CN109337762A - A kind of preparation method and applications of cigarette alfalfa reactant - Google Patents
A kind of preparation method and applications of cigarette alfalfa reactant Download PDFInfo
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- CN109337762A CN109337762A CN201811214779.1A CN201811214779A CN109337762A CN 109337762 A CN109337762 A CN 109337762A CN 201811214779 A CN201811214779 A CN 201811214779A CN 109337762 A CN109337762 A CN 109337762A
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- alfalfa
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- cigarette
- drying
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- 235000017587 Medicago sativa ssp. sativa Nutrition 0.000 title claims abstract description 78
- 239000000376 reactant Substances 0.000 title claims abstract description 26
- 235000019504 cigarettes Nutrition 0.000 title claims abstract description 24
- 238000002360 preparation method Methods 0.000 title claims abstract description 17
- 241000219823 Medicago Species 0.000 title claims abstract 20
- 238000006243 chemical reaction Methods 0.000 claims abstract description 35
- 238000004108 freeze drying Methods 0.000 claims abstract description 20
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 20
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims abstract description 9
- 229960000935 dehydrated alcohol Drugs 0.000 claims abstract description 9
- 239000000203 mixture Substances 0.000 claims abstract description 8
- 150000001413 amino acids Chemical class 0.000 claims abstract description 7
- 239000000706 filtrate Substances 0.000 claims abstract description 7
- 238000001914 filtration Methods 0.000 claims abstract description 7
- 239000012535 impurity Substances 0.000 claims abstract description 7
- 238000004064 recycling Methods 0.000 claims abstract description 7
- 241000208125 Nicotiana Species 0.000 claims description 10
- 235000002637 Nicotiana tabacum Nutrition 0.000 claims description 10
- 238000002156 mixing Methods 0.000 claims description 9
- 238000000034 method Methods 0.000 claims description 8
- 230000001376 precipitating effect Effects 0.000 claims description 8
- 238000000859 sublimation Methods 0.000 claims description 7
- 230000008022 sublimation Effects 0.000 claims description 7
- DHMQDGOQFOQNFH-UHFFFAOYSA-N Glycine Chemical compound NCC(O)=O DHMQDGOQFOQNFH-UHFFFAOYSA-N 0.000 claims description 6
- 102000018697 Membrane Proteins Human genes 0.000 claims description 6
- 108010052285 Membrane Proteins Proteins 0.000 claims description 6
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 claims description 6
- 238000003756 stirring Methods 0.000 claims description 5
- 239000004471 Glycine Substances 0.000 claims description 3
- MTCFGRXMJLQNBG-UHFFFAOYSA-N Serine Natural products OCC(N)C(O)=O MTCFGRXMJLQNBG-UHFFFAOYSA-N 0.000 claims description 3
- AYFVYJQAPQTCCC-UHFFFAOYSA-N Threonine Natural products CC(O)C(N)C(O)=O AYFVYJQAPQTCCC-UHFFFAOYSA-N 0.000 claims description 3
- 239000004473 Threonine Substances 0.000 claims description 3
- 239000000126 substance Substances 0.000 claims description 3
- MTCFGRXMJLQNBG-REOHCLBHSA-N (2S)-2-Amino-3-hydroxypropansäure Chemical compound OC[C@H](N)C(O)=O MTCFGRXMJLQNBG-REOHCLBHSA-N 0.000 claims description 2
- AYFVYJQAPQTCCC-GBXIJSLDSA-N L-threonine Chemical compound C[C@@H](O)[C@H](N)C(O)=O AYFVYJQAPQTCCC-GBXIJSLDSA-N 0.000 claims description 2
- 235000011114 ammonium hydroxide Nutrition 0.000 claims description 2
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 claims 2
- 241000219793 Trifolium Species 0.000 claims 1
- 239000002253 acid Substances 0.000 claims 1
- 229910021529 ammonia Inorganic materials 0.000 claims 1
- 240000004658 Medicago sativa Species 0.000 abstract description 59
- UGFAIRIUMAVXCW-UHFFFAOYSA-N Carbon monoxide Chemical compound [O+]#[C-] UGFAIRIUMAVXCW-UHFFFAOYSA-N 0.000 abstract description 8
- 239000003546 flue gas Substances 0.000 abstract description 8
- 230000000694 effects Effects 0.000 abstract description 4
