CN109270254A - Method for detecting color fastness of textiles to perspiration and friction - Google Patents

Method for detecting color fastness of textiles to perspiration and friction Download PDF

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Publication number
CN109270254A
CN109270254A CN201811429026.2A CN201811429026A CN109270254A CN 109270254 A CN109270254 A CN 109270254A CN 201811429026 A CN201811429026 A CN 201811429026A CN 109270254 A CN109270254 A CN 109270254A
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sample
perspiration
friction
adjacent fabric
textile
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麦裔强
黄明华
张颖欣
刘周海
闵雯
杨珊
雷丽芬
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Zhongshan Zhongce Weaving Industry Technology Research Center
Zhongshan Polytechnic
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Zhongshan Zhongce Weaving Industry Technology Research Center
Zhongshan Polytechnic
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    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N33/00Investigating or analysing materials by specific methods not covered by groups G01N1/00 - G01N31/00
    • G01N33/36Textiles

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  • Food Science & Technology (AREA)
  • Medicinal Chemistry (AREA)
  • Physics & Mathematics (AREA)
  • Textile Engineering (AREA)
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  • General Health & Medical Sciences (AREA)
  • General Physics & Mathematics (AREA)
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  • Investigating Or Analysing Materials By The Use Of Chemical Reactions (AREA)
  • Treatment Of Fiber Materials (AREA)

Abstract

The method for detecting the color fastness of the textiles to perspiration and friction comprehensively considers the influence of perspiration and friction on the color fastness of the textiles, and comprises the steps of shearing two samples from the textiles to be detected, recording the samples as a first sample and a second sample respectively, detecting the color fastness of the first sample by using acidic artificial sweat and friction, and detecting the color fastness of the second sample by using alkaline artificial sweat and friction. The application provides a detection method for the color fastness of the textile to perspiration and rubbing, which comprehensively considers the color fastness of the textile under the comprehensive action of sweat and external rubbing in the using process. Compared with the color fastness under the influence of single factor, the color fastness is closer to reality, and the color fastness of the textile can be reflected more accurately.

