CN109504515B - Energy-saving environment-friendly agricultural machine oil and preparation method thereof - Google Patents
Energy-saving environment-friendly agricultural machine oil and preparation method thereof Download PDFInfo
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- CN109504515B CN109504515B CN201910034557.XA CN201910034557A CN109504515B CN 109504515 B CN109504515 B CN 109504515B CN 201910034557 A CN201910034557 A CN 201910034557A CN 109504515 B CN109504515 B CN 109504515B
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- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M169/00—Lubricating compositions characterised by containing as components a mixture of at least two types of ingredient selected from base-materials, thickeners or additives, covered by the preceding groups, each of these compounds being essential
- C10M169/04—Mixtures of base-materials and additives
- C10M169/044—Mixtures of base-materials and additives the additives being a mixture of non-macromolecular and macromolecular compounds
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- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
- C10N2030/00—Specified physical or chemical properties which is improved by the additive characterising the lubricating composition, e.g. multifunctional additives
- C10N2030/06—Oiliness; Film-strength; Anti-wear; Resistance to extreme pressure
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- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
- C10N2030/00—Specified physical or chemical properties which is improved by the additive characterising the lubricating composition, e.g. multifunctional additives
- C10N2030/08—Resistance to extreme temperature
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- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
- C10N2030/00—Specified physical or chemical properties which is improved by the additive characterising the lubricating composition, e.g. multifunctional additives
- C10N2030/10—Inhibition of oxidation, e.g. anti-oxidants
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- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
- C10N2030/00—Specified physical or chemical properties which is improved by the additive characterising the lubricating composition, e.g. multifunctional additives
- C10N2030/12—Inhibition of corrosion, e.g. anti-rust agents or anti-corrosives
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
- C10N2030/00—Specified physical or chemical properties which is improved by the additive characterising the lubricating composition, e.g. multifunctional additives
- C10N2030/40—Low content or no content compositions
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- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
- C10N2030/00—Specified physical or chemical properties which is improved by the additive characterising the lubricating composition, e.g. multifunctional additives
- C10N2030/64—Environmental friendly compositions
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- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Organic Chemistry (AREA)
- Lubricants (AREA)
Abstract
The invention provides energy-saving environment-friendly agricultural oil which comprises the following components in percentage by weight: the base oil and the additive comprise the following components in percentage by weight: the base oil comprises base oil and additives, wherein the additives account for 7.151-16.102% of the weight of the base oil, and the additives comprise six components: 0.5-2% of ethylene glycol oleate, 0.45-0.6% of ash-free, wear-resistant, oxidation-resistant and corrosion-resistant agent RC9300, 3-10% of polymethacrylate viscosity index improver, 0.001-0.002% of composite anti-foaming agent, 0.2-1% of organic molybdenum nitride and 1.5-4% of boronized polyisobutenyl succinimide. The invention adopts environment-friendly IV and V base oils and is assisted by excellent additives, thus having excellent anti-friction performance, excellent low-temperature performance, excellent oxidation resistance and excellent rust resistance, and the oil product does not contain harmful substances, thereby being energy-saving, environment-friendly and long in service life.
Description
Technical Field
The invention belongs to the field of chemical industry, and particularly relates to energy-saving and environment-friendly agricultural machine oil and a preparation method thereof.
Background
In 2020 proposed in the agricultural machinery development action scheme (2016-.
Disclosure of Invention
The invention provides energy-saving and environment-friendly agricultural machine oil and a preparation method thereof, and solves the problems of environmental pollution and low quality caused by mineral oil products.
