CN109473197A - It is a kind of to contain silver-supramolecular organogel high-resolution conductive silver paste and preparation method thereof - Google Patents
It is a kind of to contain silver-supramolecular organogel high-resolution conductive silver paste and preparation method thereof Download PDFInfo
- Publication number
- CN109473197A CN109473197A CN201811351475.XA CN201811351475A CN109473197A CN 109473197 A CN109473197 A CN 109473197A CN 201811351475 A CN201811351475 A CN 201811351475A CN 109473197 A CN109473197 A CN 109473197A
- Authority
- CN
- China
- Prior art keywords
- silver
- parts
- silver paste
- argentiferous
- organogel
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- BQCADISMDOOEFD-UHFFFAOYSA-N Silver Chemical compound [Ag] BQCADISMDOOEFD-UHFFFAOYSA-N 0.000 title claims abstract description 103
- 238000002360 preparation method Methods 0.000 title claims abstract description 19
- 229910052709 silver Inorganic materials 0.000 claims abstract description 38
- 239000004332 silver Substances 0.000 claims abstract description 38
- 239000000843 powder Substances 0.000 claims abstract description 17
- 239000011521 glass Substances 0.000 claims abstract description 13
- 238000002844 melting Methods 0.000 claims abstract description 10
- 230000008018 melting Effects 0.000 claims abstract description 10
- 239000006185 dispersion Substances 0.000 claims abstract description 7
- 239000002994 raw material Substances 0.000 claims abstract description 3
- YMWUJEATGCHHMB-UHFFFAOYSA-N Dichloromethane Chemical compound ClCCl YMWUJEATGCHHMB-UHFFFAOYSA-N 0.000 claims description 15
- DYUQAZSOFZSPHD-UHFFFAOYSA-N Phenylpropyl alcohol Natural products CCC(O)C1=CC=CC=C1 DYUQAZSOFZSPHD-UHFFFAOYSA-N 0.000 claims description 12
- 239000000203 mixture Substances 0.000 claims description 12
- 238000002156 mixing Methods 0.000 claims description 11
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 claims description 10
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 claims description 10
- 238000006243 chemical reaction Methods 0.000 claims description 10
- 239000013078 crystal Substances 0.000 claims description 10
- OEYQBKYISMRWQB-UHFFFAOYSA-N Santal Chemical compound C=1C(OC)=CC(O)=C(C2=O)C=1OC=C2C1=CC=C(O)C(O)=C1 OEYQBKYISMRWQB-UHFFFAOYSA-N 0.000 claims description 8
- 125000003282 alkyl amino group Chemical group 0.000 claims description 7
- 235000001014 amino acid Nutrition 0.000 claims description 7
- 238000003756 stirring Methods 0.000 claims description 7
- WYURNTSHIVDZCO-UHFFFAOYSA-N Tetrahydrofuran Chemical class C1CCOC1 WYURNTSHIVDZCO-UHFFFAOYSA-N 0.000 claims description 5
- -1 alcohol ester Chemical class 0.000 claims description 5
- 238000004090 dissolution Methods 0.000 claims description 5
- 150000002148 esters Chemical class 0.000 claims description 5
- 238000000227 grinding Methods 0.000 claims description 5
- 238000010438 heat treatment Methods 0.000 claims description 5
- 238000003801 milling Methods 0.000 claims description 5
- 229910052757 nitrogen Inorganic materials 0.000 claims description 5
- 235000008729 phenylalanine Nutrition 0.000 claims description 5
- 239000013049 sediment Substances 0.000 claims description 5
- 125000003866 trichloromethyl group Chemical group ClC(Cl)(Cl)* 0.000 claims description 5
- 125000000217 alkyl group Chemical group 0.000 claims description 4
- 230000005484 gravity Effects 0.000 claims description 4
- 239000003960 organic solvent Substances 0.000 claims description 4
- 150000002994 phenylalanines Chemical class 0.000 claims description 4
- 238000012545 processing Methods 0.000 claims description 4
- ILRSCQWREDREME-UHFFFAOYSA-N dodecanamide Chemical compound CCCCCCCCCCCC(N)=O ILRSCQWREDREME-UHFFFAOYSA-N 0.000 claims description 3
- RBNWAMSGVWEHFP-UHFFFAOYSA-N trans-p-Menthane-1,8-diol Chemical compound CC(C)(O)C1CCC(C)(O)CC1 RBNWAMSGVWEHFP-UHFFFAOYSA-N 0.000 claims description 3
- FATBGEAMYMYZAF-KTKRTIGZSA-N oleamide Chemical compound CCCCCCCC\C=C/CCCCCCCC(N)=O FATBGEAMYMYZAF-KTKRTIGZSA-N 0.000 claims description 2
- FATBGEAMYMYZAF-UHFFFAOYSA-N oleicacidamide-heptaglycolether Natural products CCCCCCCCC=CCCCCCCCC(N)=O FATBGEAMYMYZAF-UHFFFAOYSA-N 0.000 claims description 2
- 125000001997 phenyl group Chemical group [H]C1=C([H])C([H])=C(*)C([H])=C1[H] 0.000 claims description 2
- 239000002002 slurry Substances 0.000 abstract description 8
- 239000000835 fiber Substances 0.000 abstract description 7
