CN109452273A - A kind of agricultural builder of safflower seed oil and its preparation method and application - Google Patents

A kind of agricultural builder of safflower seed oil and its preparation method and application Download PDF

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Publication number
CN109452273A
CN109452273A CN201811342848.7A CN201811342848A CN109452273A CN 109452273 A CN109452273 A CN 109452273A CN 201811342848 A CN201811342848 A CN 201811342848A CN 109452273 A CN109452273 A CN 109452273A
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China
Prior art keywords
seed oil
safflower seed
agricultural
weight
builder
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CN201811342848.7A
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Chinese (zh)
Inventor
邓万平
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Zhongxiang Poinsettia Plant Immune Technology Co Ltd
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Zhongxiang Poinsettia Plant Immune Technology Co Ltd
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Priority to CN201811342848.7A priority Critical patent/CN109452273A/en
Publication of CN109452273A publication Critical patent/CN109452273A/en
Pending legal-status Critical Current

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    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N25/00Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests
    • A01N25/30Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests characterised by the surfactants
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N25/00Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests
    • A01N25/02Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests containing liquids as carriers, diluents or solvents
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N65/00Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N65/00Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
    • A01N65/08Magnoliopsida [dicotyledons]
    • A01N65/12Asteraceae or Compositae [Aster or Sunflower family], e.g. daisy, pyrethrum, artichoke, lettuce, sunflower, wormwood or tarragon

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  • Life Sciences & Earth Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • General Health & Medical Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Zoology (AREA)
  • Agronomy & Crop Science (AREA)
  • Plant Pathology (AREA)
  • Environmental Sciences (AREA)
  • Dentistry (AREA)
  • Wood Science & Technology (AREA)
  • Pest Control & Pesticides (AREA)
  • Toxicology (AREA)
  • Biotechnology (AREA)
  • Microbiology (AREA)
  • Mycology (AREA)
  • Natural Medicines & Medicinal Plants (AREA)
  • Botany (AREA)
  • Agricultural Chemicals And Associated Chemicals (AREA)

Abstract

The invention discloses a kind of agricultural builder of safflower seed oil, the agricultural builder of the safflower seed oil is made of the safflower seed oil of 2-9.5 parts by weight and the fatty alcohol polyoxyethylene ether of 0.5-3 parts by weight.The present invention also provides the applications that the agricultural builder of safflower seed oil is used to kill pest such as red spider, aphid, trialeurodes vaporariorum and pear sucker.There is the agricultural builder of safflower seed oil provided by the invention closing pest valve to make its death by suffocation, and dissolution pest body wall, the effect for causing its dehydration dead;The agricultural builder of the safflower seed oil has extremely low surface tension effects simultaneously, there are preferable wetability, adherence, scalability and permeability, it is suitble to be used in mixed way with insecticide, fungicide, herbicide and foliar fertilizer, it can also be used as and fly the spraying special synergistic auxiliary agent use of anti-or ultralow molten amount, in addition, also having the characteristics that not hurting natural enemy, not hurting crop, nontoxic residue-free, Environmental Safety.

