CN109399967A - Heat-insulated vacuum glass of nano-film coating tempering and preparation method thereof - Google Patents
Heat-insulated vacuum glass of nano-film coating tempering and preparation method thereof Download PDFInfo
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- CN109399967A CN109399967A CN201811350792.XA CN201811350792A CN109399967A CN 109399967 A CN109399967 A CN 109399967A CN 201811350792 A CN201811350792 A CN 201811350792A CN 109399967 A CN109399967 A CN 109399967A
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- Prior art keywords
- glass
- panels
- tempered glass
- nano
- heat
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- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Classifications
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C27/00—Joining pieces of glass to pieces of other inorganic material; Joining glass to glass other than by fusing
- C03C27/06—Joining glass to glass by processes other than fusing
- C03C27/10—Joining glass to glass by processes other than fusing with the aid of adhesive specially adapted for that purpose
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03B—MANUFACTURE, SHAPING, OR SUPPLEMENTARY PROCESSES
- C03B27/00—Tempering or quenching glass products
- C03B27/012—Tempering or quenching glass products by heat treatment, e.g. for crystallisation; Heat treatment of glass products before tempering by cooling
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C17/00—Surface treatment of glass, not in the form of fibres or filaments, by coating
- C03C17/02—Surface treatment of glass, not in the form of fibres or filaments, by coating with glass
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C17/00—Surface treatment of glass, not in the form of fibres or filaments, by coating
- C03C17/22—Surface treatment of glass, not in the form of fibres or filaments, by coating with other inorganic material
Abstract
The invention discloses a kind of heat-insulated vacuum glass of nano-film coating tempering, the vacuum glass is the double glazing that the connection sealed around being combined by two panels tempered glass, intermediate seal chamber vacuumize, and the seal chamber side of the sheet glass in two panels tempered glass is coated with nanometer transparent energy-saving glass coating.And it is printed with fulcrum evenly dispersedly between two panels tempered glass.Fulcrum uses pyroceram glaze.About 600 DEG C of the nanometer transparent energy-saving glass coating high temperature resistant.Also disclose the preparation method of the vacuum glass.The present invention is vacuumized using two panels tempered glass and is combined into, and in a piece of interior surfaces of glass coated with nano transparent energy-saving glass coating, not only sunshading and heat-insulating performance is improved, and safety is also obviously improved.Preparation method of the present invention was by first carrying out tempering processing to two panels plate glass, then tempered glass is crossed to two panels to carry out surface coating, combination, edge sealing, move back tempering while vacuumizing, obtain the heat-insulated vacuum glass of nano-film coating tempering that thermal insulation, sun-shade has a safety feature.
Description
Technical field
The present invention relates to heat-insulated tempering glass technology fields, more particularly to a kind of heat-insulated vacuum glass of nano-film coating tempering
And preparation method thereof.
Background technique
Vacuum glass is to enclose two panels plate glass surrounding, its gap is evacuated and seal aspirating hole and
At.Existing vacuum glass could be used without the structure of film mostly, or using the structure for being coated with low-e plated film.Using existing true
Window made of empty glass is there are heat transfer coefficient height, and heat transfer coefficient is generally in 2.5W/ (m2.K more than), amount of heat passes through door and window
It is lost, the air-tightness of forms is poor, and indoor dew condensation phenomenon is serious.And the glass for being coated with low-e plated film is unable to high temperature resistant, also
It is exactly to use the rigidity of vacuum glass made of general plate glass inadequate, then safety is not high.
It can be seen that above-mentioned existing vacuum glass is in structure, method and using upper, it is clear that there are still have it is inconvenient with it is scarce
It falls into, and needs to be further improved.How a kind of new nano-film coating tempering heat-insulated vacuum glass and its preparation side are founded
Method makes it that can obtain larger raising in terms of insulation and safety, and becoming current industry pole needs improved target.
Summary of the invention
The technical problem to be solved in the present invention is to provide a kind of heat-insulated vacuum glass of nano-film coating tempering, make it in thermal insulation separation
Larger raising can be obtained in terms of heat and safety, to overcome the shortcomings of existing vacuum glass.
