CN109304472A - It is hydraulic atomized to produce noble metal powder equipment - Google Patents

It is hydraulic atomized to produce noble metal powder equipment Download PDF

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Publication number
CN109304472A
CN109304472A CN201811357129.2A CN201811357129A CN109304472A CN 109304472 A CN109304472 A CN 109304472A CN 201811357129 A CN201811357129 A CN 201811357129A CN 109304472 A CN109304472 A CN 109304472A
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CN
China
Prior art keywords
metal powder
spray chamber
connect
atomized
atomization
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Withdrawn
Application number
CN201811357129.2A
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Chinese (zh)
Inventor
尹荔松
涂驰周
马思琪
蓝键
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Wuyi University
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Wuyi University
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Filing date
Publication date
Application filed by Wuyi University filed Critical Wuyi University
Priority to CN201811357129.2A priority Critical patent/CN109304472A/en
Publication of CN109304472A publication Critical patent/CN109304472A/en
Withdrawn legal-status Critical Current

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Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B22CASTING; POWDER METALLURGY
    • B22FWORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
    • B22F9/00Making metallic powder or suspensions thereof
    • B22F9/02Making metallic powder or suspensions thereof using physical processes
    • B22F9/06Making metallic powder or suspensions thereof using physical processes starting from liquid material
    • B22F9/08Making metallic powder or suspensions thereof using physical processes starting from liquid material by casting, e.g. through sieves or in water, by atomising or spraying
    • B22F9/082Making metallic powder or suspensions thereof using physical processes starting from liquid material by casting, e.g. through sieves or in water, by atomising or spraying atomising using a fluid
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B22CASTING; POWDER METALLURGY
    • B22FWORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
    • B22F9/00Making metallic powder or suspensions thereof
    • B22F9/02Making metallic powder or suspensions thereof using physical processes
    • B22F9/06Making metallic powder or suspensions thereof using physical processes starting from liquid material
    • B22F9/08Making metallic powder or suspensions thereof using physical processes starting from liquid material by casting, e.g. through sieves or in water, by atomising or spraying
    • B22F9/082Making metallic powder or suspensions thereof using physical processes starting from liquid material by casting, e.g. through sieves or in water, by atomising or spraying atomising using a fluid
    • B22F2009/0824Making metallic powder or suspensions thereof using physical processes starting from liquid material by casting, e.g. through sieves or in water, by atomising or spraying atomising using a fluid with a specific atomising fluid
    • B22F2009/0828Making metallic powder or suspensions thereof using physical processes starting from liquid material by casting, e.g. through sieves or in water, by atomising or spraying atomising using a fluid with a specific atomising fluid with water

Abstract

Noble metal powder equipment is produced the invention discloses hydraulic atomized, the smelting apparatus of melting is carried out to alloy material including being set in rack, the spray chamber for being connect with smelting apparatus and the metal liquid after melting being atomized, the loading head of discharging collection is connect and carried out to the metal powder of atomization formation with spray chamber, the centrifuge for being connect with loading head and metal powder being dehydrated, the drying machine for being connect with centrifuge and dewatered metal powder being dried, it is connect with drying machine and to the screw conveyor transported to the metal powder of drying, it is connected in screw conveyor and carries out the vibrator of vibration sub-sieve to metal powder, it is connect with vibrator and vacuum-packed packing machine is carried out to the metal powder after sub-sieve.The equipment carries out powder processed using hydraulic atomized mode, and by inert gas shielding in fusion process, oxidation is few, and high production efficiency, size distribution is good, the high spherical or subsphaeroidal or irregular shape of the metal powder of output.