Description

The detection method of textile perspiration resistance, the compound color fastness of friction
[technical field]
This application involves the detection method of textile perspiration resistance, the compound color fastness of friction, specifically comprehensively considered sweat stain, The influence to rub to textile color stability resists sweat stain by a kind of evaluation textile that serial experiment determines, friction synthesis is made With effective detection method.
[background technique]
Color fastness (Color fastness) is also known as dyefastness, refers to the color of textile in the process of processing and using To the resistivity of various effects.It is matched by the discoloration of tested sample with discoloration gray card, and the adjacent fabric that is unstained Staining matched with staining gray card to evaluate color fastness grade.Textile in use, dyestuff by it is extraneous it is various because The influence of element, causing chromophoric group to change by destruction is the bad basic reason of textile color stability.Extraneous various factors Including water, sweat, chlorination water, friction, illumination, pressing, soap.
Color fastness it is bad not only influence clothes beauty, the dyestuff to fall off in human skin contact process, easily to people Body health causes damages.The detection method of color fastness has a individual event examination criterias up to a hundred at present, but rarely tertiary colour jail The examination criteria of degree, the detection of individual event color fastness are only capable of representing the fastness properties that textile resists certain single factors, and cannot be comprehensive Fastness properties of the reflection textile under many factors effect are closed, therefore often will appear every individual event color fastness detection and close The phenomenon that fastness properties of lattice but product can not meet customer demand.In daily life, textile may be by outer The comprehensive function of boundary's difference natural conditions, color fastness of the textile under comprehensive function may be lower than individual event color fastness, therefore, It is necessary to carry out the research of two kinds and the textile color stability detection method under the effect of two or more natural conditions.
So far, the achievement for studying compound color fastness detection method is few, and there are no about perspiration resistance, friction tertiary colour The detection method and correlative study of fastness.
[summary of the invention]
In order to solve the above technical problems, the application's is designed to provide textile perspiration resistance, friction compound color fastness It is firm to have comprehensively considered color of the textile in use simultaneously under the comprehensive function of sweat and extraneous friction for detection method Degree.Closer to reality compared with color fastness under the influence of single factors, be conducive to the color fastness for more accurately reflecting textile.
The application is achieved through the following technical solutions:
The detection method of textile perspiration resistance, the compound color fastness of friction, comprising the following steps:
S1, from a length of 138~142mm of clip on tested textile, width is two pieces of sample of 38~42mm, is denoted as the respectively One sample and the second sample;
First sample is immersed in acid synthetic perspiration by S2, and second sample is immersed in alkaline artificial perspiration In liquid;
S3 selects a length of 98~102mm corresponding with tested textile fabric, and width is two parts of adjacent fabric of 38~42mm, point It is not denoted as the first adjacent fabric and the second adjacent fabric, first adjacent fabric is put into the acid synthetic perspiration, it will Second adjacent fabric is put into the alkaline synthetic perspiration;
S4, by the acid synthetic perspiration the first sample and the first adjacent fabric impregnate and place 30~40 minutes, and Stirring or pressure-lift keep first sample and first adjacent fabric completely wet frequently in soaking process, by the alkaline people The second sample and the second adjacent fabric in work sweat, which impregnate, to be placed 30~40 minutes, and stirring or pressure-lift frequently in soaking process Keep second sample and second adjacent fabric completely wet;
S5 takes out by step S4 treated first sample and first adjacent fabric and is distinguished with glass bar Folder goes excessive acid synthetic perspiration, takes out by step S4 treated second sample and second adjacent fabric simultaneously It is pressed from both sides respectively with glass bar and goes excessive alkaline synthetic perspiration;
S6, by cotton friction cloth on the friction head of frictiograph, and will be by step S5 treated first sample Positive friction and reverse friction are carried out on the frictiograph respectively with second sample, forward direction friction and reverse friction are one Secondary rub cycle carries out 10 rub cycles altogether;
S7, by by step S6 processing first sample and second sample cut out between two parties respectively grow into 98~ 102mm, width are the specification of 38~42mm;
S8, will be by step S5 treated the first adjacent fabric and the first sample composition first by step S7 processing The second sample by step S5 treated the second adjacent fabric and by step S7 processing is formed second group by composite sample Close sample;
First composite sample is placed on two pieces and forms the first clamping body between glass plate or acrylic resin board by S9, Second composite sample is individually placed to other two pieces and forms the second clamping body between glass plate or acrylic resin board, by institute It states the first clamping body and is placed in the first colour fastness to perspiration frame the pressure for applying 11.6~13.4kPa, and keep the pressure 35 Placed 4~6 hours in~39 DEG C of baking oven, by the second clamping body be placed in the second colour fastness to perspiration frame apply 11.6~ The pressure of 13.4kPa, and the pressure is kept to place 4~6 hours in 35~39 DEG C of baking oven;
