CN109490467A - The prior-warning device and method for early warning of NMP concentration over-standard in lithium titanate battery coating process - Google Patents
The prior-warning device and method for early warning of NMP concentration over-standard in lithium titanate battery coating process Download PDFInfo
- Publication number
- CN109490467A CN109490467A CN201710824231.8A CN201710824231A CN109490467A CN 109490467 A CN109490467 A CN 109490467A CN 201710824231 A CN201710824231 A CN 201710824231A CN 109490467 A CN109490467 A CN 109490467A
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- Prior art keywords
- nmp
- standard
- baking oven
- coating process
- lithium titanate
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- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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- 238000000576 coating method Methods 0.000 title claims abstract description 35
- WHXSMMKQMYFTQS-UHFFFAOYSA-N Lithium Chemical compound [Li] WHXSMMKQMYFTQS-UHFFFAOYSA-N 0.000 title claims abstract description 26
- 229910052744 lithium Inorganic materials 0.000 title claims abstract description 26
- RTAQQCXQSZGOHL-UHFFFAOYSA-N Titanium Chemical compound [Ti] RTAQQCXQSZGOHL-UHFFFAOYSA-N 0.000 title claims abstract description 24
- 238000000034 method Methods 0.000 title claims abstract description 17
- 238000001514 detection method Methods 0.000 claims abstract description 25
- 239000011888 foil Substances 0.000 claims abstract description 14
- 239000011248 coating agent Substances 0.000 claims abstract description 11
- 239000003795 chemical substances by application Substances 0.000 claims abstract description 3
- 238000002347 injection Methods 0.000 claims description 3
- 239000007924 injection Substances 0.000 claims description 3
- 238000011897 real-time detection Methods 0.000 claims description 3
- 239000000463 material Substances 0.000 claims description 2
- SECXISVLQFMRJM-UHFFFAOYSA-N N-Methylpyrrolidone Chemical compound CN1CCCC1=O SECXISVLQFMRJM-UHFFFAOYSA-N 0.000 description 41
- 238000004519 manufacturing process Methods 0.000 description 3
- BAVYZALUXZFZLV-UHFFFAOYSA-N Methylamine Chemical compound NC BAVYZALUXZFZLV-UHFFFAOYSA-N 0.000 description 2
- 230000008901 benefit Effects 0.000 description 2
- 238000010586 diagram Methods 0.000 description 2
- 239000007788 liquid Substances 0.000 description 2
- 239000002002 slurry Substances 0.000 description 2
- YEJRWHAVMIAJKC-UHFFFAOYSA-N 4-Butyrolactone Chemical compound O=C1CCCO1 YEJRWHAVMIAJKC-UHFFFAOYSA-N 0.000 description 1
- HBBGRARXTFLTSG-UHFFFAOYSA-N Lithium ion Chemical compound [Li+] HBBGRARXTFLTSG-UHFFFAOYSA-N 0.000 description 1
- 208000027418 Wounds and injury Diseases 0.000 description 1
- 230000006378 damage Effects 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 238000004880 explosion Methods 0.000 description 1
- 208000014674 injury Diseases 0.000 description 1
- 229910001416 lithium ion Inorganic materials 0.000 description 1
- 238000012544 monitoring process Methods 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 238000004064 recycling Methods 0.000 description 1
- 239000000243 solution Substances 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
- 238000006467 substitution reaction Methods 0.000 description 1
- 231100000331 toxic Toxicity 0.000 description 1
- 230000002588 toxic effect Effects 0.000 description 1
Classifications
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N33/00—Investigating or analysing materials by specific methods not covered by groups G01N1/00 - G01N31/00
- G01N33/0004—Gaseous mixtures, e.g. polluted air
- G01N33/0009—General constructional details of gas analysers, e.g. portable test equipment
- G01N33/0062—General constructional details of gas analysers, e.g. portable test equipment concerning the measuring method or the display, e.g. intermittent measurement or digital display
- G01N33/0063—General constructional details of gas analysers, e.g. portable test equipment concerning the measuring method or the display, e.g. intermittent measurement or digital display using a threshold to release an alarm or displaying means
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- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Health & Medical Sciences (AREA)
- Medicinal Chemistry (AREA)
- Food Science & Technology (AREA)
- Combustion & Propulsion (AREA)
- Physics & Mathematics (AREA)
- Analytical Chemistry (AREA)
- Biochemistry (AREA)
- General Health & Medical Sciences (AREA)
- General Physics & Mathematics (AREA)
- Immunology (AREA)
- Pathology (AREA)
- Battery Electrode And Active Subsutance (AREA)
Abstract
The invention discloses the prior-warning devices and method for early warning of NMP concentration over-standard in lithium titanate battery coating process, prior-warning device includes for the coater head of coating sizing-agent, baking oven, detection unit and alarm unit on foil band, the coater head and baking oven are arranged in same level, and the detection unit is arranged in baking oven and connect with the alarm unit being arranged in outside baking oven;When foil band by the coater head complete coating after by the baking oven when, detection unit detect oven interior NMP concentration, when concentration be greater than preset value when, alarm unit alarm, avoid the problem of influencing pole piece caking property because of NMP concentration over-standard.