- 238000010008 shearing Methods 0.000 abstract description 5
- 238000001338 self-assembly Methods 0.000 abstract description 2
- 239000013008 thixotropic agent Substances 0.000 description 12
- 235000013339 cereals Nutrition 0.000 description 9
- 239000002245 particle Substances 0.000 description 8
- 238000000034 method Methods 0.000 description 6
- 238000005245 sintering Methods 0.000 description 6
- 230000000052 comparative effect Effects 0.000 description 4
- 229920002521 macromolecule Polymers 0.000 description 4
- 239000000243 solution Substances 0.000 description 4
- 239000004952 Polyamide Substances 0.000 description 3
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 3
- 230000008901 benefit Effects 0.000 description 3
- 238000012986 modification Methods 0.000 description 3
- 230000004048 modification Effects 0.000 description 3
- 229920002647 polyamide Polymers 0.000 description 3
- 239000001856 Ethyl cellulose Substances 0.000 description 2
- ZZSNKZQZMQGXPY-UHFFFAOYSA-N Ethyl cellulose Chemical compound CCOCC1OC(OC)C(OCC)C(OCC)C1OC1C(O)C(O)C(OC)C(CO)O1 ZZSNKZQZMQGXPY-UHFFFAOYSA-N 0.000 description 2
- 241000209094 Oryza Species 0.000 description 2
- 235000007164 Oryza sativa Nutrition 0.000 description 2
- 229910000278 bentonite Inorganic materials 0.000 description 2
- 239000000440 bentonite Substances 0.000 description 2
- SVPXDRXYRYOSEX-UHFFFAOYSA-N bentoquatam Chemical compound O.O=[Si]=O.O=[Al]O[Al]=O SVPXDRXYRYOSEX-UHFFFAOYSA-N 0.000 description 2
- 238000007796 conventional method Methods 0.000 description 2
- 238000010586 diagram Methods 0.000 description 2
- 238000001035 drying Methods 0.000 description 2
- 229920001249 ethyl cellulose Polymers 0.000 description 2
- 235000019325 ethyl cellulose Nutrition 0.000 description 2
- 229910021485 fumed silica Inorganic materials 0.000 description 2
- 239000001257 hydrogen Substances 0.000 description 2
- 229910052739 hydrogen Inorganic materials 0.000 description 2
- 230000002209 hydrophobic effect Effects 0.000 description 2
- 239000005416 organic matter Substances 0.000 description 2
- 235000009566 rice Nutrition 0.000 description 2
- 239000007787 solid Substances 0.000 description 2
- 239000002904 solvent Substances 0.000 description 2
- 230000006641 stabilisation Effects 0.000 description 2
- 238000011105 stabilization Methods 0.000 description 2
- 239000004094 surface-active agent Substances 0.000 description 2
- 229940100616 topical oil Drugs 0.000 description 2
- 229910002012 Aerosil® Inorganic materials 0.000 description 1
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 1
- COLNVLDHVKWLRT-QMMMGPOBSA-N L-phenylalanine Chemical compound OC(=O)[C@@H](N)CC1=CC=CC=C1 COLNVLDHVKWLRT-QMMMGPOBSA-N 0.000 description 1
- 230000001133 acceleration Effects 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 239000000654 additive Substances 0.000 description 1
- 230000000996 additive effect Effects 0.000 description 1
- 239000000853 adhesive Substances 0.000 description 1
- 230000001070 adhesive effect Effects 0.000 description 1
- PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 description 1
- 150000001408 amides Chemical class 0.000 description 1
- 238000010923 batch production Methods 0.000 description 1
- 239000011230 binding agent Substances 0.000 description 1
- 229910052799 carbon Inorganic materials 0.000 description 1
- 238000000354 decomposition reaction Methods 0.000 description 1
- 238000000280 densification Methods 0.000 description 1
- 238000011161 development Methods 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 230000005611 electricity Effects 0.000 description 1
- 239000007789 gas Substances 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 239000007791 liquid phase Substances 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 239000011259 mixed solution Substances 0.000 description 1
- 238000000465 moulding Methods 0.000 description 1
- 239000011858 nanopowder Substances 0.000 description 1
- 238000011056 performance test Methods 0.000 description 1
- COLNVLDHVKWLRT-UHFFFAOYSA-N phenylalanine Natural products OC(=O)C(N)CC1=CC=CC=C1 COLNVLDHVKWLRT-UHFFFAOYSA-N 0.000 description 1
- 238000000053 physical method Methods 0.000 description 1
- 229920000642 polymer Polymers 0.000 description 1
- 230000008569 process Effects 0.000 description 1
- 238000011084 recovery Methods 0.000 description 1
- 230000009467 reduction Effects 0.000 description 1
- 230000004044 response Effects 0.000 description 1
