CN109511676A - 一种氧化型水、烟两用复合消毒杀菌剂及其制备方法 - Google Patents

一种氧化型水、烟两用复合消毒杀菌剂及其制备方法 Download PDF

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CN109511676A
CN109511676A CN201811425391.6A CN201811425391A CN109511676A CN 109511676 A CN109511676 A CN 109511676A CN 201811425391 A CN201811425391 A CN 201811425391A CN 109511676 A CN109511676 A CN 109511676A
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贾文彬
王振亚
刘伟宇
孟庆楠
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Xuzhou Eall Environmental Technology Co Ltd
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    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N59/00—Biocides, pest repellants or attractants, or plant growth regulators containing elements or inorganic compounds
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    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
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    • A01N43/04—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom
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    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
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    • A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
    • A01N43/34—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one nitrogen atom as the only ring hetero atom
    • A01N43/36—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one nitrogen atom as the only ring hetero atom five-membered rings
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N47/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom not being member of a ring and having no bond to a carbon or hydrogen atom, e.g. derivatives of carbonic acid
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    • A01N47/42—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom not being member of a ring and having no bond to a carbon or hydrogen atom, e.g. derivatives of carbonic acid the carbon atom having a double or triple bond to nitrogen, e.g. cyanates, cyanamides containing —N=CX2 groups, e.g. isothiourea
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N59/00—Biocides, pest repellants or attractants, or plant growth regulators containing elements or inorganic compounds

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Abstract

一种氧化型水、烟两用复合消毒杀菌剂及其制备方法，其主要原料组分如下：氯代异氰尿酸碱金属盐12～15份、供热剂23～28份、助剂10～14份、分散剂13～21份、引燃剂6.5～9.5份、过氧化氢17～19份、增效剂10.5～15.5份、稳定剂18～22份、去离子水25～35份、稀碱液20～30份、干酪素17～19份、凝胶剂7～12份、聚乙烯吡咯烷酮碘6.5～9.5份、乳化剂10～20.5份，该氧化型消毒杀菌剂属复方消毒杀菌剂为无色、无味、无毒透明液体，安全，高效，绿色环保，杀菌彻底，延时缓释，药效持久，留物无有效成分，可广泛用于畜牧、养殖、养蚕等领域。