Description
Technical field
The invention belongs to lithium ion power battery technology fields, and in particular to NMP concentration in lithium titanate battery coating process
Exceeded prior-warning device and method for early warning.
Background technique
N-Methyl pyrrolidone (NMP) is colourless transparent liquid, is one kind using gamma-butyrolacton as raw material, is condensed with methylamine
Into liquid, it is widely used in the production of lithium batteries.
In electrode of lithium cell manufacturing process, gaseous state, NMP gas will form after solvent NMP in coating machine slurry is heated
Body is toxic, there is the possibility of explosion when having injury to human body, and mixing with air;In addition, the concentration of NMP has pole piece caking property
Very big influence, the rate of volatilization of surface pole piece NMP will have a direct impact on the caking property of pole piece, and the pole piece of bad adhesion can not carry out
Compacting;And NMP takes away not in time, and NMP excessive concentration also will affect the caking property of coating pole piece inside coater oven;Therefore
The monitoring of NMP is not only related to the energy-saving and emission-reduction benefit of battery production enterprise with recycling, and even more concern personnel health and life peace
Full cardinal task.
Summary of the invention
The object of the present invention is to provide the prior-warning devices of NMP concentration over-standard in lithium titanate battery coating process, pass through detection
The cooperation of unit and alarm unit solves the problems, such as to influence pole piece caking property because of NMP concentration over-standard.
It is a further object of the present invention to provide the method for early warning of NMP concentration over-standard in lithium titanate battery coating process.
The technical scheme adopted by the invention is that:
The prior-warning device of NMP concentration over-standard in lithium titanate battery coating process comprising for being coated with slurry on foil band
Coater head, baking oven, detection unit and the alarm unit of material, the coater head and baking oven are arranged in same level, institute
Detection unit is stated to be arranged in baking oven and connect with the alarm unit being arranged in outside baking oven;
When foil band by the coater head complete coating after by the baking oven when, detection unit detect oven interior
The concentration of NMP, when concentration is greater than preset value, alarm unit alarm.
The features of the present invention also characterized in that
Air outlet is provided on the baking oven.
The detection unit is gas detector, and the gas detector is arranged at air outlet.
The coater head is direct injection coater head.
The alarm unit is tri coloured lantern.
The method for early warning of NMP concentration over-standard in lithium titanate battery coating process, using above-mentioned lithium titanate battery coating process
The prior-warning device of middle NMP concentration over-standard, is specifically implemented according to the following steps:
Step 1, foil band is coated by coater head;
Step 2, the foil band after being coated by baking oven to the step 1 toasts, while detection unit is real-time
Detect the concentration of oven interior NMP;
Step 3, when the concentration of the NMP of the step 2 detection is greater than secure threshold, alarm unit alarm.
The features of the present invention also characterized in that
The walking speed of coater head is less than or equal to 25m/min in the step 1.
The concentration of oven interior NMP is detected in the step 2 method particularly includes: by exhausting motor by gas in baking oven
It is evacuated at air outlet, the concentration of NMP is detected by the way that the gas detector at air outlet is arranged in.
The range of the concentration secure threshold of NMP in the step 3 are as follows: 14%-16%.
The exhausting motor power is 7.5-10kw, frequency 50HZ.
Compared with prior art, in use, passing through the concentration of NMP in detection unit real-time detection baking oven, when concentration is greater than
When secure threshold, alarm unit alarm avoids the problem of influencing pole piece caking property because of NMP concentration over-standard.
Detailed description of the invention
Fig. 1 is that the embodiment of the present invention provides the structure of the prior-warning device of NMP concentration over-standard in lithium titanate battery coating process
Schematic diagram;
Fig. 2 be the embodiment of the present invention provide lithium titanate battery coating process in NMP concentration over-standard prior-warning device in baking oven
Structural schematic diagram.
Specific embodiment
In order to make the objectives, technical solutions, and advantages of the present invention clearer, with reference to the accompanying drawings and embodiments, right
The present invention is further elaborated.It should be appreciated that the specific embodiments described herein are merely illustrative of the present invention, and
It is not used in the restriction present invention.
The embodiment of the present invention provides the prior-warning device of NMP concentration over-standard in lithium titanate battery coating process, such as Fig. 1-2 institute
Show comprising for the coater head 1 of coating sizing-agent, baking oven 2, detection unit 3 and alarm unit 4 on foil band, coating
Head 1 and baking oven 2 are arranged in same level, detection unit 3 be arranged in baking oven 2 and with the alarm list that is arranged in outside baking oven 2
Member 4 connects, and coater head 1 is direct injection coater head;In this way, when foil band by coater head 1 complete coating after through baking
When case 2, detection unit 3 detects the concentration of 2 inside NMP of baking oven, and when concentration is greater than secure threshold, alarm unit 4 is alarmed.