Description

A kind of agricultural builder of safflower seed oil and its preparation method and application
Technical field
The present invention relates to agriculture field, in particular to a kind of agricultural builder of safflower seed oil and preparation method thereof and answer With.
Background technique
With the specification and execution of China's agricultural administrative regulation, high-toxic pesticide exits pesticide market completely;Recessive pesticide (third ingredient is added in registered ingredient) carries out pesticide label two dimensional code with country, and pesticide producing producer does not add completely Add third ingredient pesticide;It is efficient, environmentally friendly, organic, less toxic and low with environment protection treating, the remaining requirement of vegetable and fruit organic zero Remaining Pesticidal products demand is increasing;As the exploitation of noval chemical compound is slow, the resistance of pest and disease damage is more and more stronger, Nong Minfang Cure the disease insect pest cost it is higher and higher, the bad prevention and treatment of insect pest has become in current plant protection field very distinct issues.It is badly in need of A kind of environmentally friendly, organic, nontoxic, noresidue, physical pest killing and non-resistant forever Prevention Technique.Simultaneously, it is desirable to reduce pesticide residue, Pesticide utilization rate is improved, preserves the ecological environment and reduces drug cost.
Summary of the invention
In view of the foregoing drawbacks, the purpose of the present invention is to provide it is a kind of can kill pest for example red spider, aphid, trialeurodes vaporariorum, Pear sucker, while the kardiseed that can be reduced pesticide residue again, improve pesticide utilization rate, drug cost of preserving the ecological environment, reduce The agricultural builder of oil.
The present invention provides a kind of agricultural builders of safflower seed oil, and the agricultural builder of the safflower seed oil is by 2-9.5 weight Measure the safflower seed oil of part, the fatty alcohol polyoxyethylene ether composition of 0.5-3 parts by weight.
In one embodiment, safflower seed oil and 1 parts by weight of the agricultural builder of the safflower seed oil by 9 parts by weight Fatty alcohol polyoxyethylene ether composition.
The present invention also provides a kind of method for preparing the agricultural builder of safflower seed oil, this method are as follows: by 2-9.5 weight The safflower seed oil of part and the fatty alcohol polyoxyethylene ether of 0.5-3 parts by weight, while being added in agitator tank and being stirred 10 minutes, Then the temperature in agitator tank is increased to 100 DEG C -200 DEG C, continuous heating 4-6 hours.
In one embodiment, the above-mentioned temperature by agitator tank is increased to 150 DEG C.
In one embodiment, above-mentioned continuous heating 5 hours.
The present invention also provides the agricultural builder of safflower seed oil for kill pest for example red spider, aphid, trialeurodes vaporariorum and Application in pear sucker.
In one embodiment, above-mentioned application includes that the agricultural builder of the safflower seed oil is watered to 1000 times of dilution Liquid is spray applied.
There is the agricultural builder of safflower seed oil provided by the invention closing pest valve to make its asphyxia Death, and dissolution pest body wall, the effect for causing its dehydration dead;The agricultural builder of the safflower seed oil has extremely low simultaneously Surface tension effects have preferable wetability, adherence, scalability and permeability, are suitble to and insecticide, fungicide, herbicide It is used in mixed way with foliar fertilizer, can also be used as and fly the spraying special synergistic auxiliary agent use of anti-or ultralow molten amount, in addition, also having not Hurt natural enemy, hurt the features such as crop, nontoxic residue-free, Environmental Safety.
Specific embodiment
Detailed description of the preferred embodiments below.It should be understood that described herein specific Embodiment is merely to illustrate and explain the present invention, and is not intended to restrict the invention.
The present invention provides a kind of agricultural builders of safflower seed oil, and the agricultural synergy of the safflower seed oil is by 2-9.5 parts by weight Safflower seed oil, 0.5-3 parts by weight fatty alcohol polyoxyethylene ether composition.
