CN109463510A - A method of pressed candy is prepared using the long-acting coolant agent of eutectic - Google Patents
A method of pressed candy is prepared using the long-acting coolant agent of eutectic Download PDFInfo
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- CN109463510A CN109463510A CN201811590765.XA CN201811590765A CN109463510A CN 109463510 A CN109463510 A CN 109463510A CN 201811590765 A CN201811590765 A CN 201811590765A CN 109463510 A CN109463510 A CN 109463510A
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- coolant agent
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- eutectic
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- 239000003795 chemical substances by application Substances 0.000 title claims abstract description 100
- 239000002826 coolant Substances 0.000 title claims abstract description 98
- 235000009508 confectionery Nutrition 0.000 title claims abstract description 50
- 230000005496 eutectics Effects 0.000 title claims abstract description 40
- 238000000034 method Methods 0.000 title claims abstract description 31
- 239000007788 liquid Substances 0.000 claims abstract description 58
- 239000000203 mixture Substances 0.000 claims abstract description 31
- 239000002904 solvent Substances 0.000 claims abstract description 26
- DNIAPMSPPWPWGF-UHFFFAOYSA-N Propylene glycol Chemical compound CC(O)CO DNIAPMSPPWPWGF-UHFFFAOYSA-N 0.000 claims abstract description 24
- NOOLISFMXDJSKH-UTLUCORTSA-N (+)-Neomenthol Chemical compound CC(C)[C@@H]1CC[C@@H](C)C[C@@H]1O NOOLISFMXDJSKH-UTLUCORTSA-N 0.000 claims abstract description 19
- NOOLISFMXDJSKH-UHFFFAOYSA-N DL-menthol Natural products CC(C)C1CCC(C)CC1O NOOLISFMXDJSKH-UHFFFAOYSA-N 0.000 claims abstract description 19
- 229940041616 menthol Drugs 0.000 claims abstract description 19
- RWAXQWRDVUOOGG-UHFFFAOYSA-N N,2,3-Trimethyl-2-(1-methylethyl)butanamide Chemical compound CNC(=O)C(C)(C(C)C)C(C)C RWAXQWRDVUOOGG-UHFFFAOYSA-N 0.000 claims abstract description 17
- VUNOFAIHSALQQH-UHFFFAOYSA-N Ethyl menthane carboxamide Chemical compound CCNC(=O)C1CC(C)CCC1C(C)C VUNOFAIHSALQQH-UHFFFAOYSA-N 0.000 claims abstract description 15
- XHXUANMFYXWVNG-ADEWGFFLSA-N (-)-Menthyl acetate Chemical compound CC(C)[C@@H]1CC[C@@H](C)C[C@H]1OC(C)=O XHXUANMFYXWVNG-ADEWGFFLSA-N 0.000 claims abstract description 12
- HQKMJHAJHXVSDF-UHFFFAOYSA-L magnesium stearate Chemical compound [Mg+2].CCCCCCCCCCCCCCCCCC([O-])=O.CCCCCCCCCCCCCCCCCC([O-])=O HQKMJHAJHXVSDF-UHFFFAOYSA-L 0.000 claims abstract description 12
- FBPFZTCFMRRESA-JGWLITMVSA-N D-glucitol Chemical compound OC[C@H](O)[C@@H](O)[C@H](O)[C@H](O)CO FBPFZTCFMRRESA-JGWLITMVSA-N 0.000 claims abstract description 11
- 235000010482 polyoxyethylene sorbitan monooleate Nutrition 0.000 claims abstract description 8
- 229920000053 polysorbate 80 Polymers 0.000 claims abstract description 8
- 239000001605 (5-methyl-2-propan-2-ylcyclohexyl) acetate Substances 0.000 claims abstract description 6
- BJEPYKJPYRNKOW-REOHCLBHSA-N (S)-malic acid Chemical compound OC(=O)[C@@H](O)CC(O)=O BJEPYKJPYRNKOW-REOHCLBHSA-N 0.000 claims abstract description 6
- 108010011485 Aspartame Proteins 0.000 claims abstract description 6
- XHXUANMFYXWVNG-UHFFFAOYSA-N D-menthyl acetate Natural products CC(C)C1CCC(C)CC1OC(C)=O XHXUANMFYXWVNG-UHFFFAOYSA-N 0.000 claims abstract description 6
- BJEPYKJPYRNKOW-UHFFFAOYSA-N alpha-hydroxysuccinic acid Natural products OC(=O)C(O)CC(O)=O BJEPYKJPYRNKOW-UHFFFAOYSA-N 0.000 claims abstract description 6
- 239000000605 aspartame Substances 0.000 claims abstract description 6
- IAOZJIPTCAWIRG-QWRGUYRKSA-N aspartame Chemical compound OC(=O)C[C@H](N)C(=O)N[C@H](C(=O)OC)CC1=CC=CC=C1 IAOZJIPTCAWIRG-QWRGUYRKSA-N 0.000 claims abstract description 6
