CN109266200A - A kind of aqueous dumb light skin sense coating and preparation method thereof - Google Patents
A kind of aqueous dumb light skin sense coating and preparation method thereof Download PDFInfo
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- CN109266200A CN109266200A CN201811094153.1A CN201811094153A CN109266200A CN 109266200 A CN109266200 A CN 109266200A CN 201811094153 A CN201811094153 A CN 201811094153A CN 109266200 A CN109266200 A CN 109266200A
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- aqueous
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- dumb light
- coating
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D175/00—Coating compositions based on polyureas or polyurethanes; Coating compositions based on derivatives of such polymers
- C09D175/04—Polyurethanes
- C09D175/06—Polyurethanes from polyesters
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D175/00—Coating compositions based on polyureas or polyurethanes; Coating compositions based on derivatives of such polymers
- C09D175/04—Polyurethanes
- C09D175/08—Polyurethanes from polyethers
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/60—Additives non-macromolecular
- C09D7/61—Additives non-macromolecular inorganic
- C09D7/62—Additives non-macromolecular inorganic modified by treatment with other compounds
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/65—Additives macromolecular
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/02—Polymer mixtures characterised by other features containing two or more polymers of the same C08L -group
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/03—Polymer mixtures characterised by other features containing three or more polymers in a blend
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- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Paints Or Removers (AREA)
Abstract
The invention discloses a kind of aqueous dumb light skin sense coatings and preparation method thereof, it by mass percentage include following component: polyurethane 8%-88%, aqueous elastic resin 5%-90%, dumb light agent 5%-20%, pH adjusting agent 0.1%-1%, moistening flatting agent 0.3%-0.9%, feel auxiliary agent 0.3%-1.2%, curing agent 1%-8%, organic solvent 1%-10%, scratch resistant dose of 0.5%-1.8%；Without noxious materials such as formaldehyde in the present invention, and make that coating is fast light, anti-yellowing property is more preferable by adding dumb light agent, form a film good toughness, it is low to the strong product modulus of substrate adhesive force, tensile strength is bigger, excellent extensibility and resistance to bent immunity energy, and extinction capability is strong, water-fast humidity resistance can be improved after delustering agent, use can be lowered, good film-forming property, by scratch resistant dose of addition, make coating that there is good film forming and antiflex cracking, and makes coating that there is water-fast, wear-resisting, anti scuffing and yellowing-resistant and other effects.
Description
Technical field
The invention discloses a kind of aqueous dumb light skin sense coatings and preparation method thereof, belong to technical field of paint preparation.
Background technique
The variation of packages printing field aesthetic conceptions, aqueous dumb light skin sense coating receives people and widely likes, existing
Containing noxious materials such as formaldehyde in aqueous dumb light skin sense coating processes, and coating is fast light, anti-yellowing property is poor, not at film toughness
Good, tensile strength is low, and extensibility and resistance to bent immunity can be undesirable, and extinction capability is poor, and can not lower can after delustering agent, use
Water-fast humidity resistance is improved, coating does not have good film forming and antiflex cracking, water-fast, wear-resisting and anti scuffing and other effects.
Summary of the invention
A kind of aqueous dumb light skin sense coating and preparation method thereof is provided the purpose of the present invention is to solve above-mentioned insufficient,
The anti-scraping coating of dumb light is without noxious materials such as formaldehyde in the main present invention, and makes by addition dumb light agent that coating is fast light, resistance to Huang
Denaturation can be more preferable, and form a film good toughness, and low to the strong product modulus of substrate adhesive force, tensile strength is bigger, excellent extensibility and resistance to
Bent immunity energy, and extinction capability is strong, and water-fast humidity resistance, good film-forming property, by adding can be improved after can lowering delustering agent, use
Add scratch resistant dose, makes coating that there is good film forming and antiflex cracking, water-fast, wear-resisting scratch-resisting wound, yellowing-resistant and other effects.
