylhexylglycerin.
In the following examples, the mixture of "cetostearyl olive oil and olive oil sorbitol esters" is sold under the trade name of olivem1000, the mixture of cetearyl and cetearyl glucoside "is sold under the trade name of MONTANOV 68, the mixture of Jojoba oil" is sold under the trade name of Jojoba oil, the mixture of cyclopentasiloxane and cyclohexasiloxane "is sold under the trade name of DC345, the mixture of Jojoba oil and Pomegranate flower extract" is sold under the trade name of Pomegranate Olact @, the mixture of deionized water, glycerol, PCA sodium, erythritol, Chondrus crispus extract and xanthan gum is sold under the trade name of Lubrajel Marine, the copolymer of acrylic acid (ester)/behenyl polyether-25 methacrylate copolymer "is sold under the trade name of Volarst FL, and the mixture of phenoxy ethanol and ethylhexyl glycerol is sold under the trade name of euxyl PE 9010.
Example 1
The embodiment provides an emulsion spray, which is composed of the following components in percentage by mass: 2.5% of emulsifier, 4% of emollient, 0.25% of preservative, 1% of efficacy additive, 0.05% of anti-inflammatory agent, 5% of humectant, 0.02% of chelating agent, 0.85% of thickening agent, 0.19% of pH regulator, 0.01% of flavoring agent and the balance of deionized water;
the efficacy additive is compounded by a mixture of jojoba seed oil and pomegranate flower extract and tetrahydro-methyl pyrimidine carboxylic acid in a mass ratio of 0.5: 0.5, the emulsifier is compounded by a mixture of cetostearyl olive oil and olive oil sorbitol ester, a mixture of cetearyl alcohol and cetearyl glucoside and cetearyl alcohol in a mass ratio of 3:1: 0.5, the emollient is compounded by polydimethylsiloxane, jojoba oil and a mixture of cyclopentasiloxane and cyclohexasiloxane in a mass ratio of 4:1: 1, the preservative is compounded by a mixture of methylparaben, ethylparaben and phenoxyethanol and ethylhexylglycerin in an emulsion spray in a mass percentage of 0.2%, 0.05% and 0.1%, and the humectant is compounded by a mixture of sodium pyrrolidone carboxylate, glycerin and 1, 3-butanediol in a mass ratio of 9:1: 1, the sodium pyrrolidone carboxylate mixture is prepared by compounding deionized water, glycerol, sodium pyrrolidone carboxylate, erythritol, a carrageen crispus extract and xanthan gum, the thickening agent is prepared by compounding acrylic acid (ester)/behenyl alcohol polyether-25 methacrylate copolymer and xanthan gum according to the mass ratio of 0.8: 0.2, the chelating agent is disodium ethylene diamine tetraacetate, the pH regulator is sodium hydroxide, the flavoring agent is essence, and the anti-inflammatory agent is 5-uridylethanolamide.
The present invention also provides a method for preparing the emulsion spray, which comprises the following steps:
s1) preparing phase a starting material comprising: mixtures of cetearyl olive oil and olive oil sorbitol esters, mixtures of cetearyl alcohol and cetearyl glucoside, cetearyl alcohol, dimethicone, jojoba oil, mixtures of cyclopentasiloxane and cyclohexasiloxane, mixtures of methylparaben, ethylparaben, jojoba seed oil and pomegranate flower extract; uniformly mixing the raw materials of the phase A, and heating to 80-85 ℃ to obtain a phase A;
s2) preparing a raw material of a phase B, wherein the raw material of the phase B comprises the following components: deionized water, glycerol, 1, 3-butanediol, ethylene diamine tetraacetic acid disodium salt, 5-urethyllactam, a mixture of pyrrolidone carboxylic acid sodium salt, tetrahydro-methylpyrimidine carboxylic acid and xanthan gum; uniformly mixing the raw materials of the phase B, and heating to 80-85 ℃ to obtain a phase B;
s3) adding the phase A into the phase B, and homogenizing for 2-5 min; homogenizing, adding acrylic acid (ester)/behenyl alcohol polyether-25 methacrylate copolymer, stirring and mixing to obtain phase C;
s4) adding sodium hydroxide into the phase C, and uniformly stirring; and (3) cooling to 40-45 ℃, adding the mixture of phenoxyethanol and ethylhexyl glycerin and the essence, and uniformly stirring.
