CN109289223A - A kind of fractionation machine - Google Patents
A kind of fractionation machine Download PDFInfo
- Publication number
- CN109289223A CN109289223A CN201811482213.7A CN201811482213A CN109289223A CN 109289223 A CN109289223 A CN 109289223A CN 201811482213 A CN201811482213 A CN 201811482213A CN 109289223 A CN109289223 A CN 109289223A
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- CN
- China
- Prior art keywords
- pipe
- outlet
- valve
- condenser pipe
- water
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Classifications
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
- B01D3/14—Fractional distillation or use of a fractionation or rectification column
Abstract
The invention discloses a kind of fractionation machine, including body, feed pipe, body side upper end is equipped with feed inlet, and feed inlet is connected with feed pipe, is provided with liquid feed valve on feed pipe；Outlet pipe is provided with above body, outlet pipe includes the first outlet pipe, the second outlet pipe, valve is provided on outlet pipe, valve includes the first valve, the second valve, condenser pipe is provided on pipeline, condenser pipe includes the first condenser pipe, the second condenser pipe, and the first condenser pipe is set in first pipe, second condenser pipe is set to second pipe, is provided with electric heating tube in body.The present invention can real-time control heating temperature, avoid it is too high or too low for temperature material fractionation is not thorough, effectively improve fractionating efficiency, improve product quality；Structure is simple, strong applicability, and fractionating effect is good.
Description
Technical field
The present invention relates to chemical field equipment, and in particular to a kind of fractionation machine.
Background technique
Currently, being used for the device of chemical industry Fractionation Experiment, relatively simple for structure, organic solvent vapor temperature can not be detected by existing
And the temperature of fractionation body organic solvent, the problems such as distillate cooling can not be timely.
Summary of the invention
In order to solve the above technical problems, the present invention provides following technical schemes:
A kind of fractionation machine, including body, feed pipe, body side upper end be equipped with feed inlet, feed inlet be connected with into
Expects pipe is provided with liquid feed valve on feed pipe；Outlet pipe is provided with above the body, outlet pipe includes the first escape pipe
Road, the second outlet pipe, valve is provided on outlet pipe, and the valve includes the first valve, the second valve, the pipeline
On be provided with condenser pipe, condenser pipe includes the first condenser pipe, the second condenser pipe, and first condenser pipe is set to the first escape pipe
On road, the second condenser pipe is set on the second outlet pipe, is provided with electric heating tube in the body；The organism bottom side
It is provided with discharge outlet, discharge outlet is connected with drainpipe, and the drainpipe is provided with drain valve.
Preferably, the body side is provided with temperature sensor, and temperature sensor and electric heating tube are electrically connected by conducting wire
It connects, the temperature sensor is HD701 model.
Preferably, the body side is provided with pond, and water cover is provided with above pond, is provided with receipts at left and right sides of body
Collect bottle, the receiving flask includes the first receiving flask and the second receiving flask.
Preferably, the condenser pipe includes water inlet, water outlet, air inlet pipe, and air inlet pipe one end is connected to gas outlet pipeline,
The air inlet pipe other end is connected to inside receiving flask by pipeline.
Preferably, the water top is provided with water pump, and the water inlet of water pump is connected in pond by pipeline, water pump
Water outlet is connected to the water inlet pipe of condenser pipe by pipeline.
Preferably, the water outlet of the condenser pipe is connected to inside pond by pipeline.
Preferably, the outlet pipe is connected to receiving flask inner end and is provided with strainer.
Preferably, form is provided at the upper side of the body.
Preferably, an outside is provided with the second form above the second housing, has method by baffle plate setting under the second form
Orchid is covered, and is provided with handle on the blind flange.
Beneficial effect of the present invention
(1) present invention may filter that impurity prevents polluted product by setting strainer.
(2) present invention is by setting heating tube and temperature sensor, can real-time control heating temperature, avoid temperature excessively high or
It is too low that material fractionation is not thorough, fractionating efficiency is effectively improved, product quality is improved.
(3) present invention is by being arranged removable stirring motor, can accelerating the fractionation rate of solution and avoiding machine intracorporal useless
Liquid impurity excessively causes to be difficult to discharge from drainpipe, causes the blocking of drainpipe.
(4) present invention accelerates the collection of product by setting condenser pipe, condensable liquefied gas, improves working efficiency.
(5) the configuration of the present invention is simple, easy to operate, strong applicability.