In order to solve the above technical problems, the present invention provides a kind of heat-insulated vacuum glass of nano-film coating tempering, the vacuum glass
Glass is the double glazing that the connection sealed around being combined by two panels tempered glass, intermediate seal chamber vacuumize, the two panels
The seal chamber side of a sheet glass in tempered glass is coated with nanometer transparent energy-saving glass coating.
It is further improved, is printed with fulcrum evenly dispersedly between the two panels tempered glass.
It is further improved, the fulcrum uses pyroceram glaze.
It is further improved, about 600 DEG C of the nanometer transparent energy-saving glass coating high temperature resistant.
Be further improved, the heat-insulated vacuum glass of nano-film coating tempering the preparation method comprises the following steps:
(1) two panels plate glass is sent into continuous annealing furnace and carried out tempering processing, obtained two panels and cross tempered glass;
(2) the wherein a piece of inner surface for crossing tempered glass is uniformly smeared into one layer of nanometer transparent energy conservation glass using coating processes
Glass coating;
(3) another is crossed on tempered glass surface again and prints pyroceram glaze evenly dispersedly, after natural drying
It is dried in drying oven;
(4) step (2) and (3) resulting two panels tempered glass is crossed to combine, and step (2) obtain cross tempered glass
Nanometer transparent energy-saving glass coating side is in contact with the pyroceram glaze side for crossing tempered glass that step (3) obtains, and
Two panels crosses the periphery filling low melting point sealing material of tempered glass, forms two panels and crosses the seal chamber among tempered glass, and one
Piece, which is crossed, is arranged aspirating hole on tempered glass, the aspirating hole is communicated with the seal chamber, and the lower part of the aspirating hole is put into one
Piece evaporable air-absorbing agent;
(5) the edge sealing furnace low temperature crossed tempered glass and be sent into 100 DEG C~400 DEG C after the two panels for obtaining step (4) combines
Heating makes low melting point sealing material melt sealing, while so that two panels is crossed tempered glass and moving back tempering, becomes the tempering glass of two panels combination
Glass;
(6) vacuum suction device is utilized simultaneously, the seal chamber is vacuumized by the aspirating hole, and seal pumping
Hole is to get the heat-insulated vacuum glass of nano-film coating tempering.
The present invention also provides a kind of preparation method of heat-insulated vacuum glass of nano-film coating tempering, the preparation method includes such as
Lower step:
(1) two panels plate glass is sent into continuous annealing furnace and carried out tempering processing, obtained two panels and cross tempered glass;
(2) the wherein a piece of inner surface for crossing tempered glass is uniformly smeared into one layer of nanometer transparent energy conservation glass using coating processes
Glass coating;
(3) another is crossed on tempered glass surface again and prints pyroceram glaze evenly dispersedly, after natural drying
It is dried in drying oven;
(4) step (2) and (3) resulting two panels tempered glass is crossed to combine, and step (2) obtain cross tempered glass
Nanometer transparent energy-saving glass coating side is in contact with the pyroceram glaze side for crossing tempered glass that step (3) obtains, and
Two panels crosses the periphery filling low melting point sealing material of tempered glass, forms two panels and crosses the seal chamber among tempered glass, and one
Piece, which is crossed, is arranged aspirating hole on tempered glass, the aspirating hole is communicated with the seal chamber, and the lower part of the aspirating hole is put into one
Piece evaporable air-absorbing agent;
(5) the edge sealing furnace low temperature crossed tempered glass and be sent into 100 DEG C~400 DEG C after the two panels for obtaining step (4) combines
Heating makes low melting point sealing material melt sealing, while so that two panels is crossed tempered glass and moving back tempering, becomes the tempering glass of two panels combination
Glass;
(6) vacuum suction device is utilized simultaneously, the seal chamber is vacuumized by the aspirating hole, and seal pumping
Hole is to get the heat-insulated vacuum glass of nano-film coating tempering.
It is further improved, 690~720 DEG C of temperature that tempering processing is crossed in the step (1).
It is further improved, about 600 DEG C of nanometer transparent energy-saving glass coating high temperature resistant in the step (2).