The technical scheme of the invention is realized as follows: an energy-saving environment-friendly agricultural oil comprises the following components in percentage by weight: the base oil comprises base oil and additives, wherein the additives account for 7.151-16.102% of the weight of the base oil, and the additives comprise six components: 0.5-2% of ethylene glycol oleate, 0.45-0.6% of ash-free, wear-resistant, oxidation-resistant and corrosion-resistant agent RC9300, 3-10% of polymethacrylate viscosity index improver, 0.001-0.002% of composite anti-foaming agent, 0.2-1% of organic molybdenum nitride and 1.5-4% of boronized polyisobutenyl succinimide;
preferably, the composition comprises the following components in percentage by weight: a base oil and an additive, the additive being 12.0215% by weight of the base oil, the additive comprising six components: 1.2 percent of ethylene glycol oleate, 0.52 percent of RC9300 ashless, wear-resistant, oxidation-resistant and corrosion-resistant agent, 7 percent of polymethacrylate viscosity index improver, 0.0015 percent of composite antifoaming agent, 0.6 percent of organic molybdenum nitride and 2.7 percent of boronized polyisobutenyl succinimide;
preferably, the base oil is polyalphaolefin, alkyl naphthalene and polyester, wherein the base oil polyalphaolefin accounts for 75-85%, the alkyl naphthalene accounts for 10-15% and the polyester accounts for 5-10%;
the method for preparing the environment-friendly agricultural oil comprises the following steps:
(1) adding base oil, a polymethacrylate viscosity index improver and a composite antifoaming agent into a reaction kettle, heating to 60-70 ℃, and stirring for 8-10 minutes;
(2) sequentially adding ethylene glycol oleate, the RC9300 ashless, wear-resistant, anti-oxidation and corrosion-resistant agent, organic molybdenum nitride and boronized polyisobutenyl succinimide, keeping the temperature at 60-70 ℃, stirring for 30 minutes, and filtering by a filter bag of 15 mu m to obtain a finished product.
Polyalphaolefins, which belong to group IV base oils, are made by hydrogenating olefinic oligomers through the polymerization of linear alpha olefins, have a regular wax-free, isoparaffin structure, good low temperature properties, high viscosity index, low volatility and better thermal stability, and are particularly suitable for lubricating oil applications requiring good stability under extreme operating conditions.
Alkyl naphthalene, belonging to group V base oil, is prepared by alkylation of naphthalene and linear alpha olefin, has good thermal stability, oxidation stability and hydrolytic stability, has good solubility, can improve the solubility of base oil to additives and oxidation products, and has excellent detergency.
The polyester belongs to group V base oil and ester copolymer, and has excellent lubricating capacity, high viscosity index, high shearing stability, high oxidation stability, high oil film strength, clean evaporation, low volatility and excellent sealing compatibility.
The oleic acid glycol ester, yellow or brown liquid, has excellent oiliness, oxidation resistance, anti-emulsifying property and antirust property.
The RC9300 ashless, wear-resistant, oxidation-resistant and corrosion-resistant agent has excellent oxidation stability, high bearing capacity, good emulsification resistance and good filterability.
The polymethacrylate viscosity index improver has excellent shear resistance and low-temperature performance, and can improve the fuel economy.
The organic boron nitride has good wear resistance, friction reduction and oxidation resistance, has no corrosiveness, can reduce the friction coefficient of a moving part, and has the performances of energy conservation, temperature reduction and noise reduction.
And (3) composite antifoaming agent: non-silicone oil type antifoaming agents, which can reduce the foaming properties of the product.
A boronized polyisobutenyl succinimide, belonging to a boronized ashless dispersant, has excellent detergency and dispersibility, excellent antioxidant property and high wear resistance.
The invention has the beneficial effects that: the invention has excellent anti-friction performance, excellent low-temperature performance, excellent oxidation resistance and excellent rust resistance, does not contain harmful substances in the oil product, and has the advantages of energy saving, environmental protection and long service life.
Detailed Description
For better understanding and implementation, the following detailed description describes an energy-saving and environment-friendly agricultural oil and a preparation method thereof:
example 1: an energy-saving environment-friendly agricultural oil is prepared from 820kg of base oil poly-alpha-olefin (PAO 6), 120kg of alkyl naphthalene (synestic 5), 60kg of polyester (KL 135), 10kg of additive ethylene glycol oleate, 5kg of RC9300 ashless, anti-wear, anti-oxidation and anti-corrosion agent, 45kg of polymethacrylate viscosity index improver, 0.01kg of composite anti-foaming agent, 7kg of organic molybdenum nitride and 20kg of boronized polyisobutenyl succinimide.
