CN109520815B - Metallographic phase replica film preparation device - Google Patents
Metallographic phase replica film preparation device Download PDFInfo
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- CN109520815B CN109520815B CN201811395334.8A CN201811395334A CN109520815B CN 109520815 B CN109520815 B CN 109520815B CN 201811395334 A CN201811395334 A CN 201811395334A CN 109520815 B CN109520815 B CN 109520815B
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- film preparation
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- 238000002360 preparation method Methods 0.000 title claims abstract description 51
- 238000011084 recovery Methods 0.000 claims abstract description 26
- 238000009423 ventilation Methods 0.000 claims abstract description 13
- 238000010438 heat treatment Methods 0.000 claims abstract description 7
- 239000000853 adhesive Substances 0.000 claims description 3
- 230000001070 adhesive effect Effects 0.000 claims description 3
- 238000009434 installation Methods 0.000 claims description 3
- 238000003466 welding Methods 0.000 claims 1
- 239000002994 raw material Substances 0.000 abstract description 11
- 239000012535 impurity Substances 0.000 abstract description 8
- 230000009286 beneficial effect Effects 0.000 abstract description 2
- CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 description 6
- 239000000463 material Substances 0.000 description 6
- 238000000034 method Methods 0.000 description 6
- 239000002699 waste material Substances 0.000 description 6
- 239000000428 dust Substances 0.000 description 5
- 239000011521 glass Substances 0.000 description 5
- 230000007547 defect Effects 0.000 description 4
- 238000001035 drying Methods 0.000 description 3
- 230000007797 corrosion Effects 0.000 description 2
- 238000005260 corrosion Methods 0.000 description 2
- 238000007689 inspection Methods 0.000 description 2
- 239000012528 membrane Substances 0.000 description 2
- 239000003960 organic solvent Substances 0.000 description 2
- 230000032683 aging Effects 0.000 description 1
- 230000003749 cleanliness Effects 0.000 description 1
- 238000010276 construction Methods 0.000 description 1
- 230000001276 controlling effect Effects 0.000 description 1
- 239000011162 core material Substances 0.000 description 1
- 238000005520 cutting process Methods 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 230000002349 favourable effect Effects 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 239000007769 metal material Substances 0.000 description 1
- 238000005088 metallography Methods 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 230000001105 regulatory effect Effects 0.000 description 1
Classifications
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N1/00—Sampling; Preparing specimens for investigation
- G01N1/28—Preparing specimens for investigation including physical details of (bio-)chemical methods covered elsewhere, e.g. G01N33/50, C12Q
- G01N1/44—Sample treatment involving radiation, e.g. heat
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- Physics & Mathematics (AREA)
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Analytical Chemistry (AREA)
- Biochemistry (AREA)
- General Health & Medical Sciences (AREA)
- General Physics & Mathematics (AREA)
- Immunology (AREA)
- Pathology (AREA)
- Sampling And Sample Adjustment (AREA)
Abstract
The invention discloses a metallographic replica film preparation device, which structurally comprises a heatable base, a fixed side wall, a drainage inclined table, a solution recovery tank, a base power socket, a special housing, a vent hole, a foot screw part, a bubble level and a T-shaped clamping block, and has the following beneficial effects: the levelness of the device is adjusted by utilizing the foot screw part, and a constant-temperature heating base is adopted to provide the selection of properly accelerating the preparation speed; the special matched housing is designed, and impurity pollution is prevented on the premise of ensuring ventilation, so that the purposes of improving the preparation quality of the complex film and improving the preparation speed are achieved; the forming working surface of the film is regular and is provided with a raw material solution recovery tank, and the preparation process does not need to worry about the difficulty in controlling or wasting the shape of the film caused by excessive pouring of the raw material solution; the scheme also has the following advantages: the whole design is simple, the disassembly and assembly of the parts are simple, and the operation is convenient; the device is portable and convenient to move or carry.
Description
Technical Field
The invention relates to a metallographic replica film preparation device, and belongs to the field of metallographic replica film preparation devices.