Safflower seed oil is also known as safflower oil, is the oil product using kardiseed as waste.Safflower seed oil is in yellow, and standard type is red The fatty acid group of flower seed oil become palmitinic acid 5~9%, stearic acid 1~4.9%, oleic acid 11~15%, linoleic acid 69~79%, Iodine value 140 or so belongs to drying oil.Oleic acid-induced safflower seed oil accounts for about 60% based on oleic acid, linoleic acid 25%, and iodine value 105 is left The right side belongs to semi-drying oil.Containing nutritional ingredients such as vitamin E, oryzanol, sterols in oil, there is prevention and treatment artery sclerosis and reduce blood gallbladder The effect of sterol can reconcile into the health medicines such as " healthy oil ", " nutritional oil ", or manufacture linoleic acid pill with other edible oils First-class raw material.Paint raw materials industrially are mainly used as, are added in milk cow forage, the linoleic acid content of milk can be improved.Safflower Seed oil the agricultural synergist effect be main material, have wettability more better than other vegetable oil, plate-out ability, diffusivity and Permeate the effect of sexual function and low-temperature resistance.In addition, safflower seed oil is plant oil, it is not compatible with water, and pesticide, foliar fertilizer are all Be it is mixed with water after carry out spraying, compatible with water synergistic effect cannot not be just had yet, therefore it is necessary to which safflower seed oil is cooked Synergistic effect just can be really played at finish can be dispersed in water.Safflower seed oil and fatty alcohol polyoxyethylene ether Hybrid Heating Afterwards, safflower seed oil can be uniformly dispersed in water in the form of Water-In-Oil, to reach safflower seed oil synergy purpose.
In the case of, according to the invention it is preferred to, safflower seed oil and 1 weight of the agricultural builder of the safflower seed oil by 9 parts by weight Measure the fatty alcohol polyoxyethylene ether of part.The safflower seed oil agricultural synergist that the weight ratio makes dilutes 1000 times of liquid, converts Can be dispersed in water naturally such as magic mushroom cloud form after water dilution, be pale suspension liquid, can by safflower seed oil effectively at Point substantially uniformity is dispersed in water in the form of Water-In-Oil, to reach when medical fluid acts on target boomerang, can be played and be opened up, expands Scattered, wet, infiltration effect.The agricultural synergist that the weight ratio makes is advantageous in that:
1) surface tension can be reduced to 30N/m, there is very strong diffusivity and permeability.
2) the distinctive oiliness feature of safflower seed oil itself has stronger plate-out ability and wettability.
3) Pesticide use cost the utilization rate of pesticide can be effectively improved (up to 50% or more), is reduced.
The present invention will be described in detail by way of examples below, but the present invention is not limited in following embodiments.
Embodiment 1
The present embodiment is used to illustrate the preparation of the agricultural builder of safflower seed oil provided by the invention.
By the fatty alcohol polyoxyethylene ether of the safflower seed oil of 9 parts by weight and 1 parts by weight, while being added in agitator tank and carrying out Stirring 10 minutes, then, raises the temperature to 150 DEG C, continuous heating 5 hours.
Embodiment 2
The present embodiment is used to illustrate the preparation of the agricultural builder of safflower seed oil provided by the invention.
By the fatty alcohol polyoxyethylene ether of the safflower seed oil of 9.5 parts by weight and 3 parts by weight, at the same be added in agitator tank into Row stirring 10 minutes, then, raises the temperature to 200 DEG C, continuous heating 6 hours.
Embodiment 3
The present embodiment is used to illustrate the preparation of the agricultural builder of safflower seed oil provided by the invention.
By the fatty alcohol polyoxyethylene ether of the safflower seed oil of 2 parts by weight and 0.5 parts by weight, at the same be added in agitator tank into Row stirring 10 minutes, then, raises the temperature to 100 DEG C, continuous heating 4 hours.
Safflower seed oil and 1 weight of the agricultural builder formula of safflower seed oil that following example 4-8 is applied by 9 parts by weight The fatty alcohol polyoxyethylene ether composition of part.
4 the present embodiment of embodiment is for illustrating the agricultural builder of safflower seed oil provided by the invention for killing red spider The application of spider.
Test period: 6 pm on October 20th, 2018
Test site: the Hechi City, Guangxi rivers and ponds town village the Hong Sha base Wo Gan
Subjects: citrus red mite
Weather condition: 18 degree of temperature, cloudy
Test medicine and use multiple:
