CN109370257A - A kind of alkali resistant dispersion gray dye mixture - Google Patents
A kind of alkali resistant dispersion gray dye mixture Download PDFInfo
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- CN109370257A CN109370257A CN201811531997.8A CN201811531997A CN109370257A CN 109370257 A CN109370257 A CN 109370257A CN 201811531997 A CN201811531997 A CN 201811531997A CN 109370257 A CN109370257 A CN 109370257A
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- dye
- dyestuff
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
- C09B67/00—Influencing the physical, e.g. the dyeing or printing properties of dyestuffs without chemical reactions, e.g. by treating with solvents grinding or grinding assistants, coating of pigments or dyes; Process features in the making of dyestuff preparations; Dyestuff preparations of a special physical nature, e.g. tablets, films
- C09B67/0033—Blends of pigments; Mixtured crystals; Solid solutions
- C09B67/0046—Mixtures of two or more azo dyes
- C09B67/0051—Mixtures of two or more azo dyes mixture of two or more monoazo dyes
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/16—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using dispersed, e.g. acetate, dyestuffs
- D06P1/18—Azo dyes
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/16—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using dispersed, e.g. acetate, dyestuffs
- D06P1/19—Nitro dyes
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P3/00—Special processes of dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form, classified according to the material treated
- D06P3/34—Material containing ester groups
- D06P3/52—Polyesters
- D06P3/54—Polyesters using dispersed dyestuffs
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- Chemical & Material Sciences (AREA)
- Dispersion Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Textile Engineering (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Chemistry (AREA)
- Coloring (AREA)
Abstract
A kind of alkali resistant dispersion gray dye mixture, it is made of dyestuff and the mixing of auxiliary agent two parts, it is characterized by: dye moiety contains medium temperature type dye and low temperature type dye, medium temperature type dye contains medium temperature indigo plant dyestuff, medium temperature yellow dye and medium temperature red dye, and low temperature type dye contains low temperature indigo plant dyestuff, low temperature yellow dye and low temperature red dye.Dispersion gray dye mixture of the invention has good alkali resistance, and then pre-treatment desizing workshop section can be merged with dyeing workshop section, realizes the new process of desizing dyeing one-bath one-step dyeing, plays the effect of good energy-saving and emission-reduction;Meanwhile dispersion gray dye mixture of the invention has good washing fastness and sublimation reliability, and it is good and cheap, guide the application idea of user's optimization of enterprises dyestuff.
Description
Technical field
The present invention devises a kind of alkali resistant dispersion gray dye mixture, in particular to a kind of to be suitable for polyester fiber or face
The dyeing of the Oxford gray of material is belonged to using the dye mixtures such as the disperse blue of the alkali resistance of low form and middle warm type, Huang, red
Application technical field.
Background technique
In order to deepen the energy-saving and emission-reduction of dyeing and finishing industry, realize that desizing pre-treatment and dyeing course are merged into one-bath one-step dyeing
Dyeing, it is necessary to carry out the optimum organization of alkali resistance dyestuff, the dyeing time could be saved, reduce energy consumption, few blowdown
Water.
The conventional use of C.I. Disperse Blue-79 in dyeing and finishing field, C.I. Red 167, the combination of C.I. disperse orange 30 are one at present
Play dyeing, it is necessary to adjust acidity pH value be 6 hereinafter, could normal dyeing, so dyeing workshop section and pre-treatment desizing workshop section
PH value 8-11 does not match that front and back cannot merge synchronization, therefore must be produced with two one-bath two-step process, causes the production time long, is formed
Secondary sewage increases energy consumption.