- 235000010357 aspartame Nutrition 0.000 claims abstract description 6
- 229960003438 aspartame Drugs 0.000 claims abstract description 6
- 235000019359 magnesium stearate Nutrition 0.000 claims abstract description 6
- 239000001630 malic acid Substances 0.000 claims abstract description 6
- 235000011090 malic acid Nutrition 0.000 claims abstract description 6
- 238000002360 preparation method Methods 0.000 claims description 33
- 239000003507 refrigerant Substances 0.000 claims description 15
- 230000008569 process Effects 0.000 claims description 9
- 239000013078 crystal Substances 0.000 claims description 8
- 238000007791 dehumidification Methods 0.000 claims description 8
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 8
- 239000007787 solid Substances 0.000 claims description 6
- 239000000796 flavoring agent Substances 0.000 claims description 5
- 235000019634 flavors Nutrition 0.000 claims description 5
- 235000000346 sugar Nutrition 0.000 claims description 5
- 244000144730 Amygdalus persica Species 0.000 claims description 4
- 241000167854 Bourreria succulenta Species 0.000 claims description 4
- 235000016623 Fragaria vesca Nutrition 0.000 claims description 4
- 240000009088 Fragaria x ananassa Species 0.000 claims description 4
- 235000011363 Fragaria x ananassa Nutrition 0.000 claims description 4
- 235000006040 Prunus persica var persica Nutrition 0.000 claims description 4
- 235000019693 cherries Nutrition 0.000 claims description 4
- 235000009754 Vitis X bourquina Nutrition 0.000 claims description 3
- 235000012333 Vitis X labruscana Nutrition 0.000 claims description 3
- 240000006365 Vitis vinifera Species 0.000 claims description 3
- 235000014787 Vitis vinifera Nutrition 0.000 claims description 3
- XMGQYMWWDOXHJM-UHFFFAOYSA-N limonene Chemical compound CC(=C)C1CCC(C)=CC1 XMGQYMWWDOXHJM-UHFFFAOYSA-N 0.000 claims description 3
- 239000007968 orange flavor Substances 0.000 claims description 3
- CZMRCDWAGMRECN-UGDNZRGBSA-N Sucrose Chemical compound O[C@H]1[C@H](O)[C@@H](CO)O[C@@]1(CO)O[C@@H]1[C@H](O)[C@@H](O)[C@H](O)[C@@H](CO)O1 CZMRCDWAGMRECN-UGDNZRGBSA-N 0.000 claims description 2
- 229930006000 Sucrose Natural products 0.000 claims description 2
- 239000005720 sucrose Substances 0.000 claims description 2
- 238000003756 stirring Methods 0.000 abstract description 6
- 239000004376 Sucralose Substances 0.000 abstract description 4
- 238000002156 mixing Methods 0.000 abstract description 4
- BAQAVOSOZGMPRM-QBMZZYIRSA-N sucralose Chemical compound O[C@@H]1[C@@H](O)[C@@H](Cl)[C@@H](CO)O[C@@H]1O[C@@]1(CCl)[C@@H](O)[C@H](O)[C@@H](CCl)O1 BAQAVOSOZGMPRM-QBMZZYIRSA-N 0.000 abstract description 4
- 235000019408 sucralose Nutrition 0.000 abstract description 4
- 238000010438 heat treatment Methods 0.000 abstract description 2
- 230000000694 effects Effects 0.000 description 7
- 238000001816 cooling Methods 0.000 description 4
- 239000000126 substance Substances 0.000 description 4
- 239000000843 powder Substances 0.000 description 3
- RDOXTESZEPMUJZ-UHFFFAOYSA-N anisole Chemical compound COC1=CC=CC=C1 RDOXTESZEPMUJZ-UHFFFAOYSA-N 0.000 description 2
- 230000008901 benefit Effects 0.000 description 2
- 235000013305 food Nutrition 0.000 description 2
- ZHNUHDYFZUAESO-UHFFFAOYSA-N formamide Substances NC=O ZHNUHDYFZUAESO-UHFFFAOYSA-N 0.000 description 2
- 230000002045 lasting effect Effects 0.000 description 2
- 239000000463 material Substances 0.000 description 2
- 238000002844 melting Methods 0.000 description 2
- 230000008018 melting Effects 0.000 description 2