Description

It is hydraulic atomized to produce noble metal powder equipment
Technical field
The present invention relates to the technical fields of metallurgical equipment, more particularly to a kind of hydraulic atomized noble metal powder of producing to set It is standby.
Background technique
(98% or more sphericity >, lack without hollow powder, satellite powder, bonded powder currently, metal powder need to have spheric granules Deng), Narrow diameter distribution (D50≤45 μm), low oxygen content (< 100ppm), high apparent density, (impurity content is or not low impurity content Higher than master alloy, without ceramic inclusions) etc. fundamental characteristics.Therefore, the powder-making technique requirement and powder processed for determining metal powder are set Standby is very high.And the equipment majority of existing metal powder uses gas atomization mode, but traditional gas atomization equipment Due to structure problem, the air velocity and pressure sprayed cannot carry out in a high voltage state, cause the metal powder of output Not only reach fine powder state, and the metal powder of output cannot form high spherical or approximate sphericity, cannot continuous output powder, and The moisture of the metal powder of output is not dry enough, of low quality.Therefore, existing powder manufacturing apparatus need to have much room for improvement.
Summary of the invention
The purpose of the invention is to overcome the above-mentioned prior art, provides and a kind of hydraulic atomized produce noble metal Powder apparatus, the hydraulic atomized noble metal powder equipment of producing use hydraulic atomized mode to carry out powder processed, can satisfy Water atomization pulverization under atmospheric conditions;The rack of the equipment uses non-magnetic rustproof steel construction, and intensity is big, and the service life is long;Alloy material exists By inert gas shielding in fusion process, oxidation is few;Fusing quick heating, high production efficiency, size distribution are good;The metal powder of output The spherical or subsphaeroidal or irregular shape of last height, energy continuous production extract powder, the high yield rate of powder out.
The technical solution adopted by the present invention to solve the technical problems is: it is hydraulic atomized to produce noble metal powder equipment, Including the rack using non-magnetic rustproof steel construction, further include in the rack to alloy material carry out melting smelting apparatus, with Smelting apparatus connection and the spray chamber that the metal liquid after melting is atomized, the gold for being connect with spray chamber and atomization being formed Belong to powder and carries out the loading head of discharging collection, the centrifuge and centrifuge for connecting with loading head and being dehydrated to metal powder Connect and dewatered metal powder is dried drying machine, connect with drying machine and carried out to the metal powder of drying The screw conveyor of transport connects in screw conveyor and carries out the vibrator of vibration sub-sieve to metal powder, connects with vibrator It connects and vacuum-packed packing machine is carried out to the metal powder after sub-sieve;Smelting apparatus include for ramming mass ramming crucible and Alloy material is melt into the medium frequency induction melting furnace of metal liquid;Spray chamber includes being equipped with hydraulic atomized spray disk and exhaust The upper spray chamber of valve, is equipped with discharge outlet and collection at the middle spray chamber for being equipped with protection inert gas entrance and constant level device The lower spray chamber of powder funnel;Loading head includes splicing bucket and the water discharging valve in splicing bucket, and centrifuge includes true Empty pump filter and filter cloth, drying machine is dried using steel belt furnace or heat-circulation oven drying, vibrator use ternary vibrating screen.
Further, the spray chamber includes atomization staving, and upper spray chamber, middle spray chamber and lower spray chamber are respectively arranged on It is atomized the position of staving upper, middle and lower, the top for being atomized staving is equipped with the heat preservation tundish with restraint-type diversion pipe, high-pressure water mist Change spray disk to be set to below heat preservation tundish, hydraulic atomized spray disk is equipped with nozzle, and exhaust valve is connected with exhaust pipe, upper atomization Room be additionally provided with monitoring atomization situation monitor, monitor can height digital display measurement monitoring atomized water, make atomization process parameter control System is stablized.
Further, the water level monitor being monitored to water level is additionally provided on the middle spray chamber.
Further, the splicing bucket of the loading head passes through the collection powder funnel of stainless steel connecting pipe and lower spray chamber Connection communicates.
The hydraulic atomized main technique for producing noble metal powder equipment is as follows: (1) alloy material passes through ramming Crucible ramming mass forms metal liquid up to melting in 1700 DEG C of medium frequency induction melting furnace into smelting temperature;(2) in inertia Under conditions of gas shield, metal liquid is stayed by heat preservation tundish and restraint-type diversion pipe into spray chamber, and spray chamber passes through spray Metal liquid atomization is broken into a large amount of tiny molten drops by super-pressure water flow by mouth, tiny drop in flight course by The metal powder of almost spherical or scrambling particle, metal powder are cooperatively formed to the rapid cooling of surface tension and water It is deposited on and collects on powder funnel and tentatively drained by discharge outlet;(3) metal powder is defeated by stainless steel connecting pipe Out in splicing bucket and passing through water discharging valve and carry out second and drain;(4) metal powder, which enters, carries out centrifugal dehydration in centrifuge; (5) metal powder after centrifugal dehydration enters steel belt furnace drying or heat-circulation oven drying, the metal powder water content after drying It is delivered on vibrator less than 5%, then through screw conveyor;(6) vibrator uses ternary shaker vibration sub-sieve, send after sub-sieve It is vacuum-packed to packing machine, obtains noble metal powder finished product.