It is further improved, the naturally dry time about 1.5 hours in the step (3), dries about 120 DEG C of furnace temperature, drying
Time about 15 minutes.
By adopting such a design, the present invention has at least the following advantages:
1, in vacuum glass, wherein a piece of interior surfaces of glass coats heat-barrier material to the present invention, and both nanometer transparent energy-saving glass applied
Material, is able to achieve fabulous heat preservation, sunshade, heat-insulated purpose;And vacuum glass is combined using two panels tempered glass, safety
The safety of conventional vacuum glass can be much higher than.
2, then preparation method of the present invention crosses tempering to the two panels by first carrying out tempering processing to two panels plate glass
Glass carries out surface coating respectively, combines, and finally carries out edge sealing again, moves back tempering, vacuum step, finally obtains satisfactory
The heat-insulated vacuum glass of nano-film coating tempering.
3, applied nanometer transparent energy-saving glass coating can be about 600 DEG C of high temperature resistant in the present invention, which is to realize the invention
Preparation method provides possibility.
Detailed description of the invention
The above is merely an overview of the technical solutions of the present invention, in order to better understand the technical means of the present invention, below
In conjunction with attached drawing, the present invention is described in further detail with specific embodiment.
Fig. 1 is the schematic structural cross-sectional view of the heat-insulated vacuum glass of nano-film coating tempering of the present invention.
Wherein, 1, low melting point sealing material, 2, fulcrum, 3, seal chamber, 4, glass, 5, aspirating hole, 6, evaporable air-absorbing agent,
7, glass, 8, sealing of hole, 9, nanometer transparent energy-saving glass coating.
Specific embodiment
Referring to shown in attached drawing 1, the heat-insulated vacuum glass of the present embodiment nano-film coating tempering by two panels tempered glass 4,7 in conjunction with and
At the connection sealed around of the two panels tempered glass 4,7, intermediate formation vacuum-sealed cavity 3.And it is a piece of in two panels tempered glass
The seal chamber side of glass 7 is coated with nanometer transparent energy-saving glass coating 9.
The nanometer transparent energy-saving glass coating 9 uses existing intelligent nano transparent insulating glass coating, can rise
To better function of heat insulation.The nanometer transparent energy-saving glass coating 9 uses the first patent of invention of applicant in the present embodiment
Apply for intelligence disclosed in (application number 200910091203.5, denomination of invention: intelligent nano transparent insulating glass coating)
Nanometer transparent heat insulation glass coating.Its specific formula and the preparation method comprises the following steps: with organic siliconresin, nano-indium stannum oxide or receiving
Rice tin-antiomony oxide slurry, nano silica or nano-aluminium oxide slurry, doping nano vanadium dioxide slurry, diluent and
Auxiliary agent is composition, and is prepared by following weight (%): organic siliconresin 24-70%;Nano-indium stannum oxide or nanometer
Tin-antiomony oxide slurry 18-45%;Nano silica or nano-aluminium oxide slurry 1-10%;Doping nano vanadium dioxide slurry
Expect 10-15%;Diluent 0-5%;Auxiliary agent 0-3%.After each ingredient is selected, then nano-indium stannum oxide or nano antimony tin oxide starched
Material, nano silica or nano-aluminium oxide slurry, doping nano vanadium dioxide slurry, auxiliary agent and diluent are added dropwise respectively
Into organic siliconresin, and stir the 10-30 minutes intelligent nano transparent insulating glass coatings to get synthesis.
After the intelligent nano transparent insulating glass coating is coated on glass, intelligence can be played and adjust room temperature
Effect, such as when outdoor temperature is higher than 35 DEG C, which can reduce the transmitance of near infrared ray, and when lower than 35 DEG C, it can be improved
The transmitance of near infrared ray realizes the winter so as to vary with temperature the automatic adjustment for realizing glass near infrared ray transmitance
Ji Baowen, get Re and summer sunshade, daylighting, heat-insulated function, greatly improve energy-saving effect.