- 239000000523 sample Substances 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 239000000758 substrate Substances 0.000 description 1
- 230000009974 thixotropic effect Effects 0.000 description 1
- 238000012546 transfer Methods 0.000 description 1
Classifications
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01B—CABLES; CONDUCTORS; INSULATORS; SELECTION OF MATERIALS FOR THEIR CONDUCTIVE, INSULATING OR DIELECTRIC PROPERTIES
- H01B1/00—Conductors or conductive bodies characterised by the conductive materials; Selection of materials as conductors
- H01B1/14—Conductive material dispersed in non-conductive inorganic material
- H01B1/16—Conductive material dispersed in non-conductive inorganic material the conductive material comprising metals or alloys
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01B—CABLES; CONDUCTORS; INSULATORS; SELECTION OF MATERIALS FOR THEIR CONDUCTIVE, INSULATING OR DIELECTRIC PROPERTIES
- H01B1/00—Conductors or conductive bodies characterised by the conductive materials; Selection of materials as conductors
- H01B1/20—Conductive material dispersed in non-conductive organic material
- H01B1/22—Conductive material dispersed in non-conductive organic material the conductive material comprising metals or alloys
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01B—CABLES; CONDUCTORS; INSULATORS; SELECTION OF MATERIALS FOR THEIR CONDUCTIVE, INSULATING OR DIELECTRIC PROPERTIES
- H01B13/00—Apparatus or processes specially adapted for manufacturing conductors or cables
Landscapes
- Chemical & Material Sciences (AREA)
- Dispersion Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Physics & Mathematics (AREA)
- Spectroscopy & Molecular Physics (AREA)
- Engineering & Computer Science (AREA)
- Manufacturing & Machinery (AREA)
- Conductive Materials (AREA)
- Manufacture Of Metal Powder And Suspensions Thereof (AREA)
Abstract
Description
Claims (5)
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201811351475.XA CN109473197B (en) | 2018-11-14 | 2018-11-14 | High-resolution conductive silver paste containing silver-supermolecule organogel and preparation method thereof |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201811351475.XA CN109473197B (en) | 2018-11-14 | 2018-11-14 | High-resolution conductive silver paste containing silver-supermolecule organogel and preparation method thereof |
Publications (2)
Publication Number | Publication Date |
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CN109473197A true CN109473197A (en) | 2019-03-15 |
CN109473197B CN109473197B (en) | 2020-11-03 |
Family
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Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
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CN201811351475.XA Active CN109473197B (en) | 2018-11-14 | 2018-11-14 | High-resolution conductive silver paste containing silver-supermolecule organogel and preparation method thereof |
Country Status (1)
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CN (1) | CN109473197B (en) |
Cited By (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN112768113A (en) * | 2020-12-31 | 2021-05-07 | 合肥工业大学 | Preparation method of responsive nano composite polymer conductive film |
CN114605959A (en) * | 2022-03-09 | 2022-06-10 | 轻工业部南京电光源材料科学研究所 | Poly-o-epoxy-N-methylaniline conductive organic carrier and preparation method thereof |
CN114682787A (en) * | 2020-12-30 | 2022-07-01 | 苏州银瑞光电材料科技有限公司 | Method for preparing spherical silver powder suitable for electronic silver paste and surface modification |
Citations (8)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN101271928A (en) * | 2008-05-04 | 2008-09-24 | 常州亿晶光电科技有限公司 | High-viscosity solar cell front silver paste and preparation method thereof |
US20120279762A1 (en) * | 2011-05-03 | 2012-11-08 | Industry-Academic Cooperation Foundation, Yonsei University | Composition for forming stretchable conductive pattern, method of producing the stretchable conductive pattern using the composition, and electronic device including stretchable conductive electrode |
CN103400634A (en) * | 2013-07-22 | 2013-11-20 | 上海玻纳电子科技有限公司 | Conductive silver paste used for crystalline silicon solar cell front electrode and preparation method thereof |
US9005484B2 (en) * | 2009-03-31 | 2015-04-14 | Xerox Corporation | Low polarity nano silver gels |
CN106952675A (en) * | 2017-03-22 | 2017-07-14 | 西北大学 | Graphene-based organic carrier and preparation method thereof, electric slurry and preparation method thereof |