The agricultural builder 15ml of safflower seed oil is watered 15 kilograms (1000 times of dilutions) and is sprayed
Insect population: there is 30 red spiders (adult mite and deutonymph) on average every leaf
Pay a return visit effect:
20 minutes: the death rate 50%
24 hours: the death rate 80%
48 hours: the death rate 98%.
5 the present embodiment of embodiment is for illustrating the agricultural builder of safflower seed oil provided by the invention for killing aphid Application.
Test period: at 4 points in afternoon on June 27th, 2018
Test site: the company's Cot-ton base of Aksu of Xinjiang the 16th eight
Subjects: cotton/aphid
Weather condition: 38 degree of temperature, fine day
Test medicine and use multiple:
The agricultural builder 15ml of safflower seed oil is watered 15 kilograms (1000 times of dilutions) and is sprayed
Insect population: top lobus cardiacus, average every aphid 120 (yellow aphids, green aphid, black aphid)
Pay a return visit effect:
30 minutes: the death rate 90%
24 hours: the death rate 98%.
6 the present embodiment of embodiment is for illustrating the agricultural builder of safflower seed oil provided by the invention for killing white powder The application of lice.
Test period: August in 2018 at 3 points in afternoon on the 10th
Test site: Guangdong Province, the town Qu Sanjiang, Zengcheng end of the bridge village Vegetable Base
Subjects: eggplant trialeurodes vaporariorum
Weather condition: 28 degree of temperature, fine day
Test medicine and use multiple:
The agricultural builder 15ml of safflower seed oil is watered 15 kilograms (1000 times of dilutions) and is sprayed
Insect population: every leaf trialeurodes vaporariorum 210 average
Pay a return visit effect:
5 minutes: the death rate 95%
24 hours: the death rate 98%
7 the present embodiment of embodiment is for illustrating the agricultural builder of safflower seed oil provided by the invention for killing pear wood The application of lice.
Test period: 10 points of the morning of August in 2018 19 day
Test site: Hebei province, peach garden town, the Jinzhou City village Yuan Jia village
Subjects: pear tree/pear sucker
Weather condition: 32 degree of temperature, fine day
Test medicine and use multiple:
The agricultural builder 15ml of safflower seed oil is watered 15 kilograms (1000 times of dilutions) and is sprayed
Insect population: every leaf pear sucker 32 average
Pay a return visit effect:
24 hours: the death rate 95%.
8 the present embodiment of case study on implementation reduces surface for illustrating that the agricultural builder of safflower seed oil provided by the invention has The effect of tension.
The agricultural builder of safflower seed oil provided by the invention is watered 1000 times of liquid of dilution, is surveyed through surface tension apparatus Fixed, surface tension is 30 dynes per centimeters, is sprayed to fruit tree, vegetables, on field crop, can effectively be adhered on blade, have compared with Good adhesion strength, scalability, permeability and wetability.
The effect of embodiment 4 and 9 is the safflower seed oil agricultural builder of different proportion formula compares.
9 the present embodiment of embodiment is used to illustrate the safflower seed oil of different weight part and the kardiseed of fatty alcohol polyoxyethylene ether The effect of oily agricultural builder, is different.
The safflower seed oil of the agricultural builder of safflower seed oil and the weight part ratio of fatty alcohol polyoxyethylene ether are 6:4
Test period: 6 pm on October 20th, 2018
Test site: the Hechi City, Guangxi rivers and ponds town village the Hong Sha base Wo Gan
Subjects: citrus red mite
Weather condition: 18 degree of temperature, cloudy
Test medicine and use multiple:
The agricultural builder 15ml of safflower seed oil is watered 15 kilograms (1000 times of dilutions) and is sprayed
Insect population: there is 30 red spiders (adult mite and deutonymph) on average every leaf
Pay a return visit effect:
20 minutes: the death rate 35%
24 hours: the death rate 62%
48 hours: the death rate 86%.
Comparative example 4 and the discovery of embodiment 9, safflower seed oil and 1 weight of the agricultural builder of safflower seed oil by 9 parts by weight The formula for measuring the fatty alcohol polyoxyethylene ether composition of part is optimization formula.
The above description is merely a specific embodiment, but scope of protection of the present invention is not limited thereto, any Those familiar with the art in the technical scope disclosed by the present invention, can easily think of the change or the replacement, and should all contain Lid is within protection scope of the present invention.Therefore, protection scope of the present invention should be subject to the protection scope in claims.