Example 2
The embodiment provides an emulsion spray, which is composed of the following components in percentage by mass: 5% of emulsifier, 7% of emollient, 1% of preservative, 3.8% of efficacy additive, 0.2% of anti-inflammatory agent, 15% of humectant, 0.1% of chelating agent, 1.2% of thickening agent, 0.3% of pH regulator, 0.02% of flavoring agent and the balance of deionized water;
the efficacy additive is compounded by mixture of jojoba seed oil and pomegranate flower extract and tetrahydro-methyl pyrimidine carboxylic acid in a mass ratio of 4:3, the emulsifier is compounded by mixture of cetearyl olive oil and olive oil sorbitol ester, mixture of cetearyl alcohol and cetearyl glucoside and cetearyl alcohol in a mass ratio of 1:3: 1.5, the emollient is compounded by mixture of polydimethylsiloxane, jojoba oil and cyclopentasiloxane and cyclohexasiloxane in a mass ratio of 2:5: 5, the preservative is compounded by mixture of 0.1%, 0.15% and 1% of methyl hydroxybenzoate, ethylparaben and phenoxyethanol and ethylhexylglycerin in emulsion spray, the humectant is compounded by mixture of sodium pyrrolidone carboxylate, glycerin and 1, 3-butanediol in a mass ratio of 3:10: 10, the sodium pyrrolidone carboxylate mixture is prepared by compounding deionized water, glycerol, sodium pyrrolidone carboxylate, erythritol, a carrageen crispus extract and xanthan gum, the thickening agent is prepared by compounding acrylic acid (ester)/behenyl polyether-25 methacrylate copolymer and xanthan gum according to the mass ratio of 2:0.05, the chelating agent is disodium ethylene diamine tetraacetate, the pH regulator is sodium hydroxide, the flavoring agent is essence, and the anti-inflammatory agent is 5-uroethyl lactam.
This example also provides a method of making the above emulsion spray, which is the same as example 1.
Example 3
The embodiment provides an emulsion spray, which is composed of the following components in percentage by mass: emulsifier 7.5%, emollient 14%, antiseptic 1.35%, efficacy additive 7%, anti-inflammatory agent 0.2%, humectant 29%, chelating agent 0.2%, thickener 2.2%, pH regulator 0.42%, perfuming agent 0.03%, and balance deionized water;
the efficacy additive is compounded by a mixture of jojoba seed oil and pomegranate flower extracts and tetrahydro-methyl pyrimidine carboxylic acid in a mass ratio of 3:2, the emulsifier is compounded by a mixture of cetearyl olive oil and olive oil sorbitol ester, a mixture of cetearyl stearyl alcohol and cetearyl glucoside and cetearyl alcohol in a mass ratio of 2.3:1.5: 1, the emollient is compounded by polydimethylsiloxane in a mass ratio of 3.4:2.1: 4.4, jojoba oil and a mixture of cyclopentasiloxane and cyclohexasiloxane, the preservative is compounded by a mixture of 0.16%, 0.1% and 0.4% of methylparaben, ethylparaben and phenoxyethanol and hexylglycerin in emulsion spray, the humectant is compounded by a mixture of sodium pyrrolidone carboxylate, glycerin and 1, 3-butanediol in a mass ratio of 7:9: 4, the sodium pyrrolidone carboxylate mixture is prepared by compounding deionized water, glycerol, sodium pyrrolidone carboxylate, erythritol, a carrageen crispus extract and xanthan gum, the thickening agent is prepared by compounding acrylic acid (ester)/behenyl alcohol polyether-25 methacrylate copolymer and xanthan gum according to the mass ratio of 1.2:0.1, the chelating agent is disodium ethylene diamine tetraacetate, the pH regulator is sodium hydroxide, the flavoring agent is essence, and the anti-inflammatory agent is 5-uridylethanolamide.
