CN109378682A - A kind of device generating novel substance using laser bombardment target - Google Patents

A kind of device generating novel substance using laser bombardment target Download PDF

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Publication number
CN109378682A
CN109378682A CN201811372958.8A CN201811372958A CN109378682A CN 109378682 A CN109378682 A CN 109378682A CN 201811372958 A CN201811372958 A CN 201811372958A CN 109378682 A CN109378682 A CN 109378682A
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Prior art keywords
substance
target
laser
detecting chamber
supersonic nozzle
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CN201811372958.8A
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CN109378682B (en
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刘万发
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Dalian Institute of Chemical Physics of CAS
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Dalian Institute of Chemical Physics of CAS
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    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01SDEVICES USING THE PROCESS OF LIGHT AMPLIFICATION BY STIMULATED EMISSION OF RADIATION [LASER] TO AMPLIFY OR GENERATE LIGHT; DEVICES USING STIMULATED EMISSION OF ELECTROMAGNETIC RADIATION IN WAVE RANGES OTHER THAN OPTICAL
    • H01S3/00Lasers, i.e. devices using stimulated emission of electromagnetic radiation in the infrared, visible or ultraviolet wave range
    • H01S3/0007Applications not otherwise provided for
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25BREFRIGERATION MACHINES, PLANTS OR SYSTEMS; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS
    • F25B19/00Machines, plants or systems, using evaporation of a refrigerant but without recovery of the vapour
    • F25B19/02Machines, plants or systems, using evaporation of a refrigerant but without recovery of the vapour using fluid jet, e.g. of steam

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  • Physics & Mathematics (AREA)
  • Engineering & Computer Science (AREA)
  • Electromagnetism (AREA)
  • Plasma & Fusion (AREA)
  • Mechanical Engineering (AREA)
  • Thermal Sciences (AREA)
  • General Engineering & Computer Science (AREA)
  • Chemical & Material Sciences (AREA)
  • Combustion & Propulsion (AREA)
  • Optics & Photonics (AREA)
  • Investigating Or Analyzing Materials By The Use Of Ultrasonic Waves (AREA)
  • Physical Or Chemical Processes And Apparatus (AREA)

Abstract

It is a kind of using laser bombardment target generate novel substance device belong to laser application technique field, including laser condensing lens, target room, supersonic nozzle, substance detecting chamber.Target room one end is equipped with quartz window, is equipped with admission line at quartz window.Target indoor location placement platform is equipped with target on placement platform.It is equipped with sampling pipe close near supersonic nozzle outlet port in substance detecting chamber, the substance detecting chamber other end is provided with pump-line and pressure gauge.Vacuum pump is first turned on when work, buffer gas is passed through target room by admission line, and uses the air pressure of pressure gauge monitoring substance detecting chamber.It is then turned on laser, bombards target by laser condensing lens, the substance for bombarding generation flows to substance detecting chamber by supersonic nozzle with buffer gas.The substance finally generated enters substance testing instrument by sampling pipe, measures to the property for generating substance.The present invention has many advantages, such as that compact-sized, device is succinct, easy to use.

