CN109485039A - A kind of purification devices and its method of graphene oxide - Google Patents
A kind of purification devices and its method of graphene oxide Download PDFInfo
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- CN109485039A CN109485039A CN201811373362.XA CN201811373362A CN109485039A CN 109485039 A CN109485039 A CN 109485039A CN 201811373362 A CN201811373362 A CN 201811373362A CN 109485039 A CN109485039 A CN 109485039A
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- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B32/00—Carbon; Compounds thereof
- C01B32/15—Nano-sized carbon materials
- C01B32/182—Graphene
- C01B32/198—Graphene oxide
Abstract
The invention discloses a kind of purification devices of graphene oxide and its methods, the purification devices of graphene oxide therein include agitator tank and the Rose Box positioned at agitator tank side, filter plate is fixedly installed in the bottom interior wall of the Rose Box, the top of filter plate is extended to the over the top of filter box, the top of filter plate offers the first groove, the first hole is offered on the two sides inner wall of first groove, sealing is slidably installed in first groove, and there are two sliding seats, the same filter membrane is fixedly installed between two sliding seats, the first magnet is fixedly installed at the top of a sliding seat in two sliding seats, the top of first magnet is equipped with one end of the first spring.The present invention has rational design, and practical performance is high, convenient for shaking in use to filter membrane, to place the blocking of filter membrane, and convenient for dismantling to filter membrane, convenient for replacing to filter membrane, is conducive to the use of people.
Description
Technical field
The present invention relates to a kind of purifying of the purifier apparatus technical field of graphene oxide more particularly to graphene oxide dresses
It sets and its method.
Background technique
Graphene oxide is the oxide of graphene, and color is brown color, and common product has powdered, piece on the market
Shape and solution shape.Through retrieving, Authorization Notice No. is that the patent document of CN108275677A discloses one kind for purifying oxygen
The right side of the reaction chamber is arranged in the equipment of graphite alkene solution, including reaction chamber and Rose Box, the Rose Box, and described
It is connected between reaction chamber and Rose Box by liquid pass hole, stirring rod, the interior bottom of the reaction chamber is provided in the reaction chamber
Left side is provided with supersonic generator；The inside of the Rose Box is provided with filter membrane, and the inside of filtering is divided by the filter membrane
The left-hand face top of two parts, the filter membrane is provided with spray head, and the spray head is mounted on the output end of solenoid valve, described
The input terminal of solenoid valve and the output end of water pump are connected by pipeline.Water pump is sucked the solution in reaction chamber by pipette,
Then control out liquid by solenoid valve, the attachment of filter membrane surface washed away, it is easy to use, by supersonic generator and
Stirring rod makes the solution motion in reaction chamber, can accelerate the speed of solution reaction.
But above-mentioned design, there is also shortcoming, filter membrane is easy to happen blocking in above-mentioned design, rushes with water to filter membrane
Brush is easily damaged filter membrane, and when filter membrane damage, is not easy to replace filter membrane, is unfavorable for the use of people, therefore we mention
The purification devices and its method for having gone out a kind of graphene oxide are for solving the above problems.
Summary of the invention
Technical problems based on background technology, the invention proposes a kind of purification devices of graphene oxide and its sides
Method.