- 210000000214 mouth Anatomy 0.000 abstract description 4
- 230000000638 stimulation Effects 0.000 abstract description 4
- 238000009777 vacuum freeze-drying Methods 0.000 abstract description 3
- 238000002604 ultrasonography Methods 0.000 abstract 1
- 150000004676 glycans Chemical class 0.000 description 6
- 229920001282 polysaccharide Polymers 0.000 description 6
- 239000005017 polysaccharide Substances 0.000 description 6
- 235000018102 proteins Nutrition 0.000 description 5
- 102000004169 proteins and genes Human genes 0.000 description 5
- 108090000623 proteins and genes Proteins 0.000 description 5
- 235000001014 amino acid Nutrition 0.000 description 4
- 239000003205 fragrance Substances 0.000 description 4
- 239000002304 perfume Substances 0.000 description 4
- 238000005516 engineering process Methods 0.000 description 3
- QNAYBMKLOCPYGJ-REOHCLBHSA-N L-alanine Chemical compound C[C@H](N)C(O)=O QNAYBMKLOCPYGJ-REOHCLBHSA-N 0.000 description 2
- 235000004279 alanine Nutrition 0.000 description 2
- 238000011156 evaluation Methods 0.000 description 2
- 239000000463 material Substances 0.000 description 2
- 239000000047 product Substances 0.000 description 2
- 230000001953 sensory effect Effects 0.000 description 2
- 230000000391 smoking effect Effects 0.000 description 2
- 238000002791 soaking Methods 0.000 description 2
- 235000013599 spices Nutrition 0.000 description 2
- SHZGCJCMOBCMKK-UHFFFAOYSA-N D-mannomethylose Natural products CC1OC(O)C(O)C(O)C1O SHZGCJCMOBCMKK-UHFFFAOYSA-N 0.000 description 1
- WQZGKKKJIJFFOK-QTVWNMPRSA-N D-mannopyranose Chemical compound OC[C@H]1OC(O)[C@@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-QTVWNMPRSA-N 0.000 description 1
- 241000196324 Embryophyta Species 0.000 description 1
- WQZGKKKJIJFFOK-GASJEMHNSA-N Glucose Natural products OC[C@H]1OC(O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-GASJEMHNSA-N 0.000 description 1
- SHZGCJCMOBCMKK-JFNONXLTSA-N L-rhamnopyranose Chemical compound C[C@@H]1OC(O)[C@H](O)[C@H](O)[C@H]1O SHZGCJCMOBCMKK-JFNONXLTSA-N 0.000 description 1
- PNNNRSAQSRJVSB-UHFFFAOYSA-N L-rhamnose Natural products CC(O)C(O)C(O)C(O)C=O PNNNRSAQSRJVSB-UHFFFAOYSA-N 0.000 description 1
- 235000010624 Medicago sativa Nutrition 0.000 description 1
- 239000000654 additive Substances 0.000 description 1
- 230000000996 additive effect Effects 0.000 description 1
- WQZGKKKJIJFFOK-VFUOTHLCSA-N beta-D-glucose Chemical compound OC[C@H]1O[C@@H](O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-VFUOTHLCSA-N 0.000 description 1
- 150000001720 carbohydrates Chemical class 0.000 description 1
- 238000006757 chemical reactions by type Methods 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 235000013399 edible fruits Nutrition 0.000 description 1
- 239000000835 fiber Substances 0.000 description 1
- 239000012530 fluid Substances 0.000 description 1
- 238000007710 freezing Methods 0.000 description 1
- 230000008014 freezing Effects 0.000 description 1
- 239000007789 gas Substances 0.000 description 1
- 239000008103 glucose Substances 0.000 description 1
- 239000004615 ingredient Substances 0.000 description 1
- 230000005764 inhibitory process Effects 0.000 description 1
- 230000007794 irritation Effects 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 229920002521 macromolecule Polymers 0.000 description 1
- 238000007254 oxidation reaction Methods 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- -1 saccharide compound Chemical class 0.000 description 1
- 239000000779 smoke Substances 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 238000006467 substitution reaction Methods 0.000 description 1
- 235000019505 tobacco product Nutrition 0.000 description 1
- 235000014101 wine Nutrition 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/0003—Compounds of unspecified constitution defined by the chemical reaction for their preparation
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/28—Treatment of tobacco products or tobacco substitutes by chemical substances