Detailed description of the invention
Fig. 1 is schematic diagram of the present invention.
Fig. 2 is condenser pipe schematic diagram.
Description of symbols: 1- body, 2- feed pipe, 3- liquid feed valve, the first outlet pipe of 4-, the second outlet pipe of 5-,
The first valve of 6-, the second valve of 7-, the first receiving flask of 8-, the second receiving flask of 9-, 10- electric heating tube, 11- drainpipe, 12- draining
Valve, 13- temperature sensor, 14- strainer, the first condenser pipe of 15-, the second condenser pipe of 16-, 17- form, 18- clear water reserviors, 19- water
Pump, 21- water inlet, 22- water outlet, 23- air inlet pipe.
Specific embodiment
Below in conjunction with the attached drawing in the embodiment of the present invention, the technical solution in the embodiment of the present invention is carried out clear
Chu is fully described by, it is clear that described embodiments are only a part of the embodiments of the present invention, instead of all the embodiments.
Based on the embodiments of the present invention, obtained by those of ordinary skill in the art without making creative efforts all
Other embodiments shall fall within the protection scope of the present invention.
Embodiment 1
A kind of fractionation machine, including body 1, feed pipe 2, the 1 side upper end of body are equipped with feed inlet, and feed inlet is connected with
Feed pipe 2, feed pipe 2 are to be bolted with body 1, liquid feed valve 3 have been bolted on feed pipe 2, liquid feed valve 3 can control material
Investment；Outlet pipe is provided with above the body 1, outlet pipe includes the first outlet pipe 4, the second outlet pipe 5, out
Valve is provided in feed channel, the valve includes the first valve 6, the second valve 7, it is provided with condenser pipe on the pipeline,
Condenser pipe includes the first condenser pipe 15, the second condenser pipe 16, and first condenser pipe 15 is bolted in the first outlet pipe 4
On, the second condenser pipe 16 is bolted on the second outlet pipe 5, and condenser pipe plays the role of condensation liquefaction gas, and valve can
The effect that control gas imports and prevent gas liquefaction from flowing back；Receiving flask is provided at left and right sides of body 1, the receiving flask includes
First receiving flask 8 and the second receiving flask 9, the condenser pipe include water inlet 21, water outlet 22, air inlet pipe 23, air inlet pipe 23 1
End is connected to gas outlet pipeline, and 23 other end of air inlet pipe is connected to inside receiving flask by pipeline, and receiving flask collects liquefied
Gas；Electric heating tube 10 is provided in the body 1,1 side of body is provided with temperature sensor 13, temperature sensor 13 and electricity
Heating tube 10 is electrically connected by conducting wire, and temperature sensor 13 can monitor the temperature in body 1 in real time, can stop when reaching required temperature
It only heats, when needing to continue heating, 13 numerical value of temperature-adjustable sensor can continue to heat；1 side of body is provided with
Pond 18 is provided with water cover above pond 18, and water pump 19 is provided with above the water cover, and the water inlet of water pump 19 passes through pipeline company
It passes in pond, the water outlet of water pump 19 is connected to the water inlet 21 of condenser pipe, the water outlet 22 of the condenser pipe by pipeline
It is connected to inside pond by pipeline, the water in pond 18 can play the role of circulating condensing；1 bottom side of the body setting
There is discharge outlet, discharge outlet has been bolted drainpipe 11, and the drainpipe 11 has been bolted drain valve 12, and drainpipe 11 can be arranged
Waste liquid and impurity in body 1 out；Form 17, the feelings in 17 observable body 1 of form are provided at the upper side of the body 1
Condition facilitates operation.
Working principle
The liquid feed valve 3 opened on feed pipe 2 is passed through two component mixtures, simultaneously closes off valve, water pump 19, drain valve 12；
It opens the setting required temperature of temperature sensor 13 and manipulates heating tube 10 and begin to warm up, when reaching required temperature, open second
Valve 7 simultaneously closes off the first valve 6 and opens water pump 19, and gaseous state is into second after the mixture heating evaporation in body 1
Admission line 5 reaches the second condenser pipe 16, is collected after the second condenser pipe 16 is condensed into liquid by duct bottom interface second
Bottle 9 is collected；When temperature heating reaches the second component minimum boiling point, the second valve 7 is closed immediately and opens the first valve 1, to
Receiving flask, which is collected, completes required material.