Background
The metallographic replica technique is a common means for on-site metallographic structure inspection, can be used for judging the manufacturing quality of metal materials, the installation quality of equipment and the change of structure performance in use, and judging creep damage of aging parts, is an internationally-used experimental method, and the replica film is a core material of the metallographic replica technique, the quality of the replica film determines the accuracy of a metallographic inspection result to a great extent, and at present, the mode of preparing the replica film by practitioners is simple and rough, and the process is described as follows: pouring the prepared complex film solution on a flat clean glass plate, covering the complex film solution but leaving gaps, naturally drying and forming the complex film solution, and taking off the complex film solution for later use, wherein the process has several defects: the levelness of the glass plate cannot be ensured, and the film thickness is easy to be uneven; the natural drying takes a long time, the preparation period is uncontrollable, and the preparation cannot be performed in time if the product is used in emergency; the special cover shell is not needed, the special cover shell is replaced by an analogue at random, the gap ventilation condition cannot be ensured, impurities such as dust and the like are easy to introduce, and the complex film is polluted; the amount of raw material solution for preparing the film and the shape of a film finished product are difficult to control each time, the edge cannot be used, waste is caused by cutting off the waste, and the problems bring a plurality of uncertain factors to quality, speed, cost and the like of the preparation of the replica film, so that a metallographic replica film preparation device is provided.
Disclosure of Invention
Aiming at the defects existing in the prior art, the invention aims to provide a metallographic replica film preparation device which solves the problems that the levelness of a glass plate in the prior art cannot be ensured and the film thickness is easy to be uneven; the natural drying takes a long time, the preparation period is uncontrollable, and the preparation cannot be performed in time if the product is used in emergency; the special cover shell is not needed, the special cover shell is replaced by an analogue at random, the gap ventilation condition cannot be ensured, impurities such as dust and the like are easy to introduce, and the complex film is polluted; the amount of raw material solution for preparing the film and the shape of the film finished product are difficult to control each time, the edge cannot be used, and the waste is mostly cut off, so that the waste is caused.
In order to achieve the above object, the present invention is realized by the following technical scheme: the utility model provides a metallographic replica film preparation facilities, includes heatable base, fixed lateral wall, drainage sloping platform, solution recovery tank, base power socket, special housing, ventilation hole, foot screw part, bubble spirit level, T type fixture block, the T type draw-in groove and metallographic film preparation working face of assembly recovery tank, heatable base rear end upside welds with fixed lateral wall lower extreme, the drainage sloping platform right-hand member bonds with heatable base left end through the adhesive, solution recovery tank right-hand member bonds with T type fixture block left end, base power socket rear end is pegged graft with heatable base front end, special housing right-hand member is provided with the ventilation hole, foot screw part upper end carries out perpendicular threaded connection through screw and heatable base bottom right side, the bubble spirit level sets up in fixed lateral wall upper end middle part, T type fixture block left end carries out the buckle with the T type draw-in groove right-hand member of assembly recovery tank and is connected, the T type fixture block of assembly recovery tank sets up at heatable base right-hand member front side, metallographic film preparation working face sets up at heatable base upper end.
Furthermore, the metallographic film has the advantages that the surface of the working surface for preparing the metallographic film is smooth and clean, no scratch, pit or bulge exists, and the surface defect of uneven deformation of the film can be avoided.
Further, the drainage inclined tables are provided with two drainage inclined tables which are inclined downwards by 15 degrees, and the drainage inclined tables have the advantage of being used for guiding redundant raw material solution into the solution recovery tank.
Furthermore, the heating element is arranged in the heatable base, and the constant temperature of the metallographic film preparation working surface is ensured to be 30 ℃ after the heating element is started, so that the preparation speed can be improved.
Further, the ventilation holes are all provided with more than two, and the filter screen sheets are attached to the ventilation holes, so that the filter screen sheets have the advantage of preventing impurities such as dust from entering the pollution replica film.
Furthermore, the contact surface of the special housing is manufactured by adopting a frosting process, and the special housing has the advantages of ensuring good contact and being difficult to slide.
Furthermore, fixed lateral wall, drainage sloping platform and metallography membrane preparation working face all adopt organic glass material to make, and its advantage is favorable to guaranteeing smooth clean, and no scratch, pit, arch can not influence the unevenness and the deformation of membrane.
Furthermore, the material of the solution recovery tank is a material which is not mutually soluble with organic solvents such as acetone and the like, and the solution recovery tank has the advantage of corrosion resistance.