- A24B15/30—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances
- A24B15/302—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances by natural substances obtained from animals or plants
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Agronomy & Crop Science (AREA)
- Botany (AREA)
- Health & Medical Sciences (AREA)
- General Health & Medical Sciences (AREA)
- Toxicology (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
Abstract
The present invention provides a kind of preparation method of cigarette alfalfa reactant, and including the alfalfa that (1) cradles squaring period, clear water cleans the floating ash in surface, drains, is cut into segment；(2), above-mentioned alfalfa is subjected to precooling；(3), vacuum freeze drying will be carried out by the alfalfa of precooling；(4), weigh it is freeze-dried after alfalfa dehydrated alcohol is added, ultrasound is placed in refrigerator and stands；(5), by said mixture after qualitative filter paper filters, filtrate recycling leaves freeze-drying alfalfa, and washes with water；(6), above-mentioned treated freeze-drying alfalfa is placed in Maillard reaction container, amino acid is added and carries out Maillard reaction；(7), system temperature after reaction, is down to 50 DEG C hereinafter, up to the alfalfa reactant after filtering and impurity removing.Alfalfa reactant prepared by the present invention can increase flue gas concentration, reduce throat's stimulation, improve the flue gas property sent out and oral cavity pleasant impression thoroughly, there is preferable application effect in cigarette.
Description
Technical field
The present invention relates to the preparation method of essence spice for cigarette, the preparation method of specifically a kind of cigarette alfalfa reactant
And its application.
Background technique
Maillard reaction refers to that reproducibility saccharide compound and amino acid or protein ultimately generate palm fibre by complex reaction
The macromolecular substance black essence of color even black, also known as " nonenzymatic browning reaction ".Maillard reaction is tobacco characteristic perfume
One of the important reaction formed, reactant have good inhibition and cover effect to irritation and cigarettes, wines and miscellaneous goods gas, can promote
Cigarette cigarette perfume and jealous.
Vacuum Freezing & Drying Technology is moisture after material glaciation, will to be made direct without liquid under certain vacuum degree
By solid state sublimation at gaseous state, finally make the dry technology of material dewatering.The technology carries out under conditions of low-temp low-pressure, effectively keeps away
The loss of oxidation reaction and heat-sensitive ingredients is exempted from.Using dehydrated alcohol cold soaking after vacuum freeze drying, plant weight can be destroyed
Connection structure between protein and polysaccharide, precipitating proteins make polysaccharide separate out, are easy to extract.
Alfalfa also known as alfalfa, yield is high, abundance.Contents of saccharide is abundant in alfalfa, and that appears in the newspapers is main
The polysaccharide being made of glucose, mannose, rhamnose and galactolipin etc. has bioactivity and significant health-care effect.
The present inventor has found after study: can prepare perfume (or spice) by Maillard reaction using reducing sugar substance abundant in alfalfa
The natural tobacco aromaticss of tolerance high-quality abundant.Alfalfa P.E is applied less in tobacco product at present, and U.S. ladd is anti-
The preparation and application for answering object have not been reported.
Summary of the invention
The object of the present invention is to provide a kind of cigarette preparation method and applications of alfalfa reactant, prepared by this method
Alfalfa reactant can increase flue gas concentration, reduce throat's stimulation, improve the flue gas property sent out and oral cavity pleasant impression thoroughly, in cigarette
There is preferable application effect.