This example also provides a method of making the above emulsion spray, which is the same as example 1.
Example 4
The embodiment provides an emulsion spray, which is composed of the following components in percentage by mass: 5% of emulsifier, 9% of emollient, 0.75% of preservative, 3% of efficacy additive, 0.1% of anti-inflammatory agent, 16% of humectant, 0.1% of chelating agent, 1.1% of thickening agent, 0.23% of pH regulator, 0.02% of flavoring agent and the balance of deionized water;
the efficacy additive is prepared by compounding a mixture of jojoba oil and pomegranate flower extract in a mass ratio of 2:1 and tetrahydro-methyl pyrimidine carboxylic acid; the emulsifier is compounded by a mixture of hexadecyl-octadecyl olive oil and olive oil sorbitol ester, a mixture of cetearyl alcohol and cetearyl glucoside and cetearyl alcohol in a mass ratio of 2:2: 1; the emollient is compounded by polydimethylsiloxane, jojoba oil and a mixture of cyclopentasiloxane and cyclohexasiloxane according to the mass ratio of 3:3: 3; the preservative is compounded by 0.15 percent, 0.1 percent and 0.5 percent of methylparaben and ethylparaben and a mixture of phenoxyethanol and ethylhexyl glycerol in the emulsion spray by mass percentage; the humectant is prepared by compounding a sodium pyrrolidone carboxylic acid mixture, glycerol and 1, 3-butanediol in a mass ratio of 6:5:5, wherein the sodium pyrrolidone carboxylic acid mixture is prepared by compounding deionized water, glycerol, sodium pyrrolidone carboxylic acid, erythritol, a carrageen crispus extract and xanthan gum; the thickening agent is compounded by acrylic acid (ester)/behenyl alcohol polyether-25 methacrylate copolymer and xanthan gum with the mass ratio of 1: 0.1; the chelating agent is disodium ethylene diamine tetraacetate, the pH regulator is sodium hydroxide, the flavoring agent is essence, and the anti-inflammatory agent is 5-uroethyl lactam.
This example also provides a method of making the above emulsion spray, which is the same as example 1.
Example 5
This example provides an emulsion spray which differs from example 4 in that:
1) the efficacy additive is prepared by compounding a mixture of jojoba oil and pomegranate flower extract in a mass ratio of 3:1 and tetrahydro-methyl pyrimidine carboxylic acid;
2) the thickening agent is compounded by acrylic acid (ester)/behenyl alcohol polyether-25 methacrylate copolymer and xanthan gum with the mass ratio of 1: 0.2;
3) the humectant is prepared by compounding a sodium pyrrolidone carboxylate mixture, glycerol and 1, 3-butanediol in a mass ratio of 4:5: 5.
This example also provides a method of making the above emulsion spray, which is the same as example 4.
Example 6
This example provides an emulsion spray which differs from example 4 in that:
1) the efficacy additive is prepared by compounding a mixture of jojoba oil and pomegranate flower extract and tetrahydro-methyl pyrimidine carboxylic acid in a mass ratio of 4: 0.8;
2) the thickening agent is compounded by acrylic acid (ester)/behenyl alcohol polyether-25 methacrylate copolymer and xanthan gum with the mass ratio of 1.2: 0.2;
3) the humectant is prepared by compounding a mixture of sodium pyrrolidone carboxylate with a mass ratio of 3:5:5, glycerin and 1, 3-butanediol.
This example also provides a method of making the above emulsion spray, which is the same as example 4.
Example 7
This example provides an emulsion spray which differs from example 4 in that:
1) the efficacy additive is prepared by compounding a mixture of jojoba oil and pomegranate flower extract in a mass ratio of 4:2 and tetrahydro-methyl pyrimidine carboxylic acid;
2) the thickening agent is compounded by acrylic acid (ester)/behenyl alcohol polyether-25 methacrylate copolymer and xanthan gum with the mass ratio of 1.5: 0.2;
3) the humectant is prepared by compounding a mixture of sodium pyrrolidone carboxylate with a mass ratio of 7:5:5, glycerin and 1, 3-butanediol.