The metallographic replica film preparation device has the following beneficial effects: the levelness of the device is adjusted by utilizing the foot screw part, and a constant-temperature heating base is adopted to provide the selection of properly accelerating the preparation speed; the special matched housing is designed, and impurity pollution is prevented on the premise of ensuring ventilation, so that the purposes of improving the preparation quality of the complex film and improving the preparation speed are achieved; the forming working surface of the film is regular and is provided with a raw material solution recovery tank, and the preparation process does not need to worry about the difficulty in controlling or wasting the shape of the film caused by excessive pouring of the raw material solution; the scheme also has the following advantages: the whole design is simple, the disassembly and assembly of the parts are simple, and the operation is convenient; the device is portable and convenient to move or carry.
Drawings
Other features, objects and advantages of the present invention will become more apparent upon reading of the detailed description of non-limiting embodiments, given with reference to the accompanying drawings in which:
FIG. 1 is a schematic diagram of the overall composition of the present invention;
FIG. 2 is a perspective linear schematic of the construction of the various components of the present invention;
FIG. 3 is a top perspective linear view of the present invention;
in the figure: the device comprises a heatable base-1, a fixed side wall-2, a drainage inclined table-3, a solution recovery tank-4, a base power socket-5, a special housing-6, a vent hole-7, a foot screw component-8, a bubble level-9, a T-shaped clamping block-10, a T-shaped clamping groove-11 for assembling the recovery tank and a metallographic film preparation working face-12.
Detailed Description
The invention is further described in connection with the following detailed description, in order to make the technical means, the creation characteristics, the achievement of the purpose and the effect of the invention easy to understand.
Referring to fig. 1, 2 and 3, the present invention provides a metallographic replica film preparation device: comprises a heatable base 1, a fixed side wall 2, a drainage inclined table 3, a solution recovery tank 4, a base power socket 5, a special housing 6, a vent hole 7, a foot screw part 8, a bubble level 9, a T-shaped clamping block 10, a T-shaped clamping groove 11 for assembling the recovery tank and a metallographic film preparation working surface 12, wherein the upper side of the rear end of the heatable base 1 is welded with the lower end of the fixed side wall 2, the right end of the drainage inclined table 3 is adhered with the left end of the heatable base 1 through an adhesive, the right end of the solution recovery tank 4 is adhered with the left end of the T-shaped clamping block 10, the rear end of the base power socket 5 is spliced with the front end of the heatable base 1, the right end of the special housing 6 is provided with the vent hole 7, the upper end of the foot screw part 8 is vertically connected with the right side of the bottom end of the heatable base 1 through a screw, the bubble level 9 is arranged in the middle of the upper end of the fixed side wall 2, the left end of the T-shaped clamping block 10 is in snap-in connection with the right end of the T-shaped clamping groove 11 for assembling the recovery tank, the T-shaped clamping groove 11 for assembling the recovery groove is arranged at the front side of the right end of the heatable base 1, the metallographic film preparation working surface 12 is arranged at the upper end of the heatable base 1, the surface of the metallographic film preparation working surface 12 is smooth and clean, no scratch, pit and bulge are generated, the advantages are that the surface defects of uneven deformation of the film can not be caused, the drainage inclined tables 3 are both provided with two and are inclined downwards by 15 degrees, the advantages are that the waste raw material solution used for drainage enters the solution recovery groove 4, the heating element is arranged in the heatable base 1, the metallographic film preparation working surface 12 is ensured to be constant at 30 ℃ after opening, the preparation speed can be improved, the vent holes 7 are both provided with more than two, the filter screen sheets are attached at the vent holes 7, the advantages are that the impurities such as dust are prevented from entering the polluted complex film, the contact surface of the special housing 6 is manufactured by adopting the frosting process, the advantages are that the contact is good, the sliding is not easy, the fixed side wall 2, the drainage inclined table 3 and the metallographic film preparation working surface 12 are all made of organic glass materials, the advantages are that the smoothness and the cleanliness are guaranteed, no scratch, pit and bulge are generated, the unevenness and deformation of the film are not affected, the material of the solution recovery tank 4 is selected from materials which are not mutually dissolved with organic solvents such as acetone, and the advantages are corrosion resistance.