Above-mentioned purpose is achieved through the following technical solutions:
A kind of preparation method of cigarette alfalfa reactant, comprising the following steps:
1, the alfalfa for cradling squaring period, clear water clean the floating ash in surface, drain, be cut into the segment of 3~5cm；
2, above-mentioned alfalfa is carried out to 5~7h of precooling at -45~-55 DEG C；
3, will by precooling alfalfa move into vacuum freeze drier hothouse in, vacuum chamber pressure be 30~
50pa, sublimation temperature are freeze-dried 10~12h under the conditions of being 40~50 DEG C, and moisture content is controlled in 15%~20%；
4, weigh it is freeze-dried after alfalfa the dehydrated alcohol of 5~7 times of its weight is added, surpass under the conditions of 150Hz
After 10~15min of sound, it is placed in 3~5h of standing in 4 DEG C of refrigerators；
5, by said mixture after qualitative filter paper filters, filtrate recycling leaves freeze-drying alfalfa, and washes with water freeze-drying
Alfalfa 2~3 times, removal surface protein precipitating；
6, above-mentioned treated freeze-drying alfalfa is placed in Maillard reaction container, the water of 5~8 times of its weight is added
With 1~1.5 times of amino acid of its weight, the pH to 8~12 of reaction system is adjusted after mixing, temperature control is 95~120 DEG C, is stirred
Mix progress 3~4h of Maillard reaction under state；
7, system temperature after reaction, is down to 50 DEG C hereinafter, up to the alfalfa reactant after filtering and impurity removing.
Further, the amino acid is the mixing of one or more of alanine, glycine, threonine, serine.
Further, the substance for adjusting reaction system pH is the mixed of one or more of concentrated ammonia liquor, NaOH, KOH
It closes.
A kind of application of the cigarette of method as described above preparation with alfalfa reactant in the tobacco, by its according to 0.05%~
0.1% mass ratio is added in pipe tobacco.
The invention has the following advantages:
(1) present invention prepares Maillard reaction type tobacco aromaticss using the sugar source of alfalfa itself for the first time, passes through addition
A certain amount of amino acid, rationally controls process conditions, can prepare the natural tobacco aromaticss of perfume quantity high-quality abundant.
(2) present invention can destroy the connection knot between protein and polysaccharide using dehydrated alcohol cold soaking after vacuum freeze drying
Structure, precipitating proteins make alfalfa polysaccharide separate out, and method has easy to operate, stable processing technique, and polysaccharide is easy to extract
The features such as.
(3) present invention has the characteristics that low raw-material cost, strong operability, stable processing technique, prepared purple lucerne
Mu reactant fragrance enriches strong, is applied in cigarette, can increase flue gas concentration, reduce throat's stimulation, improves flue gas and send out thoroughly
Property and oral cavity pleasant impression.
Specific embodiment
Below in conjunction with specific embodiment, the technical solution in the present invention is clearly and completely described.
Embodiment 1
A kind of preparation method of cigarette alfalfa reactant, comprising the following steps:
1, the alfalfa for cradling squaring period, clear water clean the floating ash in surface, drain, be cut into the segment of 3cm；
2, by above-mentioned alfalfa -45~DEG C at carry out precooling 7h；
3, it will be moved by the alfalfa of precooling in the hothouse of vacuum freeze drier, be in vacuum chamber pressure
30pa, sublimation temperature are freeze-dried 10h under the conditions of being 45 DEG C, and moisture content is controlled in 20%.
4, weigh it is freeze-dried after alfalfa the dehydrated alcohol of 5 times of its weight is added, it is ultrasonic under the conditions of 150Hz
After 15min, it is placed in 4 DEG C of refrigerators and stands 5h；
5, by said mixture after qualitative filter paper filters, filtrate recycling leaves freeze-drying alfalfa, and washes with water freeze-drying
Alfalfa 2 times, removal surface protein precipitating.
6, above-mentioned treated freeze-drying alfalfa is placed in Maillard reaction container, be added 5 times of its weight water and
The alanine of 1 times of its weight adjusts the pH to 10 of reaction system after mixing, temperature control is 100 DEG C, carries out under stirring
Maillard reaction 3h.