- CRPPMKFSMRODIQ-JDXPBYPHSA-N Hydroxy-gamma-sanshool Chemical compound C\C=C\C=C\C=C/CC\C=C\C=C\C(=O)NCC(C)(C)O CRPPMKFSMRODIQ-JDXPBYPHSA-N 0.000 description 1
- 241000218195 Lauraceae Species 0.000 description 1
- 235000017858 Laurus nobilis Nutrition 0.000 description 1
- 235000005212 Terminalia tomentosa Nutrition 0.000 description 1
- 244000269722 Thea sinensis Species 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 230000008859 change Effects 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 235000013399 edible fruits Nutrition 0.000 description 1
- 150000002148 esters Chemical class 0.000 description 1
- 239000002360 explosive Substances 0.000 description 1
- 235000003599 food sweetener Nutrition 0.000 description 1
- 235000021552 granulated sugar Nutrition 0.000 description 1
- 230000006872 improvement Effects 0.000 description 1
- 230000007794 irritation Effects 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- UZKWTJUDCOPSNM-UHFFFAOYSA-N methoxybenzene Substances CCCCOC=C UZKWTJUDCOPSNM-UHFFFAOYSA-N 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 210000004400 mucous membrane Anatomy 0.000 description 1
- 239000002245 particle Substances 0.000 description 1
- 230000000144 pharmacologic effect Effects 0.000 description 1
- 239000000049 pigment Substances 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 239000003765 sweetening agent Substances 0.000 description 1
- 230000009967 tasteless effect Effects 0.000 description 1
- 238000002525 ultrasonication Methods 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23G—COCOA; COCOA PRODUCTS, e.g. CHOCOLATE; SUBSTITUTES FOR COCOA OR COCOA PRODUCTS; CONFECTIONERY; CHEWING GUM; ICE-CREAM; PREPARATION THEREOF
- A23G3/00—Sweetmeats; Confectionery; Marzipan; Coated or filled products
- A23G3/34—Sweetmeats, confectionery or marzipan; Processes for the preparation thereof
- A23G3/36—Sweetmeats, confectionery or marzipan; Processes for the preparation thereof characterised by the composition containing organic or inorganic compounds
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23G—COCOA; COCOA PRODUCTS, e.g. CHOCOLATE; SUBSTITUTES FOR COCOA OR COCOA PRODUCTS; CONFECTIONERY; CHEWING GUM; ICE-CREAM; PREPARATION THEREOF
- A23G3/00—Sweetmeats; Confectionery; Marzipan; Coated or filled products
- A23G3/34—Sweetmeats, confectionery or marzipan; Processes for the preparation thereof
- A23G3/36—Sweetmeats, confectionery or marzipan; Processes for the preparation thereof characterised by the composition containing organic or inorganic compounds
- A23G3/48—Sweetmeats, confectionery or marzipan; Processes for the preparation thereof characterised by the composition containing organic or inorganic compounds containing plants or parts thereof, e.g. fruits, seeds, extracts
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
Landscapes
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Inorganic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Food Science & Technology (AREA)
- Polymers & Plastics (AREA)
- Botany (AREA)
- Confectionery (AREA)
Abstract
A method of pressed candy is prepared using the long-acting coolant agent of eutectic, coolant agent WS-12, coolant agent WS-3, coolant agent WS-23, menthol mix in proportion to obtain mixture A, propylene glycol, Tween-80, ten polyglycereol monolaurates mix in proportion to obtain solvent B, solvent B, menthyl acetate are added into mixture A, heating stirring obtains the long-acting coolant agent liquid of eutectic to colorless and transparent simultaneously；By coolant agent and liquid essence, D-sorbite, magnesium stearate malic acid, Sucralose, Aspartame are mixed in proportion, are dehumidified, after mixing evenly, and pressed candy is made in tabletting.