This example also provides a method of making the above emulsion spray, which is the same as example 4.
Comparative example 1
This comparative example provides an emulsion spray having the same ingredients except that the thickener and solvent deionized water are different from example 5: the mass percentage content of the acrylic acid (ester)/behenyl alcohol polyether-25 methacrylate copolymer in the emulsion spray is 0.3%, and the mass percentage content of the xanthan gum in the emulsion spray is 0.2%.
This example also provides a method for preparing the above emulsion spray, which can be the same as in reference example 4.
Comparative example 2
This comparative example provides an emulsion spray having the same ingredients except that the thickener is different from example 5: the emulsion spray thickener consists of a mixture of sodium acrylate/sodium acryloyldimethyl taurate copolymer, isohexadecane and polysorbate-80 (sold under the trade name SIMULGEL ™ EG), xanthan gum; the mass percentage of the two components in the emulsion spray is respectively 1 percent and 0.1 percent.
This example also provides a method for preparing the above emulsion spray, which can be the same as in reference example 4.
Comparative example 3
This comparative example provides an emulsion spray with the same ingredients except that the performance additives and solvent deionized water are different from example 5: the mass percentage of the mixture of jojoba oil and pomegranate flower extract in the emulsion spray was 0.1%, and the mass percentage of the tetrahydro-methyl pyrimidine carboxylic acid in the emulsion spray was 1%.
This example also provides a method for preparing the above emulsion spray, which can be the same as in reference example 4.
Comparative example 4
This comparative example provides an emulsion spray having the same ingredients except that the efficacy additive was different from example 5: the mass percentage of the mixture of jojoba oil and pomegranate flower extract in the emulsion spray was 2.9%, and the mass percentage of the tetrahydro-methyl pyrimidine carboxylic acid in the emulsion spray was 0.1%.
This example also provides a method for preparing the above emulsion spray, which can be the same as in reference example 4.
Comparative example 5
This comparative example provides an emulsion spray with the same ingredients except that the humectant is different from example 5: the mass percentage of the mixture of the pyrrolidone carboxylic acid sodium in the emulsion spray is 0.5 percent, the mass percentage of the glycerol in the emulsion spray is 8.5 percent, and the mass percentage of the 1, 3-butanediol in the emulsion spray is 7 percent.
This example also provides a method for preparing the above emulsion spray, which can be the same as in reference example 4.
Comparative example 6
This comparative example provides an emulsion spray having the same ingredients except that the performance additive, solvent deionized water are different from example 5: the mass percentage of the mixture of jojoba oil and pomegranate flower extract in the emulsion spray was 0.1%, and the mass percentage of the tetrahydro-methyl pyrimidine carboxylic acid in the emulsion spray was 0.1%.
This example also provides a method for preparing the above emulsion spray, which can be the same as in reference example 4.
Stability test
The emulsion sprays prepared in examples 4 to 7 and comparative examples 1 to 5 were placed at 48 ℃, normal temperature, 5 ℃ and-18 ℃ respectively, and continuously observed for one month, and the test results are shown in table 1.
TABLE 1
| Example 4 | Example 5 | Example 6 | Example 7 | Comparative example 1 | Comparative example 2 | Comparative example 3 | Comparative example 4 | Comparative example 5 | |
| Presence or absence of delamination and precipitation | Is free of | Is free of | Is free of | Is free of | Is provided with | Is free of | Is free of | Is free of | Is free of |
As shown in table 1, when the thickener is in the appropriate range, the emulsion spray stability is good; when the thickening agent is too little, the sample can be layered.
Test of ejection effect
Respectively filling the emulsion sprays prepared in examples 4-7 and comparative examples 1-5 into a binary spray bottle, respectively weighing and recording the first mass, wherein the mass is the total mass; pressing the pump head of the binary spray bottle to spray all samples, observing whether the sprayed liquid drops are uniformly dispersed or not at the same time until the samples cannot be sprayed even if the pump head is pressed, respectively weighing the mass of the second time and recording the mass, wherein the mass is the residual mass; calculating an ejection rate, the ejection rate = (total mass-remaining mass)/total mass × 100%; the test results are shown in table 2.