7, system temperature after reaction, is down to 50 DEG C hereinafter, up to the alfalfa reactant after filtering and impurity removing.
Embodiment 2
A kind of preparation method of cigarette alfalfa reactant, comprising the following steps:
1, the alfalfa for cradling squaring period, clear water clean the floating ash in surface, drain, be cut into the segment of 5cm；
2, above-mentioned alfalfa is carried out to precooling 5h at 55 DEG C；
3, it will be moved by the alfalfa of precooling in the hothouse of vacuum freeze drier, be in vacuum chamber pressure
50pa, sublimation temperature are freeze-dried 12h under the conditions of being 50 DEG C, and moisture content is controlled in 15%.
4, weigh it is freeze-dried after alfalfa the dehydrated alcohol of 6 times of its weight is added, it is ultrasonic under the conditions of 150Hz
After 15min, it is placed in 4 DEG C of refrigerators and stands 4h；
5, by said mixture after qualitative filter paper filters, filtrate recycling leaves freeze-drying alfalfa, and washes with water freeze-drying
Alfalfa 3 times, removal surface protein precipitating.
6, above-mentioned treated freeze-drying alfalfa is placed in Maillard reaction container, be added 8 times of its weight water and
The serine of 1.5 times of its weight, after mixing adjust reaction system pH to 12, temperature control be 120 DEG C, under stirring into
Row Maillard reaction 4h.
7, system temperature after reaction, is down to 50 DEG C hereinafter, up to the alfalfa reactant after filtering and impurity removing.
Embodiment 3
A kind of preparation method of cigarette alfalfa reactant, comprising the following steps:
1, the alfalfa for cradling squaring period, clear water clean the floating ash in surface, drain, be cut into the segment of 5cm；
2, above-mentioned alfalfa is subjected to precooling 6h at -50 DEG C；
3, it will be moved by the alfalfa of precooling in the hothouse of vacuum freeze drier, be in vacuum chamber pressure
40pa, sublimation temperature are freeze-dried 12h under the conditions of being 50 DEG C, and moisture content is controlled in 18%.
4, weigh it is freeze-dried after alfalfa the dehydrated alcohol of 6 times of its weight is added, it is ultrasonic under the conditions of 150Hz
After 15min, it is placed in 4 DEG C of refrigerators and stands 6h；
5, by said mixture after qualitative filter paper filters, filtrate recycling leaves freeze-drying alfalfa, and washes with water freeze-drying
Alfalfa 3 times, removal surface protein precipitating.
6, above-mentioned treated freeze-drying alfalfa is placed in Maillard reaction container, be added 8 times of its weight water and
The threonine of 1 times of its weight adjusts the pH to 10 of reaction system after mixing, temperature control is 100 DEG C, carries out under stirring
Maillard reaction 3h.
7, system temperature after reaction, is down to 50 DEG C hereinafter, up to the alfalfa reactant after filtering and impurity removing.
Embodiment 4
A kind of preparation method of cigarette alfalfa reactant, comprising the following steps:
1, the alfalfa for cradling squaring period, clear water clean the floating ash in surface, drain, be cut into the segment of 5cm；
2, above-mentioned alfalfa is subjected to precooling 6h at -50 DEG C；
3, it will be moved by the alfalfa of precooling in the hothouse of vacuum freeze drier, be in vacuum chamber pressure
40pa, sublimation temperature are freeze-dried 12h under the conditions of being 50 DEG C, and moisture content is controlled in 18%.
4, weigh it is freeze-dried after alfalfa the dehydrated alcohol of 6 times of its weight is added, it is ultrasonic under the conditions of 150Hz
After 15min, it is placed in 4 DEG C of refrigerators and stands 5h；
5, by said mixture after qualitative filter paper filters, filtrate recycling leaves freeze-drying alfalfa, and washes with water freeze-drying
Alfalfa 3 times, removal surface protein precipitating.
6, above-mentioned treated freeze-drying alfalfa is placed in Maillard reaction container, be added 10 times of its weight water and
The glycine of 1.5 times of its weight, after mixing adjust reaction system pH to 10, temperature control be 100 DEG C, under stirring into
Row Maillard reaction 3h.