A kind of purification devices of graphene oxide proposed by the present invention, the filtering including agitator tank and positioned at agitator tank side
Case is fixedly installed with filter plate in the bottom interior wall of the Rose Box, and the top of filter plate is extended to the over the top of filter box, filtering
The top of plate offers the first groove, and the first hole is offered on the two sides inner wall of the first groove, sealing sliding in the first groove
Installation is fixedly installed with the same filter membrane, a sliding seat in two sliding seats between two sliding seats there are two sliding seat
Top be fixedly installed with the first magnet, the top of the first magnet is equipped with one end of the first spring, and the other end of the first spring is solid
Surely it is connected with fixing seat, and fixing seat is adapted with the first groove, the two sides of fixing seat offer fixing groove, the first groove
The second groove is offered on the inner wall of two sides, is slidably fitted with fixed link in the second groove, and fixed link and corresponding fixing groove
It is adapted, one end that two fixed links are located remotely from each other is fixedly installed with one end of pull rod, and the other end of pull rod extends to filtering
The outside of plate is simultaneously fixedly installed with the first in command, and the first in command is the top of Rose Box, and movable sleeve is equipped with the second bullet on pull rod
Spring, the other end of second spring are fixedly installed in corresponding fixed link, and the other end of second spring is fixedly mounted on corresponding
On the inner wall of second groove, the second hole is offered in the top inner wall of the second groove, screw rod set, spiral shell are fixedly installed on the second hole
Thread bush is equipped with screw rod in rod set, and the bottom of screw rod is in contact with fixed link, and the top of filter plate is extended to the at the top of screw rod simultaneously
It is fixedly installed with rotary switch；
Third hole is offered in the bottom interior wall of first groove, and vertical bar, and the top of vertical bar are slidably fitted in third hole
It is in contact with the other end sliding seat in two sliding seats, the bottom of vertical bar is extended to the over the lower section of filter box, the bottom of Rose Box
It being fixedly mounted there are two attachment base, is rotatably equipped with the same shaft between two attachment bases, fixing sleeve is equipped with cam in shaft,
And cam is adapted with vertical bar, one end of shaft through an attachment base and is fixedly installed with the first sprocket wheel, the bottom of Rose Box
It is fixedly installed with rotating electric machine, the second sprocket wheel, and the second sprocket wheel and the first sprocket wheel are fixedly installed on the output shaft of rotating electric machine
Between be sequentially connected with chain.
Preferably, ring groove is offered on the sliding seat, and sealing ring, and sealing ring are fixedly installed in ring groove
It is slidably and sealingly connected with the first groove.
Preferably, the same support rod is fixedly installed between two sliding seats, and support rod is located at the side of filter membrane.
Preferably, the first limiting slot is offered in the bottom interior wall of second groove, the bottom of fixed link is fixedly mounted
There is the first limited block, and the first limited block is slidably connected with corresponding first limiting slot.
Preferably, the first intercommunicating pore is offered on side inner wall of second groove far from its opening, and pull rod runs through
Corresponding first intercommunicating pore.
Preferably, the screw rod, which is put on, offers threaded hole, and screw rod is threadedly coupled with corresponding threaded hole.
Preferably, the bottom of the Rose Box offers the second intercommunicating pore, and the second intercommunicating pore is connected with third hole, and perpendicular
Bar is slidably connected with the second intercommunicating pore.
Preferably, the side of the vertical bar offers the second limiting slot, is fixedly mounted on the side inner wall of the second intercommunicating pore
There is the second limited block, and the second limited block is slidably connected with the second limiting slot.
Preferably, the other end fixing sleeve of the shaft is equipped with bearing, and the outer ring of bearing is fixedly mounted on another company
On joint chair.
The invention also provides a kind of application methods of the purification devices of graphene oxide, comprising the following steps:
S1: when Rose Box works, starting rotating electric machine, and rotating electric machine drives the second sprocket wheel to be rotated by output shaft, due to
Second sprocket wheel is sequentially connected by chain and the first sprocket wheel, so the rotation of the second sprocket wheel is carried out by the first sprocket wheel of chain-driving
Rotation, the first sprocket wheel drive shaft to be rotated；
S2: carrying out rotating shaft, and the rotation band moving cam of shaft is rotated, and the rotation of cam drives vertical bar to carry out up and down reciprocatingly
Movement, when vertical bar moves up, vertical bar drives another sliding seat to be moved, another sliding seat drives filter membrane to moving up
Dynamic, filter membrane drives another sliding seat to move up and compresses the first spring, when vertical bar moves down, in the bullet of the first spring
Under power effect, so that filter membrane and sliding seat move down, so that the vibration of filter membrane is realized, to place the blocking of filter membrane；
S3: when filter membrane uses overlong time, when the poor filtration effect of filter membrane, filter membrane is replaced, turning knob is opened first
It closes, rotary switch drives screw rod to be moved, and under the action of screw rod set, screw rod moves while rotating, thus with fixation
Bar separation releases the purpose that fixed link is fixed, the mobile first in command, and the first in command drives pull rod to move, pull rod
Fixed link is driven to be moved and compressed second spring, the movement of fixed link, so that fixed link is detached from fixing groove, thus releasing pair
The fixation of fixing seat, moves up fixing seat, and fixing seat drives the first spring to be moved, the first spring drive the first magnet into
Row movement, the first magnet drives sliding seat to be moved, to dismantle to filter membrane, consequently facilitating replacing to filter membrane.