TABLE 2
| Example 4 | Example 5 | Example 6 | Example 7 | Comparative example 1 | Comparative example 2 | Comparative example 3 | Comparative example 4 | Comparative example 5 | |
| Ejection rate | 99.83% | 99.73% | 99.74% | 99.78% | 20.33% | 9.57% | 99.71% | 99.68% | 99.75% |
| Whether the droplets are uniformly dispersed | Is that | Is that | Is that | Is that | Whether or not | Whether or not | Is that | Is that | Is that |
As shown in Table 2, the emulsion sprays of examples 4 to 7 and comparative examples 3 to 5 have good spraying effects, and sprayed droplets are also very uniformly dispersed, which shows that the thickener of the invention is prepared by compounding acrylic acid (ester)/behenyl alcohol polyether-25 methacrylate copolymer and xanthan gum, and has good shear thinning property in a proper range; the amount of the acrylic acid (ester)/behenyl alcohol polyether-25 methacrylate copolymer of comparative example 1 was not ideal, the ejection effect was not good, and the droplets were not uniformly dispersed; in contrast, comparative example 2, which uses SIMULGEL. EG, a conventional thickener, had poor ejection performance and had no uniform droplet dispersion because of its lack of shear thinning properties.
Test of moisturizing Effect
180 females aged 20-35 years are selected and averagely divided into A, B, C, D, E, F, G, H, I9 groups of 20 females. After the face of each group of testees is cleaned, shaving body hairs at the same position, sitting still for 15 minutes, then carrying out skin moisture test on each group of testees by using a skin moisture tester, and recording the initial skin moisture value of each group after average treatment; the emulsion spray of example 4 was used in group A, the emulsion spray of example 5 was used in group B, the emulsion spray of example 6 was used in group C, the emulsion spray of example 7 was used in group D, the emulsion spray of comparative example 1 was used in group E, the emulsion spray of comparative example 2 was used in group F, the emulsion spray of comparative example 3 was used in group G, the emulsion spray of comparative example 4 was used in group H, the emulsion spray of comparative example 5 was used in group I, the amount of the emulsion spray used in each group of subjects was the same, the application was uniform, the skin moisture content of the same place of each group of subjects was tested after the application for 3H, 6H and 8H, respectively, and the skin moisture content of each group was recorded after the average treatment, and the test results.
TABLE 3
| Group of | Initial moisture value of skin (%) | Skin moisture value after 3h (%) | Skin moisture value after 6h (%) | Skin moisture value after 8h (%) |
| A | 40.12 | 87.62 | 85.92 | 84.62 |
| B | 40.12 | 86.62 | 83.92 | 80.62 |
| C | 40.12 | 86.11 | 83.71 | 80.58 |
| D | 40.12 | 85.79 | 82.83 | 79.41 |
| E | 40.12 | 85.93 | 83.37 | 80.43 |
| F | 40.12 | 86.26 | 83.94 | 80.97 |
| G | 40.12 | 72.67 | 67.18 | 58.83 |
| H | 40.12 | 72.86 | 67.59 | 58.96 |
| I | 40.12 | 63.58 | 58.48 | 53.11 |
As shown in Table 3, the emulsion spray of the embodiments 4 to 7 of the invention has better moisturizing effect, especially the emulsion spray of the embodiment 4; the spray moisturizing effect of the emulsion of the comparative examples 3 to 5 is not ideal, and particularly the formula of the moisturizing agent in the emulsion spray of the comparative example 5 is generated; therefore, when the humectant is prepared by compounding a pyrrolidone sodium carboxylate mixture, glycerol and 1, 3-butanediol in a mass ratio of (3-9) to (1-10), the emulsion spray has a good moisturizing effect; in addition, the efficacy additive in the emulsion spray can also synergistically promote moisturizing.