It is provided with air outlet on baking oven 2, in this way, taking the NMP inside baking oven 2 in time away by air outlet, avoids baking
NMP excessive concentration influences the caking property of coating pole piece inside case.
Detection unit 3 is gas detector, gas detector model MicroGAS D9200Ex, gas detector setting
At air outlet, in this way, the concentration of NMP can be detected at air outlet.
Alarm unit 4 is tri coloured lantern, in this way, tri coloured lantern flashing reminds operator to pay attention to NMP concentration.
The method for early warning of NMP concentration over-standard in lithium titanate battery coating process, using above-mentioned lithium titanate battery coating process
The prior-warning device of middle NMP concentration over-standard, is specifically implemented according to the following steps:
Step 1, foil band is coated by coater head 1, the walking speed of coater head 1 is less than or equal to 25m/min;
Step 2, the foil band after being coated by baking oven 2 to step 1 toasts, while detection unit 3 is examined in real time
Survey the concentration of 2 inside NMP of baking oven;Method particularly includes: gas in baking oven 2 is evacuated at air outlet by exhausting motor, by setting
The concentration of the gas detector detection NMP at air outlet is set, exhausting motor power is 7.5-10kw, frequency 50HZ;
Step 3, when the concentration of the NMP detected when step 2 is greater than secure threshold, alarm unit 4 is alarmed, the concentration peace of NMP
The range of full threshold value are as follows: 14%-16%.
Using the above scheme, compared with prior art, in use, by detection unit real-time detection baking oven NMP it is dense
Degree, when concentration is greater than secure threshold, alarm unit alarm, avoiding influences asking for pole piece caking property because of NMP concentration over-standard
Topic.
The foregoing is only a preferred embodiment of the present invention, but scope of protection of the present invention is not limited thereto,
In the technical scope disclosed by the present invention, any changes or substitutions that can be easily thought of by anyone skilled in the art,
It should be covered by the protection scope of the present invention.Therefore, protection scope of the present invention should be with scope of protection of the claims
Subject to.
Claims (10)
1. the prior-warning device of NMP concentration over-standard in a kind of lithium titanate battery coating process, which is characterized in that it includes in foil
The coater head of coating sizing-agent, baking oven, detection unit and alarm unit on material band, the coater head and baking oven are arranged same
One horizontal plane, the detection unit are arranged in baking oven and connect with the alarm unit being arranged in outside baking oven;
When foil band after the coater head completes coating by the baking oven when, the detection unit detects oven interior
The concentration of NMP, when concentration is greater than secure threshold, alarm unit alarm.
2. the prior-warning device of NMP concentration over-standard, feature exist in lithium titanate battery coating process according to claim 1
In being provided with air outlet on the baking oven.
3. the prior-warning device of NMP concentration over-standard, feature exist in lithium titanate battery coating process according to claim 2
In the detection unit is gas detector, and the gas detector is arranged at air outlet.
4. the prior-warning device of NMP concentration over-standard in lithium titanate battery coating process according to claim 1-3,
It is characterized in that, the coater head is direct injection coater head.
5. the prior-warning device of NMP concentration over-standard, feature exist in lithium titanate battery coating process according to claim 4
In the alarm unit is tri coloured lantern.
6. a kind of early warning using NMP concentration over-standard in the described in any item lithium titanate battery coating process of claim 1-5 fills
The method for early warning set, which is characterized in that this method is specifically implemented according to the following steps:
Step 1, foil band is coated by coater head;
Step 2, the foil band after being coated by baking oven to the step 1 toasts, while detection unit real-time detection
The concentration of oven interior NMP;
Step 3, when the concentration of the NMP of the step 2 detection is greater than secure threshold, alarm unit alarm.
7. the method for early warning of NMP concentration over-standard, feature exist in lithium titanate battery coating process according to claim 6
In the walking speed of coater head is less than or equal to 25m/min in the step 1.
8. the method for early warning of NMP concentration over-standard, feature exist in lithium titanate battery coating process according to claim 7
In the concentration of detection oven interior NMP in the step 2 method particularly includes: be evacuated to gas in baking oven by exhausting motor
At air outlet, the concentration of NMP is detected by the way that the gas detector at air outlet is arranged in.
9. the method for early warning of NMP concentration over-standard, feature exist in lithium titanate battery coating process according to claim 8
In the range of the concentration secure threshold of NMP in the step 3 are as follows: 14%-16%.
10. the method for early warning of NMP concentration over-standard, feature exist in lithium titanate battery coating process according to claim 9
In the exhausting motor power is 7.5-10kw, frequency 50HZ.
Priority Applications (1)
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CN201710824231.8A CN109490467A (en) | 2017-09-13 | 2017-09-13 | The prior-warning device and method for early warning of NMP concentration over-standard in lithium titanate battery coating process |
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CN201710824231.8A CN109490467A (en) | 2017-09-13 | 2017-09-13 | The prior-warning device and method for early warning of NMP concentration over-standard in lithium titanate battery coating process |
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-
2017
- 2017-09-13 CN CN201710824231.8A patent/CN109490467A/en active Pending
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