In conclusion hydraulic atomized noble metal powder equipment of producing of the invention is using hydraulic atomized mode system Powder can satisfy water atomization pulverization in atmospheric conditions;The rack of the equipment uses non-magnetic rustproof steel construction, and intensity is big, the service life It is long;For alloy material by inert gas shielding in fusion process, oxidation is few;Melt quick heating, high production efficiency, size distribution It is good;The high spherical or subsphaeroidal or irregular shape of the metal powder of output, energy continuous production extract powder, the high yield rate of powder out.
Detailed description of the invention
Fig. 1 is the hydraulic atomized simple connection block diagram for producing noble metal powder equipment of the embodiment of the present invention 1;
Fig. 2 is the simplified schematic diagram of spray chamber.
Specific embodiment
Embodiment 1
It is hydraulic atomized described in the present embodiment 1 to produce noble metal powder equipment, as shown in Figure 1 and Figure 2, including use The rack (not shown) of non-magnetic rustproof steel construction further includes the smelting apparatus for carrying out melting to alloy material in rack 1, connect with smelting apparatus and the metal liquid after melting is atomized spray chamber 2, connect with spray chamber and to atomization shape At metal powder carry out the loading head 3 of discharging collection, the centrifuge 4 that connect with loading head and metal powder is dehydrated, Connect with centrifuge and dewatered metal powder is dried drying machine 5, connect with drying machine and to the gold to drying Belong to powder transported screw conveyor 6, in screw conveyor connect and to metal powder carry out vibration sub-sieve vibrator 7, it is connect with vibrator and vacuum-packed packing machine 8 is carried out to the metal powder after sub-sieve;Smelting apparatus includes being used for ramming The ramming crucible (not shown) of material and the medium frequency induction melting furnace that alloy material is melt into metal liquid (is not shown in figure Show);Spray chamber includes the upper spray chamber 22 for being equipped with hydraulic atomized spray disk 9 and exhaust valve 10, is equipped with protection inert gas The middle spray chamber 23 of entrance 11 and constant level device 12, the lower spray chamber 24 equipped with discharge outlet 13 and collection powder funnel 14; Loading head includes splicing bucket (not shown) and the water discharging valve (not shown) in splicing bucket, and centrifuge includes There are vacuumfilter (not shown) and filter cloth (not shown), drying machine is dried using steel belt furnace or heat-circulation oven dries Dry, vibrator uses ternary vibrating screen.
In this embodiment, which includes atomization staving 15, and upper spray chamber, middle spray chamber and lower spray chamber are set respectively In the position of atomization staving upper, middle and lower, the top for being atomized staving is equipped with the heat preservation tundish 16 with restraint-type diversion pipe 21, high Water atomization spray disk is pressed to be set to below heat preservation tundish, hydraulic atomized spray disk is equipped with nozzle 20, and exhaust valve is connected with exhaust pipe Road 17, upper spray chamber be additionally provided with monitoring atomization situation monitor 18, monitor can height digital display measurement monitoring atomized water, make mist Change process parameter control to stablize.
In the present embodiment, the water level monitor 19 being monitored to water level is additionally provided in this on spray chamber.
In the present embodiment, the splicing bucket of the loading head passes through stainless steel connecting pipe (not shown) and lower spray chamber Collection powder funnel connection communicate.
The hydraulic atomized main technique for producing noble metal powder equipment is as follows: (1) alloy material passes through ramming Crucible ramming mass forms metal liquid up to melting in 1700 DEG C of medium frequency induction melting furnace into smelting temperature;(2) in inertia Under conditions of gas shield, metal liquid is stayed by heat preservation tundish and restraint-type diversion pipe into spray chamber, and spray chamber passes through spray Metal liquid atomization is broken into a large amount of tiny molten drops by super-pressure water flow by mouth, tiny drop in flight course by The metal powder of almost spherical or scrambling particle, metal powder are cooperatively formed to the rapid cooling of surface tension and water It is deposited on and collects on powder funnel and tentatively drained by discharge outlet;(3) metal powder is defeated by stainless steel connecting pipe Out in splicing bucket and passing through water discharging valve and carry out second and drain;(4) metal powder, which enters, carries out centrifugal dehydration in centrifuge; (5) metal powder after centrifugal dehydration enters steel belt furnace drying or heat-circulation oven drying, the metal powder water content after drying It is delivered on vibrator less than 5%, then through screw conveyor;(6) vibrator uses ternary shaker vibration sub-sieve, send after sub-sieve It is vacuum-packed to packing machine, obtains noble metal powder finished product.
The above described is only a preferred embodiment of the present invention, not making any form to technical solution of the present invention On limitation.According to the technical essence of the invention any simple modification to the above embodiments, equivalent variations and repair Decorations, in the range of still falling within technical solution of the present invention.

