CN109381889A - A kind of segregative alkaloid extraction equipment of solid-liquid - Google Patents
A kind of segregative alkaloid extraction equipment of solid-liquid Download PDFInfo
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- CN109381889A CN109381889A CN201811420504.3A CN201811420504A CN109381889A CN 109381889 A CN109381889 A CN 109381889A CN 201811420504 A CN201811420504 A CN 201811420504A CN 109381889 A CN109381889 A CN 109381889A
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- tower body
- solid
- segregative
- liquid
- extraction
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D11/00—Solvent extraction
- B01D11/02—Solvent extraction of solids
- B01D11/0215—Solid material in other stationary receptacles
- B01D11/0253—Fluidised bed of solid materials
- B01D11/0257—Fluidised bed of solid materials using mixing mechanisms, e.g. stirrers, jets
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- Extraction Or Liquid Replacement (AREA)
Abstract
The invention discloses a kind of segregative alkaloid extraction equipments of solid-liquid, including tower body, tower body two sides top is fitted with the mother tube and liquid extraction pipe protruded into inside tower body respectively, it is extraction chamber inside the tower body, it is intracavitary equipped with stirring structure extracting, the stirring structure includes agitator disk, the agitator disk is in vertically arranged disk, and multiple turbulator rods being distributed uniformly and circumferentially are equipped in stirring disc side, the agitator disk is sequentially connected by agitating shaft with the stirring motor being fixed on tower body outer wall；The tower body internal upper part is equipped with the fine and closely woven strainer docked with tower body inner wall sealing and thick intercept net；The present apparatus respectively screens raw material in fill process and during discharging, realizes solid-liquid separation effect, facilitate the classification work in later period by this fine and closely woven strainer of tower body internal upper part and thick intercept net, and by the setting of enhancing tube.
Description
Technical field
The present invention relates to chemical industry equipment, specifically a kind of segregative alkaloid extraction equipment of solid-liquid.
Background technique
Extraction is that have different solubility come the operating unit of separating mixture, i.e. benefit in a solvent using component in system
With substance, solubility or distribution coefficient are different in two kinds of mutual exclusive solvents, are transferred to solute substance out of a kind of solvent
Method in another solvent, it is industrial that abstraction technique is widely used in chemistry, metallurgy and food etc.；Extraction be divided into liquid-liquid extraction,
Liquid-solid extraction and supercritical fluid extraction.
Alkaloid is a kind of nitrogenous alkalinity being present in nature (predominantly plant, but some exists in animal)
Organic compound has the property like alkali, so being also known as counterfeit alkali in the past.Most of to have complicated cyclic structure, nitrogen includes more
In ring, there is significant bioactivity, is one of effective component important in Chinese herbal medicine.
The extraction of alkaloid at present mainly using plus alkali extraction method, using plant material and extract liquor be sufficiently mixed into
Row, but solid-liquid needs the problem of being separated again, production efficiency is caused to decline after hybrid extraction.
Summary of the invention
The purpose of the present invention is to provide a kind of segregative alkaloid extraction equipments of solid-liquid, to solve above-mentioned background technique
The problem of middle proposition.
To achieve the above object, the invention provides the following technical scheme:
A kind of segregative alkaloid extraction equipment of solid-liquid, including tower body, tower body two sides top is fitted with respectively to be protruded into
Mother tube and liquid extraction pipe inside tower body, the tower body inside is extraction chamber, intracavitary equipped with stirring structure extracting, described to stir
Mixing structure includes agitator disk, and the agitator disk is to be equipped with multiple circumferentially sides in vertically arranged disk, and in stirring disc side
To equally distributed turbulator rod, the agitator disk is sequentially connected by agitating shaft with the stirring motor being fixed on tower body outer wall；
The tower body internal upper part be equipped with the tower body inner wall fine and closely woven strainer that docks of sealing and thick intercept net, fine and closely woven strainer and thick intercept net it
Between be sundries chamber, it is intracavitary that the nozzle of the mother tube and liquid extraction pipe one end in tower body is located at sundries, and sets in tower body
There is the enhancing tube through fine and closely woven strainer and thick intercept net, there are gaps between the enhancing tube lower end and tower body inner bottom surface, are mentioning
Rise cylinder in be equipped with promoted axis, and promoted axis on be equipped with helical blade, the promotions axis upper end be fixed on tower body center of top
Promotion motor drive connection；The extraction bottom of chamber portion is connected with outlet tube.
Pedestal is equipped with below tower body, the axis lower end that promoted is protruded into pedestal and turned with the bearing block being fixed in pedestal
Dynamic connection；Impurities removal door is also provided on the tower body side wall, the impurities removal door and sundries chamber are located in same level.