The content of present invention
The present invention provides a kind of alkali resistant dispersion gray dye mixture, solves existing polyester fiber and fabric in middle depth
When color one-bath dyeing, because dyestuff C.I. Disperse Blue-79, C.I. disperse orange 30, C.I. Red 167 are in preceding processing alkaline condition
Lower color development is abnormal, and is unable to satisfy the problem of pre-treatment desizing is with one-bath one-step dyeing energy-saving and emission-reduction are dyed.Pass through the excellent of dyestuff
Change combination, has selected the dyestuff of one group of low temperature and middle warm type to arrange in pairs or groups mutually, had adjusted the level-dyeing property of dyestuff, obtained matching well
Wu Xing realizes the new process of desizing dyeing one-bath one-step dyeing, plays the effect of good energy-saving and emission-reduction.
In order to achieve the above objectives, the technical solution adopted by the present invention is that: a kind of alkali resistant dispersion gray dye mixture, by contaminating
Material and auxiliary agent two parts mixing composition, the dye moiety contain medium temperature type dye and low temperature type dye, the medium temperature type dye
Containing medium temperature indigo plant dyestuff, medium temperature yellow dye and medium temperature red dye, the low temperature type dye contains low temperature indigo plant dyestuff, low temperature xanthochromia
Material and low temperature red dye;
The medium temperature indigo plant dyestuff is the dyestuff for meeting following chemical structural formula (I),
Wherein, n=1~15, R1For any one in the alkyl or alkoxy of H, OH, halogen group and C1~C4, R2
For any one in the alkyl or alkoxy of H, OH, halogen group and C1~C4, R3For the alkyl or alkoxy of C1~C4
And any one in benzyl, R4For alkyl or alkoxy, benzyl, the CH of OH, C1~43(CO) appointing in O and CN group
It anticipates one kind;
The medium temperature yellow dye is to meet the following chemical structure formula (II) and/or (II ') and chemical structural formula (III)
Dyestuff,
Wherein:
R5Selected from any one of hydrogen, methyl, the alkoxy of C1~C4, methoxyethoxy and ethoxyethoxy;
R6Selected from any one of hydrogen, methyl, chlorine and acetylamino;
R7Selected from any one of hydrogen, methyl and chlorine;
R8Selected from any one of hydrogen, methoxyl group and chlorine;
R9And R10Be selected from amino orAnd R9With R10It is different;
Wherein, X is H or Br, and Z is the alkyl or benzyl of C1~C4;
The medium temperature red dye contains C.I. disperse red 73, C.I. Red-1 200 45, C.I. Red-1 200 52, C.I. disperse red
At least one of the dyestuff of 153 and C.I. Disperse Red 343;
The low temperature indigo plant dyestuff contains at least one of C.I. disperse blue 14, dyestuff of C.I. Disperse Blue-56;
The low temperature yellow dye contains C.I. disperse yellow 54, C.I. dispersion yellow 64, C.I. disperse yellow 67, C.I. disperse yellow
143, C.I. disperse Yellow 160 150 and meet at least one of the dyestuff of chemical structural formula (IV);
The low temperature red dye contains in the dyestuff of C.I. disperse red 60, C.I. disperse red 92 and C.I. Red-1 200 46
At least one.
Related content in above-mentioned technical proposal is explained as follows:
1, in above scheme, the medium temperature indigo plant dyestuff of the formula (I) at least contains one of following 4 kinds of structures:
2, in above scheme, the medium temperature yellow dye of the formula (II) at least contains one of following 5 kinds of structures combination, every kind of group
Conjunction is a pair of of position isomer that reaction generates:
3, in above scheme, the weight percentage of the pure dye of the following structural of the dye moiety are as follows: in described
The formula (I) 2~90% of warm indigo plant dyestuff, formula (II) and/or (II ') 1~50% in the medium temperature yellow dye, the medium temperature xanthochromia
Formula (III) 1~50% in material, the medium temperature red dye 1~40%, the low temperature indigo plant dyestuff 1~80%, the low temperature xanthochromia
Material 0.5~20%, the low temperature red dye 1~80%.