Description

A kind of device generating novel substance using laser bombardment target
Technical field
The invention belongs to laser application technique fields, generate new object using laser bombardment target more particularly, to a kind of The device of matter.
Background technique
From being born from laser, the interaction of laser and substance is become for a unfailing hot research neck Domain, and the research of new material and novel substance is one of the basic research field for having significant impact to engineering technology progress.It generates New material or substance can be realized by multiple technologies, generate novel substance using superlaser bombardment target, have and use Flexibly, the advantages that process is succinct, repeatability is strong, mass production capabilities are good, right and wrong are often with one of promising technological approaches.Example Such as, in field of catalytic chemistry, certain targets are bombarded using superlaser, can produce some macromolecular complex of large specific surface area Matter has particularly good catalytic performance, can be used for the efficient production of certain industrial products.
Superlaser effect can generate a large amount of heat with target, make the substance steep temperature rise of target and generation.If ring The chemical activity of border gas is stronger, such as there are oxygen, then the substance generated can be made to chemically react with environmental gas.For Avoid the generation of chemical reaction, it is common practice to use the inert gas as protective gas.Furthermore pass through laser bombardment target The temperature for the substance that material generates is usually higher, it usually needs first cools down to it, then could measure to its property. All the substance of generation is cooled down using the method based on heat transfer at present, cooling time is longer, and cooling effect is poor.
Summary of the invention
In view of the drawbacks of the prior art, the present invention provides a kind of device that novel substance is generated using laser bombardment target.
The technical solution adopted by the present invention are as follows:
A kind of device generating novel substance using laser bombardment target, including laser condensing lens, target room, supersonic speed spray Pipe, substance detecting chamber.Described target room one end is equipped with quartz window, and laser condensing lens are equipped with below quartz window, and Admission line is provided near quartz window;The target room other end is connected to by supersonic nozzle with substance detecting chamber.It is described Target chamber interior placement platform is installed, target is housed on placement platform.The close ultrasound in one end in the substance detecting chamber Fast nozzle exit position is nearby provided with sampling pipe, and sampling pipe is connect with substance testing instrument;The substance detecting chamber other end It is provided with pump-line and pressure gauge, pump-line is controlled to a vacuum pump.
Vacuum pump is first turned on when work, and buffer gas is passed through target room by admission line, and use pressure gauge Monitor the air pressure of substance detecting chamber.It is then turned on laser, target is bombarded by laser condensing lens, bombards the substance of generation with buffering Gas flows to substance detecting chamber by supersonic nozzle.The substance finally generated enters substance testing instrument by sampling pipe Device measures the property for generating substance.
Further, a kind of device being generated novel substance using laser bombardment target, design protection gas are entered Position of the mouth relative to quartz window, enables protective gas to protect pollution caused by substance of the quartz window from generation.
Further, a kind of device generating novel substance using laser bombardment target, designs supersonic nozzle, The buffering gas for carrying the substance generated is set to realize several Mach number flow velocitys, to reduce the temperature of the substance generated.The ultrasound Fast jet pipe 10 uses Laval nozzle structure.
Further, a kind of device generating novel substance using laser bombardment target, can be used a variety of objects Matter detection instrument measures the substance of generation.
Further, a kind of device generating novel substance using laser bombardment target, buffer gas useization The inactive inert gas of property is learned, the substance of generation is under the high temperature conditions, more active with the chemical property such as ambient oxygen Gas reacts.
While the substance that the device is generated using inert gas shielding, it is quickly cooled down and is generated using supersonic nozzle technology Substance, have many advantages, such as that compact-sized, device is succinct, easy to use.
Detailed description of the invention
Fig. 1 is a kind of structural representation of device that novel substance is generated using laser bombardment target provided in an embodiment of the present invention Figure.
In Fig. 1: 1 laser;2 laser condensing lens;3 quartz windows;4 admission lines;5 target rooms;6 placement platforms;7 probe tubes Road;8 substance testing instruments;9 targets;10 supersonic nozzles;11 pressure gauges;12- substance detecting chamber;13 pump-lines;14 vacuum Pump.
Specific embodiment
In order to make the objectives, technical solutions, and advantages of the present invention clearer, with reference to the accompanying drawings and embodiments, right The present invention is further elaborated.It should be appreciated that the specific embodiments described herein are merely illustrative of the present invention, and It is not used in the restriction present invention.
The present invention provides a kind of devices that novel substance is generated using laser bombardment target.Fig. 1 shows implementation of the present invention A kind of structure for device that novel substance is generated using laser bombardment target that example provides is illustrated only and this for ease of description The relevant part of inventive embodiments, details are as follows:
A kind of device generating novel substance using laser bombardment target, laser condensing lens 2, the target for being 1000mm including focal length Material room 5, supersonic nozzle 10, substance detecting chamber 12.5 one end of target room is equipped with quartz window 3, and attached in quartz window 3 It is closely provided with admission line 4,3 side of quartz window is equipped with laser condensing lens 2.Placement platform 6 is installed in 5 chamber interior of target, Target 9 is housed, target 9 is carbon on placement platform.Near the position exported in substance detecting chamber 12 close to supersonic nozzle 10 It is provided with sampling pipe 7, sampling pipe 7 connects substance test equipment 8.12 other end of substance detecting chamber is provided with pump-line 13 and pressure gauge 11, pump-line 13 connect with vacuum pump 14.In embodiment, supersonic nozzle 10 uses Laval nozzle knot Structure.
Use He gas as buffer gas, when work first turns on vacuum pump 14, and buffer gas is passed through admission line 4 It is passed through target room 5, and monitors the air pressure of substance detecting chamber 12 using pressure gauge 11.Adjust the ginseng of admission line 4 and vacuum pump 14 It counts, the buffer gas in the supersonic nozzle made realizes the flowing of 2 or more Mach numbers, and temperature drops to 180K or so, realizes fast The purpose for the substance that quickly cooling but generates.
Carbon target is bombarded by laser condensing lens 2 using 10kW oxygen-iodine laser (COIL) when work, the substance of generation passes through Supersonic nozzle 10 is quickly cooled to 180K or so, and the substance into substance detecting chamber 12 enters substance survey by sampling pipe 7 Test instrument 8, in the present embodiment, substance testing instrument 8 measures its charge-mass ratio using time of-flight mass spectrometer, determines and generates Substance be C60.
As it will be easily appreciated by one skilled in the art that the foregoing is merely illustrative of the preferred embodiments of the present invention, not to The limitation present invention, any modifications, equivalent substitutions and improvements made within the spirit and principles of the present invention should all include Within protection scope of the present invention.