The present apparatus also has control system, and the control system includes controller, and the controller is S7-200CN model
PLC, controller has time control module and Weight control module, the Weight control module and time control module signal
Connection, the Weight control module are connected with weight induction device, and weight induction device is located on fine and closely woven strainer 13 and thick intercept net 14；
The time control module has stirring motor driving circuit and promotes motor-drive circuit.
As a preferred solution of the present invention: the extraction bottom of chamber portion has peripherally disposed sloping platform face, and sloping platform
Face is in downward closing.
Compared with prior art, the beneficial effects of the present invention are: the present apparatus passes through in this fine and closely woven strainer of tower body internal upper part
Raw material is screened respectively in fill process and during discharging with thick intercept net and by the setting of enhancing tube, it is real
Existing solid-liquid separation effect, facilitates the classification work in later period.
Detailed description of the invention
Fig. 1 is the structural diagram of the present invention.
Fig. 2 is the cross-sectional view of enhancing tube in the present invention.
Fig. 3 is the front view of agitator disk in the present invention.
Fig. 4 is the schematic diagram of control system in the present invention.
1- tower body in figure, 11- mother tube, 12- liquid extraction pipe, the fine and closely woven strainer of 13-, the thick intercept net of 14-, 15- sundries chamber,
16- impurities removal door, 2- extraction chamber, 21- sloping platform face, 22- outlet tube, 3- pedestal, 4- enhancing tube, 41- promote motor, and 42- promotes axis,
43- helical blade, 44- bearing block, 5- stirring motor, 51- agitating shaft, 52- agitator disk, 53- turbulator rod.
Specific embodiment
Following will be combined with the drawings in the embodiments of the present invention, and technical solution in the embodiment of the present invention carries out clear, complete
Site preparation description, it is clear that described embodiments are only a part of the embodiments of the present invention, instead of all the embodiments.It is based on
Embodiment in the present invention, it is obtained by those of ordinary skill in the art without making creative efforts every other
Embodiment shall fall within the protection scope of the present invention.
In the description of the present invention, it should be noted that term " center ", "upper", "lower", "left", "right" "vertical",
The orientation or positional relationship of the instructions such as "horizontal", "inner", "outside" be based on the orientation or positional relationship shown in the drawings, merely to
Convenient for description the present invention and simplify description, rather than the device or element of indication or suggestion meaning must have a particular orientation,
It is constructed and operated in a specific orientation, therefore is not considered as limiting the invention.In addition, term " first ", " second ",
" third " is used for descriptive purposes only and cannot be understood as indicating or suggesting relative importance.
In the description of the present invention, it should be noted that unless otherwise clearly defined and limited, term " installation ", " phase
Even ", " connection " shall be understood in a broad sense, for example, it may be being fixedly connected, may be a detachable connection, or be integrally connected；It can
To be mechanical connection, it is also possible to be electrically connected；It can be directly connected, can also can be indirectly connected through an intermediary
Connection inside two elements.For the ordinary skill in the art, above-mentioned term can be understood at this with concrete condition
Concrete meaning in invention.
Embodiment 1:
Please refer to Fig. 1-3, a kind of segregative alkaloid extraction equipment of solid-liquid, including tower body 1, the 1 two sides top of tower body
It is fitted with the mother tube 11 and liquid extraction pipe 12 protruded into inside tower body 1 respectively, is extraction chamber 2 inside the tower body 1, in extraction chamber
Stirring structure is equipped in 2, the stirring structure includes agitator disk 52, the agitator disk 52 be in vertically arranged disk, and
52 side of agitator disk is equipped with multiple turbulator rods 53 being distributed uniformly and circumferentially, and the agitator disk 52 is by agitating shaft 51 and admittedly
It is scheduled on stirring motor 5 on 1 outer wall of tower body to be sequentially connected, when raw material and extract liquor enter extraction by mother tube 11 and liquid extraction pipe 12
When taking in chamber 2, drives agitator disk 52 to be rotated by stirring motor 5, work is stirred to mixture by turbulator rod 53,
Mixture is made to obtain irregular mixing effect by agitator disk 52 and turbulator rod 53 its own shape and structure, to guarantee to mix
Uniformity improves effect of extracting；
Specifically, extracting later separation of solid and liquid for convenience, 1 internal upper part of tower body is equipped with to be docked with the sealing of 1 inner wall of tower body
Fine and closely woven strainer 13 and thick intercept net 14, be sundries chamber 15,11 He of mother tube between fine and closely woven strainer 13 and thick intercept net 14
The nozzle of the one end in tower body 1 of liquid extraction pipe 12 is located in sundries chamber 15, and is equipped in tower body 1 and runs through fine and closely woven 13 He of strainer
The enhancing tube 4 of thick intercept net 14, there are gaps between 4 lower end of enhancing tube and 1 inner bottom surface of tower body, are equipped in enhancing tube 4
Promoted axis 42, and promoted axis 42 on be equipped with helical blade 43, promotions 42 upper end of axis be fixed on 1 center of top of tower body
Motor 41 is promoted to be sequentially connected；When promoting the rotation of motor 4, promotes axis 42 and rotate synchronously, enabled to by helical blade 43
The solid component of 4 lower part of enhancing tube moves up；When carrying out extraction work, raw material and extract liquor are made by stirring structure first
It carries out standing after being sufficiently mixed and completes precipitating, starting promotes motor 41 after the completion of precipitating, so that the solid component sunk to the bottom is to moving up
It is dynamic to be exported from 4 top of enhancing tube, and fine and closely woven filter is then passed through by the liquid component that fine and closely woven strainer 13 is intercepted, and is obtained by extraction
Net 13 and thick intercept net 14 flow back downwards, complete solid-liquid separation effect；2 bottom of extraction chamber is connected with outlet tube 22, out liquid
The discharge of liquid phase after pipe 22 is used to extract.