Testing of repair Effect
Selecting 100 females with age range of 20-35 years and obvious non-hereditary erythema and acne marks on faces, averagely dividing into A, B, C, D, E5 groups, spraying the emulsion of example 4 in group A, spraying the emulsion of example 5 in group B, spraying the emulsion of comparative example 3 in group C, spraying the emulsion of comparative example 4 in group D, and spraying the emulsion of comparative example 6 in group E; each group of testees must be smeared with corresponding emulsion spray every morning and evening, and the condition of erythema and acne marks is observed every other week for 4 weeks; the test results are shown in table 4.
TABLE 4
| Group of | Day 3 | Day 6 | Day 9 | Day 12 |
| A | Slight erythema and acne marks Desalination effect of | Has good erythema and acne marks Desalination effect | Both erythema and acne marks Good desalination effect | Basically eliminate erythema and acne marks Medicine for treating chronic hepatitis B |
| B | Slight erythema and acne marks Desalination effect of | Has good erythema and acne marks Desalination effect | Both erythema and acne marks Good desalination effect | Basically eliminate erythema and acne marks Medicine for treating chronic hepatitis B |
| C | Erythema and acne marks substantially free Any desalination effect | Slight erythema and acne marks Desalination effect | Both erythema and acne marks are better Good desalination effect | Has good erythema and acne marks Desalination effect of |
| D | Erythema and acne marks substantially free Any desalination effect | Basically no erythema and acne marks What desalination effect | The erythema and acne marks are all slight Slight desalination effect | Slight erythema and acne marks Desalination effect of |
| E | Basic erythema and acne marksUpper is provided with Any desalination effect | Basically no erythema and acne marks What desalination effect | Erythema and acne marks Without any desalination effect | Erythema and acne marks substantially free Any desalination effect |
As shown in Table 4, after the emulsion of the invention is continuously used for spraying for 12 days, the erythema and the acne marks basically disappear, after the emulsion of the comparative example 3 is continuously used for spraying for 12 days, the erythema and the acne marks have better fading effect, and after the emulsion of the comparative example 4 is continuously used for spraying for 12 days, the fading effect of the erythema and the acne marks is very slight; after continuously using the emulsion of the comparative example 6 for spraying for 4 weeks, the fading of the erythema and the acne marks basically has no effect; therefore, the mixture of the jojoba oil and the pomegranate flower extract and the tetrahydro-methyl pyrimidine carboxylic acid in the efficacy additive have the repairing efficacy, and when the efficacy additive is compounded by the mixture of the jojoba oil and the pomegranate flower extract and the tetrahydro-methyl pyrimidine carboxylic acid in the mass ratio of (0.5-4) - (0.5-3), and the mass percentage of the efficacy additive is 1% -7%, the repairing of emulsion spraying is better.
Finally, it should be noted that the above embodiments are intended to illustrate the technical solutions of the present invention and not to limit the scope of the present invention, and although the present invention has been described in detail with reference to the preferred embodiments, it should be understood by those skilled in the art that modifications and equivalent substitutions can be made to the technical solutions of the present invention without departing from the spirit and scope of the technical solutions of the present invention.
Claims (10)
1. The moisturizing and repairing emulsion spray is characterized by comprising the following components in percentage by mass: 2.5-7.5% of emulsifier, 4-14% of emollient, 0.25-1.35% of preservative, 1-7% of efficacy additive, 0.05-0.2% of anti-inflammatory agent, 5-29% of humectant, 0.02-0.2% of chelating agent, 0.85-2.2% of thickening agent, 0.19-0.42% of pH regulator, 0.01-0.03% of flavoring agent and the balance of deionized water; the efficacy additive is prepared by compounding a mixture of jojoba oil and pomegranate flower extract and tetrahydro-methyl pyrimidine carboxylic acid in a mass ratio of (0.5-4) to (0.5-3);
the thickening agent is prepared by compounding acrylic acid (ester)/behenyl polyether-25 methacrylate copolymer and xanthan gum according to the mass ratio of (0.8-2) to (0.05-0.2).