4, in above scheme, the weight percentage of the pure dye of the following structural of the dye moiety are as follows: in described
Warm indigo plant dyestuff formula (I) 5~70%, formula (II) and/or (II ') 2~30% in the medium temperature yellow dye, the medium temperature yellow dye
In formula (III) 2~30%, the medium temperature red dye 2~30%, the low temperature indigo plant dyestuff 2~50%, the low temperature yellow dye
0.5~20%, the low temperature red dye 2~50%.
5, in above scheme, the auxiliary agent includes the auxiliary agents such as diffusant and dispersing agent, and diffusant selects MF or/and NNO, point
Powder selects sodium lignin sulfonate class, and the dosage of the auxiliary agents such as diffusant and dispersing agent is remaining after deducting dye moiety total weight
Amount.
6, in above scheme, the low temperature indigo plant dyestuff can also be suitably added in C.I. disperse violet 27 and C.I. disperse violet 28
At least one.
7, in above scheme, in the dyestuff of the formula (I), when n is 1, R1For H or methyl, R2For H, R3For methyl or second
Base, then formula (I) represents Penglai Huamao Fine Chemical Industry Co., Ltd's dye product, patent document CN1227299C;Other situations
Represent Yantai Aotu Composite Materials Co., Ltd.'s dye product, patent document CN105907126B.
8, in above scheme, the dyestuff of the formula (II) represents the production of Peng Lai Jia Xin dye chemical industry limited liability company dyestuff
Product, patent document CN108276304A.
9, in above scheme, in the dyestuff of the formula (III), commercial dye can be used when X is H, and Z is ethyl
C.I. disperse orange 25;X is Br, and Z be ethyl when commercial dye C.I. disperse orange 61 can be used;X is H, and Z be benzyl when can adopt
With orange 288 commercial dyes of Home-Made Disperse.
10, in above scheme, all of above dyestuff is commercially available or is prepared with existing known technology.
11, in above scheme, the C.I. on dyestuff title head is English Color Index abbreviation, i.e. Colour Index, is indicated
Dyestuff common name dyes association of family (Society of Dyers and Colorists by Britain;SDC) chemical with U.S. textile
Family and dyeing association of family (American Association of Textile Chemists and Colorists;AATCC)
Establishment.
12, in above scheme, " dye moiety " refers to the substance of pure dye in dye mixture of the invention, does not wrap
Include Aid Portions.It is well known that being needed during the former dyestuff of synthetic disperse dyes is processed into commodity disperse dyes
A large amount of auxiliary agent is added, such as dispersing agent (Anyang produces sodium lignin sulfonate B and import sodium lignin sulfonate 85A), diffusant (expand
Powder MF and NNO) and a small amount of dust-proofing agent (dust-proofing agent JH2112).Obviously, in each dye of the dye mixture of aforementioned present invention
Between material on the basis of usage ratio, the product that addition auxiliary agent dilutes is still within protection of the invention.
13, in above scheme, the percentage composition of " dye moiety ", which refers to, removes the pure dye dry product except auxiliary agent
Percentage composition.And general industry formula is using former dyestuff dry product metering.Contain a certain amount of impurity in former dyestuff dry product, it can be with
It is scaled pure dye dosage by measurement, but often former dyestuff dry product content approximation can also be replaced pure dye dry product content.
Former dyestuff dry product can be converted to as the former dyestuff wet cake being synthesized to measure.Some commercial formulations are also with containing a large amount of
The standard sample (such as standard sample of staining power 100% or 200%) of certain trade mark commodity disperse dyes of auxiliary agent is used as base
Standard indicates content, which can also be scaled pure dye dry product content.
14, in above scheme, the dye moiety can also contain minute quantity to other a small amount of not alkaline-resisting middle warm types
Dyestuff and/or low temperature type dye and/or high temperature type dye.The basis of all necessary components contained in technical solution of the present invention
On, then a small amount of high temperature type dye or other not alkaline-resisting medium temperature type dyes or low temperature type dye are added, it is all according to the present invention
Equivalent change or modification made by Spirit Essence.