In order to guarantee the stability in lifting process, pedestal 3 is equipped with below tower body 1,42 lower end of promotion axis is protruded into
It is rotatablely connected in pedestal 3 and with the bearing block 44 being fixed in pedestal 3, is trembled to avoid promote axis 42 during rotation
It is dynamic.
Impurities removal door 16 is also provided on 1 side wall of tower body, the impurities removal door 16 is located at same level with sundries chamber 15
On, for carrying out discharge work to the Solid raw materials in fine and closely woven strainer 13 and thick intercept net 14.
The present apparatus also has control system, and control system is for controlling the working condition of each device, the control
System includes controller, and the controller is the PLC of S7-200CN model, and controller has time control module and Weight control
Module, the Weight control module are connect with time control module signal, and the Weight control module is connected with weight induction device,
Weight induction device is located on fine and closely woven strainer 13 and thick intercept net 14, by weight induction device come to fine and closely woven strainer 13 and thick intercept net
14 weight is detected, and weight information is fed back operator is facilitated to carry out cleaning work to Solid raw materials；When described
Between control module there is stirring motor driving circuit and promote motor-drive circuit, electricity is stirred by setting time parameter
Machine 5 and working time and the operating interval for promoting motor 41, to control different extraction situations, simultaneously also
Time control module can be controlled by Weight control module, when the received weight information of weight induction device in lifting process
When being not up to setting value always, time control module can be cancelled by Weight control module for promoting motor-drive circuit work
The setting for making the time, until being separated by solid-liquid separation quality until meeting.
Embodiment 2:
The difference from embodiment 1 is that in order to faster carry out the mask work of solid-liquid, 2 bottom of extraction chamber has circumferentially
The sloping platform face 21 of direction setting, and sloping platform face 21 is in downward closing, so that solid phase material is during staticly settling to mentioning
It rises 4 bottom of cylinder to collect, so that convenient can enter inside enhancing tube 4 faster during being lifted up.
It is obvious to a person skilled in the art that invention is not limited to the details of the above exemplary embodiments, Er Qie
In the case where without departing substantially from spirit or essential attributes of the invention, the present invention can be realized in other specific forms.Therefore, no matter
From the point of view of which point, the present embodiments are to be considered as illustrative and not restrictive, and the scope of the present invention is by appended power
Benefit requires rather than above description limits, it is intended that all by what is fallen within the meaning and scope of the equivalent elements of the claims
Variation is included within the present invention.Any reference signs in the claims should not be construed as limiting the involved claims.
In addition, it should be understood that although this specification is described in terms of embodiments, but not each embodiment is only wrapped
Containing an independent technical solution, this description of the specification is merely for the sake of clarity, and those skilled in the art should
It considers the specification as a whole, the technical solutions in the various embodiments may also be suitably combined, forms those skilled in the art
The other embodiments being understood that.
Claims (7)
1. a kind of segregative alkaloid extraction equipment of solid-liquid, including tower body (1) and control system, tower body (1) two sides
Top is fitted with respectively protrudes into tower body (1) internal mother tube (11) and liquid extraction pipe (12), is extraction inside the tower body (1)
Chamber (2) is equipped with stirring structure in extraction chamber (2)；It is characterized in that, tower body (1) internal upper part is equipped with and tower body (1) inner wall
The fine and closely woven strainer (13) and thick intercept net (14) for sealing docking are sundries chamber between fine and closely woven strainer (13) and thick intercept net (14)
(15), the nozzle of the mother tube (11) and liquid extraction pipe (12) in tower body (1) interior one end is located in sundries chamber (15), and
The enhancing tube (4) through fine and closely woven strainer (13) and thick intercept net (14), enhancing tube (4) lower end and tower are equipped in tower body (1)
There are gaps between body (1) inner bottom surface, are equipped in enhancing tube (4) and promote axis (42), and spiral is equipped on promoting axis (42)
Blade (43), promotion motor (41) transmission connection for promoting axis (42) upper end and being fixed on tower body (1) center of top；It is described
Extraction chamber (2) bottom is connected with outlet tube (22).