To achieve the above object, the invention provides the following technical scheme: a kind of aqueous dumb light skin sense coating and its preparation side
Method includes following component: polyurethane 8%-88%, aqueous elastic resin 5%-90%, dumb light agent 5%- by mass percentage
20%, pH adjusting agent 0.1%-1%, moistening flatting agent 0.3%-0.9%, feel auxiliary agent 0.3%-1.2%, curing agent 1%-
8%, organic solvent 1%-10%, scratch resistant dose of 0.5%-1.8%.
Preferably, the polyurethane is aqueous polyurethane, and partial size < 0.001 micron of the middle aqueous polyurethane solution,
And the polyurethane appearance transparent.
Preferably, the polyurethane is the one or two of polyether polyurethane or polyester polyurethane.
Preferably, the aqueous elastic resin is aqueous aliphatic polyurethane dispersion, and the aqueous aliphatic poly ammonia
Ester is aqueous elastic PU resin X-PU632 aqueous polyurethane.
Preferably, the dumb light agent is improved silica delustring slurry.
Preferably, described scratch resistant dose is composite multi-functional silicone master batch.
Preferably, the pH adjusting agent is one of ammonium hydroxide, triethylamine, AMP-95 or a variety of.
Preferably, the moistening flatting agent is as isophorone, diacetone alcohol, Solvesso150 are one or two kinds of.
Preferably, the curing agent be vinyl triamine, DETA, aminoethyl piperazine AE, m-phenylene diamine (MPD) m-PDA, MPD,
One of diaminodiphenyl-methane DDM, HT-972, DEH-50 or a variety of.
Preferably, the organic solvent includes styrene, perchloroethylene, trichloro ethylene, ethylene glycol ether and three second
One of hydramine is a variety of.
Preferably, comprising the following steps:
A: mixing each component according to the mass percent, is sufficiently mixed stirring by different rotating speeds, is configured to apply
Layer aqueous dispersion；
B: the coating aqueous dispersion that the A is obtained to substrate, the coating for obtaining the A are sufficiently reacted with substrate
Mixing；
C: by the coating that the B is obtained be under sealed environment carry out temperature be 80-130 DEG C, the time is 5min's or so
Preheating；
D: carrying out temperature to the coating that the C is obtained is 150 DEG C or so, the curing that the time is three days, to obtain aqueous
The low and hoarse anti-scraping coating of light.
Compared with prior art, beneficial effects of the present invention are as follows:
Without the noxious materials such as formaldehyde in the present invention, and by addition dumb light agent make coating is fast light, anti-yellowing property more
Good, form a film good toughness, and low to the strong product modulus of substrate adhesive force, tensile strength is bigger, excellent extensibility and resistance to bent immunity energy,
And extinction capability is strong, can lower and water-fast humidity resistance can be improved after delustering agent, use, good film-forming property, by scratch resistant dose of addition,
Make coating that there is good film forming and antiflex cracking, and makes coating that there is water-fast, wear-resisting, anti scuffing and yellowing-resistant and other effects.
Specific embodiment
The following is a clear and complete description of the technical scheme in the embodiments of the invention, it is clear that described embodiment
Only a part of the embodiment of the present invention, instead of all the embodiments.Based on the embodiments of the present invention, the common skill in this field
Art personnel every other embodiment obtained without making creative work belongs to the model that the present invention protects
It encloses.
A kind of aqueous dumb light skin sense coating and preparation method thereof includes following component: polyurethane by mass percentage
8%-88%, aqueous elastic resin 5%-90%, dumb light agent 5%-20%, pH adjusting agent 0.1%-1%, moistening flatting agent
0.3%-0.9%, feel auxiliary agent 0.3%-1.2%, curing agent 1%-8%, organic solvent 1%-10%, scratch resistant dose of 0.5%-
1.8%.
Wherein, the polyurethane is aqueous polyurethane, and partial size < 0.001 micron of the middle aqueous polyurethane solution, and
The polyurethane appearance transparent.
Wherein, the polyurethane is the one or two of polyether polyurethane or polyester polyurethane.
Wherein, the aqueous elastic resin is aqueous aliphatic polyurethane dispersion, and the aqueous aliphatic polyurethane
For aqueous elastic PU resin X-PU632 aqueous polyurethane.