S10 takes out the first colour fastness to perspiration frame for having the first clamping body and with described second from baking oven Second colour fastness to perspiration frame of clamping body, then takes out first composite sample from the first clamping body, from described Second clamping body takes out second composite sample, and by the first sample and the first adjacent fabric in first composite sample Dried respectively after separation, by second composite sample the second sample and the second adjacent fabric separation after dry respectively;
S11, in standard sources, with discoloration gray card evaluate respectively by step S10 treated first sample with The discoloration series of second sample is evaluated respectively with staining gray card by step S10 treated first adjacent fabric With the staining series of second adjacent fabric.
The detection method of textile perspiration resistance, the compound color fastness of friction as described above, the alkalinity synthetic perspiration include Following component and its parts by weight: 0.5 part of L-Histidine hydrochloride monohydrate, 5 parts of sodium chloride, disodium hydrogen phosphate 12 are hydrated 5 parts of object or 2.5 parts of disodium phosphate dihydrate, with the sodium hydroxide solution of 0.1mol/L by the pH of the alkaline synthetic perspiration Value is adjusted to 7.8~8.2.
The detection method of textile perspiration resistance, the compound color fastness of friction as described above, the acidity synthetic perspiration include Following component and its parts by weight: 0.5 part of L-Histidine hydrochloride monohydrate, 5 parts of sodium chloride, sodium dihydrogen phosphate dihydrate 2.2 parts, the pH value of the acid synthetic perspiration is adjusted to 5.3~5.7 with the sodium hydroxide solution of 0.1mol/L.
The detection method of textile perspiration resistance, the compound color fastness of friction as described above, first adjacent fabric are two Block single fiber adjacent fabric, second adjacent fabric are also two pieces of single fiber adjacent fabrics;
The process that the first composite sample is formed described in step S8 is that will pass through by the first specimen holder of step S7 processing It crosses step S5 treated between two pieces of single fiber adjacent fabrics in the first adjacent fabric, the second composite sample of the composition Process is that the second specimen holder will be handled by step S7 by two pieces of single fibers in step S5 treated the second adjacent fabric It ties up between adjacent fabric.
The detection method of textile perspiration resistance, the compound color fastness of friction as described above, the frictiograph are reciprocating rub Wipe instrument or rotary frictiograph.
The detection method of textile perspiration resistance, the compound color fastness of friction as described above, the baking oven are insulating box.
The detection method of textile perspiration resistance, the compound color fastness of friction as described above, with the first clamping body First colour fastness to perspiration frame and placement of the second colour fastness to perspiration frame in the baking oven with the second clamping body State is horizontally or vertically.
Compared with prior art, the application has the following advantages:
The textile perspiration resistance, the compound color fastness of friction detection method comprehensively considered textile in use Color fastness under the comprehensive function of sweat and extraneous friction simultaneously.Compared with color fastness under the influence of single factors closer to It is practical, be conducive to the color fastness for more accurately reflecting textile.On the other hand, the textile perspiration resistance, friction tertiary colour jail The it is proposed of the detection method of degree has facilitation to color fastness examination criteria is improved, and can be clothes production enterprise and retailer It controls product quality and practicable detection foundation is provided, have important practical significance.
[specific embodiment]
The technical issues of in order to keep the application solved, technical solution and beneficial effect are more clearly understood, below in conjunction with The application is further elaborated in embodiment.It should be appreciated that specific embodiment described herein is only used to explain The application is not used to limit the application.
The embodiment of the present application proposes the detection method of textile perspiration resistance, the compound color fastness of friction, which is characterized in that including Step S1-S11:
S1, from a length of 138~142mm of clip on tested textile, width is two pieces of sample of 38~42mm, is denoted as the respectively One sample and the second sample.
First sample is immersed in acid synthetic perspiration by S2, and second sample is impregnated alkaline synthetic perspiration In.
Wherein, the alkaline synthetic perspiration includes following component and its parts by weight: L-Histidine hydrochloride monohydrate 0.5 part, 5 parts of sodium chloride, 5 parts of disodium hydrogen phosphate dodecahydrate or 2.5 parts of disodium phosphate dihydrate, with 0.1mol/L's Sodium hydroxide solution adjusts the pH value of the alkaline synthetic perspiration to 7.8~8.2, and the acidity synthetic perspiration includes such as the following group Point and its parts by weight: 0.5 part of L-Histidine hydrochloride monohydrate, 5 parts of sodium chloride, 2.2 parts of sodium dihydrogen phosphate dihydrate, The pH value of the acid synthetic perspiration is adjusted to 5.3~5.7 with the sodium hydroxide solution of 0.1mol/L.