Claims (4)

1. hydraulic atomized produce noble metal powder equipment, which is characterized in that including the rack using non-magnetic rustproof steel construction, also Including carrying out the smelting apparatus of melting to alloy material in rack, being connect with smelting apparatus and to the metal liquid after melting The spray chamber being atomized, the metal powder for connecting with spray chamber and being formed to atomization carry out the loading head and collection of discharging collection Glassware connection and the centrifuge being dehydrated to metal powder connect with centrifuge and dry to dewatered metal powder Drying machine, connect with drying machine and connect to the screw conveyor transported to the metal powder of drying, in screw conveyor It connects and the vibrator of vibration sub-sieve is carried out to metal powder, connect with vibrator and vacuum packet is carried out to the metal powder after sub-sieve The packing machine of dress;Smelting apparatus includes the intermediate frequency sense that metal liquid is melt into for the ramming crucible of ramming mass and alloy material Answer smelting furnace;Spray chamber includes the upper spray chamber for being equipped with hydraulic atomized spray disk and exhaust valve, is equipped with protection inert gas The middle spray chamber of entrance and constant level device, the lower spray chamber equipped with discharge outlet and collection powder funnel;Loading head includes Splicing bucket and the water discharging valve in splicing bucket, centrifuge include vacuumfilter and filter cloth, and drying machine uses steel belt furnace Drying or heat-circulation oven drying, vibrator use ternary vibrating screen.
2. hydraulic atomized noble metal powder equipment is produced according to claim 1, which is characterized in that the spray chamber Including being atomized staving, upper spray chamber, middle spray chamber and lower spray chamber are respectively arranged on the position of atomization staving upper, middle and lower, are atomized bucket The top of body is equipped with the heat preservation tundish with restraint-type diversion pipe, and hydraulic atomized spray disk is set to below heat preservation tundish, high pressure Water atomization sprays disk and is equipped with nozzle, and exhaust valve is connected with exhaust pipe, and upper spray chamber is additionally provided with the monitor of monitoring atomization situation.
3. hydraulic atomized noble metal powder equipment is produced according to claim 2, which is characterized in that the middle atomization The water level monitor being monitored to water level is additionally provided on room.
4. hydraulic atomized noble metal powder equipment is produced according to claim 3, which is characterized in that the loading head Splicing bucket is connect with the collection powder funnel of lower spray chamber by stainless steel connecting pipe and is communicated.
CN201811357129.2A 2018-11-15 2018-11-15 It is hydraulic atomized to produce noble metal powder equipment Withdrawn CN109304472A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201811357129.2A CN109304472A (en) 2018-11-15 2018-11-15 It is hydraulic atomized to produce noble metal powder equipment

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201811357129.2A CN109304472A (en) 2018-11-15 2018-11-15 It is hydraulic atomized to produce noble metal powder equipment

Publications (1)

Publication Number Publication Date
CN109304472A true CN109304472A (en) 2019-02-05

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CN201811357129.2A Withdrawn CN109304472A (en) 2018-11-15 2018-11-15 It is hydraulic atomized to produce noble metal powder equipment

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Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111468737A (en) * 2020-03-07 2020-07-31 福达合金材料股份有限公司 Powder preparation and powder mixing integrated device and application thereof
CN111957981A (en) * 2020-08-18 2020-11-20 苏州鲁信新材料科技有限公司 Equipment for preparing copper alloy powder by water-gas combined atomization and use method thereof
CN112077326A (en) * 2020-08-18 2020-12-15 苏州鲁信新材料科技有限公司 Atomization device for preparing copper alloy powder
CN112620639A (en) * 2020-11-18 2021-04-09 江西鑫润材料科技有限公司 Alloy powder manufacturing equipment

Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111468737A (en) * 2020-03-07 2020-07-31 福达合金材料股份有限公司 Powder preparation and powder mixing integrated device and application thereof
CN111957981A (en) * 2020-08-18 2020-11-20 苏州鲁信新材料科技有限公司 Equipment for preparing copper alloy powder by water-gas combined atomization and use method thereof
CN112077326A (en) * 2020-08-18 2020-12-15 苏州鲁信新材料科技有限公司 Atomization device for preparing copper alloy powder
CN112620639A (en) * 2020-11-18 2021-04-09 江西鑫润材料科技有限公司 Alloy powder manufacturing equipment
CN112620639B (en) * 2020-11-18 2023-02-07 江西鑫润材料科技有限公司 Alloy powder manufacturing equipment

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Application publication date: 20190205

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