Compared with prior art, the beneficial effects of the present invention are:
(1) it is matched by rotating electric machine, the second sprocket wheel, chain, the first sprocket wheel and shaft, starts rotating electric machine, rotating electric machine
The second sprocket wheel is driven to be rotated by output shaft, since the second sprocket wheel is sequentially connected by chain and the first sprocket wheel, so the
The rotation of two sprocket wheels is rotated by the first sprocket wheel of chain-driving, and the first sprocket wheel drives shaft to be rotated；
(2) it is matched by cam, vertical bar, sliding seat, filter membrane, fixing seat, spring and the first magnet, the rotation of shaft drives convex
Wheel is rotated, and the rotation of cam drives vertical bar to pump, and when vertical bar moves up, vertical bar drives another
Sliding seat is moved, another sliding seat drives filter membrane to move up, and filter membrane drives another sliding seat to move up and presses
Contract the first spring, when vertical bar moves down, under the elastic force effect of the first spring, so that filter membrane and sliding seat move down,
To realize the vibration of filter membrane, to place the blocking of filter membrane；
(3) by rotary switch, screw rod, screw rod set, fixed link, fixing groove, the first in command, pull rod, second spring, fixing seat,
First spring, the first magnet and sliding seat match, and turning knob switch, rotary switch drives screw rod to be moved, in screw rod
Under the action of set, screw rod moves while rotating, to separate with fixed link, releases the purpose that fixed link is fixed,
The mobile first in command, the first in command drive pull rod to move, and pull rod drives fixed link to be moved and compressed second spring, Gu
The movement of fixed pole, to release the fixation to fixing seat, moves up fixing seat, fixing seat so that fixed link is detached from fixing groove
The first spring is driven to be moved, the first spring drives the first magnet to be moved, and the first magnet drives sliding seat to be moved,
To be dismantled to filter membrane, consequently facilitating being replaced to filter membrane.
The present invention has rational design, and practical performance is high, convenient for shaking in use to filter membrane, to place filter membrane
Blocking convenient for replacing to filter membrane, be conducive to the use of people and convenient for dismantling to filter membrane.
Detailed description of the invention
Fig. 1 is a kind of structural schematic diagram of the purification devices of graphene oxide proposed by the present invention；
Fig. 2 is a kind of structural schematic diagram of the part A of the purification devices of graphene oxide proposed by the present invention；
Fig. 3 is a kind of structural schematic diagram of the part B of the purification devices of graphene oxide proposed by the present invention；
Fig. 4 is a kind of structural schematic diagram of the C portion of the purification devices of graphene oxide proposed by the present invention；
Fig. 5 is a kind of structural schematic diagram of the part D of the purification devices of graphene oxide proposed by the present invention.
In figure: 1 agitator tank, 2 Rose Boxes, 3 filter plates, 4 first grooves, 5 first holes, 6 sliding seats, 7 filter membranes, 8 first magnetic
Iron, 9 first springs, 10 fixing seats, 11 fixing grooves, 12 second grooves, 13 fixed links, 14 pull rods, 15 first in command, 16 second bullets
It is spring, 17 second holes, 18 screw rod sets, 19 screw rods, 20 rotary switches, 21 third holes, 22 vertical bars, 23 attachment bases, 24 shafts, 25 convex
Wheel, 26 first sprocket wheels, 27 rotating electric machines, 28 third sprocket wheels, 29 chains.
Specific embodiment
Combined with specific embodiments below the present invention is made further to explain.