S3 selects a length of 98~102mm corresponding with tested textile fabric, and width is two parts of adjacent fabric of 38~42mm, point It is not denoted as the first adjacent fabric and the second adjacent fabric, first adjacent fabric is put into the acid synthetic perspiration, it will Second adjacent fabric is put into the alkaline synthetic perspiration, it should be noted that the selection of the adjacent fabric can foundation Regulation in " GB/T3922-2013 textile color stability tests colour fastness to perspiration " is selected.
Wherein, first adjacent fabric is two pieces of single fiber adjacent fabrics, and second adjacent fabric is also two pieces of lists Fiber adjacent fabric, the process that the first composite sample is formed described in step S8 is the first specimen holder that will be handled by step S7 By between two pieces of single fiber adjacent fabrics in step S5 treated the first adjacent fabric, the second combination of composition examination The process of sample is that the second specimen holder will be handled by step S7 by two pieces in step S5 treated the second adjacent fabric Between single fiber adjacent fabric.
S4, by the acid synthetic perspiration the first sample and the first adjacent fabric impregnate and place 30~40 minutes, it is excellent It is selected as 30 minutes, and stirring or pressure-lift keep first sample and first adjacent fabric completely wet frequently in soaking process Profit, by the alkaline synthetic perspiration the second sample and the second adjacent fabric impregnate and place 30~40 minutes, preferably 30 points Clock, and stirring or pressure-lift keep second sample and second adjacent fabric completely wet frequently in soaking process.
S5 takes out by step S4 treated first sample and first adjacent fabric and is distinguished with glass bar Folder goes excessive acid synthetic perspiration, takes out by step S4 treated second sample and second adjacent fabric simultaneously It is pressed from both sides respectively with glass bar and goes excessive alkaline synthetic perspiration.
S6, by cotton friction cloth on the friction head of frictiograph, and will be by step S5 treated first sample Positive friction and reverse friction are carried out on the frictiograph respectively with second sample, forward direction friction and reverse friction are one Secondary rub cycle, altogether carry out 10 rub cycles, wherein the frictiograph be reciprocating friction instrument or rotary frictiograph, it is excellent It is selected as reciprocating friction instrument.
S7, by by step S6 processing first sample and second sample cut out between two parties respectively grow into 98~ 102mm, width are the specification of 38~42mm.
S8, will be by step S5 treated the first adjacent fabric and the first sample composition first by step S7 processing The second sample by step S5 treated the second adjacent fabric and by step S7 processing is formed second group by composite sample Close sample.
First composite sample is placed on two pieces and forms the first clamping body between glass plate or acrylic resin board by S9, Second composite sample is individually placed to other two pieces and forms the second clamping body between glass plate or acrylic resin board, by institute It states the first clamping body and is placed in the first colour fastness to perspiration frame the pressure for applying 11.6~13.4kPa, and keep the pressure 35 4~6 hours, preferably 4 hours are placed in~39 DEG C of baking oven, and the second clamping body is placed in the second colour fastness to perspiration frame The middle pressure for applying 11.6~13.4kPa, and the pressure is kept to place 4~6 hours, preferably 4 in 35~39 DEG C of baking oven Hour, wherein the baking oven is insulating box, the first colour fastness to perspiration frame with the first clamping body and with described the Placement status of the second colour fastness to perspiration frame of two clamping bodies in the baking oven is horizontally or vertically.
S10 takes out the first colour fastness to perspiration frame for having the first clamping body and with described second from baking oven Second colour fastness to perspiration frame of clamping body, then takes out first composite sample from the first clamping body, from described Second clamping body takes out second composite sample, and by the first sample and the first adjacent fabric in first composite sample Dried respectively after separation, by second composite sample the second sample and the second adjacent fabric separation after dry respectively.
S11, in standard sources, with discoloration gray card evaluate respectively by step S10 treated first sample with The discoloration series of second sample is evaluated respectively with staining gray card by step S10 treated first adjacent fabric With the staining series of second adjacent fabric.
The textile perspiration resistance, the compound color fastness of friction detection method comprehensively considered textile in use Color fastness under the comprehensive function of sweat and extraneous friction simultaneously.Compared with color fastness under the influence of single factors closer to It is practical, be conducive to the color fastness for more accurately reflecting textile.On the other hand, the textile perspiration resistance, friction tertiary colour jail The it is proposed of the detection method of degree has facilitation to color fastness examination criteria is improved, and can be clothes production enterprise and retailer It controls product quality and practicable detection foundation is provided, have important practical significance.
It is the one or more embodiments provided in conjunction with particular content as described above, does not assert the specific reality of the application It applies and is only limited to these instructions.It is all approximate with the present processes, structure etc., identical, or under the application concept thereof It makes several technologies to deduce, or replacement all should be considered as the protection scope of the application.