CN107658045A (en) * | 2017-08-30 | 2018-02-02 | 南通天盛新能源股份有限公司 | A kind of unleaded PERC batteries back electrode silver paste and preparation method |
CN107759092A (en) * | 2017-09-28 | 2018-03-06 | 浙江光达电子科技有限公司 | It is a kind of to be used to carry on the back lead-free glass powder of passivation crystal silicon solar battery back face silver paste and preparation method thereof |
CN108417292A (en) * | 2018-03-28 | 2018-08-17 | 山东建邦胶体材料有限公司 | Crystal silicon solar energy battery front side silver paste of the organic silver containing nanometer and preparation method thereof |
-
2018
- 2018-11-14 CN CN201811351475.XA patent/CN109473197B/en active Active
Patent Citations (8)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN101271928A (en) * | 2008-05-04 | 2008-09-24 | 常州亿晶光电科技有限公司 | High-viscosity solar cell front silver paste and preparation method thereof |
US9005484B2 (en) * | 2009-03-31 | 2015-04-14 | Xerox Corporation | Low polarity nano silver gels |
US20120279762A1 (en) * | 2011-05-03 | 2012-11-08 | Industry-Academic Cooperation Foundation, Yonsei University | Composition for forming stretchable conductive pattern, method of producing the stretchable conductive pattern using the composition, and electronic device including stretchable conductive electrode |
CN103400634A (en) * | 2013-07-22 | 2013-11-20 | 上海玻纳电子科技有限公司 | Conductive silver paste used for crystalline silicon solar cell front electrode and preparation method thereof |
CN106952675A (en) * | 2017-03-22 | 2017-07-14 | 西北大学 | Graphene-based organic carrier and preparation method thereof, electric slurry and preparation method thereof |
CN107658045A (en) * | 2017-08-30 | 2018-02-02 | 南通天盛新能源股份有限公司 | A kind of unleaded PERC batteries back electrode silver paste and preparation method |
CN107759092A (en) * | 2017-09-28 | 2018-03-06 | 浙江光达电子科技有限公司 | It is a kind of to be used to carry on the back lead-free glass powder of passivation crystal silicon solar battery back face silver paste and preparation method thereof |
CN108417292A (en) * | 2018-03-28 | 2018-08-17 | 山东建邦胶体材料有限公司 | Crystal silicon solar energy battery front side silver paste of the organic silver containing nanometer and preparation method thereof |
Non-Patent Citations (1)
Title |
---|
付新建 等: "十八烷基-L-苯丙氨酸齐聚物在有机溶剂中的自组装", 《化学学报》 * |
Cited By (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN114682787A (en) * | 2020-12-30 | 2022-07-01 | 苏州银瑞光电材料科技有限公司 | Method for preparing spherical silver powder suitable for electronic silver paste and surface modification |
CN112768113A (en) * | 2020-12-31 | 2021-05-07 | 合肥工业大学 | Preparation method of responsive nano composite polymer conductive film |
CN114605959A (en) * | 2022-03-09 | 2022-06-10 | 轻工业部南京电光源材料科学研究所 | Poly-o-epoxy-N-methylaniline conductive organic carrier and preparation method thereof |
CN114605959B (en) * | 2022-03-09 | 2023-10-24 | 南京工大光电材料研究院有限公司 | Poly-o-epoxy-N-methylaniline conductive organic carrier and preparation method thereof |
Also Published As
Publication number | Publication date |
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CN109473197B (en) | 2020-11-03 |
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Address after: 210015 No.5, jinchuanmenwai, Gulou District, Nanjing City, Jiangsu Province Patentee after: Nanjing University of Technology Optoelectronic Materials Research Institute Co.,Ltd. Patentee after: NANJING YUQUN MATERIAL TECHNOLOGY Co.,Ltd. Address before: 210015 No.5, jinchuanmenwai, Gulou District, Nanjing City, Jiangsu Province Patentee before: LIGHT INDUSTRY DEPARTMENT THE Research Institute OF NANJING ELECTRIC LIGHT SOURCE MATERIALS Patentee before: NANJING YUQUN MATERIAL TECHNOLOGY Co.,Ltd. |
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TR01 | Transfer of patent right |
Effective date of registration: 20240507 Address after: No. 5 Jinchuan Outer Gate, Gulou District, Nanjing City, Jiangsu Province, 210015 Patentee after: Nanjing University of Technology Optoelectronic Materials Research Institute Co.,Ltd. Country or region after: China Address before: 210015 No.5, jinchuanmenwai, Gulou District, Nanjing City, Jiangsu Province Patentee before: Nanjing University of Technology Optoelectronic Materials Research Institute Co.,Ltd. Country or region before: China Patentee before: NANJING YUQUN MATERIAL TECHNOLOGY Co.,Ltd. |
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