Description
Technical field
The present invention relates to a kind of methods for preparing pressed candy using the long-acting coolant agent of eutectic, belong to foods processing technique neck
Domain.
Background technique
Candy is a kind of universal favorite food of people, be with white granulated sugar or other allow using sweetener, eat
Pigment is primary raw material, the solid-state or semisolid confectionery being processed into according to certain manufacturing technique requirent.General candy
People can only be met and like that taste is single to sweet tea, as the improvement of people's living standards, general candy is not able to satisfy increasingly
People are to the diversified demand of candy flavors.The development in market is met the tendency of, the weight at confectionery industry of characteristic taste candy is developed
Task is wanted, and cool taste candy is exactly one of them.
Traditional cool taste candy is that Natural menthol is added in candy, and Natural menthol itself has special minty note
There is cool taste to generate the features such as speed is fast, and explosive force is strong, and cool feeling is of short duration, also allow for the candy for being added to Natural menthol for gas
Although it is fast that cool feeling generates speed, cool feeling is not lasting, and has the taste of one menthol, or even can generate a kind of hardship
Taste.
With the development in market, coolant agent has been had increasingly been used in candy.Coolant agent is that all energy generations are refrigerant
The general name of effect and the not strong chemical substance of pharmacological property.The most common coolant agent is menthol, but due to its tanginess and right
Skin, mucous membrane tissue, eyes have intense irritation, greatly limit their application.
Coolant agent WS-3, chemical name: N- ethyl-is to menthyl -3- formamide, molecular formula C13H25NO, white crystal powder
End, is insoluble in water by 91-102 DEG C of fusing point.Coolant agent WS-3 is long-acting coolant agent, and cooling effect is significant and lasting, can be continued
10-20 minutes, cool feeling effect was 1.5 times of menthol.
Coolant agent WS-12(N-Ethyl-p-menthane-3-carboxamide), chemical name: N- (methoxybenzene)-is to base-formamide, molecular formula C18H27NO2,
The tasteless crystal powder of white, is insoluble in water by 179-183 DEG C of fusing point.WS-12 is the long-acting coolant agent of discovered in recent years, and cool feeling is held
Continue the time up to 50-70 minutes, is 5-6 times of common coolant agent.
Coolant agent WS-23, chemical name: 2-Isopropyl-N,2,3-trimethylbutyramide, molecular formula C10H21NO, white crystal
Powder, is insoluble in water by 62-64 DEG C of fusing point.Coolant agent WS-23 has extremely strong cool taste, and cooling effect is 15-30 minutes sustainable,
Continuing 200 DEG C of high temperature will not influence the Cooling intensity of product.Coolant agent WS-3, coolant agent WS-12 and the equal indissoluble of coolant agent WS-23
Yu Shui is applied to generate great limitation.
Summary of the invention
The purpose of the present invention is to provide a kind of methods for preparing pressed candy using the long-acting coolant agent of eutectic.