Claims (7)

1. the detection method of textile perspiration resistance, the compound color fastness of friction, which comprises the following steps:
S1, from a length of 138~142mm of clip on tested textile, width is two pieces of sample of 38~42mm, is denoted as the first examination respectively Sample and the second sample;
First sample is immersed in acid synthetic perspiration by S2, and second sample is immersed in alkaline synthetic perspiration;
S3 selects a length of 98~102mm corresponding with tested textile fabric, and width is two parts of adjacent fabric of 38~42mm, remembers respectively For the first adjacent fabric and the second adjacent fabric, first adjacent fabric is put into the acid synthetic perspiration, it will be described Second adjacent fabric is put into the alkaline synthetic perspiration;
S4, by the acid synthetic perspiration the first sample and the first adjacent fabric impregnate and place 30~40 minutes, and impregnate Stirring or pressure-lift keep first sample and first adjacent fabric completely wet frequently in the process, by the alkaline artificial perspiration The second sample and the second adjacent fabric in liquid, which impregnate, to be placed 30~40 minutes, and stirring or pressure-lift make institute frequently in soaking process It is completely wet to state the second sample and second adjacent fabric;
S5 takes out and goes by step S4 treated first sample and first adjacent fabric and being pressed from both sides respectively with glass bar Excessive acid synthetic perspiration takes out by step S4 treated second sample and second adjacent fabric and uses glass Glass stick presss from both sides respectively goes excessive alkaline synthetic perspiration;
S6, by cotton friction cloth on the friction head of frictiograph, and will be by step S5 treated first sample and institute It states the second sample and carries out positive friction and reverse friction on the frictiograph respectively, forward direction friction and reverse friction are once to rub Circulation is wiped, carries out 10 rub cycles altogether;
S7, by by step S6 processing first sample and second sample cut out between two parties respectively grow into 98~ 102mm, width are the specification of 38~42mm;
S8 will form first with the first sample by step S7 processing by step S5 treated the first adjacent fabric and combine Sample will form second with the second sample by step S7 processing by step S5 treated the second adjacent fabric and combine examination Sample;
First composite sample is placed on two pieces and forms the first clamping body between glass plate or acrylic resin board, by institute by S9 It states the second composite sample and is individually placed to other two pieces and form the second clamping body between glass plate or acrylic resin board, by described One clamping body is placed in the first colour fastness to perspiration frame the pressure for applying 11.6~13.4kPa, and keeps the pressure 35~39 DEG C baking oven in place 4~6 hours, by the second clamping body be placed in the second colour fastness to perspiration frame apply 11.6~ The pressure of 13.4kPa, and the pressure is kept to place 4~6 hours in 35~39 DEG C of baking oven;
S10 takes out the first colour fastness to perspiration frame with the first clamping body from baking oven and has second clamping Second colour fastness to perspiration frame of body, then takes out first composite sample from the first clamping body, from described second Clamping body takes out second composite sample, and by first composite sample the first sample and the first adjacent fabric separate Dry respectively afterwards, by second composite sample the second sample and the second adjacent fabric separation after dry respectively;
S11 evaluate respectively with discoloration gray card in standard sources and is passed through step S10 treated first sample and described The discoloration series of second sample is evaluated respectively with staining gray card by step S10 treated first adjacent fabric and institute State the staining series of the second adjacent fabric.
2. the detection method of textile perspiration resistance according to claim 1, the compound color fastness of friction, which is characterized in that institute Stating alkaline synthetic perspiration includes following component and its parts by weight: 0.5 part of L-Histidine hydrochloride monohydrate, 5 parts of sodium chloride, 5 parts of disodium hydrogen phosphate dodecahydrate or 2.5 parts of disodium phosphate dihydrate, with the sodium hydroxide solution of 0.1mol/L by institute The pH value for stating alkaline synthetic perspiration is adjusted to 7.8~8.2.
3. the detection method of textile perspiration resistance according to claim 1, the compound color fastness of friction, which is characterized in that institute Stating acid synthetic perspiration includes following component and its parts by weight: 0.5 part of L-Histidine hydrochloride monohydrate, 5 parts of sodium chloride, 2.2 parts of sodium dihydrogen phosphate dihydrate, the pH value of the acid synthetic perspiration is adjusted with the sodium hydroxide solution of 0.1mol/L To 5.3~5.7.
4. the detection method of textile perspiration resistance according to claim 1, the compound color fastness of friction, which is characterized in that institute Stating the first adjacent fabric is two pieces of single fiber adjacent fabrics, and second adjacent fabric is also two pieces of single fiber adjacent fabrics;
The process that the first composite sample is formed described in step S8 is by the first specimen holder by step S7 processing by walking Between two pieces of single fiber adjacent fabrics in rapid S5 treated the first adjacent fabric, the process of the second composite sample of the composition The second specimen holder is handled by two blocks of single fibers patch in step S5 treated the second adjacent fabric for step S7 will be passed through It serves as a contrast between fabric.
5. the detection method of textile perspiration resistance according to claim 1, the compound color fastness of friction, which is characterized in that institute Stating frictiograph is reciprocating friction instrument or rotary frictiograph.
6. the detection method of textile perspiration resistance according to claim 1, the compound color fastness of friction, the baking oven is constant temperature Case.
7. the detection method of textile perspiration resistance according to claim 1, the compound color fastness of friction, with first folder The first fit colour fastness to perspiration frame and the second colour fastness to perspiration frame with the second clamping body are in the baking oven Placement status be horizontally or vertically.
CN201811429026.2A 2018-11-27 2018-11-27 Method for detecting color fastness of textiles to perspiration and friction Pending CN109270254A (en)

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