2. The emulsion spray of claim 1, wherein the emulsifier is prepared by mixing a mixture of cetearyl olive oil and an olive oil sorbitol ester, a mixture of cetearyl alcohol and cetearyl glucoside, and cetearyl alcohol in a mass ratio of (1-3): (0.5-1.5).
3. The emulsion spray of claim 1, wherein the emollient is a mixture of dimethicone, jojoba oil, and cyclopentasiloxane and cyclohexasiloxane in a mass ratio of (2-4): (1-5): 1-5).
4. The emulsion spray of claim 1, wherein the preservative is formulated from 0.1-0.2%, (0.05-0.15)%, (0.1-1)% by mass of methyl paraben, ethyl paraben, and a mixture of phenoxyethanol and ethylhexylglycerin.
5. The emulsion spray of claim 1, wherein the humectant is formed by compounding a mixture of sodium pyrrolidone carboxylate in a mass ratio of (3-9): (1-10): 1-10), glycerin, and 1, 3-butanediol, and the mixture of sodium pyrrolidone carboxylate is formed by compounding deionized water, glycerin, sodium pyrrolidone carboxylate, erythritol, a Chondrus crispus extract, and xanthan gum.
6. The emulsion spray of claim 1, wherein the chelating agent is disodium edetate, the pH adjusting agent is sodium hydroxide, the fragrance vehicle is a fragrance, and the anti-inflammatory agent is 5-uroethyllactam.
7. The emulsion spray of claim 1, comprising the following components in percent by mass: 2.5-7.5% of emulsifier, 4-14% of emollient, 0.25-1.35% of preservative, 1-7% of efficacy additive, 0.05-0.2% of anti-inflammatory agent, 5-29% of humectant, 0.02-0.2% of chelating agent, 0.85-2.2% of thickening agent, 0.19-0.42% of pH regulator, 0.01-0.03% of flavoring agent and the balance of deionized water; the efficacy additive is prepared by compounding a mixture of jojoba oil and pomegranate flower extracts and tetrahydro-methyl pyrimidine carboxylic acid in a mass ratio of (0.5-4) - (0.5-3), the emulsifier is prepared by compounding a mixture of hexadecadecyl olive oil and olive oil sorbitol ester, a mixture of cetearyl alcohol and cetearyl glucoside and cetearyl alcohol in a mass ratio of (1-3) - (0.5-1.5), the emollient is prepared by compounding polydimethylsiloxane, jojoba oil and a mixture of cyclopentasiloxane and cyclohexasiloxane in a mass ratio of (2-4) - (1-5), the preservative is prepared by compounding a mixture of methylparaben, ethylparaben and a mixture of ethanol and ethylhexyl glycerol in an emulsion spray in a mass percentage of (0.1-0.2%), (0.05-0.15%), (0.1-1%), the humectant is compounded by sodium pyrrolidone carboxylate mixture, glycerin and 1, 3-butanediol in a mass ratio of (3-9) - (1-10), the sodium pyrrolidone carboxylate mixture is compounded by deionized water, glycerin, sodium pyrrolidone carboxylate, erythritol, a carrageen crispatus extract and xanthan gum, the thickener is compounded by acrylic acid (ester)/behenyl alcohol polyether-25 methacrylate copolymer and xanthan gum in a mass ratio of (0.8-2) - (0.05-0.2), the chelating agent is disodium ethylene diamine tetraacetate, the pH regulator is sodium hydroxide, the flavoring agent is essence, and the anti-inflammatory agent is 5-urethyl lactam.
8. The emulsion spray of claim 7, consisting of the following components in mass percent: 5% of emulsifier, 9% of emollient, 0.75% of preservative, 3% of efficacy additive, 0.1% of anti-inflammatory agent, 16% of humectant, 0.1% of chelating agent, 1.1% of thickening agent, 0.23% of pH regulator, 0.02% of flavoring agent and the balance of deionized water.