Wherein, the dumb light agent is improved silica delustring slurry.
Wherein, described scratch resistant dose is composite multi-functional silicone master batch.
Wherein, the pH adjusting agent is one of ammonium hydroxide, triethylamine, AMP-95 or a variety of.
Wherein, the moistening flatting agent is as isophorone, diacetone alcohol, Solvesso150 are one or two kinds of.
Wherein, the curing agent is vinyl triamine, DETA, aminoethyl piperazine AE, m-phenylene diamine (MPD) m-PDA, MPD, two
One of aminodiphenylmethane DDM, HT-972, DEH-50 or a variety of.
Wherein, the organic solvent includes styrene, perchloroethylene, trichloro ethylene, ethylene glycol ether and three ethyl alcohol
One of amine is a variety of.
Embodiment 1, a kind of aqueous dumb light skin sense coating and preparation method thereof include following component by mass percentage:
Polyurethane 80%, aqueous elastic resin 5%, dumb light agent 5%, pH adjusting agent 0.5%, moistening flatting agent 0.5%, feel auxiliary agent
0.5%, curing agent 5%, organic solvent 2%, scratch resistant dose 0.5%.
The following steps are included:
A: mixing each component according to the mass percent, and it is sufficiently mixed that blender revolving speed is adjusted to 800-900r/min
Stirring 30min is closed, coating aqueous dispersion is configured to；
B: the coating aqueous dispersion that the A is obtained to substrate, the coating for obtaining the A are sufficiently reacted with substrate
Mixing；
C: by the coating that the B is obtained be under sealed environment carry out temperature be 80-130 DEG C, the time is 5min's or so
Preheating；
D: carrying out temperature to the coating that the C is obtained is 150 DEG C or so, the curing that the time is three days, to obtain aqueous
The low and hoarse anti-scraping coating of light.
Embodiment 2, a kind of aqueous dumb light skin sense coating and preparation method thereof include following component by mass percentage:
Polyurethane 75%, aqueous elastic resin 5%, dumb light agent 5%, pH adjusting agent 0.5%, moistening flatting agent 0.5%, feel auxiliary agent
0.5%, curing agent 6%, organic solvent 7%, scratch resistant dose 0.5%.
The following steps are included:
A: mixing each component according to the mass percent, and it is abundant that blender revolving speed is adjusted to 900-1000r/min
25min is mixed, is configured to coating aqueous dispersion；
B: the coating aqueous dispersion that the A is obtained to substrate, the coating for obtaining the A are sufficiently reacted with substrate
Mixing；
C: by the coating that the B is obtained be under sealed environment carry out temperature be 80-130 DEG C, the time is 5min's or so
Preheating；
D: carrying out temperature to the coating that the C is obtained is 150 DEG C or so, the curing that the time is three days, to obtain aqueous
The low and hoarse anti-scraping coating of light.
Embodiment 3, a kind of aqueous dumb light skin sense coating and preparation method thereof include following component by mass percentage:
Polyurethane 70%, aqueous elastic resin 8%, dumb light agent 6%, pH adjusting agent 0.5%, moistening flatting agent 0.5%, feel auxiliary agent
0.5%, curing agent 8%, organic solvent 6%, scratch resistant dose 0.5%.
The following steps are included:
A: mixing each component according to the mass percent, and it is abundant that blender revolving speed is adjusted to 1000-1200r/min
20min is mixed, is configured to coating aqueous dispersion；
B: the coating aqueous dispersion that the A is obtained to substrate, the coating for obtaining the A are sufficiently reacted with substrate
Mixing；
C: by the coating that the B is obtained be under sealed environment carry out temperature be 80-130 DEG C, the time is 5min's or so
Preheating；
D: carrying out temperature to the coating that the C is obtained is 150 DEG C or so, the curing that the time is three days, to obtain aqueous
The low and hoarse anti-scraping coating of light.