Design feature of the invention and the utility model has the advantages that the present invention has selected one group of low temperature by the optimum organization of dyestuff
It arranges in pairs or groups mutually with the dyestuff of middle warm type, in dosage based on medium temperature type dye, supplemented by low temperature type dye.This is because of the invention
Alkali resistance medium temperature type dye outstanding is selected, but in order to guarantee that coloured light reaches the requirement of grey, while having guaranteed dyestuff mixing again
The washing fastness and sublimation reliability of object are good, and the present invention has selected the level dyeing of a part of low temperature type dye adjusting dye mixture again
Property.
In short, dispersion gray dye mixture of the invention has good alkali resistance, and then can be by pre-treatment desizing work
Section merges with dyeing workshop section, realizes the new process of desizing dyeing one-bath one-step dyeing, plays the effect of good energy-saving and emission-reduction;
Meanwhile dispersion gray dye mixture of the invention has good washing fastness and sublimation reliability, good and cheap, guidance user enterprise
The application idea of industry optimization dyestuff.
The present invention will be further described below with reference to examples:
A kind of embodiment 1: alkali resistant dispersion gray dye mixture and preparation method thereof
1, it is formulated
The dosage of the above commercial goods dyestuff, if being scaled pure dye, it is known that meet inventive formulation range just.On
Stating dispersing agent can choose Anyang production sodium lignin sulfonate B, and above-mentioned diffusant can choose MF, and above-mentioned dust-proofing agent can choose
JH2112。
2, prepared by dye mixture
By formula weighing stock, puts into blender and be mixed, until stirring evenly, then spray into a small amount of dust-proofing agent again
JH2112 carries out dust-proof processing, finally carries out being packaged to be finished product.
A kind of embodiment 2: alkali resistant dispersion gray dye mixture and preparation method thereof
1, it is formulated
The dosage of the above commercial goods dyestuff, if being scaled pure dye, it is known that meet inventive formulation range just.On
Stating dispersing agent can choose Anyang production sodium lignin sulfonate B, and above-mentioned diffusant can choose MF, and above-mentioned dust-proofing agent can choose
JH2112。
2, prepared by dye mixture, with embodiment 1.
A kind of embodiment 3: alkali resistant dispersion gray dye mixture and preparation method thereof
1, it is formulated
The dosage of the above commercial goods dyestuff, if being scaled pure dye, it is known that meet inventive formulation range just.On
Stating dispersing agent can choose Anyang production sodium lignin sulfonate B, and above-mentioned diffusant can choose MF, and above-mentioned dust-proofing agent can choose
JH2112。
2, prepared by dye mixture, with embodiment 1.
A kind of embodiment 4: alkali resistant dispersion gray dye mixture and preparation method thereof
1, it is formulated
The dosage of the above commercial goods dyestuff, if being scaled pure dye, it is known that meet inventive formulation range just.On
Stating dispersing agent can choose Anyang production sodium lignin sulfonate B, and above-mentioned diffusant can choose MF, and above-mentioned dust-proofing agent can choose
JH2112。
2, prepared by dye mixture, with embodiment 1.
A kind of embodiment 5: alkali resistant dispersion gray dye mixture and preparation method thereof
1, it is formulated
The dosage of the above commercial goods dyestuff, if being scaled pure dye, it is known that meet inventive formulation range just.On
Stating dispersing agent can choose Anyang production sodium lignin sulfonate B, and above-mentioned diffusant can choose MF, and above-mentioned dust-proofing agent can choose
JH2112。
2, prepared by dye mixture, with embodiment 1.
Disperse dyes made from 1~embodiment of embodiment 5 are contaminated to the looped fabric of different materials with 130 DEG C of high temperature and high pressure methods,
Dyeing concentration is 1~2%, and then adopt international standards IS0105-C10, IS0105-X11 test its water-fastness, resistance to distillation respectively
Color fastness is specifically shown in Table 1:
Table 1
From sublimation reliability one of table 1 as can be seen that after conventional disperse ash dyeing cloth specimen staining it is more, and embodiment 1
Cloth specimen staining is few after~5 dyeings.