The nanometer transparent energy-saving glass coating 9 is coated in the inside of toughened vacuum glass by the application, its tempering can be made true
Empty glass not only keeps the temperature, is heat-insulated, shading performance is greatly improved, but also security performance has also obtained great promotion.Such as energy conservation
Glass transition coefficient is down to 2.1W/ (m2) below .k shading coefficient SC is 0.4~0.7.
And another improvement of the present invention is how to realize the preparation of the above-mentioned heat-insulated vacuum glass of nano-film coating tempering,
Preparation method includes:
(1) two panels plate glass 4,7 is sent into continuous annealing furnace and carried out tempering processing, which reaches
600 DEG C or more are crossed tempered glass to get to two panels.
(2) the wherein a piece of inner surface for crossing tempered glass 7 is uniformly smeared into one layer of nanometer transparent energy conservation using coating processes
Glass coating 9;About 600 DEG C of high temperature resistant of the nanometer transparent energy-saving glass coating energy, which provides for the implementation of this preparation method
It may.
(3) another is crossed on 4 surface of tempered glass again and prints pyroceram glaze, naturally dry evenly dispersedly
1.5 hours or more, place into drying about 15 minutes in about 120 DEG C of drying ovens;The pyroceram glaze is convenient for as fulcrum 2
Gap is formed between two sheet glass.
(4) step (2) and (3) resulting two panels tempered glass is crossed to combine, and step (2) obtain cross tempered glass
Nanometer transparent energy-saving glass coating side is in contact with the pyroceram glaze side for crossing tempered glass that step (3) obtains, and
Two panels crosses the periphery filling low melting point sealing material 1 of tempered glass, forms two panels and crosses the seal chamber 3 among tempered glass, and
Aspirating hole 5 is arranged in a piece of cross on tempered glass, which communicates with seal chamber 3, and the lower part of aspirating hole 5 place into it is a piece of
Evaporable air-absorbing agent 6;The evaporable air-absorbing agent 6 can absorb the gas in seal chamber, guarantee the transparency of double glazing.
(5) the edge sealing furnace low temperature crossed tempered glass and be sent into 100 DEG C~400 DEG C after the two panels for obtaining step (4) combines
Heating makes low melting point sealing material melt sealing, while so that two panels is crossed tempered glass and moving back tempering, becomes two panels tempered glass.
(6) vacuum suction device is utilized simultaneously, seal chamber 3 is vacuumized by aspirating hole 5, and to the sealing of aspirating hole 58
It is blocked to get the heat-insulated vacuum glass of nano-film coating tempering.
The heat-insulated vacuum glass of nano-film coating tempering is not only able to achieve fabulous heat preservation, sunshade, heat-insulated purpose, also has
High security performance, it is much better more than conventional vacuum glass or hollow glass, it is suitable as energy saving door and window, energy-saving ring
It protects.
The above described is only a preferred embodiment of the present invention, be not intended to limit the present invention in any form, this
Field technical staff makes a little simple modification, equivalent variations or modification using the technology contents of the disclosure above, all falls within this hair
In bright protection scope.
Claims (9)
1. a kind of heat-insulated vacuum glass of nano-film coating tempering, which is characterized in that the vacuum glass is by two panels tempered glass knot
Connection sealed around, the double glazing that vacuumizes of intermediate seal chamber made of conjunction, the sheet glass in the two panels tempered glass
Seal chamber side be coated with nanometer transparent energy-saving glass coating.
2. the heat-insulated vacuum glass of nano-film coating tempering according to claim 1, which is characterized in that the two panels tempered glass
Between be printed with fulcrum evenly dispersedly.
3. the heat-insulated vacuum glass of nano-film coating tempering according to claim 2, which is characterized in that the fulcrum uses resistance to height
Warm glass glaze.
4. the heat-insulated vacuum glass of nano-film coating tempering according to claim 1, which is characterized in that the nanometer transparent energy conservation
About 600 DEG C of glass coating high temperature resistant.