Description

一种氧化型水、烟两用复合消毒杀菌剂及其制备方法
技术领域
本发明涉及一种氧化型水、烟两用复合消毒杀菌剂及其制备方法，涉及消毒剂技术领域。
背景技术
水产养殖消毒药品是直接影响水产品质量的重要因素，高效、低毒环保型消毒药品研究势在必行，现有的碘制剂消毒剂虽杀菌效果好，但易受光线、温度的影响，易蒸发失效，突破传统的水剂等剂型，发明胶体保持长效高效适应市场需求。
水溶性消毒剂应用普遍，溶于水后，可采用喷洒、浸泡、擦拭等方法消毒。但是有些场所的消毒，又必须采用烟熏的方法，而目前使用的烟熏消毒剂，是在氯代异氰尿酸碱金属盐类中加入一定量的高锰酸钾、甲醛、聚甲醛、硝铵锯末等原料组成。这些烟熏消毒剂有些是分别包装，使用时再配，有些是复配包装，但因涉及安全问题，只能限量加入引燃剂而影响点燃及发烟效果。
发明内容
本发明针对现有技术的不足，提供一种氧化型水、烟两用复合消毒杀菌剂及其制备方法，采用分步制备各组分，该氧化型消毒杀菌剂属复方消毒杀菌剂为无色、无味、无毒透明液体，安全，高效，绿色环保，杀菌彻底，延时缓释，药效持久，方便实用，易水溶、易点燃、水溶迅速、扩散力强，烟熏消毒时，点燃后，迅速放出浓烟，发烟量大，残留物无有效成分，可广泛用于畜牧、养殖、养蚕等领域。
为了实现上述目的，本发明提供一种氧化型水、烟两用复合消毒杀菌剂及其制备方法，包括以下步骤：
一种氧化型水、烟两用复合消毒杀菌剂及其制备方法，其主要原料组分如下：氯代异氰尿酸碱金属盐12～15份、供热剂23～28份、柔软剂25～33份、缓释剂5～13份、羧甲基纤维素钠11～17份、助剂10～14份、分散剂13～21份、引燃剂6.5～9.5份、过氧化氢17～19份、增效剂10.5～15.5份、稳定剂18～22份、去离子水25～35份、稀碱液20～30份、干酪素17～19份、凝胶剂7～12份、聚乙烯吡咯烷酮碘6.5～9.5份、乳化剂10～20.5份；；
所述其制备方法按下列步骤进行，
(1)制备增效剂的水溶液，得到有银离子的银组分；
(2)将稳定剂加入上述有银离子的银组分中；
(3)与过氧化氢水溶液混合；
(4)加磷酸作酸值调节剂调节PH值及加水补足重量达100％，上述制备方法过程中，得到的溶液常温下边搅拌边缓慢倒入含有55-75％的过氧化氢水溶液中；加酸值调节剂时同样在常温下边搅拌边缓慢加入；
所述增效剂可以是银盐，包括硫酸银、硝酸银，稳定剂可以为三聚磷酸钠，磷酸可以作为调节剂。
本发明一种氧化型水、烟两用复合消毒杀菌剂及其制备方法，采用分步制备各组分，该氧化型消毒杀菌剂属复方消毒杀菌剂为无色、无味、无毒透明液体，安全，高效，绿色环保，杀菌彻底，延时缓释，药效持久，方便实用，易水溶、易点燃、水溶迅速、扩散力强，烟熏消毒时，点燃后，迅速放出浓烟，发烟量大，残留物无有效成分，可广泛用于畜牧、养殖、养蚕等领域。
具体实施方式
下面通过实施例对本发明做进一步详细说明。
实施例1
一种氧化型水、烟两用复合消毒杀菌剂及其制备方法，其主要原料组分如下：氯代异氰尿酸碱金属盐12份、供热剂23份、柔软剂25份、缓释剂5份、羧甲基纤维素钠11份、助剂10份、分散剂13份、引燃剂6.5份、过氧化氢17份、增效剂10.5份、稳定剂18份、去离子水25份、稀碱液20份、干酪素17份、凝胶剂7份、聚乙烯吡咯烷酮碘6.5份、乳化剂10份；
所述其制备方法按下列步骤进行，
(1)制备增效剂的水溶液，得到有银离子的银组分；
(2)将稳定剂加入上述有银离子的银组分中；
(3)与过氧化氢水溶液混合；
(4)加磷酸作酸值调节剂调节PH值及加水补足重量达100％，上述制备方法过程中，得到的溶液常温下边搅拌边缓慢倒入含有55％的过氧化氢水溶液中；加酸值调节剂时同样在常温下边搅拌边缓慢加入；
所述增效剂可以是银盐，包括硫酸银、硝酸银，稳定剂可以为三聚磷酸钠，磷酸可以作为调节剂。
实施例2
一种氧化型水、烟两用复合消毒杀菌剂及其制备方法，其主要原料组分如下：氯代异氰尿酸碱金属盐15份、供热剂28份、柔软剂33份、缓释剂13份、羧甲基纤维素钠17份、助剂14份、分散剂21份、引燃剂9.5份、过氧化氢19份、增效剂15.5份、稳定剂22份、去离子水35份、稀碱液30份、干酪素19份、凝胶剂12份、聚乙烯吡咯烷酮碘9.5份、乳化剂20.5份；
所述其制备方法按下列步骤进行，
(1)制备增效剂的水溶液，得到有银离子的银组分；
(2)将稳定剂加入上述有银离子的银组分中；
(3)与过氧化氢水溶液混合；
(4)加磷酸作酸值调节剂调节PH值及加水补足重量达100％，上述制备方法过程中，得到的溶液常温下边搅拌边缓慢倒入含有75％的过氧化氢水溶液中；加酸值调节剂时同样在常温下边搅拌边缓慢加入；
所述增效剂可以是银盐，包括硫酸银、硝酸银，稳定剂可以为三聚磷酸钠，磷酸可以作为调节剂。
实施例3
一种氧化型水、烟两用复合消毒杀菌剂及其制备方法，其主要原料组分如下：氯代异氰尿酸碱金属盐13份、供热剂25份、柔软剂28份、缓释剂9份、羧甲基纤维素钠14份、助剂12份、分散剂16份、引燃剂8.5份、过氧化氢18份、增效剂12.5份、稳定剂20份、去离子水30份、稀碱液25份、干酪素18份、凝胶剂10份、聚乙烯吡咯烷酮碘7.5份、乳化剂15.5份；；
所述其制备方法按下列步骤进行，
(1)制备增效剂的水溶液，得到有银离子的银组分；
(2)将稳定剂加入上述有银离子的银组分中；
(3)与过氧化氢水溶液混合；
(4)加磷酸作酸值调节剂调节PH值及加水补足重量达100％，上述制备方法过程中，得到的溶液常温下边搅拌边缓慢倒入含有65％的过氧化氢水溶液中；加酸值调节剂时同样在常温下边搅拌边缓慢加入；
所述增效剂可以是银盐，包括硫酸银、硝酸银，稳定剂可以为三聚磷酸钠，磷酸可以作为调节剂。