In order to achieve the above objects and other related objects, present invention provide the technical scheme that it is a kind of long using eutectic
The method that effect coolant agent prepares pressed candy, the preparation of the long-acting coolant agent of preparation, eutectic of preparation, solvent B including mixture A
With the preparation of refrigerant pressed candy；
The preparation of the mixture A includes: by coolant agent WS-3,17-25 of the menthol of 7-25 parts by weight, 17-25 parts by weight
The coolant agent WS-23 of coolant agent WS-12 and the 25-55 parts by weight of parts by weight is uniformly mixed, and obtains liquid mixture A；Institute
Stating menthol is granular crystals, and coolant agent WS-12, coolant agent WS-3 and coolant agent WS-23 are pulverulent solids；
The preparation of the solvent B includes: by the propylene glycol of 30-60 parts by weight, the Tween-80 of 20-35 parts by weight, 20-35 weight
The ten polyglycereol monolaurates of part are uniformly mixed, and obtain solvent B；
The preparation of the long-acting coolant agent of eutectic includes: solvent B to be added into mixture A, and add solvent B and mixture
The menthyl acetate of A quality sum 1.0-1.5%, is stirred under conditions of temperature is 90-150 DEG C, revolving speed is 30-60r/min,
Obtain the long-acting coolant agent liquid of eutectic；
The preparation of the refrigerant pressed candy includes: by the long-acting coolant agent liquid of eutectic and pressed candy liquid essence according to 1:4-
6 mass ratio is uniformly mixed, and D-sorbite surface is then sprayed at, and be uniformly mixed to obtain primary product, through dehumidifying
After technique, the magnesium stearate of the quality 1-3% of the primary product after adding dehumidifying, the malic acid of 3-5%, the trichlorine of 0.1-0.2%
Sucrose, the Aspartame of 0.05-0.2%, after being mixed evenly, tabletting is up to long-acting refrigerant tabletting sugar product.
Preferred technical solution are as follows: the dehumidification process be in vacuum drier, vacuum gauge pressure -0.07~-
0.10MPa, under the conditions of 50-60 DEG C of temperature, 120-180min is handled, until primary product water content is less than or equal to 5%.
Preferred technical solution are as follows: the pressed candy is liquid peach flavor, liquid cherry essence, liquid with liquid essence
One of body grape essence, liquid flavoring orange essence, liquid orange flavor, liquid strawberry essence.
Preferred technical solution are as follows: the quality of the D-sorbite is the 8-15 of the long-acting coolant agent liquid quality of eutectic
Times.
Since above-mentioned technical proposal is used, the present invention has the advantage, that compared with prior art
The present invention, which passes through, compounds a variety of coolant agents, obtains low molten coolant agent liquid altogether, as solid, taste and do not have
The WS-12 of any taste, becomes liquid, realizes the good use of WS-12；Meanwhile by proportion optimizing, so that mixing cool taste
The cooling effect of agent reaches 50-60 minutes, considerably beyond single coolant agent.
Specific embodiment
Embodiments of the present invention are illustrated by particular specific embodiment below, those skilled in the art can be by this implementation
Content disclosed by example is understood other advantages and efficacy of the present invention easily.
The purpose of term used herein, which is only that, illustrates particular embodiment, it is not intended to be limited to the present invention.It removes
Non- context is explicitly shown, otherwise singular " one " used herein, "one" also include plural form.
When illustrating preferred embodiment, it is potentially based on clear purpose and uses special term；However, this specification institute
Revealer is not intended to be limited in the selected special term；And it is to be understood that each particular element includes having
Identical function, all equivalence techniques for operating in a similar manner and reaching similar effects.
Embodiment one: a method of pressed candy is prepared using the long-acting coolant agent of eutectic
A method of pressed candy, including following process flow are prepared using the long-acting coolant agent of eutectic.
(1) mixture A is prepared
Menthol, coolant agent WS-3, coolant agent WS-12, coolant agent WS-23 are mixed in a certain ratio uniformly, obtain mixture A.