Specifically, without the noxious materials such as formaldehyde in the present invention, and make by addition dumb light agent that coating is fast light, color inhibition
Performance is more preferable, and form a film good toughness, and low to the strong product modulus of substrate adhesive force, tensile strength is bigger, excellent extensibility and resistance to song
Immunity energy, and extinction capability is strong, water-fast humidity resistance can be improved after can lowering delustering agent, use, good film-forming property passes through addition
Scratch resistant dose, make coating that there is good film forming and antiflex cracking, and makes coating that there is water-fast, wear-resisting, anti scuffing and yellowing-resistant
And other effects.
It although an embodiment of the present invention has been shown and described, for the ordinary skill in the art, can be with
A variety of variations, modification, replacement can be carried out to these embodiments without departing from the principles and spirit of the present invention by understanding
And modification, the scope of the present invention is defined by the appended.
Claims (10)
1. a kind of aqueous dumb light skin sense coating and preparation method thereof, it is characterised in that: by mass percentage include following component:
Polyurethane 8%-88%, aqueous elastic resin 5%-90%, dumb light agent 5%-20%, pH adjusting agent 0.1%-1% soak levelling
Agent 0.3%-0.9%, feel auxiliary agent 0.3%-1.2%, curing agent 1%-8%, organic solvent 1%-10%, scratch resistant dose of 0.5%-
1.8%.
2. a kind of aqueous dumb light skin sense coating according to claim 1 and preparation method thereof, it is characterised in that: the poly- ammonia
Ester is the one or two of polyether polyurethane or polyester polyurethane.
3. a kind of aqueous dumb light skin sense coating according to claim 1 and preparation method thereof, it is characterised in that: described aqueous
Elastic resin is aqueous aliphatic polyurethane dispersion, and the aqueous aliphatic polyurethane is aqueous elastic PU resin X-
PU632 aqueous polyurethane.
4. a kind of aqueous dumb light skin sense coating according to claim 1 and preparation method thereof, it is characterised in that: the dumb light
Agent is improved silica delustring slurry.
5. a kind of aqueous dumb light skin sense coating according to claim 1 and preparation method thereof, it is characterised in that: described scratch resistant
Agent is composite multi-functional silicone master batch.
6. a kind of aqueous dumb light skin sense coating according to claim 1 and preparation method thereof, it is characterised in that: the pH tune
Section agent is one of ammonium hydroxide, triethylamine, AMP-95 or a variety of.
7. a kind of aqueous dumb light skin sense coating according to claim 1 and preparation method thereof, it is characterised in that: the wetting
Levelling agent is as isophorone, diacetone alcohol, Solvesso150 are one or two kinds of.
8. a kind of aqueous dumb light skin sense coating according to claim 1 and preparation method thereof, it is characterised in that: described consolidates
Agent is vinyl triamine, DETA, aminoethyl piperazine AE, m-phenylene diamine (MPD) m-PDA, MPD, diaminodiphenyl-methane DDM, HT-
972, one of DEH-50 or a variety of.
9. a kind of aqueous dumb light skin sense coating according to claim 1 and preparation method thereof, it is characterised in that: described has
Solvent includes one of styrene, perchloroethylene, trichloro ethylene, ethylene glycol ether and triethanolamine or a variety of.