9. The emulsion spray of claim 8, wherein the efficacy additive is formulated from a mixture of jojoba oil and pomegranate flower extract, and tetrahydro-methyl pyrimidine carboxylic acid in a mass ratio of 2: 1; the emulsifier is prepared by compounding a mixture of hexadecyl-octadecyl olive oil and an olive oil sorbitol ester, a mixture of cetearyl alcohol and cetearyl glucoside and cetearyl alcohol in a mass ratio of 2:2: 1; the emollient is compounded by polydimethylsiloxane, jojoba oil and a mixture of cyclopentasiloxane and cyclohexasiloxane in a mass ratio of 3:3: 3; the preservative is prepared by compounding 0.15 percent, 0.1 percent and 0.5 percent of methyl hydroxybenzoate, ethylparaben and a mixture of phenoxyethanol and ethylhexyl glycerol in emulsion spray by mass percentage; the humectant is prepared by compounding a sodium pyrrolidone carboxylic acid mixture, glycerol and 1, 3-butanediol in a mass ratio of 6:5:5, wherein the sodium pyrrolidone carboxylic acid mixture is prepared by compounding deionized water, glycerol, sodium pyrrolidone carboxylic acid, erythritol, a Chondrus crispus extract and xanthan gum; the thickening agent is prepared by compounding acrylic acid (ester)/behenyl alcohol polyether-25 methacrylate copolymer and xanthan gum according to the mass ratio of 1: 0.1.
10. A method of preparing an emulsion spray as claimed in any one of claims 7 to 9 comprising the steps of:
s1) preparing phase a starting material comprising: mixtures of cetearyl olive oil and olive oil sorbitol esters, mixtures of cetearyl alcohol and cetearyl glucoside, cetearyl alcohol, dimethicone, jojoba oil, mixtures of cyclopentasiloxane and cyclohexasiloxane, mixtures of methylparaben, ethylparaben, jojoba seed oil and pomegranate flower extract; uniformly mixing the raw materials of the phase A, and heating to 80-85 ℃ to obtain a phase A;
s2) preparing a raw material of a phase B, wherein the raw material of the phase B comprises the following components: deionized water, glycerol, 1, 3-butanediol, ethylene diamine tetraacetic acid disodium salt, 5-urethyllactam, a mixture of pyrrolidone carboxylic acid sodium salt, tetrahydro-methylpyrimidine carboxylic acid and xanthan gum; uniformly mixing the raw materials of the phase B, and heating to 80-85 ℃ to obtain a phase B;
s3) adding the phase A into the phase B, and homogenizing for 2-5 min; homogenizing, adding acrylic acid (ester)/behenyl alcohol polyether-25 methacrylate copolymer, stirring and mixing to obtain phase C;
s4) adding sodium hydroxide into the phase C, and uniformly stirring; and (3) cooling to 40-45 ℃, adding the mixture of phenoxyethanol and ethylhexyl glycerin and the essence, and uniformly stirring.
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| CN108524399A (en) * | 2018-07-02 | 2018-09-14 | 上海新高姿化妆品有限公司 | A kind of lotion and preparation method thereof with long-acting moisture-keeping efficacy |
| CN108578324A (en) * | 2018-07-02 | 2018-09-28 | 上海新高姿化妆品有限公司 | A kind of skin cream and preparation method thereof with long-acting moisture-keeping efficacy |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN106473935A (en) * | 2016-11-08 | 2017-03-08 | 宁夏艾伊生物工程研发有限公司 | A kind of moisturizer and preparation method thereof |
| CN108524399A (en) * | 2018-07-02 | 2018-09-14 | 上海新高姿化妆品有限公司 | A kind of lotion and preparation method thereof with long-acting moisture-keeping efficacy |
| CN108578324A (en) * | 2018-07-02 | 2018-09-28 | 上海新高姿化妆品有限公司 | A kind of skin cream and preparation method thereof with long-acting moisture-keeping efficacy |
Non-Patent Citations (1)
| Title |
|---|
| 梓颜 石榴花滋养修护霜;上海梓颜化妆品有限公司;《http://ftba.nmpa.gov.cn:8181/ftban/itownet/hzp_ba/fw/pz.jsp?processid=2017091111》;20170916;网页正文 * |
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