Formula rate: the menthol of 16 parts by weight, the coolant agent WS-3 of 16 parts by weight, 16 parts by weight coolant agent WS-12,
The coolant agent WS-23 of 40 parts by weight.The menthol is granular crystals, coolant agent WS-12, coolant agent WS-3, coolant agent
WS-23 is pulverulent solids.
Menthol, coolant agent WS-3, coolant agent WS-12, coolant agent WS-23 are uniformly mixed by formula rate at room temperature,
Eutectic phenomenon can be generated, liquid mixture A is obtained.
(2) solvent B is prepared
Propylene glycol, Tween-80, ten polyglycereol monolaurates are mixed in a certain ratio uniformly, solvent B is obtained.
Formula rate: the propylene glycol of 45 parts by weight, the Tween-80 of 27 parts by weight, 28 parts by weight ten polyglycereol list laurels
Acid esters.
Propylene glycol, Tween-80, ten polyglycereol monolaurates are uniformly mixed by formula rate at room temperature, obtain liquid
The mixture A of shape.
(3) the long-acting coolant agent of eutectic is prepared
The first step, heating stirring.Solvent B is added into mixture A, and adds solvent B and mixture A quality sum
1.25% menthyl acetate, 120 DEG C of temperature, revolving speed 45r/min, is stirred well to colourless transparent liquid for mixture, obtains low total
Melt long-acting coolant agent liquid.
Second step carries out ultrasonication to the long-acting coolant agent liquid of eutectic.Material after stirring is placed in ultrasonic wave
In environment, in ultrasonic frequency 30KHz, power density 0.4w/cm2Under the conditions of, handle 12min.It is ultrasonically treated aftereffect
Fruit is more preferable.
(4) refrigerant pressed candy preparation
The long-acting coolant agent liquid of above-mentioned gained eutectic is taken, is added in pressed candy liquid essence with 1:5 ratio, uses water mists
It is sprayed at D-sorbite surface, and is uniformly mixed, the quality of D-sorbite is the long-acting coolant agent liquid quality of eutectic
10 times；After dehumidification process, 2% magnesium stearate is added, 4% malic acid, 0.1-% Sucralose, 0.1% Aspartame, mixing stirs
After mixing uniformly, tabletting is up to long-acting refrigerant tabletting sugar product.
The dehumidification process, using vacuum dehydrating at lower temperature, under the conditions of vacuum gauge pressure -0.08MPa, 55 DEG C of temperature, place
150min is managed, until material moisture is 3%.In the present embodiment, liquid essence is liquid peach flavor.
Embodiment two: a method of pressed candy is prepared using the long-acting coolant agent of eutectic
A method of pressed candy being prepared using the long-acting coolant agent of eutectic, it is the preparation of preparation, solvent B including mixture A, low
The preparation of the long-acting coolant agent of congruent melting and the preparation of refrigerant pressed candy；
The preparation of the mixture A include: by the menthol of 7 parts by weight, the coolant agent WS-3 of 17 parts by weight, 17 parts by weight it is cool
The taste agent WS-12 and coolant agent WS-23 of 25 parts by weight is uniformly mixed, and obtains liquid mixture A；The menthol is particle
Shape crystal, coolant agent WS-12, coolant agent WS-3 and coolant agent WS-23 are pulverulent solids；
The preparation of the solvent B include: by the propylene glycol of 30 parts by weight, the Tween-80 of 20 parts by weight, 20 parts by weight ten gather it is sweet
Oily monolaurate is uniformly mixed, and obtains solvent B；
The preparation of the long-acting coolant agent of eutectic includes: solvent B to be added into mixture A, and add solvent B and mixture
The menthyl acetate of A quality sum 1.0% stirs under conditions of temperature is 90 DEG C, revolving speed is 30r/min, it is long to obtain eutectic
Imitate coolant agent liquid；
The preparation of the refrigerant pressed candy includes: by the long-acting coolant agent liquid of eutectic and pressed candy liquid essence according to 1:4
Mass ratio be uniformly mixed, be then sprayed at D-sorbite surface, the quality of D-sorbite is the long-acting coolant agent liquid of eutectic
8 times of the quality of body, and be uniformly mixed to obtain primary product, the primary product after dehumidification process, after adding dehumidifying
Quality 1% magnesium stearate, 3% malic acid, 0.1% Sucralose, 0.05% Aspartame, after being mixed evenly,
Tabletting is up to long-acting refrigerant tabletting sugar product.