Embodiment
With reference to Fig. 1-5, a kind of purification devices of graphene oxide are proposed in the present embodiment, including agitator tank 1 and be located at
The Rose Box 2 of 1 side of agitator tank is fixedly installed with filter plate 3 in the bottom interior wall of Rose Box 2, and the top of filter plate 3 extends to
The top of Rose Box 2, the top of filter plate 3 offer the first groove 4, offer first on the two sides inner wall of the first groove 4
Hole 5, sealing is slidably installed there are two sliding seat 6 in the first groove 4, is fixedly installed with the same filter membrane between two sliding seats 6
7, the top of a sliding seat 6 in two sliding seats 6 is fixedly installed with the first magnet 8, and the top of the first magnet 8 is equipped with first
One end of spring 9, the other end of the first spring 9 is fixedly connected with fixing seat 10, and fixing seat 10 is adapted with the first groove 4,
The two sides of fixing seat 10 offer fixing groove 11, the second groove 12 are offered on the two sides inner wall of the first groove 4, second is recessed
Fixed link 13 is slidably fitted in slot 12, and fixed link 13 is adapted with corresponding fixing groove 11, two fixed links 13 are mutually remote
From one end be fixedly installed with one end of pull rod 14, the other end of pull rod 14 is extended to the over the outside of filter plate 3 and fixed installation
There is the first in command 15, and the first in command 15 is the top of Rose Box 2, movable sleeve is equipped with second spring 16, the second bullet on pull rod 14
The other end of spring 16 is fixedly installed in corresponding fixed link 13, and the other end of second spring 16 is fixedly mounted on corresponding second
On the inner wall of groove 12, the second hole 17 is offered in the top inner wall of the second groove 12, is fixedly installed with screw rod on the second hole 17
Set 18, screw rod cover thread bush on 18 and are equipped with screw rod 19, and the bottom of screw rod 19 is in contact with fixed link 13, and the top of screw rod 19 extends
To filter plate 3 top and be fixedly installed with rotary switch 20, third hole 21 is offered in the bottom interior wall of the first groove 4,
Vertical bar 22 is slidably fitted in three holes 21, and the top of vertical bar 22 is in contact with the other end sliding seat 6 in two sliding seats 6,
The bottom of vertical bar 22 is extended to the over the lower section of filter box 2, and the bottom of Rose Box 2 is fixedly mounted there are two attachment base 23, and two connect
It is rotatably equipped with the same shaft 24 between seat 23, fixing sleeve is equipped with cam 25 in shaft 24, and cam 25 and 22 phase of vertical bar are suitable
Match, one end of shaft 24 through an attachment base 23 and is fixedly installed with the first sprocket wheel 26, and the bottom of Rose Box 2 is fixedly installed with
Rotating electric machine 27 is fixedly installed with the second sprocket wheel 28, and the second sprocket wheel 28 and the first sprocket wheel 26 on the output shaft of rotating electric machine 27
Between be sequentially connected with chain 29, pass through rotating electric machine 27, the second sprocket wheel 28, chain 29, the first sprocket wheel 26 and shaft 24 match
It closes, starts rotating electric machine 27, rotating electric machine 27 drives the second sprocket wheel 28 to be rotated by output shaft, since the second sprocket wheel 28 is logical
It crosses chain 29 and the first sprocket wheel 26 is sequentially connected, so the rotation of the second sprocket wheel 28 drives the first sprocket wheel 26 to carry out by chain 29
Rotation, the first sprocket wheel 26 drive shaft 24 to be rotated, pass through cam 25, vertical bar 22, sliding seat 6, filter membrane 7, fixing seat 10, bullet
Spring 9 and the first magnet 8 match, and the rotation of shaft 24 band moving cam 25 is rotated, the rotation of cam 25 drive vertical bar 22 into
Row pumps, and when vertical bar 22 moves up, vertical bar 22 drives another sliding seat 6 to be moved, another sliding
Seat 6 drive filter membranes 7 move up, filter membrane 7 drive another sliding seat 6 move up and compress the first spring 9, when vertical bar 22 to
When lower mobile, under the elastic force effect of the first spring 9, so that filter membrane 7 and sliding seat 6 move down, to realize filter membrane 7
Vibration passes through rotary switch 20, screw rod 19, screw rod set 18, fixed link 13, fixing groove 11, the to place the blocking of filter membrane 7
Leader 15, pull rod 14, second spring 16, fixing seat 10, the first spring 9, the first magnet 8 and sliding seat 6 match, rotation rotation
Button switch 20, rotary switch 20 drive screw rod 19 to be moved, and under the action of screw rod set 18, screw rod 19 moves while rotating
It is dynamic, to separate with fixed link 13, the purpose that fixed link 13 is fixed is released, the mobile first in command 15, the first in command 15