Claims (3)

1. a kind of device for generating novel substance using laser bombardment target, which is characterized in that the device includes that laser focuses Mirror, target room, supersonic nozzle, substance detecting chamber;
Quartz window is installed in described target room one end, sets laser condensing lens below quartz window, and near quartz window Admission line is set;The target room other end is connected to by supersonic nozzle with substance detecting chamber, and supersonic nozzle is for making to carry The buffering gas of the substance of generation realizes several Mach number flow velocitys, reduces the temperature of the substance of generation;The close ultrasound of target chamber interior Placement platform is installed in the position of fast jet pipe, and target is housed on placement platform;Close to supersonic nozzle in the substance detecting chamber The position of outlet is provided with sampling pipe, and sampling pipe is connect with substance testing instrument;The substance detecting chamber other end is provided with pumping Feed channel and pressure gauge, pump-line are controlled to a vacuum pump;
When work, firstly, opening vacuum pump, and buffer gas is passed through target room by admission line, and supervise using pressure gauge Survey the air pressure of substance detecting chamber;Then, laser is opened, and bombards target by laser condensing lens, bombards the substance of generation with slow Qi of chong channel ascending adversely body flows to substance detecting chamber by supersonic nozzle;Finally, the substance generated enters substance testing instrument by sampling pipe Device measures the property for generating substance.
2. a kind of device for generating novel substance using laser bombardment target as described in claim 1, which is characterized in that described Buffer gas is inert gas.
3. a kind of device for generating novel substance using laser bombardment target as claimed in claim 1 or 2, which is characterized in that institute The supersonic nozzle stated uses Laval nozzle structure.
CN201811372958.8A 2018-11-19 2018-11-19 Device for generating new substance by using laser to bombard target material Active CN109378682B (en)

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CN109378682B CN109378682B (en) 2021-08-27

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Cited By (1)

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Publication number Priority date Publication date Assignee Title
CN112448253A (en) * 2019-08-30 2021-03-05 中国科学院大连化学物理研究所 Solid laser gain module cooled by supersonic low-temperature gas and laser

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