When a user wants to use the device, before preparing, firstly, the user observes the bubble level 9 by adjusting the foot screw 8, levels the metallographic film preparation working face 12 of the device, then the pre-prepared complex film raw material solution is poured on the metallographic film preparation working face 12, the solution flows naturally, the redundant solution flows into the solution recovery grooves 4 at two sides along the drainage inclined table 3, if special requirements are met for the preparation thickness of the film, the solution fluidity can be changed by repeatedly and evenly inclining the device left and right by adjusting the foot screw 8 or manually again, so as to obtain ideal thickness, after confirming that the complex film solution thickness on the metallographic film preparation working face 12 is suitable, the special cover 6 is covered, in advance, a filter screen is adhered at the vent hole 7, the impurity pollution such as dust is blocked, finally, the solution recovery groove 4 is taken down, a proper amount of acetone can be added for dissolving, if necessary, the preparation progress is convenient, the base power socket 5 is connected, a heating element inside the base 1 can be heated to perform constant temperature forming on the film preparation working face 12, the device is used for quickly volatilizing the complex film, the device is limited, and the shape of the complex film is shaped, and the device is shaped quickly has the advantages that the following is realized, and the complex film is shaped, and the film is shaped by the following: the levelness of the device is regulated by utilizing the foot screw part 8, and the constant-temperature heatable base 1 is adopted to provide the option of properly accelerating the preparation speed; the special housing 6 is designed to prevent impurity pollution on the premise of ensuring ventilation, thereby achieving the purposes of improving the preparation quality of the complex film and improving the preparation speed; the forming metallographic film preparation working surface 12 of the film is regular in shape and is provided with the raw material solution recovery tank 4, so that the preparation process is free from worry that the shape of the film is difficult to control or waste is caused due to excessive pouring amount of the raw material solution; the scheme also has the following advantages: the whole design is simple, the disassembly and assembly of the parts are simple, and the operation is convenient; the device is portable and convenient to move or carry.
While the fundamental and principal features of the invention and advantages of the invention have been shown and described, it will be apparent to those skilled in the art that the invention is not limited to the details of the foregoing exemplary embodiments, but may be embodied in other specific forms without departing from the spirit or essential characteristics thereof. The present embodiments are, therefore, to be considered in all respects as illustrative and not restrictive, the scope of the invention being indicated by the appended claims rather than by the foregoing description, and all changes which come within the meaning and range of equivalency of the claims are therefore intended to be embraced therein. Any reference sign in a claim should not be construed as limiting the claim concerned.
Furthermore, it should be understood that although the present disclosure describes embodiments, not every embodiment is provided with a separate embodiment, and that this description is provided for clarity only, and that the disclosure is not limited to the embodiments described in detail below, and that the embodiments described in the examples may be combined as appropriate to form other embodiments that will be apparent to those skilled in the art.
Claims (2)
1. The utility model provides a metallographic replica film preparation facilities, its characterized in that includes heatable base (1), fixed lateral wall (2), drainage sloping platform (3), solution recovery tank (4), base power socket (5), special housing (6), ventilation hole (7), foot screw part (8), bubble spirit level (9), T type fixture block (10), the T type draw-in groove (11) of assembly recovery tank and metallographic film preparation working face (12), but the welding is carried out with fixed lateral wall (2) lower extreme in heatable base (1) rear end upside, drainage sloping platform (3) right-hand member is through the adhesive with heatable base (1) left end bonding, solution recovery tank (4) right-hand member is bonded with T type fixture block (10) left end, but base power socket (5) rear end is pegged graft with heatable base (1) front end, special housing (6) right-hand member is provided with ventilation hole (7), foot screw part (8) upper end is through screw thread connection perpendicularly with heatable base (1) bottom right side, spirit level (9) set up in the upper side and is at the left side of fixed lateral wall (2) and is carried out the buckle and is held in the left side of the right side of the installation tank (11) of the T type, but the left side is held in the left side of the installation tank (11), the metallographic film preparation working surface (12) is arranged at the upper end of the heatable base (1); the drainage inclined tables (3) are provided with two drainage inclined tables which are inclined downwards by 15 degrees; a heating element is arranged in the heatable base (1), and the metallographic film preparation working surface (12) is ensured to be kept at 30 ℃ after being started; the ventilation holes (7) are all provided with more than two, and filter meshes are attached to the ventilation holes (7).