The preparation method comprises the following steps: adding poly-alpha-olefin (PAO 6), alkyl naphthalene (synessic 5), polyester (KL 135), polymethacrylate viscosity index improver and composite anti-foaming agent into a reaction kettle, heating to 65 ℃, stirring for 10 minutes, then sequentially adding ethylene glycol oleate, RC9300 ashless anti-wear, anti-oxidation and anti-corrosion agent, organic molybdenum nitride and boronized polyisobutenyl succinimide, keeping the temperature at 65 ℃, stirring for 30 minutes, and filtering by a filter bag of 15 mu m to obtain a finished product.
Quality index
Example 2: 400kg of base oil polyalphaolefin (PAO 4), 400kg of polyalphaolefin (PAO 6), 100kg of alkyl naphthalene (synessic 12), 100kg of polyester (KL 135), 10kg of oleic acid glycol ester, 5.5kg of RC9300 ashless, anti-wear, anti-oxidation and anti-corrosion agent, 47kg of polymethacrylate viscosity index improver, 0.01kg of composite antifoaming agent, 6kg of organic molybdenum nitride and 25kg of boronated polyisobutenyl succinimide.
The preparation method comprises the following steps: adding poly-alpha olefin (PAO 4), poly-alpha olefin (PAO 6), alkyl naphthalene (synestic 12), polyester (KL 135), polymethacrylate viscosity index improver and composite antifoaming agent into a reaction kettle, heating to 65 ℃, stirring for 10 minutes, then sequentially adding ethylene oleate, RC9300 ashless, anti-wear, anti-oxidation and anti-corrosion agent, organic molybdenum nitride and boronized polyisobutenyl succinimide, keeping the temperature at 65 ℃, stirring for 30 minutes, and filtering by a filter bag of 15 mu m to obtain a finished product.
Quality index
The clean synthetic base oil is used, the energy-saving and environment-friendly additive is selected as the additive, and the high-temperature-resistant and anti-rust oil has excellent anti-friction performance, excellent low-temperature performance, excellent oxidation resistance and excellent rust resistance, does not contain harmful substances in the oil product, is energy-saving and environment-friendly, and has long service life.
Claims (3)
1. An energy-saving environment-friendly agricultural oil is characterized by comprising the following components in percentage by weight: the base oil comprises base oil and additives, wherein the additives account for 7.151-16.102% of the weight of the base oil, and the additives comprise six components: 0.5-2% of ethylene glycol oleate, 0.45-0.6% of ash-free, wear-resistant, oxidation-resistant and corrosion-resistant agent RC9300, 3-10% of polymethacrylate viscosity index improver, 0.001-0.002% of composite anti-foaming agent, 0.2-1% of organic molybdenum nitride and 1.5-4% of boronized polyisobutenyl succinimide; the base oil is poly-alpha-olefin, alkyl naphthalene and polyester, wherein the base oil is 75-85% of poly-alpha-olefin, 10-15% of alkyl naphthalene and 5-10% of polyester.
2. The energy-saving environment-friendly agricultural oil as claimed in claim 1, characterized by comprising the following components by weight percent: a base oil and an additive, the additive being 12.0215% by weight of the base oil, the additive comprising six components: 1.2 percent of ethylene glycol oleate, 0.52 percent of RC9300 ashless, wear-resistant, oxidation-resistant and corrosion-resistant agent, 7 percent of polymethacrylate viscosity index improver, 0.0015 percent of composite antifoaming agent, 0.6 percent of organic molybdenum nitride and 2.7 percent of boronized polyisobutenyl succinimide.