Preferred embodiment are as follows: the dehumidification process is in vacuum drier, in vacuum gauge pressure -0.07MPa, temperature
Under the conditions of 50 DEG C, 120min is handled, until primary product water content is equal to 2.5%.
Preferred embodiment are as follows: the pressed candy is liquid cherry essence with liquid essence.
Embodiment three: a method of pressed candy is prepared using the long-acting coolant agent of eutectic
A method of pressed candy being prepared using the long-acting coolant agent of eutectic, it is the preparation of preparation, solvent B including mixture A, low
The preparation of the long-acting coolant agent of congruent melting and the preparation of refrigerant pressed candy；
The preparation of the mixture A includes: by the menthol of 25 parts by weight, the coolant agent WS-3 of 25 parts by weight, 25 parts by weight
The coolant agent WS-23 of coolant agent WS-12 and 25-55 parts by weight is uniformly mixed, and obtains liquid mixture A；The menthol
For granular crystals, coolant agent WS-12, coolant agent WS-3 and coolant agent WS-23 are pulverulent solids；
The preparation of the solvent B include: by the propylene glycol of 60 parts by weight, the Tween-80 of 35 parts by weight, 35 parts by weight ten gather it is sweet
Oily monolaurate is uniformly mixed, and obtains solvent B；
The preparation of the long-acting coolant agent of eutectic includes: solvent B to be added into mixture A, and add solvent B and mixture
The menthyl acetate of A quality sum 1.5% stirs under conditions of temperature is 150 DEG C, revolving speed is 60r/min, obtains eutectic
Long-acting coolant agent liquid；
The preparation of the refrigerant pressed candy includes: by the long-acting coolant agent liquid of eutectic and pressed candy liquid essence according to 1:6
Mass ratio be uniformly mixed, be then sprayed at D-sorbite surface, the quality of D-sorbite is the long-acting coolant agent liquid of eutectic
15 times of the quality of body, and be uniformly mixed to obtain primary product, the primary product after dehumidification process, after adding dehumidifying
Quality 3% magnesium stearate, 5% malic acid, 0.2% Sucralose, the Aspartame of 0.05-0.2% is mixed equal
After even, tabletting is up to long-acting refrigerant tabletting sugar product.
Preferred embodiment are as follows: the dehumidification process is in vacuum drier, in vacuum gauge pressure -0.10MPa, temperature
Under the conditions of 60 DEG C, 180min is handled, until primary product water content is less than or equal to 5%.
Preferred embodiment are as follows: the pressed candy is liquid peach flavor, liquid cherry essence, liquid with liquid essence
One of body grape essence, liquid flavoring orange essence, liquid orange flavor, liquid strawberry essence.It is specially liquid in the present embodiment
Body strawberry essence.
As described above is only to be not intended to tool to explain the preferred embodiments of the invention to do any shape to the present invention
Limitation in formula should all wrap therefore all have any modification or change for making the related present invention under identical spirit
It includes in the scope that the invention is intended to protect.