Pull rod 14 is driven to be moved, pull rod 14 drives fixed link 13 to be moved and compressed second spring 16, the movement of fixed link 13,
So that fixed link 13 is detached from fixing groove 11, to release the fixation to fixing seat 10, fixing seat 10,10 band of fixing seat are moved up
Dynamic first spring 9 is moved, and the first spring 9 drives the first magnet 8 to be moved, and the first magnet 8 drives sliding seat 6 to be moved
Dynamic, to dismantle to filter membrane 7, consequently facilitating replacing to filter membrane 7, the present invention has rational design, and practical performance is high, is convenient for
Filter membrane 7 is shaken in use, to place the blocking of filter membrane 7, and convenient for being dismantled to filter membrane 7, convenient for pair
Filter membrane 7 is replaced, and the use of people is conducive to.
In the present embodiment, ring groove is offered on sliding seat 6, sealing ring is fixedly installed in ring groove, and seal
Circle is slidably and sealingly connected with the first groove 4, is fixedly installed with the same support rod between two sliding seats 6, and support rod is located at
The side of filter membrane 7 offers the first limiting slot in the bottom interior wall of second groove 12, and the bottom of fixed link 13 is fixedly installed with
One limited block, and the first limited block is slidably connected with corresponding first limiting slot, in side of second groove 12 far from its opening
The first intercommunicating pore is offered on wall, and pull rod 14 runs through corresponding first intercommunicating pore, offers threaded hole, and spiral shell on screw rod set 18
Bar 19 is threadedly coupled with corresponding threaded hole, and the bottom of Rose Box 2 offers the second intercommunicating pore, the second intercommunicating pore and third hole 21
It is connected, and vertical bar 22 is slidably connected with the second intercommunicating pore, the side of vertical bar 22 offers the second limiting slot, the second intercommunicating pore
The second limited block is fixedly installed on the inner wall of side, and the second limited block is slidably connected with the second limiting slot, shaft 24 it is another
Fixing sleeve is held to be equipped with bearing, and the outer ring of bearing is fixedly mounted on another attachment base 23, passes through rotating electric machine 27, the second chain
Wheel 28, chain 29, the first sprocket wheel 26 and shaft 24 match, and start rotating electric machine 27, and rotating electric machine 27 is driven by output shaft
Second sprocket wheel 28 is rotated, since the second sprocket wheel 28 is sequentially connected by chain 29 and the first sprocket wheel 26, so the second sprocket wheel
28 rotation drives the first sprocket wheel 26 to be rotated by chain 29, and the first sprocket wheel 26 drives shaft 24 to be rotated, by convex
Wheel 25, vertical bar 22, sliding seat 6, filter membrane 7, fixing seat 10, spring 9 and the first magnet 8 match, and the rotation of shaft 24 drives convex
Wheel 25 is rotated, and the rotation of cam 25 drives vertical bar 22 to pump, when vertical bar 22 moves up, vertical bar 22
Another sliding seat 6 is driven to be moved, another sliding seat 6 drives filter membrane 7 to move up, and filter membrane 7 drives another sliding
Seat 6 moves up and compresses the first spring 9, when vertical bar 22 moves down, under the elastic force effect of the first spring 9, so that filter
Film 7 and sliding seat 6 move down, to realize the vibration of filter membrane 7, to place the blocking of filter membrane 7, pass through rotary switch
20, screw rod 19, screw rod set 18, fixed link 13, fixing groove 11, the first in command 15, pull rod 14, second spring 16, fixing seat 10, the
One spring 9, the first magnet 8 and sliding seat 6 match, turning knob switch 20, and rotary switch 20 drives screw rod 19 to be moved,
Under the action of screw rod set 18, screw rod 19 moves while rotating, to be separated with fixed link 13, release to fixed link 13 into
The fixed purpose of row, the mobile first in command 15, the first in command 15 drive pull rod 14 to move, pull rod 14 drive fixed link 13 into
Row is mobile and compresses second spring 16, the movement of fixed link 13, so that fixed link 13 is detached from fixing groove 11, to release to fixation
The fixation of seat 10 moves up fixing seat 10, and fixing seat 10 drives the first spring 9 to be moved, and the first spring 9 drives the first magnetic
Iron 8 is moved, and the first magnet 8 drives sliding seat 6 to be moved, to dismantle to filter membrane 7, consequently facilitating to filter membrane 7
It is replaced, the present invention has rational design, and practical performance is high, convenient for shaking in use to filter membrane 7, to place filter
The blocking of film 7, and convenient for being dismantled to filter membrane 7, convenient for replacing to filter membrane 7, be conducive to the use of people.