7, system temperature after reaction, is down to 50 DEG C hereinafter, up to the alfalfa reactant after filtering and impurity removing.
Products obtained therefrom be brown fluid, fragrance enrich it is strong, baking fragrance it is pure, by it according to 0.05%~0.1%
Mass ratio is added in blank pipe tobacco, show that the product can increase flue gas concentration through sensory evaluating smoking, reduces throat's stimulation, change
Kind the flue gas property sent out and oral cavity pleasant impression thoroughly.
Adding proportion of the fixed fragrance in blank pipe tobacco is 0.08%, is evaluated, is commented referring to State Bureau's evaluation standard
Suction group is made of 13 cigarette sensory evaluation experts, and does control to be not added with the blank cigarette of additive and smoke panel test.Specific knot
Fruit is as shown in table 1.
1 smoking result of table
The above description is merely a specific embodiment, but scope of protection of the present invention is not limited thereto, any
Belong to those skilled in the art in the technical scope disclosed by the present invention, any changes or substitutions that can be easily thought of, all answers
It is included within the scope of the present invention.
Claims (4)
1. a kind of cigarette preparation method of alfalfa reactant, it is characterised in that include the following steps:
(1), the alfalfa for cradling squaring period, clear water clean the floating ash in surface, drain, be cut into the segment of 3~5cm；
(2), above-mentioned alfalfa is carried out to 5~7h of precooling at -45~-55 DEG C；
(3), will by precooling alfalfa move into vacuum freeze drier hothouse in, vacuum chamber pressure be 30~
50pa, sublimation temperature are freeze-dried 10~12h under the conditions of being 40~50 DEG C, and moisture content is controlled in 15%~20%；
(4), weigh it is freeze-dried after alfalfa the dehydrated alcohol of 5~7 times of its weight is added, it is ultrasonic under the conditions of 150Hz
After 10~15min, it is placed in 3~5h of standing in 4 DEG C of refrigerators；
(5), by said mixture after qualitative filter paper filters, filtrate recycling leaves freeze-drying alfalfa, and it is purple to wash with water freeze-drying
Clover 2~3 times, removal surface protein precipitating；
(6), above-mentioned treated freeze-drying alfalfa is placed in Maillard reaction container, be added 5~8 times of its weight water and
The amino acid of 1~1.5 times of its weight adjusts the pH to 8~12 of reaction system after mixing, temperature control is 95~120 DEG C, stirring
3~4h of Maillard reaction is carried out under state；
(7), system temperature after reaction, is down to 50 DEG C hereinafter, up to the alfalfa reactant after filtering and impurity removing.
2. the cigarette as described in claim 1 preparation method of alfalfa reactant, it is characterised in that: the amino acid is the third ammonia
The mixing of one or more of acid, glycine, threonine, serine.
3. the cigarette as described in claim 1 preparation method of alfalfa reactant, it is characterised in that: the adjusting reaction system
The substance of pH is the mixing of one or more of concentrated ammonia liquor, NaOH, KOH.
4. a kind of application such as the cigarette of any one of claim 1-3 the method preparation with alfalfa reactant in the tobacco,
It is added in pipe tobacco according to 0.05%~0.1% mass ratio.
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111074684A (en) * | 2020-01-20 | 2020-04-28 | 中国烟草总公司郑州烟草研究院 | Colored cigarette paper and preparation method thereof |
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| CN104905398A (en) * | 2015-05-29 | 2015-09-16 | 湖北中烟工业有限责任公司 | Alfalfa leaf extract preparation method and use as tobacco product additive |
| CN105062675A (en) * | 2015-07-27 | 2015-11-18 | 湖北中烟工业有限责任公司 | Preparation method of beta vulgaris Maillard reactant for tobacco |
| CN105837704A (en) * | 2016-06-14 | 2016-08-10 | 山东农业大学 | Extraction and purification method of alfalfa polysaccharide |
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2018
- 2018-10-18 CN CN201811214779.1A patent/CN109337762A/en active Pending
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