Disperse dyes made from Examples 1 to 5 and conventional disperse ash dyestuff are contaminated into knitting under conditions of 5 or more pH value again
Cloth, dyeing concentration 2%, dye sample carries out the detection of dyeability, specific as shown in table 2:
In table 2, conventional disperse ash dyestuff can occur to lack blue phenomenon when pH value is greater than 6, and Examples 1 to 5 dyestuff exists
PH value is likely to occur to lack blue phenomenon when being greater than 9.
The above embodiments merely illustrate the technical concept and features of the present invention, and its object is to allow person skilled in the art
Scholar cans understand the content of the present invention and implement it accordingly, and it is not intended to limit the scope of the present invention.It is all according to the present invention
Equivalent change or modification made by Spirit Essence, should be covered by the protection scope of the present invention.
Claims (7)
1. a kind of alkali resistant dispersion gray dye mixture is made of, it is characterised in that: the dye dyestuff and the mixing of auxiliary agent two parts
Material part contain medium temperature type dye and low temperature type dye, the medium temperature type dye contain medium temperature indigo plant dyestuff, medium temperature yellow dye and
Medium temperature red dye, the low temperature type dye contain low temperature indigo plant dyestuff, low temperature yellow dye and low temperature red dye;
The medium temperature indigo plant dyestuff is the dyestuff for meeting following chemical structural formula (I),
Wherein, n=1~15, R1For any one in the alkyl or alkoxy of H, OH, halogen group and C1~C4, R2For H,
OH, the alkyl of halogen group and C1~C4 or any one in alkoxy, R3For C1~C4 alkyl or alkoxy and
Any one in benzyl, R4For alkyl or alkoxy, benzyl, the CH of OH, C1~43(CO) any one in O and CN group
Kind;
The medium temperature yellow dye is the dye for meeting the following chemical structure formula (II) and/or (II ') and chemical structural formula (III)
Material,
Wherein:
R5Selected from any one of hydrogen, methyl, the alkoxy of C1~C4, methoxyethoxy and ethoxyethoxy;
R6Selected from any one of hydrogen, methyl, chlorine and acetylamino;
R7Selected from any one of hydrogen, methyl and chlorine;
R8Selected from any one of hydrogen, methoxyl group and chlorine;
R9And R10Be selected from amino orAnd R9With R10It is different;
Wherein, X is H or Br, and Z is the alkyl or benzyl of C1~C4;
The medium temperature red dye contains C.I. disperse red 73, C.I. Red-1 200 45, C.I. Red-1 200 52, C.I. Red-1 200 53
And at least one of dyestuff of C.I. Disperse Red 343;
The low temperature indigo plant dyestuff contains at least one of C.I. disperse blue 14, dyestuff of C.I. Disperse Blue-56;
The low temperature yellow dye contain C.I. disperse yellow 54, C.I. dispersion yellow 64, C.I. disperse yellow 67, C.I. disperse yellow 143,
C.I. disperse Yellow 160 150 and meet at least one of the dyestuff of chemical structural formula (IV);
The low temperature red dye contains in the dyestuff of C.I. disperse red 60, C.I. disperse red 92 and C.I. Red-1 200 46 extremely
Few one kind.
2. alkali resistant dispersion gray dye mixture according to claim 1, it is characterised in that: the medium temperature of the formula (I) is blue
Dyestuff at least contains one of following 4 kinds of structures:
3. alkali resistant dispersion gray dye mixture according to claim 1, it is characterised in that: the medium temperature of the formula (II) is yellow
Dyestuff at least contains one of following 5 kinds of structures combination, and every kind of combination is a pair of of position isomer that reaction generates:
4. alkali resistant dispersion gray dye mixture according to claim 1, it is characterised in that: the dye moiety it is following
The weight percentage of the pure dye of structural formula are as follows: the formula (I) 2~90% of the medium temperature indigo plant dyestuff, in the medium temperature yellow dye
Formula (II) and/or (II ') 1~50%, the formula (III) 1~50% in the medium temperature yellow dye, the medium temperature red dye 1~
40%, the low temperature indigo plant dyestuff 1~80%, the low temperature yellow dye 0.5~20%, the low temperature red dye 1~80%.