5. the heat-insulated vacuum glass of nano-film coating tempering according to claim 1, which is characterized in that the nano-film coating tempering
Heat-insulated vacuum glass the preparation method comprises the following steps:
(1) two panels plate glass is sent into continuous annealing furnace and carried out tempering processing, obtained two panels and cross tempered glass;
(2) the wherein a piece of inner surface for crossing tempered glass one layer of nanometer transparent energy-saving glass is uniformly smeared using coating processes to apply
Material;
(3) another is crossed on tempered glass surface again and prints pyroceram glaze evenly dispersedly, dried after natural drying
Drying in dry furnace;
(4) step (2) and (3) resulting two panels are crossed tempered glass to combine, and the nanometer for crossing tempered glass that step (2) obtains
Transparent energy-saving glass coating side is in contact with the pyroceram glaze side for crossing tempered glass that step (3) obtains and two panels
The periphery filling low melting point sealing material for crossing tempered glass, forms two panels and crosses the seal chamber among tempered glass, and in a piece of mistake
Aspirating hole is set on tempered glass, and the aspirating hole is communicated with the seal chamber, and the lower part of the aspirating hole is put into a piece of steaming
Dissipate type getter;
(5) the edge sealing furnace low-temperature heat crossed tempered glass and be sent into 100 DEG C~400 DEG C after the two panels for obtaining step (4) combines,
So that low melting point sealing material is melted sealing, while so that two panels is crossed tempered glass and moving back tempering, becomes the tempered glass of two panels combination;
(6) vacuum suction device is utilized simultaneously, the seal chamber is vacuumized by the aspirating hole, and seal aspirating hole, i.e.,
Obtain the heat-insulated vacuum glass of nano-film coating tempering.
6. a kind of preparation method of the heat-insulated vacuum glass of nano-film coating tempering, which is characterized in that the preparation method includes as follows
Step:
(1) two panels plate glass is sent into continuous annealing furnace and carried out tempering processing, obtained two panels and cross tempered glass;
(2) the wherein a piece of inner surface for crossing tempered glass one layer of nanometer transparent energy-saving glass is uniformly smeared using coating processes to apply
Material;
(3) another is crossed on tempered glass surface again and prints pyroceram glaze evenly dispersedly, dried after natural drying
Drying in dry furnace;
(4) step (2) and (3) resulting two panels are crossed tempered glass to combine, and the nanometer for crossing tempered glass that step (2) obtains
Transparent energy-saving glass coating side is in contact with the pyroceram glaze side for crossing tempered glass that step (3) obtains and two panels
The periphery filling low melting point sealing material for crossing tempered glass, forms two panels and crosses the seal chamber among tempered glass, and in a piece of mistake
Aspirating hole is set on tempered glass, and the aspirating hole is communicated with the seal chamber, and the lower part of the aspirating hole is put into a piece of steaming
Dissipate type getter;
(5) the edge sealing furnace low-temperature heat crossed tempered glass and be sent into 100 DEG C~400 DEG C after the two panels for obtaining step (4) combines,
So that low melting point sealing material is melted sealing, while so that two panels is crossed tempered glass and moving back tempering, becomes the tempered glass of two panels combination;
(6) vacuum suction device is utilized simultaneously, the seal chamber is vacuumized by the aspirating hole, and seal aspirating hole, i.e.,
Obtain the heat-insulated vacuum glass of nano-film coating tempering.
7. the preparation method of the heat-insulated vacuum glass of nano-film coating tempering according to claim 6, which is characterized in that the step
Suddenly the temperature that tempering processing is crossed in (1) is 690~720 DEG C.
8. the preparation method of the heat-insulated vacuum glass of nano-film coating tempering according to claim 6, which is characterized in that the step
Suddenly about 600 DEG C of nanometer transparent energy-saving glass coating high temperature resistant in (2).
9. the preparation method of the heat-insulated vacuum glass of nano-film coating tempering according to claim 6, which is characterized in that the step
Suddenly naturally dry time about 1.5 hours in (3) dry about 120 DEG C of furnace temperature, drying time about 15 minutes.
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Cited By (1)
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CN109928649A (en) * | 2019-05-07 | 2019-06-25 | 陈贞辉 | A kind of energy-saving glass and preparation method thereof for building |
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Application publication date: 20190301 |