The present embodiment also proposed a kind of application method of the purification devices of graphene oxide, comprising the following steps:
S1: when Rose Box 2 works, start rotating electric machine 27, rotating electric machine 27 drives 28 turns of the second sprocket wheel by output shaft
It is dynamic, since the second sprocket wheel 28 is sequentially connected by chain 29 and the first sprocket wheel 26, so the rotation of the second sprocket wheel 28 passes through chain
29 the first sprocket wheels 26 of drive are rotated, and the first sprocket wheel 26 drives shaft 24 to be rotated；
S2: carrying out rotating shaft 24, and the rotation band moving cam 25 of shaft 24 is rotated, the rotation of cam 25 drive vertical bar 22 into
Row pumps, and when vertical bar 22 moves up, vertical bar 22 drives another sliding seat 6 to be moved, another sliding
Seat 6 drive filter membranes 7 move up, filter membrane 7 drive another sliding seat 6 move up and compress the first spring 9, when vertical bar 22 to
When lower mobile, under the elastic force effect of the first spring 9, so that filter membrane 7 and sliding seat 6 move down, to realize filter membrane 7
Vibration, to place the blocking of filter membrane 7；
S3: when filter membrane 7 is using overlong time, when the poor filtration effect of filter membrane 7, filter membrane 7 is replaced, first turning knob
Switch 20, rotary switch 20 drive screw rod 19 to be moved, and under the action of screw rod set 18, screw rod 19 moves while rotating
It is dynamic, to separate with fixed link 13, the purpose that fixed link 13 is fixed is released, the mobile first in command 15, the first in command 15
Pull rod 14 is driven to be moved, pull rod 14 drives fixed link 13 to be moved and compressed second spring 16, the movement of fixed link 13,
So that fixed link 13 is detached from fixing groove 11, to release the fixation to fixing seat 10, fixing seat 10,10 band of fixing seat are moved up
Dynamic first spring 9 is moved, and the first spring 9 drives the first magnet 8 to be moved, and the first magnet 8 drives sliding seat 6 to be moved
It is dynamic, to be dismantled to filter membrane 7, consequently facilitating being replaced to filter membrane 7.
The foregoing is only a preferred embodiment of the present invention, but scope of protection of the present invention is not limited thereto,
Anyone skilled in the art in the technical scope disclosed by the present invention, according to the technique and scheme of the present invention and its
Inventive concept is subject to equivalent substitution or change, should be covered by the protection scope of the present invention.