5. alkali resistant dispersion gray dye mixture according to claim 1, it is characterised in that: the dye moiety it is following
The weight percentage of the pure dye of structural formula are as follows: the medium temperature indigo plant dyestuff formula (I) 5~70%, in the medium temperature yellow dye
Formula (II) and/or (II ') 2~30%, the formula (III) 2~30% in the medium temperature yellow dye, the medium temperature red dye 2~
30%, the low temperature indigo plant dyestuff 2~50%, the low temperature yellow dye 0.5~20%, the low temperature red dye 2~50%.
6. alkali resistant dispersion gray dye mixture according to claim 1, it is characterised in that: the auxiliary agent includes diffusant
MF or/and NNO is selected with auxiliary agents, diffusants such as dispersing agents, dispersing agent selects sodium lignin sulfonate class, diffusant and dispersing agent etc.
The dosage of auxiliary agent is the surplus deducted after dye moiety total weight.
7. alkali resistant dispersion gray dye mixture according to claim 1, it is characterised in that: the low temperature indigo plant dyestuff also contains
There are at least one of C.I. disperse violet 27 and C.I. disperse violet 28.
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Cited By (5)
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CN111057395A (en) * | 2019-12-24 | 2020-04-24 | 浙江闰土股份有限公司 | Disperse dye composition, disperse dye, and preparation method and application thereof |
CN111454589A (en) * | 2020-05-12 | 2020-07-28 | 浙江山峪集团股份有限公司 | Disperse yellow dye composition and preparation method thereof |
CN111875983A (en) * | 2020-08-24 | 2020-11-03 | 苏州市吴江区绿洲染料有限公司 | Light fastness improved disperse yellow dye mixture |
CN114892422A (en) * | 2022-04-02 | 2022-08-12 | 福建赛孔雀新材料科技有限公司 | Smokeless or less-smokeless high-strength permeable ink and preparation method thereof |
CN115838538A (en) * | 2022-12-14 | 2023-03-24 | 浙江迪邦化工有限公司 | Disperse orange capable of replacing disperse yellow 54#, and synthesis method and application thereof |
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CN111057395A (en) * | 2019-12-24 | 2020-04-24 | 浙江闰土股份有限公司 | Disperse dye composition, disperse dye, and preparation method and application thereof |
CN111057395B (en) * | 2019-12-24 | 2022-01-07 | 浙江闰土股份有限公司 | Disperse dye composition, disperse dye, and preparation method and application thereof |
CN111454589A (en) * | 2020-05-12 | 2020-07-28 | 浙江山峪集团股份有限公司 | Disperse yellow dye composition and preparation method thereof |
CN111875983A (en) * | 2020-08-24 | 2020-11-03 | 苏州市吴江区绿洲染料有限公司 | Light fastness improved disperse yellow dye mixture |
CN114892422A (en) * | 2022-04-02 | 2022-08-12 | 福建赛孔雀新材料科技有限公司 | Smokeless or less-smokeless high-strength permeable ink and preparation method thereof |
CN114892422B (en) * | 2022-04-02 | 2024-04-30 | 福建赛孔雀新材料科技有限公司 | Smokeless or low-smoke high-strength permeation type ink and preparation method thereof |
CN115838538A (en) * | 2022-12-14 | 2023-03-24 | 浙江迪邦化工有限公司 | Disperse orange capable of replacing disperse yellow 54#, and synthesis method and application thereof |
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