Claims (7)

1. a kind of agricultural builder of safflower seed oil, it is characterised in that: the agricultural builder of the safflower seed oil is by 2-9.5 parts by weight Safflower seed oil, 0.5-3 parts by weight fatty alcohol polyoxyethylene ether composition.
2. the agricultural builder of safflower seed oil according to claim 1, it is characterised in that: the agricultural synergy of safflower seed oil Auxiliary agent is made of the safflower seed oil of 9 parts by weight and the fatty alcohol polyoxyethylene ether of 1 parts by weight.
3. a kind of method for preparing the agricultural builder of safflower seed oil, which is characterized in that this method are as follows: by 2-9.5 parts by weight The fatty alcohol polyoxyethylene ether of safflower seed oil and 0.5-3 parts by weight, while being added in agitator tank and being stirred 10 minutes, then Temperature in the agitator tank is increased to 100 DEG C -200 DEG C, continuous heating 4-6 hours.
4. according to the method described in claim 3, it is characterized by: the temperature by the agitator tank is increased to 150 DEG C.
5. according to the method described in claim 4, it is characterized by: the continuous heating 5 hours.
6. the agricultural builder of safflower seed oil as claimed in claim 1 or 2 is for killing pest such as red spider, aphid, white powder Application in lice and pear sucker.
7. application according to claim 6, which is characterized in that the application includes helping the agricultural synergy of the safflower seed oil Agent is watered 1000 times of liquid of dilution and is spray applied.
CN201811342848.7A 2018-11-13 2018-11-13 A kind of agricultural builder of safflower seed oil and its preparation method and application Pending CN109452273A (en)

Priority Applications (1)

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CN201811342848.7A CN109452273A (en) 2018-11-13 2018-11-13 A kind of agricultural builder of safflower seed oil and its preparation method and application

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201811342848.7A CN109452273A (en) 2018-11-13 2018-11-13 A kind of agricultural builder of safflower seed oil and its preparation method and application

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Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1701663A (en) * 2005-06-24 2005-11-30 福建省泉州德盛农药有限公司 Pesticide auxiliary agent
CN1926998A (en) * 2006-08-11 2007-03-14 聊城大学农学院 Vegetable oil insecticide and method of use thereof
CN102283254A (en) * 2010-03-17 2011-12-21 钟韬 Plant source environmentally-friendly pesticide preparation
CN102860301A (en) * 2011-07-05 2013-01-09 江门市新会园田生物工程有限公司 Azadirachtin preparation using vegetable oil as medium
CN106332919A (en) * 2016-08-27 2017-01-18 梁小萍 Pesticide for preventing Arbela dea and preparing method thereof
CN106561645A (en) * 2016-10-20 2017-04-19 钟祥尤生农药有限公司 Agricultural synergist, and preparation method and application of agricultural synergist

Patent Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1701663A (en) * 2005-06-24 2005-11-30 福建省泉州德盛农药有限公司 Pesticide auxiliary agent
CN1926998A (en) * 2006-08-11 2007-03-14 聊城大学农学院 Vegetable oil insecticide and method of use thereof
CN102283254A (en) * 2010-03-17 2011-12-21 钟韬 Plant source environmentally-friendly pesticide preparation
CN102860301A (en) * 2011-07-05 2013-01-09 江门市新会园田生物工程有限公司 Azadirachtin preparation using vegetable oil as medium
CN106332919A (en) * 2016-08-27 2017-01-18 梁小萍 Pesticide for preventing Arbela dea and preparing method thereof
CN106561645A (en) * 2016-10-20 2017-04-19 钟祥尤生农药有限公司 Agricultural synergist, and preparation method and application of agricultural synergist

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Title
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