Claims (4)
1. a kind of method for preparing pressed candy using the long-acting coolant agent of eutectic, it is characterised in that: preparation including mixture A,
The preparation of the long-acting coolant agent of preparation, eutectic of solvent B and the preparation of refrigerant pressed candy；
The preparation of the mixture A includes: by coolant agent WS-3,17-25 of the menthol of 7-25 parts by weight, 17-25 parts by weight
The coolant agent WS-23 of coolant agent WS-12 and the 25-55 parts by weight of parts by weight is uniformly mixed, and obtains liquid mixture A；Institute
Stating menthol is granular crystals, and coolant agent WS-12, coolant agent WS-3 and coolant agent WS-23 are pulverulent solids；
The preparation of the solvent B includes: by the propylene glycol of 30-60 parts by weight, the Tween-80 of 20-35 parts by weight, 20-35 weight
The ten polyglycereol monolaurates of part are uniformly mixed, and obtain solvent B；
The preparation of the long-acting coolant agent of eutectic includes: solvent B to be added into mixture A, and add solvent B and mixture
The menthyl acetate of A quality sum 1.0-1.5%, is stirred under conditions of temperature is 90-150 DEG C, revolving speed is 30-60r/min,
Obtain the long-acting coolant agent liquid of eutectic；
The preparation of the refrigerant pressed candy includes: by the long-acting coolant agent liquid of eutectic and pressed candy liquid essence according to 1:4-
6 mass ratio is uniformly mixed, and D-sorbite surface is then sprayed at, and be uniformly mixed to obtain primary product, through dehumidifying
After technique, the magnesium stearate of the quality 1-3% of the primary product after adding dehumidifying, the malic acid of 3-5%, the trichlorine of 0.1-0.2%
Sucrose, the Aspartame of 0.05-0.2%, after being mixed evenly, tabletting is up to long-acting refrigerant tabletting sugar product.
2. the method according to claim 1 for preparing pressed candy using the long-acting coolant agent of eutectic, it is characterised in that: described
Dehumidification process is under the conditions of -0.07~-0.10MPa of vacuum gauge pressure, 50-60 DEG C of temperature, to handle 120- in vacuum drier
180min, until primary product water content is less than or equal to 5%.
3. the method according to claim 1 for preparing pressed candy using the long-acting coolant agent of eutectic, it is characterised in that: described
Pressed candy is liquid peach flavor, liquid cherry essence, liquid grape essence, liquid flavoring orange essence, liquid with liquid essence
One of orange flavor, liquid strawberry essence.
4. the method according to claim 1 for preparing pressed candy using the long-acting coolant agent of eutectic, it is characterised in that: described
The quality of D-sorbite is 8-15 times of the long-acting coolant agent liquid quality of eutectic.
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112315833A (en) * | 2020-11-24 | 2021-02-05 | 广州途富香料科技有限公司 | Composite strong cooling agent applied to toothpaste essence |
| CN112401053A (en) * | 2020-11-30 | 2021-02-26 | 南通亚香食品科技有限公司 | Mint amide compound cooling agent and preparation process thereof |
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| CN105124517A (en) * | 2015-09-11 | 2015-12-09 | 安徽爱迪香料股份有限公司 | Preparation method of cooling compound microcapsule |
| CN107751522A (en) * | 2017-11-09 | 2018-03-06 | 安徽爱迪香料股份有限公司 | A kind of overlength cool feeling duration pressed candy and preparation method thereof |
| CN107920571A (en) * | 2015-06-30 | 2018-04-17 | Wm.雷格利 Jr.公司 | Long-acting refrigerant preparation |
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| CN107920571A (en) * | 2015-06-30 | 2018-04-17 | Wm.雷格利 Jr.公司 | Long-acting refrigerant preparation |
| CN105124517A (en) * | 2015-09-11 | 2015-12-09 | 安徽爱迪香料股份有限公司 | Preparation method of cooling compound microcapsule |
| CN107751522A (en) * | 2017-11-09 | 2018-03-06 | 安徽爱迪香料股份有限公司 | A kind of overlength cool feeling duration pressed candy and preparation method thereof |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112315833A (en) * | 2020-11-24 | 2021-02-05 | 广州途富香料科技有限公司 | Composite strong cooling agent applied to toothpaste essence |
| CN112401053A (en) * | 2020-11-30 | 2021-02-26 | 南通亚香食品科技有限公司 | Mint amide compound cooling agent and preparation process thereof |
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