Claims (5)

1.一种氧化型水、烟两用复合消毒杀菌剂及其制备方法，其特征在于：其主要原料组分如下：氯代异氰尿酸碱金属盐12～15份、供热剂23～28份、柔软剂25～33份、缓释剂5～13份、羧甲基纤维素钠11～17份、助剂10～14份、分散剂13～21份、引燃剂6.5～9.5份、过氧化氢17～19份、增效剂10.5～15.5份、稳定剂18～22份、去离子水25～35份、稀碱液20～30份、干酪素17～19份、凝胶剂7～12份、聚乙烯吡咯烷酮碘6.5～9.5份、乳化剂10～20.5份。
2.根据权利要求1所述的一种氧化型水、烟两用复合消毒杀菌剂及其制备方法，其特征在于：其主要原料组分如下：氯代异氰尿酸碱金属盐12份、供热剂23份、柔软剂25份、缓释剂5份、羧甲基纤维素钠11份、助剂10份、分散剂13份、引燃剂6.5份、过氧化氢17份、增效剂10.5份、稳定剂18份、去离子水25份、稀碱液20份、干酪素17份、凝胶剂7份、聚乙烯吡咯烷酮碘6.5份、乳化剂10份。
3.根据权利要求1所述的一种氧化型水、烟两用复合消毒杀菌剂及其制备方法其特征在于：其主要原料组分如下：氯代异氰尿酸碱金属盐15份、供热剂28份、柔软剂33份、缓释剂13份、羧甲基纤维素钠17份、助剂14份、分散剂21份、引燃剂9.5份、过氧化氢19份、增效剂15.5份、稳定剂22份、去离子水35份、稀碱液30份、干酪素19份、凝胶剂12份、聚乙烯吡咯烷酮碘9.5份、乳化剂20.5份。
4.根据权利要求1所述其制备方法按下列步骤进行，
(1)制备增效剂的水溶液，得到有银离子的银组分；
(2)将稳定剂加入上述有银离子的银组分中；
(3)与过氧化氢水溶液混合；
(4)加磷酸作酸值调节剂调节PH值及加水补足重量达100％，上述制备方法过程中，得到的溶液常温下边搅拌边缓慢倒入含有55-75％的过氧化氢水溶液中；加酸值调节剂时同样在常温下边搅拌边缓慢加入。
5.根据权利要求1所述增效剂可以是银盐，包括硫酸银、硝酸银，稳定剂可以为三聚磷酸钠，磷酸可以作为调节剂。
CN201811425391.6A 2018-11-27 2018-11-27 一种氧化型水、烟两用复合消毒杀菌剂及其制备方法 Pending CN109511676A (zh)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN114041469A (zh) * 2021-12-20 2022-02-15 肖隆 一种混合型发烟消毒剂及其使用方法

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN114041469A (zh) * 2021-12-20 2022-02-15 肖隆 一种混合型发烟消毒剂及其使用方法

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