2. The metallographic replica film preparing apparatus according to claim 1, wherein: the metallographic film preparation working surface (12) has smooth and clean surface and no scratch, pit and bulge.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811395334.8A CN109520815B (en) | 2018-11-22 | 2018-11-22 | Metallographic phase replica film preparation device |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811395334.8A CN109520815B (en) | 2018-11-22 | 2018-11-22 | Metallographic phase replica film preparation device |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN109520815A CN109520815A (en) | 2019-03-26 |
| CN109520815B true CN109520815B (en) | 2024-04-02 |
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201811395334.8A Active CN109520815B (en) | 2018-11-22 | 2018-11-22 | Metallographic phase replica film preparation device |
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| Country | Link |
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| CN (1) | CN109520815B (en) |
Families Citing this family (1)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN111442963A (en) * | 2020-05-09 | 2020-07-24 | 国电锅炉压力容器检验有限公司 | On-spot metallographic examination auxiliary device |
Citations (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB428663A (en) * | 1934-09-25 | 1935-05-16 | Gennady Frenkel | Improvements in or relating to process and apparatus for the manufacture of films and foils |
| JPH1114519A (en) * | 1997-06-23 | 1999-01-22 | Noritake Co Ltd | Method for forming duplicated film of grinding stone surface |
| JP2006300812A (en) * | 2005-04-22 | 2006-11-02 | National Institute Of Advanced Industrial & Technology | Device and method for manufacturing inorganic compound thin film library |
| CN101592570A (en) * | 2009-07-02 | 2009-12-02 | 河北省电力研究院 | A kind of metallurgical phase complex film |
| CN102581057A (en) * | 2012-01-12 | 2012-07-18 | 太原理工大学 | Method for preparing enhanced magnesium alloy composite board |
| CN105413967A (en) * | 2015-12-25 | 2016-03-23 | 齐齐哈尔大学 | Intelligent fast flat film scraper |
| CN108088724A (en) * | 2018-02-09 | 2018-05-29 | 江苏金米兰纺织有限公司 | A kind of weaving serous coat preparation facilities |
| CN108541143A (en) * | 2018-03-13 | 2018-09-14 | 广西师范大学 | A kind of preparation facilities and preparation method of polyimide copper clad lamination |
| CN209673496U (en) * | 2018-11-22 | 2019-11-22 | 大唐东北电力试验研究院有限公司 | A kind of metallurgic replica membrane preparation device |
-
2018
- 2018-11-22 CN CN201811395334.8A patent/CN109520815B/en active Active
Patent Citations (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB428663A (en) * | 1934-09-25 | 1935-05-16 | Gennady Frenkel | Improvements in or relating to process and apparatus for the manufacture of films and foils |
| JPH1114519A (en) * | 1997-06-23 | 1999-01-22 | Noritake Co Ltd | Method for forming duplicated film of grinding stone surface |
| JP2006300812A (en) * | 2005-04-22 | 2006-11-02 | National Institute Of Advanced Industrial & Technology | Device and method for manufacturing inorganic compound thin film library |
| CN101592570A (en) * | 2009-07-02 | 2009-12-02 | 河北省电力研究院 | A kind of metallurgical phase complex film |
| CN102581057A (en) * | 2012-01-12 | 2012-07-18 | 太原理工大学 | Method for preparing enhanced magnesium alloy composite board |
| CN105413967A (en) * | 2015-12-25 | 2016-03-23 | 齐齐哈尔大学 | Intelligent fast flat film scraper |
| CN108088724A (en) * | 2018-02-09 | 2018-05-29 | 江苏金米兰纺织有限公司 | A kind of weaving serous coat preparation facilities |
| CN108541143A (en) * | 2018-03-13 | 2018-09-14 | 广西师范大学 | A kind of preparation facilities and preparation method of polyimide copper clad lamination |
| CN209673496U (en) * | 2018-11-22 | 2019-11-22 | 大唐东北电力试验研究院有限公司 | A kind of metallurgic replica membrane preparation device |
Non-Patent Citations (1)
| Title |
|---|
| 现场金相复膜纸的制作方法与技巧;谢汝良;;理化检验(物理分册)(第02期);全文 * |
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| CN109520815A (en) | 2019-03-26 |
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