Claims (10)
1. a kind of purification devices of graphene oxide, including agitator tank (1) and it is located at the Rose Box (2) of agitator tank (1) side,
It is characterized in that, is fixedly installed with filter plate (3) in the bottom interior wall of the Rose Box (2), the top of filter plate (3) is extended to the over
The top of filter box (2), the top of filter plate (3) offer the first groove (4), open up on the two sides inner wall of the first groove (4)
Have the first hole (5), is sealed in the first groove (4) there are two being slidably installed sliding seat (6), fixed peace between two sliding seats (6)
Equipped with the same filter membrane (7), the first magnet (8) are fixedly installed at the top of a sliding seat (6) in two sliding seats (6),
The top of first magnet (8) is equipped with the one end of the first spring (9), and the other end of the first spring (9) is fixedly connected with fixing seat
(10), and fixing seat (10) is adapted with the first groove (4), and the two sides of fixing seat (10) offer fixing groove (11), and first
It offers on the two sides inner wall of groove (4) the second groove (12), is slidably fitted with fixed link (13) in the second groove (12), and
Fixed link (13) is adapted with corresponding fixing groove (11), and one end that two fixed links (13) are located remotely from each other is fixedly installed with drawing
One end of bar (14), the other end of pull rod (14) are extended to the over the outside of filter plate (3) and are fixedly installed with the first in command (15), and
The first in command (15) is the top of Rose Box (2), and movable sleeve is equipped with second spring (16) on pull rod (14), second spring (16)
The other end is fixedly installed on corresponding fixed link (13), and it is recessed that the other end of second spring (16) is fixedly mounted on corresponding second
It on the inner wall of slot (12), is offered in the top inner wall of the second groove (12) the second hole (17), the second hole is fixedly mounted on (17)
Having screw rod set (18), thread bush is equipped with screw rod (19) on screw rod set (18), and the bottom of screw rod (19) is in contact with fixed link (13),
It is extended to the over the top of filter plate (3) at the top of screw rod (19) and is fixedly installed with rotary switch (20)；
It is offered third hole (21) in the bottom interior wall of first groove (4), is slidably fitted with vertical bar in third hole (21)
(22), and the top of vertical bar (22) is in contact with the other end sliding seat (6) in two sliding seats (6), the bottom of vertical bar (22)
It is extended to the over the lower section of filter box (2), there are two attachment base (23), two attachment bases (23) for the bottom fixed installation of Rose Box (2)
Between be rotatably equipped with the same shaft (24), fixing sleeve is equipped with cam (25) in shaft (24), and cam (25) and vertical bar
(22) it is adapted, one end of shaft (24) through an attachment base (23) and is fixedly installed with the first sprocket wheel (26), Rose Box (2)
Bottom be fixedly installed with rotating electric machine (27), be fixedly installed on the output shaft of rotating electric machine (27) the second sprocket wheel (28), and
Chain (29) are sequentially connected between second sprocket wheel (28) and the first sprocket wheel (26).
2. a kind of purification devices of graphene oxide according to claim 1, which is characterized in that on the sliding seat (6)
Ring groove is offered, sealing ring is fixedly installed in ring groove, and sealing ring is slidably and sealingly connected with the first groove (4).
3. a kind of purification devices of graphene oxide according to claim 1, which is characterized in that two sliding seats (6) it
Between be fixedly installed with the same support rod, and support rod is located at the side of filter membrane (7).
4. a kind of purification devices of graphene oxide according to claim 1, which is characterized in that second groove (12)
Bottom interior wall on offer the first limiting slot, the bottom of fixed link (13) is fixedly installed with the first limited block, and the first limit
Block is slidably connected with corresponding first limiting slot.
5. a kind of purification devices of graphene oxide according to claim 1, which is characterized in that second groove (12)
The first intercommunicating pore is offered on side inner wall far from its opening, and pull rod (14) runs through corresponding first intercommunicating pore.
6. a kind of purification devices of graphene oxide according to claim 1, which is characterized in that on the screw rod set (18)
Threaded hole is offered, and screw rod (19) is threadedly coupled with corresponding threaded hole.
7. a kind of purification devices of graphene oxide according to claim 1, which is characterized in that the Rose Box (2)
Bottom offers the second intercommunicating pore, and the second intercommunicating pore is connected with third hole (21), and vertical bar (22) and the second intercommunicating pore slide
Connection.
8. a kind of purification devices of graphene oxide according to claim 1, which is characterized in that the one of the vertical bar (22)
Side offers the second limiting slot, is fixedly installed with the second limited block on the side inner wall of the second intercommunicating pore, and the second limited block with
Second limiting slot is slidably connected.