3. A process for preparing an environmentally friendly agricultural oil according to claim 1 or 2, comprising the steps of:
(1) adding base oil, a polymethacrylate viscosity index improver and a composite antifoaming agent into a reaction kettle, heating to 60-70 ℃, and stirring for 8-10 minutes;
(2) sequentially adding ethylene glycol oleate, the RC9300 ashless, wear-resistant, anti-oxidation and corrosion-resistant agent, organic molybdenum nitride and boronized polyisobutenyl succinimide, keeping the temperature at 60-70 ℃, stirring for 30 minutes, and filtering by a filter bag of 15 mu m to obtain a finished product.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201910034557.XA CN109504515B (en) | 2019-01-15 | 2019-01-15 | Energy-saving environment-friendly agricultural machine oil and preparation method thereof |
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| CN201910034557.XA CN109504515B (en) | 2019-01-15 | 2019-01-15 | Energy-saving environment-friendly agricultural machine oil and preparation method thereof |
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| CN109504515A CN109504515A (en) | 2019-03-22 |
| CN109504515B true CN109504515B (en) | 2022-04-12 |
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| CN201910034557.XA Active CN109504515B (en) | 2019-01-15 | 2019-01-15 | Energy-saving environment-friendly agricultural machine oil and preparation method thereof |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN109880680A (en) * | 2019-04-16 | 2019-06-14 | 江苏现代节能科技发展有限公司 | A kind of no phosphorous gasoline engine lubricant oil and preparation method thereof |
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| CN102453589A (en) * | 2010-10-18 | 2012-05-16 | 王严绪 | Sulfur-phosphor-free oil-soluble organic molybdenum additive |
| CN103642563A (en) * | 2013-11-15 | 2014-03-19 | 沈阳中科石化有限公司 | Energy-saving type total synthetic automatic transmission transmission fluid, and synthetic method thereof |
| CN104471101A (en) * | 2012-03-12 | 2015-03-25 | 欧瑞康贸易股份公司(特吕巴赫) | Coating with enhanced sliding properties |
| CN106520327A (en) * | 2016-11-04 | 2017-03-22 | 万德 | Special engine oil for improving engine oil combustion phenomenon of turbocharged engine and preparation method thereof |
| CN106609172A (en) * | 2015-10-21 | 2017-05-03 | 中国石油化工股份有限公司 | Ashless hydraulic oil composition and preparation method and application thereof |
| CN108504420A (en) * | 2017-02-24 | 2018-09-07 | 淄博大创自动化科技有限公司 | A kind of farm machinery special lube |
Family Cites Families (1)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN107828480B (en) * | 2017-10-30 | 2020-12-25 | 江苏龙蟠科技股份有限公司 | High-performance synthetic power-assisted steering oil composition and preparation method thereof |
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- 2019-01-15 CN CN201910034557.XA patent/CN109504515B/en active Active
Patent Citations (6)
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| CN102453589A (en) * | 2010-10-18 | 2012-05-16 | 王严绪 | Sulfur-phosphor-free oil-soluble organic molybdenum additive |
| CN104471101A (en) * | 2012-03-12 | 2015-03-25 | 欧瑞康贸易股份公司(特吕巴赫) | Coating with enhanced sliding properties |
| CN103642563A (en) * | 2013-11-15 | 2014-03-19 | 沈阳中科石化有限公司 | Energy-saving type total synthetic automatic transmission transmission fluid, and synthetic method thereof |
| CN106609172A (en) * | 2015-10-21 | 2017-05-03 | 中国石油化工股份有限公司 | Ashless hydraulic oil composition and preparation method and application thereof |
| CN106520327A (en) * | 2016-11-04 | 2017-03-22 | 万德 | Special engine oil for improving engine oil combustion phenomenon of turbocharged engine and preparation method thereof |
| CN108504420A (en) * | 2017-02-24 | 2018-09-07 | 淄博大创自动化科技有限公司 | A kind of farm machinery special lube |
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