2. the segregative alkaloid extraction equipment of a kind of solid-liquid according to claim 1, which is characterized in that the stirring knot
Structure includes agitator disk (52), the agitator disk (52) be in vertically arranged disk, and agitator disk (52) side be equipped with it is multiple
The turbulator rod (53) being distributed uniformly and circumferentially, the agitator disk (52) is by agitating shaft (51) and is fixed on tower body (1) outside
Stirring motor (5) transmission connection on wall.
3. the segregative alkaloid extraction equipment of a kind of solid-liquid according to claim 1 or 2, which is characterized in that the tower
Pedestal (3) are equipped with below body (1), it is described promoted axis (42) lower end protrude into pedestal (3) and with the bearing that is fixed in pedestal (3)
Seat (44) rotation connection.
4. the segregative alkaloid extraction equipment of a kind of solid-liquid according to claim 1 or 2, which is characterized in that the tower
It is also provided with impurities removal door (16) on body (1) side wall, the impurities removal door (16) and sundries chamber (15) are located in same level.
5. the segregative alkaloid extraction equipment of a kind of solid-liquid according to claim 2, it is characterised in that the extraction chamber
(2) bottom has peripherally disposed sloping platform face (21), and sloping platform face (21) are in downward closing.
6. the segregative alkaloid extraction equipment of a kind of solid-liquid according to claim 1, which is characterized in that the control system
System includes controller, and controller has time control module and Weight control module, and the Weight control module and time control
Module by signal connection, the Weight control module are connected with weight induction device, and weight induction device is located at fine and closely woven strainer (13) and slightly
In intercept net (14)；The time control module has stirring motor driving circuit and promotes motor-drive circuit.
7. the segregative alkaloid extraction equipment of a kind of solid-liquid according to claim 6, which is characterized in that the controller
For the PLC of S7-200CN model.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811420504.3A CN109381889A (en) | 2018-11-26 | 2018-11-26 | A kind of segregative alkaloid extraction equipment of solid-liquid |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811420504.3A CN109381889A (en) | 2018-11-26 | 2018-11-26 | A kind of segregative alkaloid extraction equipment of solid-liquid |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN109381889A true CN109381889A (en) | 2019-02-26 |
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ID=65429703
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201811420504.3A Withdrawn CN109381889A (en) | 2018-11-26 | 2018-11-26 | A kind of segregative alkaloid extraction equipment of solid-liquid |
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Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB2255916A (en) * | 1990-11-29 | 1992-11-25 | Terukatsu Miyauchi | Method of and device for counter-flow separation of mixture |
| CN204619883U (en) * | 2015-04-17 | 2015-09-09 | 江苏金达沥青有限公司 | A kind of asphalt mixing device |
| CN206435179U (en) * | 2016-12-08 | 2017-08-25 | 福建省梦娇兰日用化学品有限公司 | The convenient deimpurity reactor of filter of one kind |
| CN207237409U (en) * | 2017-08-31 | 2018-04-17 | 新乡市巨能合成材料有限公司 | A kind of Chemical Manufacture equipment for separating liquid from solid |
| CN207575840U (en) * | 2017-11-06 | 2018-07-06 | 云南养瑞科技集团有限公司 | A kind of alkaloid extraction equipment |
| CN108675475A (en) * | 2018-06-11 | 2018-10-19 | 滨海金海立医药化工有限公司 | A kind of cyclopropyl carboxylic acid synthesis sewage-treatment plant |
-
2018
- 2018-11-26 CN CN201811420504.3A patent/CN109381889A/en not_active Withdrawn
Patent Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB2255916A (en) * | 1990-11-29 | 1992-11-25 | Terukatsu Miyauchi | Method of and device for counter-flow separation of mixture |
| CN204619883U (en) * | 2015-04-17 | 2015-09-09 | 江苏金达沥青有限公司 | A kind of asphalt mixing device |
| CN206435179U (en) * | 2016-12-08 | 2017-08-25 | 福建省梦娇兰日用化学品有限公司 | The convenient deimpurity reactor of filter of one kind |
| CN207237409U (en) * | 2017-08-31 | 2018-04-17 | 新乡市巨能合成材料有限公司 | A kind of Chemical Manufacture equipment for separating liquid from solid |
| CN207575840U (en) * | 2017-11-06 | 2018-07-06 | 云南养瑞科技集团有限公司 | A kind of alkaloid extraction equipment |
| CN108675475A (en) * | 2018-06-11 | 2018-10-19 | 滨海金海立医药化工有限公司 | A kind of cyclopropyl carboxylic acid synthesis sewage-treatment plant |
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Application publication date: 20190226 |