9. a kind of purification devices of graphene oxide according to claim 1, which is characterized in that the shaft (24) it is another
One end fixing sleeve is equipped with bearing, and the outer ring of bearing is fixedly mounted on another attachment base (23).
10. a kind of application method of the purification devices of graphene oxide, which comprises the following steps:
S1: when Rose Box (2) works, start rotating electric machine (27), rotating electric machine (27) drives the second sprocket wheel by output shaft
(28) it is rotated, since the second sprocket wheel (28) are sequentially connected by chain (29) and the first sprocket wheel (26), so the second sprocket wheel
(28) rotation drives the first sprocket wheel (26) to be rotated by chain (29), and the first sprocket wheel (26) drives shaft (24) to be turned
It is dynamic；
S2: carrying out rotating shaft (24), and rotation band moving cam (25) of shaft (24) is rotated, and the rotation of cam (25) drives
Vertical bar (22) pumps, and when vertical bar (22) moves up, vertical bar (22) drives another sliding seat (6) to carry out
Mobile, another sliding seat (6) drives filter membrane (7) to move up, and filter membrane (7) drives another sliding seat (6) to move up simultaneously
Compress the first spring (9), when vertical bar (22) moves down, the first spring (9) elastic force effect under so that filter membrane (7) and
Sliding seat (6) moves down, so that the vibration of filter membrane (7) is realized, to place the blocking of filter membrane (7)；
S3: when filter membrane (7) use overlong time, when the poor filtration effect of filter membrane (7), filter membrane (7) is replaced, is turned first
Dynamic rotary switch (20), rotary switch (20) drives screw rod (19) to be moved, under the action of screw rod set (18), screw rod (19)
It is moved while rotating, to separate with fixed link (13), releases the purpose that fixed link (13) is fixed, movement first
Handle (15), the first in command (15) drive pull rod (14) to move, and pull rod (14) drives fixed link (13) to be moved and pressed
Contracting second spring (16), the movement of fixed link (13), so that fixed link (13) is detached from fixing groove (11), to release to fixing seat
(10) fixation moves up fixing seat (10), and fixing seat (10) drives the first spring (9) to be moved, the first spring (9) band
Dynamic first magnet (8) are moved, and the first magnet (8) drives sliding seat (6) to be moved, so that filter membrane (7) is dismantled,
Consequently facilitating being replaced to filter membrane (7).
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| CN102249219A (en) * | 2011-04-18 | 2011-11-23 | 耿世达 | Method and special high-temperature continuous vacuum ignition furnace for efficiently preparing grapheme |
| US20130260152A1 (en) * | 2012-03-30 | 2013-10-03 | Scott L. Murray | Mechanical exfoliation apparatus |
| WO2014168362A1 (en) * | 2013-04-11 | 2014-10-16 | 주식회사 아이디티인터내셔널 | Method for manufacturing graphite oxide and apparatus therefor |
| CN104118872A (en) * | 2014-08-04 | 2014-10-29 | 湖南元素密码石墨烯研究院（有限合伙） | Method and device for purifying oxidized graphene/graphene solution |
| CN208082233U (en) * | 2018-01-08 | 2018-11-13 | 中国科学院兰州化学物理研究所 | A kind of film filter of the continuous automatic cleaning graphene oxide of ultrasonic wave auxiliary |
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- 2018-11-19 CN CN201811373362.XA patent/CN109485039B/en active Active
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102249219A (en) * | 2011-04-18 | 2011-11-23 | 耿世达 | Method and special high-temperature continuous vacuum ignition furnace for efficiently preparing grapheme |
| US20130260152A1 (en) * | 2012-03-30 | 2013-10-03 | Scott L. Murray | Mechanical exfoliation apparatus |
| WO2014168362A1 (en) * | 2013-04-11 | 2014-10-16 | 주식회사 아이디티인터내셔널 | Method for manufacturing graphite oxide and apparatus therefor |
| CN104118872A (en) * | 2014-08-04 | 2014-10-29 | 湖南元素密码石墨烯研究院（有限合伙） | Method and device for purifying oxidized graphene/graphene solution |
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