Embodiment 2
As shown in Figure 1 and Figure 2, the present embodiment embodiment 1, on the basis of make advanced optimize, it is particularly described
Outlet pipe is connected to receiving flask inner end and is provided with strainer 14.
This implementation may filter that impurity, fractionated products avoided to pollute by setting strainer 14, improve product quality.
Finally, it should be noted that the foregoing is only a preferred embodiment of the present invention, it is not intended to restrict the invention,
Although the present invention is described in detail referring to the foregoing embodiments, for those skilled in the art, still may be used
To modify the technical solutions described in the foregoing embodiments or equivalent replacement of some of the technical features,
All within the spirits and principles of the present invention, any modification, equivalent replacement, improvement and so on should be included in of the invention
Within protection scope.
Claims (8)
1. a kind of fractionation machine, which is characterized in that including body (1), feed pipe (2), body (1) the side upper end is equipped with charging
Mouthful, feed inlet is connected with feed pipe (2), and liquid feed valve (3) are provided on feed pipe (2)；Outlet is provided with above the body (1)
Pipeline, outlet pipe include the first outlet pipe (4), the second outlet pipe (5), are provided with valve on outlet pipe, described
Valve includes the first valve (6), the second valve (7), and condenser pipe is provided on the pipeline, and condenser pipe includes the first condenser pipe
(15), the second condenser pipe (16), first condenser pipe (15) are set on the first outlet pipe (4), the second condenser pipe (16)
It is set on the second outlet pipe (5), electric heating tube (10) is provided in the body；Body (1) the bottom side setting
There is discharge outlet, discharge outlet is connected with the first drainpipe (11), and the drainpipe (11) is provided with drain valve (12).
2. a kind of fractionation machine according to claim 1, which is characterized in that body (1) side is provided with temperature sensing
Device (13), temperature sensor (13) are electrically connected with electric heating tube (10) by conducting wire.
3. a kind of fractionation machine according to claim 2, which is characterized in that body (1) side is provided with pond (18),
It is provided with water cover above pond (18), receiving flask is provided at left and right sides of body (1), the receiving flask includes the first receiving flask
(8) and the second receiving flask (9).
4. a kind of fractionation machine according to claim 3, which is characterized in that the condenser pipe includes water inlet (21), water outlet
Mouth (22), air inlet pipe (23), air inlet pipe (23) one end are connected to outlet pipe, and the air inlet pipe other end is connected to collection by pipeline
Bottle is internal.
5. a kind of fractionation machine according to claim 4, which is characterized in that be provided with water pump (19), water above the water cover
The water inlet for pumping (19) is connected in pond (18) by pipeline, and the water outlet of water pump (19) is connected to condenser pipe by pipeline
Water inlet (21).
6. a kind of fractionation machine according to claim 5, which is characterized in that the water outlet (22) of the condenser pipe passes through pipeline
It is internal to be connected to pond (18).
7. a kind of fractionation machine according to claim 6, which is characterized in that the outlet pipe is connected to receiving flask inner end
It is provided with the first strainer (4).
8. a kind of fractionation machine according to claim 7, which is characterized in that a lateral wall is provided with above the body (1)
First form (17).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811482213.7A CN109289223A (en) | 2018-12-05 | 2018-12-05 | A kind of fractionation machine |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811482213.7A CN109289223A (en) | 2018-12-05 | 2018-12-05 | A kind of fractionation machine |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN109289223A true CN109289223A (en) | 2019-02-01 |
Family
ID=65142603
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201811482213.7A Pending CN109289223A (en) | 2018-12-05 | 2018-12-05 | A kind of fractionation machine |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN109289223A (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113231118A (en) * | 2021-05-10 | 2021-08-10 | 海南医学院 | Fractionating device for organic chemistry experiment |
-
2018
- 2018-12-05 CN CN201811482213.7A patent/CN109289223A/en active Pending
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113231118A (en) * | 2021-05-10 | 2021-08-10 | 海南医学院 | Fractionating device for organic chemistry experiment |
| CN113231118B (en) * | 2021-05-10 | 2022-08-05 | 海南医学院 | Fractionating device for organic chemistry experiment |
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| PB01 | Publication | ||
| PB01 | Publication | ||
| WD01 | Invention patent application deemed withdrawn after publication | ||
| WD01 | Invention patent application deemed withdrawn after publication |
Application publication date: 20190201 |