10. a kind of aqueous dumb light skin sense coating according to claim 1 and preparation method thereof, it is characterised in that: including with
Lower step:
A: mixing each component according to the mass percent, is sufficiently mixed stirring by different rotating speeds, is configured to coating water
Dispersion；
B: the coating aqueous dispersion that the A is obtained to substrate, the coating for obtaining the A sufficiently react mixed with substrate
It closes；
C: by the coating that the B is obtained be under sealed environment carry out temperature be 80-130 DEG C, the preheating that the time is 5min or so；
D: carrying out temperature to the coating that the C is obtained is 150 DEG C or so, the curing that the time is three days, to obtain aqueous low and hoarse
The anti-scraping coating of light.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811094153.1A CN109266200A (en) | 2018-09-19 | 2018-09-19 | A kind of aqueous dumb light skin sense coating and preparation method thereof |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811094153.1A CN109266200A (en) | 2018-09-19 | 2018-09-19 | A kind of aqueous dumb light skin sense coating and preparation method thereof |
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| Publication Number | Publication Date |
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| CN109266200A true CN109266200A (en) | 2019-01-25 |
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201811094153.1A Pending CN109266200A (en) | 2018-09-19 | 2018-09-19 | A kind of aqueous dumb light skin sense coating and preparation method thereof |
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110066591A (en) * | 2019-05-21 | 2019-07-30 | 东莞市涂芭新材料有限公司 | A kind of aqueous skin sense woodwork coating and preparation method thereof |
| CN112644107A (en) * | 2020-12-30 | 2021-04-13 | 上海涂固安高科技有限公司 | Far infrared self-heating composite material for solving problem of cold metal surface |
| CN114591661A (en) * | 2022-01-21 | 2022-06-07 | 宁国市茂发装饰材料有限公司 | Microcrystalline color 5D skin-feel art paint and preparation method thereof |
| CN114654856A (en) * | 2022-03-15 | 2022-06-24 | 浙江锂盾新能源材料有限公司 | Full-matte lithium ion battery composite packaging aluminum-plastic film and manufacturing method thereof |
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| CN103627306A (en) * | 2013-11-07 | 2014-03-12 | 昆山大世界油墨涂料有限公司 | Mist surface hand feeling scratch-resistant coating paint and preparation method thereof |
| CN104098942A (en) * | 2013-04-03 | 2014-10-15 | 上海劲嘉建材科技有限公司 | Nanometer wear-resistant coating and floor tile using same |
| CN108129971A (en) * | 2017-12-27 | 2018-06-08 | 中山大学 | A kind of anti-scraping coating of environmental protection resistance and fingerprint resistance and its application method |
| CN108165152A (en) * | 2017-12-27 | 2018-06-15 | 广东德冠薄膜新材料股份有限公司 | A kind of anti-scraping coating of aqueous low and hoarse light and its application method |
-
2018
- 2018-09-19 CN CN201811094153.1A patent/CN109266200A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104098942A (en) * | 2013-04-03 | 2014-10-15 | 上海劲嘉建材科技有限公司 | Nanometer wear-resistant coating and floor tile using same |
| CN103627306A (en) * | 2013-11-07 | 2014-03-12 | 昆山大世界油墨涂料有限公司 | Mist surface hand feeling scratch-resistant coating paint and preparation method thereof |
| CN108129971A (en) * | 2017-12-27 | 2018-06-08 | 中山大学 | A kind of anti-scraping coating of environmental protection resistance and fingerprint resistance and its application method |
| CN108165152A (en) * | 2017-12-27 | 2018-06-15 | 广东德冠薄膜新材料股份有限公司 | A kind of anti-scraping coating of aqueous low and hoarse light and its application method |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110066591A (en) * | 2019-05-21 | 2019-07-30 | 东莞市涂芭新材料有限公司 | A kind of aqueous skin sense woodwork coating and preparation method thereof |
| CN112644107A (en) * | 2020-12-30 | 2021-04-13 | 上海涂固安高科技有限公司 | Far infrared self-heating composite material for solving problem of cold metal surface |
| CN114591661A (en) * | 2022-01-21 | 2022-06-07 | 宁国市茂发装饰材料有限公司 | Microcrystalline color 5D skin-feel art paint and preparation method thereof |
| CN114654856A (en) * | 2022-03-15 | 2022-06-24 | 浙江锂盾新能源材料有限公司 | Full-matte lithium ion battery composite packaging aluminum-plastic film and manufacturing method thereof |
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Effective date of registration: 20200526 Address after: 528000 workshop 6, block B, 276 Hefu Road, Hecheng street, Gaoming District, Foshan City, Guangdong Province Applicant after: Foshan weishiqi Technology Co., Ltd Address before: 274100 No. 052 East Road, Taliu Community School, Dingtao Town, Dingtao County, Heze City, Shandong Province Applicant before: Cai Zhongfa |
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